#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:58:55 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180935 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/15/2201563.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201563_Fobs loop_ _publ_author_name 'Mahalakshmi, L.' 'Upadhyaya, V.' 'Guru Row, T. N.' _publ_section_title ; 2,4,5-Trichloroacetanilide ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o946 _journal_page_last o947 _journal_volume 58 _journal_year 2002 _space_group_IT_number 7 _symmetry_space_group_name_Hall 'P -2yac' _symmetry_space_group_name_H-M 'P 1 n 1' _cell_angle_alpha 90.000 _cell_angle_beta 101.186 _cell_angle_gamma 90.000 _cell_length_a 3.9015 _cell_length_b 12.6579 _cell_length_c 9.6687 _exptl_crystal_F_000 240.00 _reflns_d_resolution_high 0.7562 _cod_data_source_file ob6158Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 5tca_m in Pn' _shelx_refln_list_code 4 _shelx_f_calc_maximum 65.64 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x+1/2, -y, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 0 -12 58.84 57.37 2.45 o 2 0 -12 45.88 38.42 2.11 o 0 1 -12 6.26 5.20 0.52 o 1 1 -12 53.62 55.13 1.72 o 2 1 -12 18.63 20.31 1.06 o 0 2 -12 100.73 97.04 2.45 o 1 2 -12 53.88 56.86 2.22 o 2 2 -12 26.89 29.19 1.28 o 0 3 -12 30.15 33.04 1.77 o 1 3 -12 64.32 66.11 3.84 o 0 4 -12 8.99 10.59 1.02 o 1 4 -12 32.11 36.13 1.88 o -1 0 -11 87.58 85.21 3.05 o 1 0 -11 18.32 21.06 1.36 o 3 0 -11 17.50 21.55 1.12 o -1 1 -11 13.49 13.63 0.76 o 0 1 -11 6.87 7.65 0.66 o 1 1 -11 8.60 8.14 0.63 o 2 1 -11 169.11 178.24 3.15 o 3 1 -11 23.15 22.05 0.92 o -1 2 -11 11.92 11.32 0.71 o 0 2 -11 68.72 67.46 1.84 o 1 2 -11 205.76 199.94 4.10 o 2 2 -11 38.61 38.49 1.16 o 3 2 -11 51.46 52.08 1.48 o -1 3 -11 4.31 3.88 0.45 o 0 3 -11 68.40 65.73 1.82 o 1 3 -11 55.78 52.25 1.61 o 2 3 -11 14.35 14.25 0.87 o 3 3 -11 30.99 28.46 1.34 o -1 4 -11 18.88 19.57 0.92 o 0 4 -11 32.58 32.42 1.18 o 1 4 -11 79.78 77.65 3.26 o 2 4 -11 9.40 9.49 0.73 o 3 4 -11 26.72 28.03 1.88 o -1 5 -11 4.20 4.63 0.72 o 0 5 -11 89.88 92.11 5.10 o 1 5 -11 10.53 10.04 0.68 o 2 5 -11 33.84 34.33 1.40 o 0 6 -11 45.21 46.60 1.96 o 1 6 -11 12.13 10.59 1.05 o 2 6 -11 