#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2201571.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201571_Fobs loop_ _publ_author_name 'Gainsford, Graeme J.' 'Evans, Gary B.' _publ_section_title ; 3-Bromo-7-methoxy-2-(tetrahydropyran-2-yl)pyrazolo[4,3-d]pyrimidine ; _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1021 _journal_page_last o1022 _journal_volume 58 _journal_year 2002 _space_group_IT_number 33 _symmetry_space_group_name_Hall 'P 2c -2n' _symmetry_space_group_name_H-M 'P n a 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 12.4224 _cell_length_b 17.1489 _cell_length_c 5.6680 _exptl_crystal_F_000 632.00 _reflns_d_resolution_high 0.8088 _[local]_cod_data_source_file ob6166Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' geb28 in Pna2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 167.34 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' 'x+1/2, -y+1/2, z' '-x+1/2, y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 1 -7 269.03 313.05 112.27 o 0 0 -6 1121.70 1246.97 100.15 o 2 0 -6 370.28 438.98 57.68 o 4 0 -6 423.70 487.36 48.33 o 6 0 -6 21.57 43.47 37.62 o 1 1 -6 559.39 675.96 35.85 o 2 1 -6 413.34 474.69 38.81 o 3 1 -6 515.95 609.78 37.70 o 4 1 -6 347.82 329.71 29.97 o 5 1 -6 344.03 363.24 31.65 o 6 1 -6 272.97 290.43 35.87 o 7 1 -6 24.76 38.52 42.84 o 0 2 -6 1276.24 1507.09 79.44 o 1 2 -6 227.10 222.77 27.52 o 2 2 -6 424.94 424.16 37.04 o 3 2 -6 581.84 644.36 45.03 o 4 2 -6 134.44 143.77 31.18 o 5 2 -6 924.47 963.47 57.34 o 6 2 -6 37.64 10.79 34.69 o 1 3 -6 44.27 39.22 29.42 o 2 3 -6 281.34 302.64 35.36 o 3 3 -6 57.13 66.34 28.79 o 4 3 -6 631.51 655.79 125.87 o 5 3 -6 16.63 33.19 28.60 o 6 3 -6 1172.33 1119.36 117.27 o 0 4 -6 186.29 218.85 67.15 o 1 4 -6 245.06 296.80 37.21 o 2 4 -6 359.44 382.27 39.09 o 3 4 -6 220.33 309.27 38.63 o 4 4 -6 32.56 45.27 31.46 o 5 4 -6 673.32 695.54 55.28 o 1 5 -6 635.03 865.46 56.83 o 2 5 -6 215.83 161.16 36.97 o 3 5 -6 627.83 780.83 51.91 o 4 5 -6 111.18 141.04 32.88 o 5 5 -6 18.84 64.98 35.96 o 0 6 -6 1119.25 1630.13 168.29 o 1 6 -6 7.38 11.02 58.75 o 2 6 -6 936.31 1231.92 71.76 o 3 6 -6 18.07 7.84 30.97 o 4 6 -6 522.75 616.64 48.31 o 5 6 -6 16.03 27.81 55.28 o 1 7 -6 825.81 962.06 85.34 o 2 7 -6 85.27 115.86 36.39 o 3 7 -6 905.29 1029.00 68.01 o 4 7 -6 149.41 158.60 59.16 o 0 8 -6 529.74 451.22 85.22 o 1 8 -6 31.12 -13.98 57.50 o 2 8 -6 375.00 469.29 97.27 o 3 8 -6 281.38 328.36 74.54 o 4 8 -6 67.29 19.43 98.18 o 3 9 -6 7.58 -39.54 56.59 o 4 9 -6 307.01 416.45 146.70 o 2 0 -5 1179.57 1119.72 179.67 o 4 0 -5 1038.14 923.77 88.07 o 6 0 -5 1475.13 1662.20 131.11 o 8 0 -5 1119.95 1050.31 108.35 o 0 1 -5 399.07 368.15 31.64 o 1 1 -5 98.30 59.25 15.45 o 2 1 -5 1654.18 1771.55 63.13 o 3 1 -5 533.59 585.97 32.33 o 4 1 -5 540.46 480.34 30.56 o 