#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/15/2201581.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201581_Fobs loop_ _publ_author_name 'Zhang, Quan-Zheng' 'Wu, Chuan-De' 'Yang, Wen-Bin' 'Yu, Ya-Qin' 'Chen, Shu-Mei' 'Zhan, Xiao-Ping' 'Lu, Can-Zhong' _publ_section_title ; Diazidotetraimidazolenickel(II) ; _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m566 _journal_page_last m568 _journal_volume 58 _journal_year 2002 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.00 _cell_angle_beta 110.67 _cell_angle_gamma 90.00 _cell_length_a 8.787 _cell_length_b 10.464 _cell_length_c 10.866 _exptl_crystal_F_000 428.00 _reflns_d_resolution_high 0.8399 _[local]_cod_data_source_file ob6176Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' d in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 118.31 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1207.74 1322.65 33.47 o 4 0 0 1823.11 1898.49 48.39 o 6 0 0 264.41 264.52 8.05 o 8 0 0 256.82 288.53 9.62 o 1 1 0 4384.75 4785.94 219.90 o 2 1 0 8133.84 8305.25 147.15 o 3 1 0 2687.74 2603.34 46.48 o 4 1 0 0.00 -1.10 2.01 o 5 1 0 585.38 678.97 27.99 o 6 1 0 9.62 10.39 1.55 o 7 1 0 68.35 70.76 2.79 o 8 1 0 20.74 22.26 6.54 o 9 1 0 29.89 30.49 3.06 o 0 2 0 3149.68 3020.19 62.37 o 1 2 0 3863.39 3943.20 57.10 o 2 2 0 3411.28 3473.56 61.73 o 3 2 0 1493.24 1621.80 29.14 o 4 2 0 1959.03 1929.79 34.73 o 5 2 0 115.14 121.15 7.71 o 6 2 0 837.64 869.44 16.40 o 7 2 0 0.67 -1.18 2.96 o 8 2 0 198.20 233.60 5.97 o 9 2 0 8.40 2.61 3.53 o 1 3 0 8229.21 8220.33 118.91 o 2 3 0 217.23 219.76 3.49 o 3 3 0 1873.06 1846.38 33.10 o 4 3 0 138.14 164.53 4.91 o 5 3 0 2490.83 2334.06 51.55 o 6 3 0 0.01 -2.82 2.82 o 7 3 0 80.82 83.83 4.43 o 8 3 0 30.42 22.34 3.85 o 9 3 0 50.18 61.55 5.64 o 0 4 0 5994.88 5589.67 103.39 o 1 4 0 4.87 6.15 0.78 o 2 4 0 3964.84 3904.35 56.72 o 3 4 0 2.41 2.38 1.41 o 4 4 0 32.49 18.03 1.73 o 5 4 0 33.35 32.34 1.61 o 6 4 0 163.84 175.41 6.44 o 7 4 0 60.84 49.55 3.55 o 8 4 0 46.06 50.87 4.26 o 9 4 0 0.35 -0.96 3.26 o 1 5 0 4590.98 4619.90 58.14 o 2 5 0 288.51 292.98 4.66 o 3 5 0 1280.25 1282.24 23.14 o 5 5 0 639.02 600.52 16.61 o 6 5 0 59.39 66.69 4.22 o 7 5 0 273.52 244.39 8.36 o 8 5 0 15.35 15.21 3.34 o 0 6 0 1211.76 1111.82 20.29 o 1 6 0 101.29 101.30 1.98 o 2 6 0 1785.59 1796.95 32.59 o 3 6 0 7.77 3.89 1.33 o 4 6 0 494.89 504.85 14.15 o 5 6 0 4.94 2.59 1.99 o 6 6 0 130.14 129.37 5.73 o 7 6 0 43.36 32.04 