7.64 8.70 0.74 o 0 7 -11 52.34 54.73 4.07 o 1 7 -11 5.55 5.50 0.75 o -2 0 -10 11.31 10.10 0.94 o 0 0 -10 385.44 398.68 10.02 o 2 0 -10 17.34 16.86 0.85 o -2 1 -10 0.05 0.14 0.36 o -1 1 -10 1.15 1.39 0.49 o 0 1 -10 42.07 45.51 1.36 o 1 1 -10 113.90 114.09 3.92 o 2 1 -10 2.40 2.12 0.29 o 3 1 -10 79.12 79.58 1.83 o -2 2 -10 31.57 31.34 1.17 o -1 2 -10 2.59 2.73 0.39 o 0 2 -10 0.03 0.82 0.41 o 1 2 -10 69.84 65.73 1.77 o 2 2 -10 18.87 16.48 0.60 o 3 2 -10 24.16 23.84 0.93 o -2 3 -10 1.84 2.52 0.60 o -1 3 -10 10.21 10.93 0.94 o 0 3 -10 14.36 14.54 0.73 o 1 3 -10 109.90 107.62 2.49 o 2 3 -10 92.53 89.89 1.90 o 3 3 -10 44.62 45.38 1.65 o -2 4 -10 0.66 0.83 0.53 o -1 4 -10 51.12 50.44 1.66 o 0 4 -10 31.03 30.57 1.73 o 1 4 -10 15.58 14.25 0.74 o 2 4 -10 282.30 269.61 5.45 o 3 4 -10 4.36 4.05 0.56 o -1 5 -10 33.19 32.49 1.17 o 0 5 -10 0.23 1.80 0.75 o 1 5 -10 17.19 18.65 1.71 o 2 5 -10 24.82 24.50 1.43 o 3 5 -10 1.50 0.86 0.41 o -1 6 -10 1.80 4.70 1.70 o 0 6 -10 7.86 7.66 0.57 o 1 6 -10 138.82 134.98 4.41 o 2 6 -10 10.53 8.95 0.72 o 3 6 -10 6.69 6.48 0.69 o -1 7 -10 17.06 19.56 0.90 o 0 7 -10 87.07 93.11 5.20 o 1 7 -10 94.02 94.14 3.47 o 2 7 -10 16.27 17.77 0.99 o -1 8 -10 0.13 0.10 0.31 o 0 8 -10 63.14 60.84 2.56 o 1 8 -10 70.90 78.39 3.09 o 2 8 -10 23.15 23.34 1.16 o 0 9 -10 65.43 69.32 2.86 o 1 9 -10 27.19 28.03 1.73 o 2 9 -10 3.50 3.05 0.79 o 0 10 -10 36.69 34.51 1.92 o 1 10 -10 27.12 27.46 1.77 o -1 0 -9 49.01 47.65 1.92 o 1 0 -9 89.67 90.06 2.08 o 3 0 -9 42.40 41.28 1.83 o -2 1 -9 17.06 18.36 0.84 o -1 1 -9 25.37 24.19 1.19 o 0 1 -9 93.86 83.54 1.96 o 1 1 -9 96.21 97.85 1.57 o 2 1 -9 200.97 198.68 2.83 o 3 1 -9 2.56 2.89 0.33 o 4 1 -9 2.76 2.86 0.52 o -2 2 -9 45.34 45.60 1.17 o -1 2 -9 193.10 185.70 3.65 o 0 2 -9 19.67 17.70 0.75 o 1 2 -9 87.76 91.03 1.84 o 2 2 -9 37.89 36.88 0.89 o 3 2 -9 43.05 42.35 1.22 o 4 2 -9 14.88 15.97 1.73 o -2 3 -9 47.25 47.09 1.18 o -1 3 -9 79.10 74.30 1.85 o 1 3 -9 43.08 48.19 1.13 o 2 3 -9 24.91 25.95 0.85 o 3 3 -9 43.10 42.69 1.54 o 4 3 -9 22.83 23.43 1.73 o -2 4 -9 48.47 47.90 1.20 o -1 4 -9 80.85 79.45 1.94 o 0 4 -9 61.20 63.28 1.64 o 1 4 -9 35.14 36.49 0.96 o 2 4 -9 6.11 8.47 2.60 o 3 4 -9 85.54 77.58 2.24 o 4 4 -9 9.52 