5 1 -5 894.32 894.86 43.80 o 6 1 -5 21.24 29.70 33.63 o 7 1 -5 1734.54 1982.63 106.34 o 8 1 -5 497.54 554.07 63.39 o 9 1 -5 878.86 928.89 92.67 o 10 1 -5 163.86 239.64 128.06 o 1 2 -5 1655.28 1877.54 66.10 o 2 2 -5 226.06 185.25 19.68 o 3 2 -5 1464.16 1468.96 63.17 o 4 2 -5 1331.33 1357.59 66.69 o 5 2 -5 208.41 223.95 31.64 o 6 2 -5 487.77 520.09 42.70 o 7 2 -5 18.05 9.73 40.05 o 8 2 -5 613.54 619.90 66.11 o 9 2 -5 249.87 304.90 55.24 o 10 2 -5 556.18 815.18 179.53 o 0 3 -5 1288.32 1095.07 241.00 o 1 3 -5 97.80 90.12 17.15 o 2 3 -5 2103.84 2338.86 85.31 o 3 3 -5 29.29 1.72 19.25 o 4 3 -5 545.00 627.21 41.81 o 5 3 -5 65.57 92.22 27.80 o 6 3 -5 62.24 93.32 34.83 o 7 3 -5 134.59 134.57 42.18 o 8 3 -5 298.44 329.30 52.81 o 9 3 -5 23.96 73.19 46.84 o 10 3 -5 201.75 304.87 156.81 o 1 4 -5 1741.06 1854.17 69.70 o 2 4 -5 334.43 332.75 31.44 o 3 4 -5 1257.02 1326.23 64.27 o 4 4 -5 154.40 132.69 39.10 o 5 4 -5 220.34 192.35 30.84 o 6 4 -5 443.70 404.05 39.71 o 7 4 -5 18.73 9.59 32.40 o 8 4 -5 354.40 370.27 55.34 o 9 4 -5 242.09 239.09 60.93 o 10 4 -5 160.67 330.21 160.33 o 0 5 -5 420.74 397.41 42.06 o 1 5 -5 441.60 488.63 39.27 o 2 5 -5 1076.76 1155.05 57.18 o 3 5 -5 661.07 677.75 44.26 o 4 5 -5 162.87 178.29 29.26 o 5 5 -5 751.38 823.63 51.83 o 6 5 -5 57.06 36.12 29.51 o 7 5 -5 1265.23 1399.33 75.63 o 8 5 -5 107.32 130.76 40.50 o 9 5 -5 463.70 457.03 86.25 o 1 6 -5 0.20 -4.68 23.95 o 2 6 -5 764.31 756.79 48.76 o 3 6 -5 101.00 79.88 31.83 o 4 6 -5 952.98 882.00 60.09 o 5 6 -5 22.88 15.12 28.16 o 6 6 -5 1870.20 2013.31 92.86 o 7 6 -5 67.54 130.13 39.47 o 8 6 -5 1061.56 1153.53 80.20 o 9 6 -5 11.04 88.18 85.68 o 0 7 -5 216.08 202.26 60.34 o 1 7 -5 181.88 169.33 30.26 o 2 7 -5 158.72 182.39 32.25 o 3 7 -5 555.33 566.60 45.78 o 4 7 -5 195.31 194.69 33.19 o 5 7 -5 1124.01 1333.22 70.45 o 6 7 -5 76.77 45.09 34.88 o 7 7 -5 1359.25 1669.06 124.19 o 8 7 -5 32.94 88.09 70.13 o 9 7 -5 939.73 1206.63 214.87 o 1 8 -5 570.78 649.78 74.36 o 2 8 -5 83.24 130.90 32.31 o 3 8 -5 292.87 375.15 41.72 o 4 8 -5 297.98 339.28 44.50 o 5 8 -5 218.37 240.45 44.88 o 6 8 -5 468.77 497.70 52.63 o 7 8 -5 91.58 115.61 42.91 o 8 8 -5 214.72 208.81 76.87 o 9 8 -5 144.30 329.87 165.56 o 0 9 -5 1863.39 2119.19 201.24 o 1 9 -5 5.95 -2.53 30.15 o 2 9 -5 1051.87 1217.31 69.99 o 3 9 -5 4.74 30.44 33.07 o 4 9 -5 694.47 711.50 62.33 o 5 9 -5 75.13 47.15 39.50 o 6 9 -5 190.59 167.36 49.42 o 7 9 -5 57.18 48.63 91.93 o 8 9 -5 133.32 113.29 116.36 o 1 10 -5 2338.56 2566.42 133.45 o 2 10 -5 4.17 11.83 42.93 o 3 10 -5 748.45 838.88 67.31 o 4 10 -5 129.21 164.74 45.69 o 5 10 -5 403.72 504.65 63.37 o 6 10 -5 44.27 42.03 45.95 o 7 10 -5 40.45 82.72 99.20 o 0 11 -5 475.23 621.47 90.39 o 1 11 -5 82.20 73.64 39.07 o 2 11 -5 609.28 678.16 60.99 o 3 11 -5 524.66 563.30 57.18 o 4 11 -5 157.31 