3.68 o 8 6 0 42.97 41.38 4.39 o 1 7 0 1307.15 1322.18 19.84 o 2 7 0 19.80 20.62 1.77 o 3 7 0 977.37 1014.67 19.02 o 4 7 0 45.04 38.37 3.20 o 5 7 0 50.03 44.72 3.62 o 6 7 0 1.05 -0.08 2.74 o 7 7 0 95.09 88.43 5.35 o 8 7 0 10.83 7.38 4.03 o 0 8 0 1271.57 1266.07 33.39 o 1 8 0 46.37 46.21 2.02 o 2 8 0 580.49 598.61 9.62 o 3 8 0 14.98 15.11 5.50 o 4 8 0 236.87 232.75 7.86 o 5 8 0 30.14 24.81 3.80 o 6 8 0 345.50 375.75 12.28 o 7 8 0 0.95 8.21 3.66 o 1 9 0 213.90 231.01 5.74 o 2 9 0 81.54 82.71 3.41 o 3 9 0 315.78 320.39 5.90 o 4 9 0 33.89 27.04 3.34 o 5 9 0 160.33 170.81 7.53 o 6 9 0 7.56 4.35 3.11 o 0 10 0 312.37 307.58 10.27 o 1 10 0 14.04 12.08 2.21 o 2 10 0 323.74 324.47 7.56 o 3 10 0 30.85 24.73 3.01 o 4 10 0 203.64 218.58 8.70 o 5 10 0 12.86 11.18 3.78 o 1 11 0 382.58 398.91 17.85 o 2 11 0 6.55 -2.59 5.63 o 3 11 0 48.78 53.40 3.74 o 4 11 0 2.61 3.98 3.75 o 0 12 0 95.04 79.63 5.87 o 1 12 0 9.30 9.84 2.90 o 2 12 0 80.18 85.48 4.43 o -9 0 1 350.86 381.92 12.30 o -7 0 1 140.47 139.75 5.39 o -5 0 1 1382.59 1366.05 35.17 o -3 0 1 247.00 218.66 6.05 o -1 0 1 6846.96 6683.57 167.36 o 1 0 1 2413.32 2692.29 67.65 o 3 0 1 161.12 111.21 3.68 o 5 0 1 465.19 519.41 14.30 o 7 0 1 68.81 73.82 4.39 o 9 0 1 23.66 26.83 4.76 o -10 1 1 132.87 149.60 7.65 o -9 1 1 25.92 28.34 3.17 o -8 1 1 753.55 815.93 29.15 o -7 1 1 2.56 2.50 2.37 o -6 1 1 408.46 412.44 8.26 o -5 1 1 790.52 803.92 14.93 o -4 1 1 2963.52 2959.51 52.88 o -3 1 1 663.77 683.44 12.48 o -2 1 1 1184.57 1160.29 20.76 o -1 1 1 3.75 5.18 0.76 o 0 1 1 9447.73 10303.40 148.86 o 1 1 1 1499.43 1615.19 28.83 o 2 1 1 9064.85 9981.31 176.90 o 3 1 1 355.49 413.56 7.88 o 4 1 1 1134.46 1401.87 123.78 o 5 1 1 34.24 42.89 3.18 o 6 1 1 130.96 152.86 8.41 o 7 1 1 4.48 5.63 1.94 o 8 1 1 292.31 313.40 7.99 o 9 1 1 11.74 15.51 2.82 o -9 2 1 247.44 234.66 8.76 o -8 2 1 10.73 10.72 1.90 o -7 2 1 58.14 54.38 5.65 o -6 2 1 31.46 29.45 2.74 o -5 2 1 2369.23 2278.31 41.00 o -4 2 1 1446.94 1527.55 55.14 o -3 2 1 4926.22 5111.95 90.79 o -2 2 1 42.86 38.60 1.17 o -1 2 1 50.98 42.09 1.25 o 0 2 1 1937.85 1950.42 27.64 o 1 2 1 2365.24 2387.99 34.70 o 2 2 1 5.72 6.88 0.67 o 3 2 1 3126.33 3225.04 110.36 o 4 2 1 114.51 127.09 11.51 o 5 2 1 1020.29 1085.14 20.04 o 6 2 1 84.88 83.42 5.19 o 7 2 1 203.14 218.33 5.47 o 8 2 1 5.97 2.66 3.22 o 9 2 1 11.15 14.21 4.39 o -9 3 1 47.67 40.08 4.76 o -8 3 1 269.52 280.88 9.56 o -7 3 1 15.46 14.02 2.63 o -6 3 1 1352.04 1382.91 