8.82 1.21 o -2 5 -9 23.70 25.34 0.83 o -1 5 -9 92.12 90.65 2.14 o 0 5 -9 130.98 128.87 3.77 o 1 5 -9 6.16 7.25 0.49 o 2 5 -9 41.30 42.71 1.46 o 3 5 -9 46.89 46.97 1.66 o -2 6 -9 15.66 16.27 1.17 o -1 6 -9 10.18 9.76 0.60 o 0 6 -9 48.33 48.38 1.40 o 1 6 -9 258.30 253.04 4.91 o 2 6 -9 72.71 67.09 1.97 o 3 6 -9 0.99 0.77 0.36 o -1 7 -9 72.47 71.10 1.85 o 0 7 -9 0.06 0.60 0.38 o 1 7 -9 5.45 5.49 0.51 o 2 7 -9 17.42 17.07 1.09 o 3 7 -9 38.05 37.58 1.52 o -1 8 -9 15.74 16.61 0.81 o 0 8 -9 45.54 44.12 1.34 o 1 8 -9 27.34 27.29 1.12 o 2 8 -9 135.03 137.98 3.30 o 3 8 -9 31.74 31.45 1.42 o -1 9 -9 6.84 6.33 0.75 o 0 9 -9 29.84 30.93 1.70 o 1 9 -9 24.71 25.65 1.11 o 2 9 -9 69.56 69.73 2.12 o 0 10 -9 3.11 2.15 0.57 o 1 10 -9 17.12 17.85 0.95 o 2 10 -9 10.42 10.51 0.80 o 1 11 -9 94.93 96.99 2.58 o -2 0 -8 108.59 108.38 3.47 o 0 0 -8 91.11 104.95 3.16 o 2 0 -8 209.40 212.87 4.16 o 4 0 -8 25.72 24.30 1.66 o -3 1 -8 3.98 4.54 0.49 o -2 1 -8 37.06 37.68 1.17 o -1 1 -8 28.95 26.27 1.38 o 0 1 -8 40.90 37.44 1.09 o 1 1 -8 223.84 225.56 2.98 o 2 1 -8 32.36 31.09 1.07 o 3 1 -8 46.97 44.23 1.03 o 4 1 -8 1.16 0.41 0.43 o -3 2 -8 3.04 3.18 0.38 o -2 2 -8 6.81 6.78 0.50 o -1 2 -8 153.58 154.26 3.10 o 0 2 -8 91.15 85.25 1.90 o 1 2 -8 102.31 88.80 1.42 o 2 2 -8 49.85 50.90 1.03 o 3 2 -8 18.12 17.91 0.73 o 4 2 -8 36.48 37.54 1.20 o -3 3 -8 7.84 9.41 0.55 o -2 3 -8 41.00 39.16 1.02 o -1 3 -8 295.17 301.70 4.36 o 0 3 -8 430.71 432.54 7.89 o 1 3 -8 172.19 164.07 2.67 o 2 3 -8 15.98 17.83 0.56 o 3 3 -8 15.50 15.42 0.79 o 4 3 -8 7.05 7.01 0.72 o -3 4 -8 27.36 27.46 1.70 o -2 4 -8 44.42 43.46 1.08 o -1 4 -8 70.81 69.41 1.36 o 0 4 -8 885.36 885.56 14.56 o 1 4 -8 0.29 0.24 0.19 o 2 4 -8 0.12 0.15 0.45 o 3 4 -8 23.63 24.24 1.11 o 4 4 -8 0.01 -0.29 0.41 o -2 5 -8 18.06 16.39 0.66 o -1 5 -8 28.47 29.21 1.42 o 0 5 -8 20.06 18.55 0.74 o 1 5 -8 10.56 11.41 0.50 o 2 5 -8 4.63 4.00 0.48 o 3 5 -8 72.43 71.66 2.09 o 4 5 -8 26.74 25.16 1.47 o -2 6 -8 4.75 4.83 0.60 o -1 6 -8 8.82 9.61 0.56 o 0 6 -8 43.22 43.33 1.24 o 1 6 -8 278.71 286.48 5.93 o 2 6 -8 177.87 170.41 3.69 o 3 6 -8 1.68 3.16 1.15 o -2 7 -8 8.32 8.96 1.09 o -1 7 -8 53.61 53.19 1.48 o 0 7 -8 145.45 153.02 3.80 o 1 7 -8 40.26 40.15 1.31 