#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:59:13 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180936 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/16/2201603.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201603_Fobs loop_ _publ_author_name 'Coles, Simon J.' 'Gale, Philip A.' 'Hursthouse, Michael B.' 'Warriner, Colin N.' _publ_section_title ; Tetramethyl biphenyl-3,5,3',5'-tetracarboxylate benzene sesquisolvate ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o887 _journal_page_last o888 _journal_volume 58 _journal_year 2002 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 124.860 _cell_angle_gamma 90.000 _cell_length_a 37.5570 _cell_length_b 7.0816 _cell_length_c 22.4980 _exptl_crystal_F_000 2120.00 _reflns_d_resolution_high 0.8874 _cod_data_source_file om6092Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 01SOT001 in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 486.42 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 6 0 0 32633.69 30516.55 1435.34 o 8 0 0 40963.29 38782.05 2055.36 o 10 0 0 1337.07 1238.96 93.48 o 12 0 0 121.51 64.28 48.71 o 14 0 0 23852.36 25178.93 1585.12 o 16 0 0 8661.70 9895.47 850.85 o 18 0 0 2542.86 2804.59 313.68 o 20 0 0 23121.04 27888.68 3246.50 o 22 0 0 969.86 1189.05 145.77 o 24 0 0 376.65 190.33 139.97 o 28 0 0 4120.62 4127.95 375.47 o 30 0 0 1217.93 913.21 141.51 o 32 0 0 87.07 118.87 225.26 o 34 0 0 189.26 269.30 146.61 o 1 1 0 658.42 559.67 35.64 o 3 1 0 1410.92 1154.14 85.61 o 5 1 0 82106.57 84112.41 2558.54 o 7 1 0 10146.52 9043.20 318.28 o 9 1 0 3611.59 3207.00 130.57 o 11 1 0 2409.22 2664.79 138.00 o 13 1 0 2030.08 1868.74 104.19 o 15 1 0 54485.11 60276.49 2883.61 o 17 1 0 9.94 -60.81 55.80 o 19 1 0 634.49 728.00 54.98 o 21 1 0 1027.56 1086.85 82.42 o 23 1 0 32.59 58.19 56.92 o 25 1 0 308.49 288.86 65.94 o 27 1 0 12.94 16.19 70.72 o 29 1 0 5788.53 5409.82 541.21 o 31 1 0 458.97 404.31 107.54 o 33 1 0 2716.01 2655.31 165.28 o 0 2 0 140914.34 160464.22 28347.65 o 2 2 0 33408.85 30283.55 2915.89 o 4 2 0 3863.95 3760.32 182.67 o 6 2 0 1245.85 1200.74 86.85 o 8 2 0 105.17 61.18 24.45 o 10 2 0 1127.39 1069.25 54.78 o 12 2 0 105.34 193.82 37.18 o 14 2 0 1420.82 1539.59 111.61 o 16 2 0 2528.06 2690.50 203.92 o 18 2 0 907.40 1095.53 63.64 o 20 2 0 467.91 583.81 73.50 o 22 2 0 1833.44 1818.31 225.82 o 24 2 0 871.42 774.20 175.62 o 26 2 0 90.38 118.79 68.99 o 28 2 0 2249.53 2127.50 132.35 o 