25.37 o -5 3 1 26.55 23.78 3.92 o -4 3 1 1095.79 1106.41 32.34 o -3 3 1 651.65 710.02 12.96 o -2 3 1 28.58 27.50 1.08 o -1 3 1 311.93 326.56 6.17 o 0 3 1 1422.42 1364.33 25.73 o 1 3 1 2.67 4.91 0.52 o 2 3 1 2467.35 2525.03 48.92 o 3 3 1 116.43 142.82 4.31 o 4 3 1 663.37 607.70 15.61 o 5 3 1 1.03 -0.74 2.49 o 6 3 1 307.28 344.05 28.26 o 7 3 1 67.29 69.75 4.21 o 8 3 1 72.53 75.97 5.02 o 9 3 1 4.01 2.57 3.41 o -9 4 1 186.48 179.60 7.51 o -8 4 1 44.99 30.91 4.24 o -7 4 1 759.62 719.29 19.96 o -6 4 1 27.72 21.23 2.57 o -5 4 1 313.89 279.78 5.69 o -4 4 1 53.94 60.38 4.21 o -3 4 1 3225.02 3264.87 58.12 o -2 4 1 489.43 540.10 10.14 o -1 4 1 1197.16 1177.60 38.33 o 0 4 1 447.60 489.45 6.42 o 1 4 1 3094.45 3179.81 51.52 o 2 4 1 107.17 112.21 3.05 o 3 4 1 1943.29 1945.69 34.98 o 4 4 1 8.36 7.26 1.56 o 5 4 1 617.16 634.30 12.10 o 6 4 1 33.68 31.18 3.32 o 7 4 1 286.10 307.37 10.46 o 8 4 1 9.45 7.13 3.89 o -9 5 1 5.65 7.40 3.55 o -8 5 1 99.44 91.25 5.35 o -7 5 1 0.84 -2.17 2.17 o -6 5 1 272.23 256.40 8.34 o -5 5 1 0.77 0.52 1.55 o -4 5 1 283.27 256.38 7.82 o -3 5 1 45.89 55.71 2.65 o -2 5 1 493.80 454.18 8.73 o -1 5 1 199.67 217.76 4.04 o 0 5 1 3360.36 3306.28 41.70 o 1 5 1 442.36 470.95 17.80 o 2 5 1 1280.38 1271.54 18.84 o 3 5 1 23.01 18.55 1.06 o 4 5 1 234.16 219.34 6.96 o 5 5 1 26.91 19.75 2.65 o 6 5 1 114.44 112.96 5.16 o 7 5 1 54.15 50.20 4.64 o 8 5 1 19.45 20.79 4.05 o -8 6 1 17.07 22.44 4.72 o -7 6 1 175.68 160.60 6.69 o -6 6 1 8.50 5.96 2.61 o -5 6 1 285.30 297.45 9.27 o -4 6 1 163.38 170.19 5.90 o -3 6 1 1469.42 1449.81 26.57 o -2 6 1 236.42 262.45 5.54 o -1 6 1 688.02 659.32 13.49 o 0 6 1 10.62 9.40 0.77 o 1 6 1 1368.08 1388.20 17.83 o 2 6 1 375.40 380.59 7.64 o 3 6 1 935.68 952.52 25.18 o 5 6 1 99.77 96.13 4.58 o 6 6 1 19.10 17.37 2.90 o 7 6 1 125.23 149.35 6.96 o 8 6 1 4.27 5.50 3.89 o -8 7 1 176.57 176.27 8.28 o -7 7 1 12.51 8.65 3.09 o -6 7 1 335.48 332.24 10.75 o -5 7 1 125.72 123.98 5.35 o -4 7 1 227.57 220.93 7.38 o -3 7 1 0.15 -1.57 1.57 o -2 7 1 1141.85 1210.46 18.30 o -1 7 1 43.19 47.76 3.59 o 0 7 1 55.69 39.56 1.59 o 1 7 1 105.26 112.99 2.53 o 2 7 1 1830.19 1894.52 45.45 o 3 7 1 25.87 20.61 3.90 o 4 7 1 88.92 82.35 3.93 o 5 7 1 0.62 -0.17 2.38 o 6 7 1 312.77 300.04 9.95 o 7 7 1 14.08 10.41 4.03 o -7 8 1 158.24 156.97 7.59 o -6 8 1 12.74 3.22 2.57 o -5 8 1 399.49 396.31 12.26 o -4 8 1 17.80 17.24 1.92 o -3 8 1 29.22 24.61 3.22 o -2 8 1 0.03 -0.76 1.26 o -1 8 1 550.42 