o 2 7 -8 42.68 42.64 1.45 o 3 7 -8 8.23 8.70 0.72 o -2 8 -8 21.67 23.09 0.98 o -1 8 -8 13.41 12.65 0.68 o 0 8 -8 0.03 0.40 0.73 o 1 8 -8 68.33 66.96 1.84 o 2 8 -8 8.99 7.78 0.63 o 3 8 -8 37.79 35.59 1.46 o -2 9 -8 16.64 18.13 0.89 o -1 9 -8 27.96 29.23 1.47 o 0 9 -8 29.78 28.03 1.51 o 1 9 -8 43.30 41.86 1.41 o 2 9 -8 6.43 6.69 0.61 o 3 9 -8 20.51 19.79 1.09 o -1 10 -8 94.65 93.27 3.09 o 0 10 -8 25.11 25.43 1.47 o 1 10 -8 61.23 57.81 1.76 o 2 10 -8 16.41 17.86 0.99 o 1 11 -8 43.75 48.71 1.61 o 2 11 -8 70.19 72.90 2.18 o 1 12 -8 30.50 31.58 1.30 o 2 12 -8 0.62 0.83 0.60 o -3 0 -7 52.51 51.20 2.11 o -1 0 -7 127.23 110.60 3.24 o 1 0 -7 88.39 96.04 4.07 o 3 0 -7 177.29 175.37 3.62 o -3 1 -7 35.34 34.12 1.17 o -2 1 -7 33.36 33.32 1.05 o -1 1 -7 154.40 138.76 2.70 o 0 1 -7 490.37 483.46 6.66 o 1 1 -7 141.51 156.03 2.60 o 2 1 -7 30.73 30.13 0.72 o 3 1 -7 39.99 39.53 0.92 o 4 1 -7 0.51 0.58 0.33 o -3 2 -7 41.07 42.00 1.33 o -2 2 -7 30.53 29.44 0.99 o -1 2 -7 93.81 96.25 2.04 o 0 2 -7 256.21 258.28 3.20 o 1 2 -7 303.81 306.19 3.83 o 2 2 -7 242.00 248.60 3.82 o 3 2 -7 4.17 3.37 0.36 o 4 2 -7 1.26 1.43 0.36 o -3 3 -7 0.78 0.79 0.28 o -2 3 -7 13.38 13.72 0.56 o -1 3 -7 209.79 218.24 3.24 o 0 3 -7 230.79 240.25 3.53 o 1 3 -7 619.28 611.24 8.34 o 2 3 -7 294.75 289.36 4.36 o 3 3 -7 7.38 7.78 0.49 o 4 3 -7 8.92 10.82 1.36 o -3 4 -7 14.41 13.69 0.79 o -2 4 -7 58.63 59.84 1.28 o -1 4 -7 95.96 98.17 1.70 o 0 4 -7 3.09 2.75 0.26 o 1 4 -7 1032.68 1040.66 17.05 o 2 4 -7 96.44 93.44 2.22 o 3 4 -7 8.64 8.90 0.65 o 4 4 -7 7.06 7.78 0.71 o -3 5 -7 14.48 15.51 0.85 o -2 5 -7 296.45 301.37 4.41 o -1 5 -7 45.32 46.09 1.01 o 0 5 -7 14.41 13.12 0.48 o 1 5 -7 93.78 94.06 1.68 o 2 5 -7 205.59 197.47 4.00 o 3 5 -7 3.25 2.92 0.45 o 4 5 -7 8.40 9.06 0.77 o -3 6 -7 33.03 29.65 1.20 o -2 6 -7 39.33 39.45 1.01 o -1 6 -7 337.28 337.00 4.80 o 0 6 -7 30.34 31.51 1.28 o 1 6 -7 24.19 24.39 0.91 o 2 6 -7 168.47 167.62 3.54 o 3 6 -7 2.33 2.26 0.45 o 4 6 -7 3.60 3.94 0.60 o -2 7 -7 20.91 20.11 0.88 o -1 7 -7 5.41 4.95 0.33 o 0 7 -7 2.44 2.58 0.25 o 1 7 -7 10.57 11.17 0.63 o 2 7 -7 44.13 42.57 1.41 o 3 7 -7 71.08 69.92 4.48 o 4 7 -7 12.74 12.50 0.90 o -2 8 -7 3.82 3.86 0.45 o -1 8 -7 79.62 78.92 