30 2 0 684.49 538.55 143.30 o 32 2 0 74.69 -22.36 109.09 o 1 3 0 1102.72 1221.83 92.71 o 3 3 0 2081.58 1966.12 109.59 o 5 3 0 3448.16 3296.11 175.88 o 7 3 0 1199.12 1191.66 50.81 o 9 3 0 3153.14 3068.35 128.41 o 11 3 0 13571.63 13546.77 831.93 o 13 3 0 100.09 57.59 37.09 o 15 3 0 11.75 75.16 40.74 o 17 3 0 338.85 390.45 64.27 o 19 3 0 50.26 73.66 40.97 o 21 3 0 64.37 141.67 82.77 o 23 3 0 64.13 -23.79 73.92 o 25 3 0 290.51 354.53 87.65 o 27 3 0 75.73 138.52 77.24 o 29 3 0 733.21 561.47 105.21 o 31 3 0 477.71 408.93 115.27 o 0 4 0 2518.00 2552.87 230.38 o 2 4 0 3665.62 3677.33 194.41 o 4 4 0 1994.84 1914.21 80.35 o 6 4 0 3.73 17.86 25.77 o 8 4 0 293.26 328.74 50.35 o 10 4 0 338.33 286.53 43.99 o 12 4 0 8.14 5.13 28.90 o 14 4 0 90.66 105.99 36.28 o 16 4 0 160.12 241.30 47.23 o 18 4 0 211.41 246.25 50.17 o 20 4 0 3.06 75.98 54.19 o 22 4 0 21.20 2.02 56.70 o 24 4 0 221.25 197.73 56.97 o 26 4 0 449.05 524.68 101.93 o 28 4 0 409.19 384.88 106.21 o 30 4 0 103.33 -112.94 139.13 o 1 5 0 681.39 634.06 40.50 o 3 5 0 185.55 214.70 28.24 o 5 5 0 187.41 184.50 36.80 o 7 5 0 505.21 564.92 43.24 o 9 5 0 36.79 57.74 38.97 o 11 5 0 187.37 198.94 36.48 o 13 5 0 3374.54 3010.67 167.65 o 15 5 0 109.02 135.58 40.61 o 17 5 0 596.02 617.49 95.35 o 19 5 0 116.12 46.58 56.14 o 21 5 0 59.91 62.78 83.87 o 23 5 0 49.69 58.87 72.47 o 25 5 0 112.76 64.17 81.85 o 0 6 0 40.97 73.08 50.13 o 2 6 0 89.98 91.02 30.35 o 4 6 0 448.08 413.90 40.82 o 6 6 0 427.42 391.79 65.62 o 8 6 0 55.02 66.15 42.91 o 10 6 0 161.57 162.37 50.32 o 12 6 0 72.77 164.48 62.85 o 14 6 0 238.68 326.13 49.74 o 16 6 0 74.72 47.95 47.84 o 18 6 0 67.14 81.81 51.90 o 20 6 0 163.12 253.50 70.36 o 22 6 0 30.87 -92.49 102.27 o 1 7 0 112.19 169.31 42.30 o 3 7 0 259.93 292.92 48.62 o 5 7 0 341.22 280.74 48.39 o 7 7 0 16.14 -19.66 39.16 o 9 7 0 191.66 144.45 45.26 o 11 7 0 54.18 -39.54 49.24 o 13 7 0 24.31 87.54 60.36 o 15 7 0 123.02 214.57 91.32 o -35 1 1 14.38 92.04 196.08 o -33 1 1 9.46 56.16 125.65 o -31 1 1 11.92 -29.69 83.93 o -29 1 1 83.91 -140.32 106.90 o -27 1 1 274.38 326.54 81.45 o -25 1 1 72.26 -41.28 123.91 o -23 1 1 18.81 25.41 49.36 o -21 1 1 341.39 260.17 60.74 o -19 1 1 55.58 80.91 70.64 o -17 1 1 2227.84 2496.21 199.43 o -15 1 1 15.42 -13.49 40.41 o -13 1 1 17438.95 16988.27 729.03 o -11 1 1 3.80 -8.56 38.25 o -9 1 1 17653.48 16769.99 783.17 o -7 1 1 19869.48 18621.34 646.57 o -5 1 1 467.78 453.61 45.33 o -3 1 1 864.07 876.14 41.77 o -1 1 1 274.51 282.76 19.93 o 1 1 1 187.94 207.21 14.89 o 3 1 1 408.76 478.46 29.91 o 5 1 1 46853.68 45550.28 1197.03 o 7 1 1 14437.62 14725.81 535.10 o 9 1 1 6978.96 7262.83 302.73 o 11 1 1 15414.33 16320.29 622.78 o 13 1 1 18274.88 18652.60 734.92 o 15 1 1 3218.99 3081.73 150.38 o 17 1 1 965.23 1025.94 66.31 o 19 1 1 103.75 13.77 56.92 o 21 1 1 538.86 723.80 106.49 o 23 1 1 3.21 -145.26 124.32 o 25 1 1 641.59 799.05 158.09 o 27 1 1 631.71 632.38 107.53 o 29 1 1 842.45 748.34 109.28 o 31 1 1 170.24 92.26 83.55 o 33 1 1 314.44 450.91 150.09 o -34 2 1 125.59 45.46 113.84 o -32 2 1 0.24 -53.82 98.26 o -30 2 1 89.11 -68.83 93.02 o -28 2 1 911.51 961.12 100.92 o -26 2 1 1.65 -109.62 88.42 o -24 2 1 354.07 267.60 75.63 o -22 2 1 853.80 801.14 72.25 o -20 2 1 2.58 -37.96 46.46 o -18 2 1 79.79 39.55 71.82 o -16 2 1 5849.19 6233.96 317.28 o -14 2 1 168.43 117.50 46.12 o -12 2 1 99.14 150.72 37.39 o -10 2 1 773.69 756.18 55.71 o -8 2 1 397.20 368.47 32.83 o -6 2 1 3132.69 3233.52 168.67 o -4 2 1 29266.90 28746.01 1540.92 o -2 2 1 195321.41 188734.06 16897.93 o 0 2 1 18501.51 17330.60 1628.13 o 2 2 1 106619.84 112388.34 6670.47 o 4 2 1 5806.54 5453.29 234.40 o 6 2 1 2512.48 2288.41 92.22 o 8 2 1 2014.92 2004.77 83.67 o 10 2 1 1407.86 1628.37 162.63 o 12 2 1 1140.22 1197.87 122.26 o 14 2 1 51.84 69.07 35.05 o 16 2 1 6373.98 7217.42 270.72 o 18 2 1 5575.59 6301.58 362.15 o 20 2 1 2120.85 2363.63 193.01 o 22 2 1 24.11 -7.35 46.38 o 24 2 1 0.16 -57.90 49.87 o 26 2 1 1016.16 900.24 93.66 o 28 2 1 163.54 292.27 105.75 o 30 2 1 388.07 467.39 106.03 o 32 2 1 133.87 -85.50 121.16 o -33 3 1 352.08 346.40 150.04 o -31 3 1 184.24 34.63 88.30 o -29 3 1 1.18 -55.09 85.52 o -27 3 1 97.27 54.16 71.79 o -25 3 1 115.06 93.50 68.52 o -23 3 1 27.39 -20.11 66.58 o -21 3 1 190.99 185.73 55.81 o -19 3 1 64.69 127.73 47.66 o -17 3 1 2453.54 3008.71 250.63 o -15 3 1 216.10 227.40 37.22 o -13 3 1 2502.18 2569.90 141.32 o -11 3 1 2734.63 2678.00 114.79 o -9 3 1 1461.34 1495.46 54.34 o -7 3 1 44.36 22.38 37.45 o -5 3 1 367.96 375.09 38.21 o -3 3 1 2000.42 1645.30 123.60 o -1 3 1 8525.29 7485.02 496.35 o 1 3 1 4244.68 3758.35 211.31 o 3 3 1 69.17 29.97 35.00 o 5 3 1 4291.84 3990.45 328.39 o 7 3 1 206.51 215.28 29.45 o 9 3 1 428.64 475.24 37.71 o 11 3 1 129.46 105.23 48.62 o 13 3 1 2656.59 3074.47 189.44 o 15 3 1 1146.23 1061.49 94.60 o 17 3 1 1807.39 1942.42 109.68 o 19 3 1 107.86 122.99 65.03 o 21 3 1 312.32 286.36 