#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:59:13 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180936 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/16/2201628.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201628_Fobs loop_ _publ_author_name 'Blake, Alexander J.' 'Hubberstey, Peter' 'Mackrell, Alexander D.' _publ_section_title ; 3,4,6-Tris(pyrazol-1-yl)pyridazine ; _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1408 _journal_page_last o1410 _journal_volume 58 _journal_year 2002 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 102.140 _cell_angle_gamma 90.000 _cell_length_a 13.1900 _cell_length_b 7.0030 _cell_length_c 14.3260 _exptl_crystal_F_000 576.00 _reflns_d_resolution_high 0.9294 _cod_data_source_file su6005Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' triztz in P 21/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 129.92 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2949.82 2818.80 20.20 o 4 0 0 128.50 107.63 18.52 o 6 0 0 81.10 92.00 17.21 o 8 0 0 512.55 562.87 23.00 o 10 0 0 92.47 128.31 43.92 o 12 0 0 45.38 44.53 18.08 o 1 1 0 244.94 244.67 12.19 o 2 1 0 13630.27 12380.40 433.37 o 3 1 0 13069.80 12178.55 140.49 o 4 1 0 783.53 800.83 30.59 o 5 1 0 12.94 37.43 11.11 o 6 1 0 473.69 537.96 18.84 o 7 1 0 13.03 53.05 13.40 o 8 1 0 238.55 268.66 18.45 o 9 1 0 29.69 62.99 15.72 o 10 1 0 18.26 17.83 22.87 o 11 1 0 55.10 52.58 18.42 o 12 1 0 23.85 -4.89 49.21 o 13 1 0 13.75 62.46 19.27 o 0 2 0 2188.16 2067.50 28.18 o 1 2 0 16879.46 15209.00 361.77 o 2 2 0 6709.34 6446.67 171.22 o 3 2 0 28.58 12.60 11.01 o 4 2 0 725.32 673.13 24.59 o 5 2 0 563.75 597.40 20.21 o 6 2 0 194.09 165.03 15.06 o 7 2 0 845.52 899.03 72.39 o 8 2 0 0.01 3.08 49.82 o 9 2 0 116.99 117.01 27.94 o 10 2 0 28.65 52.79 18.18 o 11 2 0 4.37 -24.74 61.89 o 12 2 0 54.42 97.91 20.32 o 13 2 0 91.47 110.45 21.39 o 1 3 0 98.38 98.56 11.97 o 2 3 0 963.40 892.65 59.42 o 3 3 0 181.29 162.09 14.04 o 4 3 0 1436.67 1443.57 44.87 o 5 3 0 254.77 264.24 16.71 o 6 3 0 14.71 37.67 13.72 o 7 3 0 61.38 56.14 15.76 o 8 3 0 0.00 -12.01 15.48 o 9 3 0 40.85 4.63 54.92 o 10 3 0 3.32 -13.71 16.94 o 11 3 0 6.12 31.77 17.41 o 12 3 0 6.00 -8.47 33.38 o 0 4 0 0.83 12.78 11.58 o 1 4 0 559.21 564.21 28.76 o 2 4 0 679.46 637.26 38.59 o 3 4 0 713.99 664.20 36.37 o 4 4 0 121.59 116.68 29.58 o 5 4 0 9.16 -7.72 26.99 o 6 4 0 0.92 41.50 15.51 o 7 4 0 0.71 -6.22 16.12 o 8 4 0 6.06 -16.12 26.23 o 9 4 0 40.52 50.46 17.72 o 10 4 0 37.90 17.01 18.66 o 11 4 0 23.34 -12.18 55.02 o 1 5 0 1.35 2.24 59.46 o 2 5 0 64.20 44.87 27.74 o 3 5 0 95.97 104.03 61.06 o 4 5 0 53.31 66.13 20.20 o 5 5 0 47.88 52.61 16.92 o 6 5 0 464.50 423.08 25.94 o 7 5 0 8.75 37.91 27.11 o 8 5 0 2.12 -15.34 33.60 o 9 5 0 83.35 45.98 45.15 o 10 5 0 0.87 7.29 18.33 o 0 6 0 78.19 105.56 19.20 o 1 6 0 11.52 38.29 16.04 o 2 6 0 1.37 -4.63 31.80 o 3 6 0 52.47 51.65 18.00 o 4 6 0 205.00 203.84 21.65 o 5 6 0 0.35 9.13 26.59 