602.66 9.65 o 0 8 1 17.70 15.97 1.76 o 1 8 1 458.71 446.52 12.11 o 2 8 1 49.08 41.90 1.88 o 3 8 1 152.33 142.84 8.00 o 4 8 1 17.88 20.94 3.01 o 5 8 1 370.56 363.09 11.55 o 6 8 1 2.77 -0.96 3.01 o 7 8 1 18.64 22.80 4.66 o -7 9 1 0.73 0.56 3.84 o -6 9 1 97.84 89.33 5.89 o -5 9 1 0.24 -2.47 2.47 o -4 9 1 324.27 329.02 9.05 o -3 9 1 67.47 56.25 2.35 o -2 9 1 376.22 392.64 8.55 o -1 9 1 98.29 89.26 3.30 o 0 9 1 161.50 153.55 4.43 o 1 9 1 139.54 125.12 3.90 o 2 9 1 295.42 279.56 7.29 o 3 9 1 132.90 118.01 4.68 o 4 9 1 314.73 302.58 9.87 o 5 9 1 40.70 40.33 4.28 o 6 9 1 78.80 83.12 6.50 o -6 10 1 0.23 -3.28 3.76 o -5 10 1 58.08 49.07 4.83 o -4 10 1 0.64 0.24 6.17 o -3 10 1 172.34 166.58 6.64 o -2 10 1 23.92 21.54 2.48 o -1 10 1 105.74 120.90 5.94 o 0 10 1 2.03 1.23 1.94 o 1 10 1 248.52 248.13 8.46 o 2 10 1 21.68 22.04 3.82 o 3 10 1 137.99 142.37 4.90 o 5 10 1 21.21 21.67 4.74 o -4 11 1 76.57 81.64 4.25 o -3 11 1 8.23 2.65 2.56 o -2 11 1 52.50 53.96 7.32 o -1 11 1 1.75 -2.58 4.46 o 0 11 1 375.27 393.54 9.83 o 1 11 1 0.07 -1.76 1.76 o 2 11 1 36.50 36.27 4.97 o 3 11 1 2.70 1.68 2.41 o 4 11 1 90.85 93.84 6.52 o -2 12 1 13.52 10.70 4.72 o -1 12 1 111.06 112.05 4.87 o 0 12 1 0.01 -0.60 2.47 o 1 12 1 94.05 108.35 4.67 o 2 12 1 6.00 4.01 7.07 o -10 0 2 129.89 148.03 7.19 o -8 0 2 626.81 649.78 18.13 o -6 0 2 647.33 656.16 17.64 o -4 0 2 184.76 173.26 5.10 o -2 0 2 25.42 26.23 1.21 o 0 0 2 9780.61 7992.46 200.28 o 2 0 2 105.36 107.07 3.53 o 4 0 2 2681.06 2817.24 71.60 o 6 0 2 14.55 14.54 2.63 o 8 0 2 305.95 310.34 10.48 o -10 1 2 0.64 -2.86 2.86 o -9 1 2 524.10 554.83 11.39 o -8 1 2 1.51 2.51 3.27 o -7 1 2 549.30 543.92 10.72 o -6 1 2 25.69 23.84 1.57 o -5 1 2 317.21 296.86 5.98 o -4 1 2 182.90 201.46 7.08 o -3 1 2 4653.31 4797.26 85.24 o -2 1 2 7370.31 7235.66 128.24 o -1 1 2 654.82 645.26 10.37 o 0 1 2 146.77 162.94 3.17 o 1 1 2 443.73 530.43 9.77 o 2 1 2 0.19 3.09 2.42 o 3 1 2 711.47 805.32 14.98 o 4 1 2 37.79 35.36 2.47 o 5 1 2 420.44 489.63 27.33 o 6 1 2 4.14 6.45 1.86 o 7 1 2 324.52 376.23 8.29 o 8 1 2 70.33 64.76 3.51 o 9 1 2 111.00 130.15 5.04 o -10 2 2 63.00 72.69 5.35 o -9 2 2 3.84 0.96 2.63 o -8 2 2 422.96 428.52 9.22 o -7 2 2 213.78 208.89 4.98 o -6 2 2 1824.03 1821.91 41.20 o -5 2 2 14.13 20.86 1.66 o -4 2 2 3473.74 3364.55 60.02 o -3 2 2 94.03 99.06 3.91 o -2 2 2 152.33 150.83 2.45 o -1 2 2 6789.93 6388.77 190.06 o 0 2 2 2142.87 2287.93 63.11 o 1 2 2 123.71 143.10 2.95 o 