140.52 45.04 o 5 11 -5 364.89 383.40 55.76 o 6 11 -5 87.95 179.88 107.72 o 1 12 -5 13.29 38.10 34.25 o 2 12 -5 164.18 130.67 43.81 o 3 12 -5 2.12 64.89 39.02 o 4 12 -5 683.08 804.10 73.32 o 5 12 -5 5.60 43.63 79.77 o 0 13 -5 154.71 116.62 56.75 o 1 13 -5 83.22 109.55 40.88 o 2 13 -5 136.90 96.19 47.49 o 3 13 -5 372.26 503.17 75.03 o 1 14 -5 213.96 384.41 97.83 o 0 0 -4 6853.36 6323.30 404.29 o 2 0 -4 5495.91 5725.81 231.13 o 4 0 -4 799.34 808.65 72.28 o 6 0 -4 33.67 51.37 47.67 o 8 0 -4 161.65 136.42 60.24 o 10 0 -4 1017.99 915.05 102.64 o 12 0 -4 1270.73 1070.83 147.83 o 1 1 -4 3314.65 3176.94 100.23 o 2 1 -4 229.60 216.90 19.43 o 3 1 -4 1655.07 1595.26 60.41 o 4 1 -4 187.63 177.58 31.64 o 5 1 -4 838.46 894.90 56.96 o 6 1 -4 1049.10 1014.59 62.94 o 7 1 -4 95.31 101.97 36.76 o 8 1 -4 303.36 360.09 52.75 o 9 1 -4 1231.20 1323.23 84.56 o 10 1 -4 173.25 181.18 52.33 o 11 1 -4 664.28 653.82 70.04 o 12 1 -4 85.30 128.87 84.23 o 0 2 -4 1511.78 1270.15 148.46 o 1 2 -4 228.97 190.53 15.73 o 2 2 -4 739.43 703.72 35.00 o 3 2 -4 666.68 680.22 35.34 o 4 2 -4 361.35 369.69 30.96 o 5 2 -4 2368.72 2625.71 121.00 o 6 2 -4 89.85 44.26 32.30 o 7 2 -4 1628.14 1784.62 96.63 o 8 2 -4 78.78 80.12 39.13 o 9 2 -4 1595.73 1543.68 110.50 o 10 2 -4 441.55 432.18 62.61 o 11 2 -4 411.78 343.03 61.36 o 12 2 -4 372.51 429.18 136.01 o 1 3 -4 215.37 182.29 17.05 o 2 3 -4 288.17 253.31 18.75 o 3 3 -4 441.19 349.83 61.22 o 4 3 -4 4582.70 4866.60 183.00 o 5 3 -4 118.02 129.38 33.55 o 6 3 -4 2371.52 2915.60 153.21 o 7 3 -4 108.16 146.17 48.29 o 8 3 -4 1298.27 1382.07 117.55 o 9 3 -4 24.59 13.55 52.50 o 10 3 -4 1635.14 1569.43 112.77 o 11 3 -4 52.93 31.76 56.07 o 0 4 -4 1661.71 1674.45 106.38 o 1 4 -4 618.62 568.17 26.39 o 2 4 -4 124.29 136.65 14.78 o 3 4 -4 520.97 609.06 43.59 o 4 4 -4 630.06 593.93 42.45 o 5 4 -4 1611.89 1875.88 91.06 o 6 4 -4 211.25 261.97 49.86 o 7 4 -4 1677.07 1827.07 145.11 o 8 4 -4 636.12 774.83 100.33 o 9 4 -4 1545.46 1652.54 124.95 o 10 4 -4 271.99 302.25 74.28 o 11 4 -4 598.50 686.78 150.79 o 1 5 -4 3585.82 3186.17 129.97 o 2 5 -4 372.44 342.33 29.14 o 3 5 -4 1276.15 1310.64 66.66 o 4 5 -4 92.82 105.21 28.24 o 5 5 -4 1306.57 1395.17 73.80 o 6 5 -4 2192.45 2498.05 138.20 o 7 5 -4 103.40 61.12 43.39 o 8 5 -4 426.02 495.33 103.39 o 9 5 -4 549.99 613.09 75.43 o 10 5 -4 196.56 130.57 115.85 o 11 5 -4 584.78 594.05 138.51 o 0 6 -4 2887.87 2713.23 211.86 o 1 6 -4 298.59 241.53 25.59 o 2 6 -4 4169.33 3871.94 184.29 o 3 6 -4 21.72 15.41 21.59 o 4 6 -4 1253.42 1229.02 76.63 o 5 6 -4 239.79 234.36 37.22 o 6 6 -4 107.62 139.97 37.49 o 7 6 -4 258.77 335.69 57.27 o 8 6 -4 60.27 28.20 40.76 o 9 6 -4 219.21 207.52 64.65 o 10 6 -4 824.20 967.78 152.83 o 1 7 -4 2525.59 2103.05 171.62 o 2 7 -4 57.25 33.09 23.43 o 3 7 -4 1545.45 1532.91 85.25 o 4 7 -4 