o 6 6 0 0.96 -34.41 23.17 o 7 6 0 2.65 -27.44 17.78 o 8 6 0 86.28 82.18 46.50 o 1 7 0 0.31 0.26 50.81 o 2 7 0 0.13 -35.49 17.74 o 3 7 0 0.24 -70.37 41.83 o 4 7 0 0.01 -7.47 18.31 o 5 7 0 52.79 66.57 24.77 o -13 0 1 27.92 46.42 48.65 o -11 0 1 29.52 31.44 29.26 o -9 0 1 254.86 259.64 40.08 o -7 0 1 630.93 680.34 21.60 o -5 0 1 1495.86 1530.74 24.65 o -3 0 1 1010.81 1032.37 17.53 o 3 0 1 1511.06 1537.73 21.03 o 5 0 1 1.35 13.56 17.98 o 7 0 1 1153.22 1317.44 96.83 o 9 0 1 637.67 548.12 35.58 o 11 0 1 91.47 86.73 19.85 o 13 0 1 71.28 26.84 58.75 o -13 1 1 16.46 55.30 37.97 o -12 1 1 120.71 97.00 24.42 o -11 1 1 124.09 48.32 18.89 o -10 1 1 29.00 26.70 17.35 o -9 1 1 32.10 28.47 15.86 o -8 1 1 711.59 682.47 32.96 o -7 1 1 121.92 112.97 21.47 o -6 1 1 206.70 190.21 56.21 o -5 1 1 17.59 5.70 11.48 o -4 1 1 1607.98 1621.25 24.21 o -3 1 1 6155.60 6026.21 116.08 o -2 1 1 11125.44 10804.19 395.81 o -1 1 1 1152.23 1104.72 36.09 o 0 1 1 127.34 98.44 7.13 o 1 1 1 3653.62 3528.64 24.44 o 2 1 1 160.11 177.97 17.69 o 3 1 1 694.94 673.64 16.50 o 4 1 1 510.71 508.90 40.72 o 5 1 1 39.54 73.02 11.68 o 6 1 1 84.30 58.64 12.87 o 7 1 1 249.93 238.64 19.35 o 8 1 1 24.13 36.27 26.83 o 9 1 1 71.12 66.85 47.09 o 10 1 1 85.26 130.71 43.13 o 11 1 1 177.53 227.89 22.60 o 12 1 1 166.64 120.99 20.44 o 13 1 1 4.27 26.17 18.88 o -13 2 1 94.64 64.37 19.96 o -12 2 1 46.30 53.66 18.64 o -11 2 1 127.26 140.08 26.81 o -10 2 1 494.45 463.64 54.31 o -9 2 1 97.55 107.41 25.28 o -8 2 1 8.12 -3.15 17.72 o -7 2 1 29.34 26.09 13.72 o -6 2 1 77.85 105.69 14.07 o -5 2 1 358.32 315.12 15.99 o -4 2 1 57.09 73.83 18.36 o -3 2 1 3465.83 3454.82 34.86 o -2 2 1 12288.96 11441.91 619.24 o -1 2 1 8079.49 7213.82 474.44 o 0 2 1 13.74 37.70 23.41 o 1 2 1 6904.53 6421.78 333.47 o 2 2 1 506.28 561.59 38.15 o 3 2 1 98.91 110.53 19.21 o 4 2 1 109.86 112.30 12.13 o 5 2 1 84.43 134.08 14.01 o 6 2 1 87.95 119.20 39.59 o 7 2 1 176.80 186.99 16.67 o 8 2 1 547.79 582.53 25.14 o 9 2 1 3.34 -41.36 20.68 o 10 2 1 2.36 -21.84 17.27 o 11 2 1 101.88 81.76 19.26 o 12 2 1 12.64 8.07 17.03 o 13 2 1 8.16 11.65 24.27 o -12 3 1 0.04 -6.21 17.02 o -11 3 1 30.62 78.35 17.53 o -10 3 1 21.85 39.36 17.43 o -9 3 1 536.50 517.73 42.63 o -8 3 1 359.71 401.26 22.55 o -7 3 1 131.66 131.57 16.53 o -6 3 1 449.82 469.18 20.97 o -5 3 1 3458.28 3375.64 86.90 o -4 3 1 830.10 813.90 22.54 o -3 3 1 5.33 59.13 33.99 o -2 3 1 31.58 16.55 11.09 o -1 3 1 805.21 802.23 21.19 o 0 3 1 582.42 613.53 25.60 o 1 3 1 0.02 14.24 11.03 o 2 3 1 48.82 68.73 12.05 o 3 3 1 235.97 243.48 15.78 o 4 3 1 341.63 320.60 17.31 o 5 3 1 6.10 25.18 17.86 o 6 3 1 19.17 16.81 17.78 o 7 3 1 1.25 -10.36 14.86 o 8 3 1 59.88 72.01 17.61 o 9 3 1 0.87 0.46 19.72 o 10 3 1 259.06 272.09 38.55 o 11 3 1 101.08 105.58 20.44 o 12 3 1 16.83 -18.67 17.95 o -11 4 1 2.05 16.93 20.27 o -10 4 1 40.04 23.27 18.30 o -9 4 1 393.24 393.21 32.56 o -8 4 1 155.90 148.81 42.79 o -7 4 1 6.12 0.59 15.81 o -6 4 1 173.18 173.34 