1.50 o 0 8 -7 203.06 201.90 3.11 o 1 8 -7 10.58 10.43 0.83 o 2 8 -7 4.88 4.58 0.49 o 3 8 -7 18.69 16.91 0.97 o -2 9 -7 7.98 8.01 0.61 o -1 9 -7 39.46 39.97 1.53 o 0 9 -7 239.55 237.56 4.52 o 1 9 -7 55.69 52.21 1.56 o 2 9 -7 19.92 17.20 0.90 o 3 9 -7 20.26 21.32 1.11 o -2 10 -7 1.30 1.25 0.41 o -1 10 -7 25.95 28.63 1.00 o 0 10 -7 99.46 95.12 2.25 o 1 10 -7 31.15 27.77 1.11 o 2 10 -7 63.06 61.96 1.89 o 3 10 -7 24.18 24.54 1.32 o -2 11 -7 8.14 9.63 0.70 o -1 11 -7 18.46 18.68 1.17 o 0 11 -7 12.13 11.83 0.98 o 1 11 -7 52.64 48.58 1.54 o 2 11 -7 49.15 47.88 2.26 o 0 12 -7 4.72 4.37 0.68 o 1 12 -7 12.02 13.39 0.81 o 2 12 -7 13.23 12.48 0.85 o 0 13 -7 6.74 7.87 0.90 o 1 13 -7 52.49 51.99 2.45 o 2 13 -7 5.26 4.60 0.94 o -4 0 -6 0.28 1.28 0.53 o -2 0 -6 406.22 404.33 9.91 o 0 0 -6 598.26 643.98 11.96 o 2 0 -6 200.40 205.85 4.22 o 4 0 -6 0.65 1.02 0.64 o -3 1 -6 18.61 18.21 0.80 o -2 1 -6 126.05 123.36 2.53 o -1 1 -6 480.88 496.49 8.39 o 0 1 -6 84.99 74.73 1.09 o 1 1 -6 597.71 591.84 6.95 o 2 1 -6 167.61 170.30 2.71 o 3 1 -6 84.74 85.18 1.47 o 4 1 -6 49.52 50.14 1.33 o -3 2 -6 14.58 17.07 0.77 o -2 2 -6 151.26 153.92 3.01 o -1 2 -6 46.20 48.84 1.20 o 0 2 -6 385.78 397.03 4.67 o 1 2 -6 239.18 242.12 3.06 o 2 2 -6 692.55 713.80 8.42 o 3 2 -6 154.05 153.91 2.67 o 4 2 -6 12.93 12.24 0.65 o -3 3 -6 41.85 41.84 1.08 o -2 3 -6 58.95 56.98 1.19 o -1 3 -6 103.24 98.29 1.64 o 0 3 -6 430.30 435.81 5.09 o 1 3 -6 43.97 47.45 0.97 o 2 3 -6 307.37 298.00 4.43 o 3 3 -6 98.91 96.40 1.91 o 4 3 -6 8.04 7.82 0.68 o -3 4 -6 5.25 5.13 0.53 o -2 4 -6 28.54 29.42 0.80 o -1 4 -6 82.63 82.58 1.45 o 0 4 -6 196.65 204.38 2.53 o 1 4 -6 44.65 45.94 0.96 o 2 4 -6 51.30 51.16 1.11 o 3 4 -6 85.85 84.29 2.83 o 4 4 -6 22.12 22.08 1.09 o -3 5 -6 0.33 0.68 0.34 o -2 5 -6 11.88 13.21 0.85 o -1 5 -6 447.05 452.44 6.15 o 0 5 -6 66.70 68.90 1.05 o 1 5 -6 166.13 165.25 12.09 o 2 5 -6 128.90 131.21 2.84 o 3 5 -6 216.10 212.01 8.34 o 4 5 -6 2.87 2.95 0.52 o -3 6 -6 6.48 6.77 0.58 o -2 6 -6 65.58 67.46 1.70 o -1 6 -6 410.65 421.13 5.77 o 0 6 -6 1000.96 1007.55 13.90 o 1 6 -6 26.34 23.85 0.65 o 2 6 -6 20.98 20.92 0.98 o 3 6 -6 4.74 4.24 0.53 o 4 6 -6 12.08 11.55 0.85 o -3 7 -6 3.43 4.33 0.50 o -2 7 -6 