24.47 52.34 27.56 o 5 7 -4 59.68 38.92 32.07 o 6 7 -4 383.58 389.63 46.09 o 7 7 -4 10.79 -15.65 31.84 o 8 7 -4 402.20 384.74 66.82 o 9 7 -4 521.23 562.92 133.74 o 10 7 -4 69.16 75.45 108.63 o 0 8 -4 979.66 946.91 68.26 o 1 8 -4 291.25 250.64 26.56 o 2 8 -4 651.68 648.53 102.01 o 3 8 -4 880.55 768.94 74.87 o 4 8 -4 363.12 453.58 49.36 o 5 8 -4 1742.84 1942.01 95.88 o 6 8 -4 39.48 54.30 35.12 o 7 8 -4 1770.20 2000.85 106.00 o 8 8 -4 53.08 55.61 47.09 o 9 8 -4 381.21 370.20 136.24 o 10 8 -4 180.80 168.06 126.70 o 1 9 -4 126.67 110.58 29.98 o 2 9 -4 611.93 640.39 78.22 o 3 9 -4 173.48 198.24 27.85 o 4 9 -4 2329.74 2369.39 124.51 o 5 9 -4 164.20 179.73 41.35 o 6 9 -4 2256.75 2466.19 137.62 o 7 9 -4 131.14 184.83 55.32 o 8 9 -4 1298.05 1427.34 127.72 o 9 9 -4 9.78 42.34 72.39 o 0 10 -4 346.41 313.70 82.04 o 1 10 -4 526.75 537.44 37.90 o 2 10 -4 232.11 267.99 30.87 o 3 10 -4 598.06 590.80 41.55 o 4 10 -4 274.51 250.15 43.84 o 5 10 -4 1313.69 1501.66 146.78 o 6 10 -4 29.80 63.44 41.60 o 7 10 -4 1529.20 1662.04 135.54 o 8 10 -4 158.89 171.30 78.43 o 9 10 -4 1313.64 1381.85 188.40 o 1 11 -4 1039.52 1096.67 59.87 o 2 11 -4 373.28 350.66 34.50 o 3 11 -4 397.78 425.85 38.47 o 4 11 -4 209.44 238.37 44.34 o 5 11 -4 254.81 241.77 50.53 o 6 11 -4 1401.08 1496.40 126.82 o 7 11 -4 59.92 91.67 67.85 o 8 11 -4 936.53 995.20 119.03 o 0 12 -4 447.42 525.99 57.18 o 1 12 -4 338.06 321.57 35.45 o 2 12 -4 1057.43 1399.42 124.25 o 3 12 -4 39.10 40.10 28.08 o 4 12 -4 589.16 649.21 50.71 o 5 12 -4 147.00 155.27 64.76 o 6 12 -4 112.66 225.88 71.98 o 7 12 -4 39.14 53.21 78.92 o 8 12 -4 3.74 0.91 91.47 o 1 13 -4 1739.68 1692.97 97.93 o 2 13 -4 50.76 75.18 32.58 o 3 13 -4 677.91 869.48 70.94 o 4 13 -4 179.43 177.33 46.42 o 5 13 -4 64.50 125.43 61.44 o 6 13 -4 265.87 303.39 81.49 o 7 13 -4 3.49 -71.70 80.90 o 0 14 -4 901.31 834.99 174.36 o 1 14 -4 61.45 65.69 37.16 o 2 14 -4 663.28 609.92 56.92 o 3 14 -4 526.01 517.94 57.31 o 4 14 -4 911.73 1074.43 128.68 o 5 14 -4 764.33 791.98 94.74 o 6 14 -4 77.58 6.59 88.97 o 1 15 -4 88.74 116.00 56.38 o 2 15 -4 287.94 428.46 66.93 o 3 15 -4 272.07 355.05 72.17 o 4 15 -4 1420.12 1981.58 199.42 o 0 16 -4 241.74 254.42 87.84 o 1 16 -4 36.15 63.19 51.58 o 2 16 -4 26.82 39.43 47.95 o 3 16 -4 432.84 630.42 121.70 o 2 0 -3 3885.77 3934.16 187.17 o 4 0 -3 2083.02 2349.29 160.84 o 6 0 -3 8037.24 9211.12 523.14 o 8 0 -3 1420.74 1410.14 163.97 o 10 0 -3 3751.41 3234.01 296.00 o 0 1 -3 316.56 331.10 23.74 o 1 1 -3 833.17 836.32 32.81 o 2 1 -3 2263.16 2283.11 105.09 o 3 1 -3 793.09 873.35 48.66 o 4 1 -3 389.13 400.79 34.38 o 5 1 -3 3218.02 3594.19 178.02 o 6 1 -3 54.99 91.23 35.29 o 7 1 -3 5802.38 6554.04 312.22 o 8 1 -3 40.35 55.01 42.17 o 9 1 -3 827.87 911.31 77.78 o 10 1 -3 733.43 734.76 75.06 o 11 1 -3 1317.48 1125.69 122.57 o 1 2 -3 4429.14 4101.25 117.42 o 2 2 -3 629.55 567.26 55.30 o 3 2 -3 2573.01 2655.62 113.69 o 4 2 -3 976.38 868.86 58.33 o 5 2 -3 727.81 794.03 59.02 o 6 2 -3 1324.64 1466.75 90.95 o 7 2 -3 420.47 392.35 46.11 o 8 2 -3 338.35 279.88 51.81 o 9 2 -3 803.47 944.00 82.28 o 10 2 -3 910.16 917.58 86.30 o 11 2 -3 1489.26 1288.67 167.83 o 0 3 -3 7355.91 6477.05 256.65 o 1 3 -3 87.94 90.44 10.81 o 2 3 -3 7805.70 7466.44 240.34 o 3 3 -3 132.10 116.50 18.21 o 4 3 -3 2075.17 2198.74 114.71 o 5 3 -3 149.17 118.11 31.97 o 6 3 -3 438.04 563.42 53.40 o 7 3 -3 110.43 125.09 41.44 o 8 3 -3 593.12 680.37 67.43 o 9 3 -3 8.32 49.59 46.86 o 10 3 -3 520.22 445.88 114.08 o 11 3 -3 25.39 30.57 108.97 o 1 4 -3 6915.91 6685.26 237.37 o 2 4 -3 262.85 270.89 22.71 o 3 4 -3 908.02 895.42 42.52 o 4 4 -3 1802.07 1750.68 120.31 o 5 4 -3 854.25 937.66 65.26 o 6 4 -3 554.72 627.23 56.97 o 7 4 -3 55.71 90.10 43.93 o 8 4 -3 694.07 720.39 68.38 o 9 4 -3 748.79 1248.59 157.41 o 10 4 -3 218.33 353.61 131.13 o 11 4 -3 1075.05 989.94 156.35 o 0 5 -3 1348.15 1225.69 83.12 o 1 5 -3 296.01 232.75 36.44 o 2 5 -3 2397.18 2374.31 107.51 o 3 5 -3 3166.10 3098.22 131.34 o 4 5 -3 389.91 435.98 35.60 o 5 5 -3 3347.33 3552.91 247.49 o 6 5 -3 135.63 159.08 41.74 o 7 5 -3 2593.05 2903.76 154.52 o 8 5 -3 287.59 426.52 60.99 o 9 5 -3 1702.46 1675.74 131.14 o 10 5 -3 97.90 116.02 95.11 o 11 5 -3 311.41 312.48 114.20 o 12 5 -3 557.59 431.22 137.26 o 1 6 -3 270.75 244.51 18.39 o 2 6 -3 421.28 347.62 28.67 o 3 6 -3 28.48 33.82 14.34 o 4 6 -3 3948.78 3639.97 153.19 o 5 6 -3 616.63 650.79 63.35 o 6 6 -3 4571.12 4749.09 231.23 o 7 6 -3 75.26 71.56 42.82 o 8 6 -3 2965.91 2925.73 158.09 o 9 6 -3 63.52 17.61 80.22 o 10 6 -3 1855.44 1660.47 197.60 o 11 6 -3 159.31 171.24 125.11 o 12 6 -3 218.18 156.35 145.56 o 0 7 -3 823.33 737.96 54.83 o 1 7 -3 47.36 52.21 15.23 o 2 7 -3 1119.52 1047.02 50.76 o 3 7 -3 1356.68 1212.20 57.79 o 4 7 -3 408.08 429.29 38.74 o 5 7 -3 1698.00 1671.97 82.39 o 6 7 -3 345.40 343.28 48.19 o 7 7 -3 2837.03 2821.09 151.95 o 8 7 -3 284.87 281.69 104.31 o 9 7 -3 2098.57 2703.02 285.32 o 10 7 -3 664.56 592.24 131.92 o 11 7 -3 536.51 463.95 148.17 o 12 7 -3 199.35 107.04 115.90 o 1 8 -3 3023.30 2567.98 108.05 o 2 8 -3 216.92 177.43 21.27 o 3 8 -3 1304.79 1134.50 56.24 o 4 8 -3 1797.38 1712.57 94.66 o 5 8 -3 1166.07 1113.86 63.78 o 6 8 -3 677.30 688.95 52.62 o 7 8 -3 244.36 254.56 55.17 o 8 8 -3 1070.10 1137.32 163.63 o 9 8 -3 393.73 348.73 131.13 o 10 8 -3 1363.71 1482.52 197.49 o 11 8 -3 578.00 598.83 161.69 o 12 8 -3 30.83 87.72 133.06 o 0 9 -3 2672.21 2397.66 144.96 o 1 9 -3 255.84 235.82 24.22 o 2 9 -3 2780.50 2537.88 108.71 o 3 9 -3 252.62 281.61 29.30 o 4 9 -3 1566.78 1408.94 68.82 o 5 9 -3 267.68 273.75 41.69 o 6 9 -3 574.29 619.14 61.47 o 7 9 -3 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o 