2 2 2 368.21 346.49 6.66 o 3 2 2 947.16 1093.97 20.00 o 4 2 2 504.65 499.80 7.86 o 5 2 2 50.68 50.73 2.27 o 6 2 2 413.75 480.87 13.79 o 7 2 2 30.51 33.02 2.63 o 8 2 2 277.56 303.56 7.27 o -9 3 2 233.34 256.71 9.68 o -8 3 2 133.32 127.01 6.19 o -7 3 2 398.79 358.26 10.90 o -6 3 2 63.34 52.10 4.12 o -5 3 2 1470.15 1464.57 28.92 o -4 3 2 26.57 22.18 1.09 o -3 3 2 398.79 367.36 6.92 o -2 3 2 387.38 402.07 6.11 o -1 3 2 748.04 736.30 21.80 o 0 3 2 309.45 333.69 4.45 o 1 3 2 97.30 105.40 3.60 o 2 3 2 106.17 94.40 2.61 o 3 3 2 983.11 940.22 17.29 o 4 3 2 151.03 168.52 3.91 o 5 3 2 964.65 970.57 21.27 o 6 3 2 99.66 93.59 3.08 o 7 3 2 247.29 256.11 8.99 o 8 3 2 0.00 -2.03 3.36 o -9 4 2 0.08 1.96 3.55 o -8 4 2 768.26 782.79 21.97 o -7 4 2 5.33 6.73 2.88 o -6 4 2 357.79 319.82 9.79 o -5 4 2 2.57 4.00 1.05 o -4 4 2 363.99 360.63 36.18 o -3 4 2 37.44 45.99 4.35 o -2 4 2 847.59 840.35 18.24 o -1 4 2 249.55 268.17 6.70 o 0 4 2 7.15 11.29 0.81 o 1 4 2 88.45 80.53 2.65 o 2 4 2 1726.94 1796.08 32.32 o 3 4 2 97.18 93.61 3.66 o 4 4 2 511.97 497.89 9.66 o 5 4 2 12.51 12.58 3.93 o 6 4 2 147.94 133.67 5.64 o 7 4 2 38.71 43.51 4.08 o 8 4 2 43.99 41.67 5.08 o -9 5 2 86.58 93.53 6.08 o -8 5 2 13.38 15.11 3.68 o -7 5 2 589.11 577.84 16.60 o -6 5 2 324.70 329.01 10.19 o -4 5 2 28.35 25.35 2.36 o -3 5 2 1186.05 1201.23 22.06 o -2 5 2 329.53 375.09 7.41 o -1 5 2 631.47 571.05 14.71 o 0 5 2 105.50 131.89 12.33 o 1 5 2 68.84 63.83 1.49 o 2 5 2 18.03 20.24 0.99 o 3 5 2 99.77 90.29 2.47 o 4 5 2 51.45 56.37 3.55 o 5 5 2 179.10 162.26 6.17 o 6 5 2 29.13 20.44 3.22 o 7 5 2 255.73 237.70 8.66 o 8 5 2 5.11 6.58 4.30 o -9 6 2 3.20 4.83 3.82 o -8 6 2 97.45 100.95 5.98 o -6 6 2 370.43 384.63 11.80 o -5 6 2 9.15 7.00 2.53 o -4 6 2 607.08 634.99 17.44 o -3 6 2 138.72 150.36 5.91 o -2 6 2 655.30 650.98 10.12 o -1 6 2 127.17 143.85 4.89 o 0 6 2 108.92 98.91 1.84 o 1 6 2 7.32 5.96 0.71 o 2 6 2 428.10 419.19 9.26 o 3 6 2 119.01 129.40 5.06 o 4 6 2 77.35 80.80 4.33 o 5 6 2 71.51 75.12 4.51 o 7 6 2 12.98 12.77 3.45 o -8 7 2 30.73 21.27 4.18 o -7 7 2 306.05 318.33 10.83 o -6 7 2 5.36 7.00 2.63 o -5 7 2 101.38 103.68 5.16 o -4 7 2 12.54 10.74 2.14 o -3 7 2 613.61 592.50 16.04 o -2 7 2 91.48 96.79 2.38 o -1 7 2 9.91 8.47 1.19 o 0 7 2 12.35 10.37 1.33 o 1 7 2 561.73 584.09 11.96 o 2 7 2 28.79 29.37 1.93 o 3 7 2 219.84 218.87 7.21 o 4 7 2 30.24 21.42 3.24 o 5 7 2 179.96 176.95 6.92 o 6 7 2 7.23 2.63 3.01 o 7 7 2 64.10 74.71 