79.80 o 23 3 1 133.94 287.19 52.33 o 25 3 1 272.87 270.45 89.41 o 27 3 1 2581.57 2863.80 385.37 o 29 3 1 103.53 67.53 131.31 o 31 3 1 342.77 465.95 136.14 o -30 4 1 5.08 131.46 108.87 o -28 4 1 25.60 102.51 110.05 o -26 4 1 400.12 311.08 111.32 o -24 4 1 182.03 162.10 69.85 o -22 4 1 19.64 28.29 58.31 o -20 4 1 192.80 210.39 56.85 o -18 4 1 0.21 -0.55 41.56 o -16 4 1 25.70 38.09 32.88 o -14 4 1 460.79 523.25 44.54 o -12 4 1 890.98 857.17 81.26 o -10 4 1 188.60 216.14 27.25 o -8 4 1 1358.69 1402.32 88.15 o -6 4 1 324.32 274.43 49.87 o -4 4 1 4988.25 5037.29 237.70 o -2 4 1 1071.52 1199.09 76.80 o 0 4 1 248.25 232.42 28.38 o 2 4 1 1802.82 1687.45 108.09 o 4 4 1 490.22 542.73 47.90 o 6 4 1 3059.14 3121.44 187.17 o 8 4 1 790.02 695.46 60.57 o 10 4 1 20.94 35.08 39.76 o 12 4 1 1450.82 1542.35 108.56 o 14 4 1 548.86 560.36 61.85 o 16 4 1 440.85 532.62 57.52 o 18 4 1 37.20 -26.70 64.14 o 20 4 1 39.83 75.09 49.78 o 22 4 1 727.38 761.67 107.38 o 24 4 1 311.14 133.07 77.83 o 26 4 1 2501.26 2875.05 385.30 o 28 4 1 94.72 -3.78 67.13 o -27 5 1 64.44 62.37 86.36 o -25 5 1 0.55 -20.10 73.41 o -23 5 1 7.80 -10.47 59.25 o -21 5 1 170.17 110.76 56.88 o -19 5 1 229.70 274.79 61.54 o -17 5 1 422.46 384.33 65.20 o -15 5 1 35.14 17.45 42.28 o -13 5 1 1763.72 1654.17 128.53 o -11 5 1 76.77 148.35 29.86 o -9 5 1 498.74 300.93 100.97 o -7 5 1 437.85 328.32 120.26 o -5 5 1 142.15 206.94 62.43 o -3 5 1 9.92 42.08 26.86 o -1 5 1 1163.15 1216.56 60.18 o 1 5 1 434.11 364.92 43.48 o 3 5 1 0.20 23.45 34.48 o 5 5 1 206.63 145.50 45.18 o 7 5 1 353.95 369.65 38.59 o 9 5 1 210.56 191.75 42.09 o 11 5 1 1326.31 1335.53 73.48 o 13 5 1 11.19 -22.76 38.63 o 15 5 1 1.51 -10.00 45.56 o 17 5 1 0.19 1.23 55.80 o 19 5 1 210.82 177.66 104.89 o 21 5 1 54.57 68.35 55.85 o 23 5 1 36.24 35.87 76.02 o 25 5 1 336.34 339.38 72.98 o -22 6 1 85.20 185.37 98.75 o -20 6 1 356.75 312.86 88.50 o -18 6 1 116.72 192.72 60.20 o -16 6 1 32.14 3.10 41.81 o -14 6 1 0.51 -23.86 39.64 o -12 6 1 20.10 -78.92 52.61 o -10 6 1 135.30 168.46 40.66 o -8 6 1 259.05 281.23 77.67 o -6 6 1 88.37 34.04 40.81 o -4 6 1 465.05 436.24 57.96 o -2 6 1 2.24 40.63 31.80 o 0 6 1 111.49 117.69 37.43 o 2 6 1 850.70 1003.02 90.39 o 4 6 1 3.52 10.37 37.82 o 6 6 1 39.66 16.02 38.19 o 8 6 1 430.22 363.09 58.01 o 10 6 1 131.34 161.79 59.54 o 12 6 1 113.49 104.49 40.98 o 14 6 1 85.22 194.21 53.04 o 16 6 1 660.96 771.89 70.20 o 18 6 1 10.56 -5.46 74.09 o 20 6 1 141.18 86.23 