8 0 1 8345.71 9704.97 774.50 o 2 1 1 227.96 218.28 39.66 o 3 1 1 4412.76 5116.96 409.41 o 4 1 1 1902.63 2425.87 147.35 o 5 1 1 4687.67 5535.94 317.33 o 6 1 1 1728.12 2005.72 213.29 o 7 1 1 9919.05 12492.98 698.10 o 8 1 1 444.23 462.39 59.30 o 9 1 1 2873.15 3002.54 273.62 o 1 2 1 5567.28 4773.12 377.48 o 2 2 1 8698.63 8776.96 687.12 o 3 2 1 10072.63 11323.85 885.74 o 4 2 1 4188.01 5178.09 418.27 o 5 2 1 457.15 495.77 39.15 o 6 2 1 2382.61 2600.19 131.28 o 7 2 1 15.80 14.29 30.47 o 8 2 1 1841.18 1969.72 135.10 o 9 2 1 615.38 563.03 88.97 o 0 3 1 27342.76 27046.86 2080.78 o 1 3 1 6680.89 5794.19 322.42 o 2 3 1 24833.47 22281.36 1719.67 o 3 3 1 524.81 619.28 70.68 o 4 3 1 2103.84 2045.78 125.59 o 5 3 1 93.71 125.58 34.01 o 6 3 1 458.06 433.69 39.52 o 7 3 1 204.59 250.72 44.84 o 8 3 1 540.79 598.83 89.54 o 9 3 1 611.35 611.55 94.88 o 1 4 1 20719.53 17370.40 994.43 o 2 4 1 4937.96 4886.79 275.99 o 3 4 1 3855.75 3790.68 296.69 o 4 4 1 124.10 192.73 33.26 o 5 4 1 2232.08 2526.20 155.62 o 6 4 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162.72 o 3 8 1 2441.67 2551.45 157.21 o 4 8 1 2891.45 2884.25 248.28 o 5 8 1 1586.83 1451.39 144.54 o 0 9 1 9405.48 8418.12 665.98 o 1 9 1 78.15 88.29 35.77 o 2 9 1 3182.74 2926.06 178.33 o 3 9 1 254.80 317.09 51.09 o 4 9 1 2856.24 2962.66 258.85 o 1 10 1 5601.50 5773.52 332.22 o 2 10 1 231.08 238.44 50.99 o 3 10 1 2174.61 1953.65 155.56 o 4 10 1 828.23 644.96 93.52 o 0 11 1 2136.22 2216.23 206.01 o 1 11 1 642.77 649.33 100.11 o 2 11 1 1394.93 1413.26 106.36 o 3 11 1 2720.25 2587.50 266.35 o 4 11 1 1150.06 1115.05 135.56 o 1 12 1 935.26 945.13 82.36 o 2 12 1 1022.73 1027.29 87.30 o 3 12 1 31.93 50.05 51.80 o 4 12 1 2947.93 3406.61 308.50 o 0 13 1 915.98 950.96 125.67 o 1 13 1 32.43 22.53 42.73 o 2 13 1 381.09 424.20 68.66 o 3 13 1 1989.45 2208.27 212.15 o 4 13 1 7.31 15.68 65.00 o 1 14 1 1381.99 1338.29 108.66 o 2 14 1 101.76 66.02 74.54 o 3 14 1 1463.96 1396.73 155.90 o 4 14 1 209.40 116.13 77.27 o 0 15 1 2398.86 2509.62 241.46 o 1 15 1 21.28 3.64 73.52 o 2 15 1 3172.88 3160.94 289.87 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7478.22 431.39 o 9 3 2 431.33 510.44 69.77 o 10 3 2 1503.15 1211.29 143.63 o 0 4 2 2381.78 2448.60 199.76 o 1 4 2 1281.94 1137.20 106.02 o 2 4 2 262.43 188.97 45.68 o 3 4 2 3679.84 3953.62 227.04 o 4 4 2 1974.93 1974.86 124.29 o 5 4 2 3773.41 3829.20 321.57 o 6 4 2 178.77 221.58 65.79 o 7 4 2 3617.23 3960.32 340.66 o 8 4 2 18.31 37.56 38.81 o 9 4 2 6279.39 5778.40 485.20 o 10 4 2 28.07 40.79 61.93 o 1 5 2 1885.23 1596.32 114.20 o 2 5 2 1547.83 1329.35 126.13 o 3 5 2 1867.48 1728.42 157.04 o 4 5 2 2258.25 2081.35 187.03 o 5 5 2 1412.20 1360.03 137.61 o 6 5 2 2160.85 2214.75 205.56 o 7 5 2 340.59 425.20 81.70 o 8 5 2 875.54 756.86 74.39 