5.77 o -7 8 2 29.72 32.83 4.20 o -6 8 2 501.66 518.23 15.55 o -5 8 2 8.25 3.45 2.38 o -4 8 2 63.16 68.72 3.07 o -3 8 2 0.35 -0.09 1.31 o -2 8 2 237.13 241.02 5.29 o -1 8 2 36.75 34.18 1.94 o 0 8 2 45.69 50.27 2.52 o 1 8 2 7.97 7.22 1.87 o 2 8 2 114.73 115.29 2.92 o 3 8 2 12.23 8.99 2.59 o 4 8 2 223.46 246.60 8.45 o 5 8 2 0.90 -2.42 2.42 o 6 8 2 164.08 145.35 6.84 o -7 9 2 121.36 106.70 6.44 o -6 9 2 1.62 2.80 3.39 o -5 9 2 262.44 280.30 9.72 o -4 9 2 115.53 111.75 4.09 o -3 9 2 271.05 285.05 5.45 o -2 9 2 7.76 8.41 2.05 o -1 9 2 41.48 40.97 5.87 o 0 9 2 25.25 20.15 2.06 o 1 9 2 15.98 20.00 2.97 o 2 9 2 78.77 71.78 3.40 o 3 9 2 136.64 141.55 16.02 o 4 9 2 0.00 -2.34 2.34 o 5 9 2 107.11 110.11 6.00 o 6 9 2 0.36 -3.01 3.01 o -6 10 2 31.83 27.73 5.08 o -5 10 2 3.29 0.08 3.01 o -4 10 2 201.26 201.23 4.72 o -3 10 2 56.87 53.72 4.38 o -2 10 2 66.24 65.43 3.38 o -1 10 2 75.89 72.78 3.34 o 0 10 2 173.72 194.52 6.48 o 1 10 2 0.12 -2.19 2.70 o 2 10 2 55.07 53.03 3.37 o 3 10 2 43.16 36.88 2.97 o 5 10 2 0.05 -1.61 3.43 o -4 11 2 8.42 11.27 2.81 o -3 11 2 4.79 3.90 2.47 o -2 11 2 0.08 -0.62 3.22 o -1 11 2 146.39 158.66 5.42 o 0 11 2 5.47 0.99 2.17 o 1 11 2 108.97 121.49 12.43 o 2 11 2 0.95 -1.76 2.11 o 3 11 2 64.83 74.65 6.35 o -2 12 2 69.64 74.31 4.25 o -1 12 2 0.00 5.05 2.88 o 0 12 2 23.58 30.51 3.77 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2.78 2.42 o 0 4 10 119.40 127.13 4.19 o 1 4 10 6.31 9.18 4.56 o 2 4 10 55.56 59.22 3.24 o -7 5 10 55.69 51.98 5.31 o -6 5 10 26.43 21.65 4.35 o -5 5 10 124.45 148.83 6.92 o -4 5 10 0.44 -1.84 1.84 o -3 5 10 181.65 183.95 7.25 o -2 5 10 0.00 -0.65 5.38 o -1 5 10 150.55 146.73 11.46 o 0 5 10 2.89 -0.88 1.70 o 1 5 10 123.27 124.58 6.27 o -5 6 10 9.02 5.06 3.76 o -4 6 10 183.97 190.09 7.61 o -3 6 10 2.34 0.13 2.47 o -2 6 10 44.01 46.62 3.99 o -1 6 10 0.50 4.41 1.87 o 0 6 10 164.31 178.32 5.11 o 1 6 10 1.18 -5.28 5.28 o -5 7 10 52.81 57.43 5.41 o -4 7 10 4.53 -1.00 3.28 o -3 7 10 99.78 110.06 6.00 o -2 7 10 0.88 -2.72 2.72 o -1 7 10 53.49 56.84 4.47 o 0 7 10 0.86 7.36 3.03 o -7 0 11 43.18 52.91 5.33 o -5 0 11 179.32 184.47 7.05 o -3 0 11 471.81 476.00 14.31 o -1 0 11 381.44 430.57 13.43 o 1 0 11 33.52 33.50 4.08 o -8 1 11 35.67 42.03 4.56 o -7 1 11 4.93 3.43 2.28 o -6 1 11 281.98 289.55 8.47 o -5 1 11 29.88 26.75 2.35 o -4 1 11 220.63 208.79 7.90 o -3 1 11 16.23 14.68 5.45 o -2 1 11 177.68 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