68.50 o -17 7 1 55.23 -81.23 73.06 o -15 7 1 399.14 537.12 103.84 o -13 7 1 107.55 75.20 56.63 o -11 7 1 707.05 627.04 62.35 o -9 7 1 226.77 255.05 64.62 o -7 7 1 6.29 35.96 42.39 o -5 7 1 48.92 43.55 40.10 o -3 7 1 0.45 -24.22 38.50 o -1 7 1 240.78 220.44 41.22 o 1 7 1 1.27 8.20 45.50 o 3 7 1 13.42 76.39 38.65 o 5 7 1 14.30 -10.21 43.29 o 7 7 1 68.18 13.26 44.87 o 9 7 1 212.42 237.69 71.08 o 11 7 1 164.58 106.76 87.42 o 13 7 1 10.39 72.64 141.33 o 15 7 1 439.06 221.43 114.68 o -36 0 2 37.88 -60.49 157.98 o -34 0 2 197.35 132.91 207.76 o -32 0 2 46.17 118.67 210.32 o -30 0 2 3104.58 1756.71 352.49 o -28 0 2 711.51 830.75 123.66 o -26 0 2 1653.58 1978.18 461.62 o -24 0 2 4.45 28.70 70.75 o -22 0 2 1391.79 1463.53 377.24 o -20 0 2 1410.51 1862.87 323.62 o -18 0 2 17269.56 18843.61 2349.76 o -16 0 2 3168.03 3253.23 289.82 o -14 0 2 39.28 66.29 66.29 o -12 0 2 1443.90 1673.16 317.75 o -10 0 2 833.01 781.97 92.20 o -8 0 2 1547.44 1455.51 89.50 o -6 0 2 19052.75 15088.60 761.13 o 2 0 2 454.41 584.50 25.02 o 4 0 2 9322.83 8891.90 506.73 o 6 0 2 47320.50 49003.92 2420.84 o 8 0 2 610.24 582.51 92.60 o 10 0 2 8461.27 7597.77 685.93 o 12 0 2 179.04 262.91 59.00 o 14 0 2 2008.52 1744.84 115.91 o 16 0 2 136.95 16.21 69.46 o 18 0 2 481.75 550.32 78.93 o 20 0 2 521.82 460.74 67.49 o 22 0 2 82.05 45.85 87.03 o 24 0 2 1163.62 1284.49 268.97 o 26 0 2 1227.52 1197.72 173.22 o 28 0 2 79.59 119.78 150.18 o 30 0 2 942.49 1305.70 179.23 o 32 0 2 52.80 31.60 165.82 o -35 1 2 917.41 695.86 133.37 o -33 1 2 35.23 43.24 99.95 o -31 1 2 4526.17 4408.39 475.78 o -29 1 2 1745.43 1578.53 162.11 o -27 1 2 0.01 -128.99 85.99 o -25 1 2 44.27 87.24 51.48 o -23 1 2 37.39 57.37 58.20 o -21 1 2 1096.98 1056.96 158.77 o -19 1 2 112.89 63.70 73.28 o -17 1 2 15367.58 17011.65 924.28 o -15 1 2 6976.03 6787.29 550.22 o -13 1 2 1367.83 1215.46 124.47 o -11 1 2 8956.27 8410.97 372.28 o -9 1 2 14881.48 13382.75 583.92 o -7 1 2 9849.24 8471.45 289.71 o -5 1 2 235.03 267.00 25.43 o -3 1 2 1609.49 1345.77 91.24 o -1 1 2 5.42 77.45 18.12 o 1 1 2 297.31 324.17 20.25 o 3 1 2 0.03 -3.20 19.22 o 5 1 2 16100.85 14607.71 563.65 o 7 1 2 710.20 753.97 50.84 o 9 1 2 20016.25 20460.99 697.97 o 11 1 2 3118.32 3439.13 188.55 o 13 1 2 2000.31 2540.39 158.12 o 15 1 2 870.34 1004.06 84.16 o 17 1 2 799.95 785.67 104.59 o 19 1 2 134.03 148.88 61.46 o 21 1 2 205.47 232.11 64.21 o 23 1 2 387.94 412.78 57.06 o 25 1 2 298.14 198.92 67.92 o 27 1 2 