o 9 5 2 301.53 197.03 73.52 o 10 5 2 530.35 476.90 108.29 o 0 6 2 3531.99 2645.06 223.51 o 1 6 2 37.30 23.18 24.49 o 2 6 2 5049.27 3667.63 211.74 o 3 6 2 112.63 145.45 43.97 o 4 6 2 4729.11 4891.86 402.59 o 5 6 2 36.75 44.54 41.93 o 6 6 2 16.26 21.14 50.34 o 7 6 2 65.99 56.47 52.61 o 8 6 2 341.71 300.89 79.43 o 9 6 2 43.46 54.54 61.02 o 10 6 2 2230.57 1979.76 207.37 o 1 7 2 8973.55 8657.38 483.80 o 2 7 2 3682.18 3416.27 286.80 o 3 7 2 7145.09 6410.86 512.13 o 4 7 2 470.61 372.93 62.16 o 5 7 2 865.04 885.97 109.31 o 6 7 2 806.47 912.33 120.22 o 7 7 2 56.30 48.18 62.38 o 8 7 2 727.97 808.81 122.15 o 9 7 2 774.70 856.88 134.76 o 10 7 2 779.31 749.04 134.99 o 0 8 2 10774.37 9429.53 741.66 o 1 8 2 2437.55 1875.91 169.54 o 2 8 2 2669.40 2465.64 218.28 o 5 8 2 2141.55 2397.92 223.85 o 6 8 2 89.11 43.75 48.07 o 7 8 2 2434.15 2443.15 235.55 o 8 8 2 75.89 -3.30 56.70 o 9 8 2 663.99 611.78 112.15 o 10 8 2 292.56 392.25 107.27 o 6 0 3 7696.42 7766.11 625.98 o 8 0 3 1685.29 1461.16 156.81 o 10 0 3 3518.02 2890.16 268.96 o 5 1 3 3192.40 3096.63 267.03 o 6 1 3 76.13 50.69 33.03 o 7 1 3 5795.38 5644.43 330.43 o 8 1 3 27.76 28.27 35.11 o 9 1 3 826.30 799.81 81.40 o 10 1 3 612.36 580.40 78.64 o 11 1 3 1288.19 1037.44 147.49 o 4 2 3 1021.23 858.81 97.27 o 5 2 3 765.55 682.34 90.34 o 6 2 3 1373.17 1459.68 150.56 o 7 2 3 430.94 407.47 54.58 o 8 2 3 539.97 519.68 66.77 o 9 2 3 672.90 668.94 76.33 o 10 2 3 990.72 943.10 97.29 o 11 2 3 1413.60 1239.24 156.35 o 2 3 3 7014.17 6175.30 492.24 o 3 3 3 123.66 111.92 46.02 o 4 3 3 2197.65 2026.69 183.40 o 5 3 3 143.75 125.56 52.95 o 6 3 3 440.65 332.93 65.00 o 7 3 3 105.57 83.74 51.59 o 8 3 3 658.08 669.85 71.75 o 9 3 3 9.92 -15.01 41.20 o 10 3 3 462.71 365.17 66.73 o 11 3 3 33.46 14.89 75.90 o 1 4 3 6816.88 6519.49 515.88 o 2 4 3 368.81 340.09 61.70 o 3 4 3 737.68 619.85 82.27 o 4 4 3 2004.00 1851.48 173.51 o 5 4 3 901.79 673.59 89.31 o 6 4 3 428.47 450.65 82.61 o 7 4 3 51.93 65.45 63.18 o 8 4 3 826.81 662.57 71.47 o 9 4 3 612.25 617.36 75.04 o 10 4 3 260.52 238.51 83.06 o 11 4 3 1083.36 908.92 129.08 o 0 5 3 1432.55 1173.11 107.15 o 1 5 3 210.94 133.36 25.96 o 2 5 3 2535.97 2441.21 211.24 o 3 5 3 3167.82 3043.68 260.78 o 4 5 3 358.04 267.26 63.52 o 5 5 3 3237.62 3069.81 269.53 o 6 5 3 95.14 125.56 62.38 o 7 5 3 2663.86 2675.06 249.76 o 9 5 3 2012.79 1744.50 129.36 o 10 5 3 142.76 119.65 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4 1452.21 1180.72 128.74 o 5 6 4 218.35 126.36 71.47 o 6 6 4 151.88 69.31 63.52 o 7 6 4 257.30 209.87 77.04 o 8 6 4 81.47 63.06 66.36 o 9 6 4 237.42 155.90 80.90 o 10 6 4 795.74 610.53 118.63 o 11 6 4 7.95 82.49 84.54 o 1 7 4 2398.03 1926.81 173.74 o 2 7 4 98.69 146.24 60.22 o 3 7 4 1354.65 1258.33 132.95 o 4 7 4 8.42 -33.41 43.29 o 5 7 4 136.32 133.86 68.06 o 6 7 4 