145.99 148.30 3.18 o -1 7 -6 161.81 166.84 2.56 o 0 7 -6 131.09 128.53 3.91 o 1 7 -6 182.60 172.65 4.69 o 2 7 -6 42.23 39.59 1.29 o 3 7 -6 1.12 1.71 0.53 o 4 7 -6 9.66 11.21 0.87 o -3 8 -6 4.18 4.11 0.51 o -2 8 -6 5.66 5.61 0.51 o -1 8 -6 38.80 38.60 0.91 o 0 8 -6 14.18 12.47 0.81 o 1 8 -6 332.67 313.07 5.75 o 2 8 -6 51.38 46.11 1.48 o 3 8 -6 32.19 28.61 1.86 o 4 8 -6 1.43 1.86 0.53 o -2 9 -6 7.79 9.14 0.61 o -1 9 -6 14.53 14.89 0.68 o 0 9 -6 14.42 13.34 0.55 o 1 9 -6 261.93 251.04 4.86 o 2 9 -6 51.62 43.25 1.44 o 3 9 -6 18.52 18.11 0.99 o -2 10 -6 39.10 42.59 1.35 o -1 10 -6 21.33 22.13 0.87 o 0 10 -6 0.81 0.90 0.51 o 1 10 -6 2.87 2.44 0.39 o 2 10 -6 67.95 61.41 1.84 o 3 10 -6 8.20 7.57 0.68 o -2 11 -6 0.59 0.82 0.36 o -1 11 -6 58.37 58.73 2.15 o 0 11 -6 123.13 123.79 3.88 o 1 11 -6 1.68 1.34 0.32 o 2 11 -6 24.10 21.61 1.04 o 3 11 -6 5.14 5.42 0.87 o -2 12 -6 10.29 13.37 0.79 o -1 12 -6 58.20 61.25 2.26 o 0 12 -6 42.36 45.24 2.03 o 1 12 -6 30.21 29.51 1.17 o 2 12 -6 16.39 16.58 0.95 o -1 13 -6 30.58 33.45 1.66 o 0 13 -6 49.90 49.76 2.22 o 1 13 -6 22.18 23.47 1.54 o 2 13 -6 8.46 9.81 0.76 o 0 14 -6 13.30 13.18 1.17 o 1 14 -6 15.24 16.39 1.36 o -3 0 -5 14.22 16.58 1.02 o -1 0 -5 1300.35 1402.77 31.91 o 1 0 -5 2694.43 2720.54 43.27 o 3 0 -5 325.72 326.54 6.97 o 5 0 -5 20.17 19.51 1.51 o -4 1 -5 1.90 1.43 0.53 o -3 1 -5 18.34 20.15 1.21 o -2 1 -5 14.87 13.12 0.64 o -1 1 -5 438.20 479.36 7.99 o 0 1 -5 1592.17 1671.90 18.94 o 1 1 -5 258.83 272.04 3.32 o 2 1 -5 22.59 19.61 0.51 o 3 1 -5 76.51 75.39 1.32 o 4 1 -5 105.13 107.15 2.12 o 5 1 -5 10.83 11.57 1.24 o -4 2 -5 0.69 0.76 0.36 o -3 2 -5 13.27 13.31 0.65 o -2 2 -5 52.37 51.44 3.24 o -1 2 -5 11.62 12.15 0.87 o 0 2 -5 121.76 129.05 1.68 o 1 2 -5 27.55 32.26 0.61 o 2 2 -5 127.25 119.37 2.02 o 3 2 -5 111.37 114.53 2.09 o 4 2 -5 22.81 23.65 1.04 o 5 2 -5 3.71 3.50 0.90 o -4 3 -5 0.73 0.87 0.49 o -3 3 -5 37.78 36.87 0.96 o -2 3 -5 116.28 117.05 1.95 o -1 3 -5 146.00 141.10 1.83 o 0 3 -5 333.68 338.75 3.97 o 1 3 -5 188.75 202.73 2.47 o 2 3 -5 272.62 266.46 6.36 o 3 3 -5 68.63 66.85 1.78 o 4 3 -5 12.67 14.22 0.85 o -4 4 -5 0.95 1.36 0.57 o -3 4 -5 5.22 5.89 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