39.40 194.32 108.52 o 29 1 2 1830.65 1742.41 226.10 o 31 1 2 194.95 151.34 107.55 o -34 2 2 24.09 82.38 89.42 o -32 2 2 47.38 140.87 136.68 o -30 2 2 1221.84 1071.32 96.09 o -28 2 2 9.14 -43.89 81.50 o -26 2 2 689.89 623.92 91.66 o -24 2 2 563.70 429.59 72.00 o -22 2 2 1920.19 2395.36 131.28 o -20 2 2 3226.07 3897.65 334.13 o -18 2 2 279.15 332.32 44.63 o -16 2 2 2571.69 2639.96 119.30 o -14 2 2 61.39 80.10 32.65 o -12 2 2 1633.20 1562.55 115.51 o -10 2 2 245.63 318.13 25.49 o -8 2 2 2.42 -8.14 54.11 o -6 2 2 10079.33 9574.16 441.75 o -4 2 2 7369.23 7135.24 456.27 o -2 2 2 114953.44 115697.61 13089.76 o 0 2 2 164713.45 178540.27 12516.29 o 2 2 2 1955.17 1879.86 98.06 o 4 2 2 12398.62 11841.59 547.34 o 6 2 2 939.40 982.48 46.23 o 8 2 2 2413.16 2614.67 106.77 o 10 2 2 1564.44 1613.61 107.88 o 12 2 2 484.98 523.33 42.85 o 14 2 2 1109.64 1196.52 97.82 o 16 2 2 789.12 917.91 79.78 o 18 2 2 1518.26 1833.29 203.07 o 20 2 2 2301.47 2424.48 235.15 o 22 2 2 64.65 34.99 60.39 o 24 2 2 3.54 -121.31 80.88 o 26 2 2 147.86 324.82 101.09 o 28 2 2 92.12 -109.04 84.58 o 30 2 2 177.26 162.04 89.79 o -33 3 2 0.00 -111.76 88.52 o -31 3 2 278.38 294.18 110.68 o -29 3 2 576.65 702.33 121.32 o -27 3 2 15.86 -73.61 101.06 o -25 3 2 13.57 52.98 112.67 o -23 3 2 65.46 5.34 54.72 o -21 3 2 453.75 420.36 42.38 o -19 3 2 899.09 1038.94 88.91 o -17 3 2 1025.54 1104.90 176.25 o -15 3 2 6853.21 7553.71 361.85 o -13 3 2 240.01 270.61 31.48 o -11 3 2 3925.45 4011.73 194.10 o -9 3 2 5476.84 5343.35 326.22 o -7 3 2 216.62 237.13 30.64 o -5 3 2 2742.98 2625.54 164.76 o -3 3 2 254.19 255.86 32.96 o -1 3 2 7703.33 7233.43 716.42 o 1 3 2 390.74 446.77 40.02 o 3 3 2 4420.17 4654.44 201.19 o 5 3 2 676.14 708.78 53.29 o 7 3 2 5271.94 5780.26 230.34 o 9 3 2 871.52 881.76 46.03 o 11 3 2 862.17 841.06 45.54 o 13 3 2 10245.64 11406.95 606.45 o 15 3 2 2359.43 2561.22 196.28 o 17 3 2 495.32 329.74 61.82 o 19 3 2 422.61 330.01 62.21 o 21 3 2 101.17 39.85 54.26 o 23 3 2 2.41 -93.55 62.37 o 25 3 2 276.91 233.86 79.77 o 27 3 2 157.44 173.99 103.31 o 29 3 2 1627.86 1871.23 166.05 o -30 4 2 622.25 466.67 100.72 o -28 4 2 10.62 -4.85 72.40 o -26 4 2 77.79 104.83 58.84 o -24 4 2 313.84 428.16 68.62 o -22 4 2 2014.34 1874.32 160.64 o -20 4 2 63.58 52.91 45.43 o -18 4 2 139.03 176.42 61.19 o -16 4 2 3.28 28.72 45.00 o -14 4 2 374.04 431.41 37.33 o -12 4 2 190.58 90.42 48.74 o -10 4 2 154.20 142.19 37.41 o -8 4 2 221.16 273.07 41.39 o -6 4 