364.71 217.49 75.22 o 7 7 4 10.71 -9.32 55.34 o 8 7 4 267.41 265.67 89.20 o 9 7 4 494.81 441.90 103.18 o 10 7 4 73.96 73.40 77.15 o 11 7 4 374.60 231.24 102.72 o 1 8 4 280.13 407.13 89.20 o 2 8 4 517.64 378.84 72.95 o 3 8 4 750.03 768.02 94.77 o 4 8 4 322.47 228.74 67.27 o 5 8 4 1722.41 1862.16 187.03 o 6 8 4 21.96 45.00 62.16 o 7 8 4 1834.12 1769.66 189.65 o 8 8 4 60.40 96.24 73.86 o 9 8 4 398.66 342.48 95.68 o 10 8 4 117.30 113.97 87.38 o 3 9 4 174.96 119.99 53.97 o 4 9 4 2388.95 2276.91 210.10 o 5 9 4 150.28 112.38 69.65 o 6 9 4 2300.27 2394.97 235.67 o 7 9 4 120.01 156.35 87.95 o 8 9 4 1264.12 1193.68 162.72 o 9 9 4 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382.90 244.42 78.63 o 7 4 5 21.59 36.25 75.45 o 8 4 5 324.04 315.09 91.47 o 9 4 5 235.04 200.73 67.37 o 10 4 5 165.31 251.23 93.74 o 1 5 5 389.32 259.07 65.00 o 2 5 5 1072.19 959.83 114.08 o 3 5 5 562.67 413.95 76.93 o 4 5 5 157.89 88.86 61.59 o 5 5 5 741.93 589.51 103.29 o 6 5 5 48.75 120.45 78.06 o 7 5 5 1323.69 1264.13 158.17 o 8 5 5 116.35 114.31 80.45 o 9 5 5 578.59 398.76 75.38 o 10 5 5 168.30 152.95 98.63 o 2 6 5 756.26 684.50 104.20 o 3 6 5 124.48 119.88 72.72 o 4 6 5 1143.46 923.69 120.11 o 5 6 5 16.19 24.88 65.79 o 6 6 5 1921.07 1899.20 195.78 o 7 6 5 68.97 138.63 93.06 o 8 6 5 970.80 833.02 137.61 o 1 7 5 232.95 105.56 55.91 o 2 7 5 171.72 45.22 57.72 o 3 7 5 609.28 484.74 84.09 o 4 7 5 175.15 102.83 71.70 o 5 7 5 1117.43 1141.07 137.95 o 6 7 5 66.82 -36.93 61.70 o 7 7 5 1403.68 1134.02 144.54 o 8 7 5 34.42 90.79 88.06 o 1 8 5 613.50 483.83 75.34 o 2 8 5 108.43 156.58 69.88 o 3 8 5 349.39 298.39 85.68 o 4 8 5 277.44 290.10 86.93 o 5 8 5 220.85 171.58 82.95 o 6 8 5 507.92 364.41 97.04 o 7 8 5 84.01 44.66 80.79 o 2 9 5 1187.22 1718.76 192.49 o 3 9 5 9.88 -19.66 55.34 o 4 9 5 644.75 650.87 114.54 o 5 9 5 71.75 132.61 85.22 o 6 9 5 170.44 246.46 98.40 o 7 9 5 69.14 273.05 107.49 o 4 10 5 129.48 459.40 122.49 o 5 10 5 375.66 338.39 97.04 o 6 10 5 69.65 95.45 87.04 o 6 0 6 19.88 52.84 69.09 o 5 1 6 299.46 287.26 83.40 o 6 1 6 280.74 175.25 56.39 o 3 2 6 495.26 356.11 77.84 o 4 2 6 173.84 176.47 76.02 o 5 2 6 836.55 712.91 113.29 o 6 2 6 28.38 5.34 66.93 o 2 3 6 371.59 375.55 82.72 o 3 3 6 50.40 -37.95 58.18 o 4 3 6 568.24 549.28 104.20 o 5 3 6 17.96 -36.59 72.84 o 1 4 6 285.64 343.05 85.22 o 2 4 6 480.40 385.54 90.90 o 3 4 6 294.47 164.76 78.29 o 4 4 6 45.81 48.29 79.31 o 5 4 6 691.90 653.14 110.56 o 1 5 6 559.83 646.21 106.58 o 2 5 6 164.29 58.52 70.11 o 3 5 6 641.99 688.03 107.27 o 4 5 6 124.24 168.06 84.09 o 5 5 6 17.83 34.88 80.00 o 2 6 6 865.37 861.42 119.99 o 3 6 6 15.35 58.86 73.75 o 4 6 6 532.81 480.08 105.11 o 2 7 6 89.46 75.11 74.43 o 3 7 6 877.72 881.99 124.88 o 4 7 6 161.59 181.81 89.77 o 2 8 6 406.88 484.86 105.79 o 3 8 6 256.84 168.51 93.06 o