2 117.58 145.29 21.14 o -4 4 2 14.41 79.11 26.98 o -2 4 2 4943.58 4652.45 329.35 o 0 4 2 35291.09 36314.03 1897.62 o 2 4 2 1993.44 2084.67 240.97 o 4 4 2 706.58 709.88 40.46 o 6 4 2 1702.54 1735.47 104.75 o 8 4 2 1588.36 1642.31 160.71 o 10 4 2 18.52 46.68 35.08 o 12 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136.99 o -36 0 20 2272.08 2553.57 584.93 o -34 0 20 3463.88 3658.39 432.88 o -32 0 20 8918.26 7962.32 805.57 o -30 0 20 607.08 639.48 114.20 o -28 0 20 996.90 808.15 131.62 o -26 0 20 283.05 186.94 114.33 o -24 0 20 119.61 14.35 111.41 o -22 0 20 65.56 156.86 109.50 o -20 0 20 408.39 340.79 89.46 o -18 0 20 19580.77 25578.30 1611.53 o -16 0 20 5118.96 5527.19 486.73 o -14 0 20 10844.50 12327.93 914.57 o -12 0 20 6294.50 5903.32 474.66 o -10 0 20 30.59 50.96 95.04 o -8 0 20 3612.70 3534.41 222.17 o -6 0 20 140.40 92.51 82.22 o -4 0 20 2015.19 1470.78 132.33 o -2 0 20 602.93 537.56 101.14 o 0 0 20 40.01 -84.97 128.05 o 2 0 20 624.23 645.24 145.56 o -39 1 20 34.12 64.44 98.46 o -37 1 20 274.58 147.73 97.24 o -35 1 20 10.14 35.69 86.64 o -33 1 20 415.93 342.80 83.13 o -31 1 20 378.59 314.79 61.51 o -29 1 20 34.21 125.92 66.53 o -27 1 20 0.62 -18.59 58.27 o -25 1 20 230.99 237.60 55.23 o -23 1 20 3958.94 4271.72 238.53 o -21 1 20 2943.40 2901.91 199.48 o -19 1 20 15625.73 18009.26 1237.14 o 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53.71 70.64 o -23 3 21 403.75 318.76 66.38 o -21 3 21 6130.48 7152.54 335.70 o -19 3 21 1415.43 1453.86 90.91 o -17 3 21 339.02 249.04 106.03 o -15 3 21 292.33 321.35 66.13 o -13 3 21 265.15 313.38 66.51 o -11 3 21 90.43 229.63 69.86 o -9 3 21 326.67 355.30 93.33 o -7 3 21 227.63 47.20 101.12 o -28 4 21 1.31 65.10 60.85 o -26 4 21 109.13 118.30 69.06 o -24 4 21 38.20 129.35 61.11 o -22 4 21 59.81 38.24 57.07 o -20 4 21 1227.17 1460.58 94.46 o -18 4 21 189.97 149.45 123.37 o -16 4 21 351.57 324.23 87.67 o -14 4 21 13.47 58.08 84.39 o -12 4 21 15.59 32.06 89.63 o -38 0 22 213.32 422.43 224.84 o -36 0 22 2459.89 2485.37 282.04 o -34 0 22 152.23 155.04 125.59 o -32 0 22 478.42 228.81 115.82 o -30 0 22 56.22 42.40 159.49 o -28 0 22 427.38 363.30 123.52 o -26 0 22 36.41 -92.76 146.72 o -24 0 22 615.66 716.86 117.45 o -22 0 22 31.35 -45.16 83.95 o -20 0 22 261.65 124.36 78.22 o -18 0 22 670.91 553.39 83.66 o -16 0 22 5124.01 5323.08 477.02 o -14 0 22 43.73 48.38 92.07 o -12 0 22 872.24 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