28.46 o -5 4 1 1197.86 1210.78 31.50 o -4 4 1 575.11 583.80 23.08 o -3 4 1 1837.22 1696.38 142.76 o -2 4 1 0.04 -16.99 13.36 o -1 4 1 61.88 78.06 13.16 o 0 4 1 376.81 355.42 24.80 o 1 4 1 14.37 -14.03 18.54 o 2 4 1 48.06 64.45 23.34 o 3 4 1 0.04 20.50 12.77 o 4 4 1 140.93 126.60 16.78 o 5 4 1 23.95 71.32 19.88 o 6 4 1 204.54 189.03 31.98 o 7 4 1 177.60 133.09 27.00 o 8 4 1 4.98 7.88 26.78 o 9 4 1 22.67 19.92 17.12 o 10 4 1 60.16 52.80 17.84 o 11 4 1 39.16 123.54 20.11 o -10 5 1 20.97 -14.19 36.40 o -9 5 1 44.87 51.70 27.01 o -8 5 1 0.48 -23.48 16.49 o -7 5 1 850.93 860.21 32.93 o -6 5 1 159.05 136.98 20.01 o -5 5 1 1.94 -52.42 26.21 o -4 5 1 30.83 79.14 91.19 o -3 5 1 5.81 4.93 14.94 o -2 5 1 7.97 -0.20 18.88 o -1 5 1 3.45 18.81 17.89 o 0 5 1 1.27 -35.71 46.55 o 1 5 1 47.32 47.61 18.65 o 2 5 1 0.32 -1.84 15.13 o 3 5 1 156.10 152.14 28.70 o 4 5 1 0.14 -31.99 41.53 o 5 5 1 20.42 9.86 30.17 o 6 5 1 75.96 121.41 18.95 o 7 5 1 48.15 30.83 25.42 o 8 5 1 27.50 11.89 41.81 o 9 5 1 0.45 25.63 40.74 o 10 5 1 7.61 -18.78 18.50 o -8 6 1 10.18 55.36 18.68 o -7 6 1 12.04 55.67 47.24 o -6 6 1 24.61 11.56 17.83 o -5 6 1 147.84 152.60 22.35 o -4 6 1 2.59 -12.50 15.63 o -3 6 1 0.15 63.28 16.28 o -2 6 1 0.00 -32.28 16.14 o -1 6 1 99.58 115.75 26.53 o 0 6 1 0.54 -11.47 17.02 o 1 6 1 0.03 -16.16 16.29 o 2 6 1 0.74 -1.07 17.68 o 3 6 1 28.21 65.54 24.28 o 4 6 1 8.35 37.09 31.71 o 5 6 1 6.50 12.84 30.12 o 6 6 1 11.65 60.61 32.82 o 7 6 1 0.23 3.83 53.10 o 8 6 1 28.42 -11.05 19.01 o -5 7 1 20.64 -6.14 18.85 o -4 7 1 6.91 -33.24 34.03 o -3 7 1 1.29 8.47 18.36 o -2 7 1 28.35 4.64 20.62 o -1 7 1 2.33 24.96 29.01 o 0 7 1 1.79 26.90 28.45 o 1 7 1 4.37 32.81 25.17 o 2 7 1 1.31 18.76 18.38 o 3 7 1 1.88 -35.05 17.53 o 4 7 1 12.80 -28.82 39.93 o -14 0 2 662.15 677.40 34.32 o -12 0 2 161.02 140.24 20.47 o -10 0 2 7.66 -18.26 37.77 o -8 0 2 0.05 22.80 15.18 o -6 0 2 105.71 135.75 13.23 o -4 0 2 112.26 96.44 30.06 o -2 0 2 4095.70 4027.98 41.11 o 0 0 2 301.96 306.72 18.89 o 2 0 2 273.36 240.33 12.29 o 4 0 2 25.20 72.19 11.83 o 6 0 2 1009.65 1043.19 28.48 o 8 0 2 1057.96 1102.18 32.39 o 10 0 2 316.38 245.39 27.66 o 12 0 2 231.67 296.61 65.85 o -14 1 2 0.01 39.71 19.99 o -13 1 2 89.04 164.50 21.74 o -12 1 2 784.64 819.65 32.47 o -11 1 2 321.78 370.05 44.14 o -10 1 2 63.62 24.66 41.38 o -9 1 2 23.58 1.89 17.53 o -8 1 2 36.19 44.30 28.59 o -7 1 2 608.04 600.48 21.55 o -6 1 2 40.38 32.92 25.78 o -5 1 2 375.63 391.62 31.67 o -4 1 2 861.48 840.07 55.51 o -3 1 2 2354.13 2416.59 26.46 o -2 1 2 424.67 459.57 20.72 o -1 1 2 568.64 591.83 55.79 o 0 1 2 1448.76 1423.59 165.20 o 1 1 2 8066.47 7932.46 456.64 o 2 1 2 27.95 18.76 21.72 o 3 1 2 1087.37 1148.51 69.86 o 4 1 2 8.66 20.96 13.19 o 5 1 2 2478.20 2634.81 90.32 o 6 1 2 1976.17 2102.85 33.89 o 7 1 2 68.03 66.70 17.16 o 8 1 2 628.98 656.68 25.48 o 9 1 2 57.15 52.98 17.50 o 10 1 2 25.11 14.72 17.47 o 11 1 2 3.49 40.06 17.56 o 12 1 2 12.01 26.05 18.72 o 13 1 2 30.24 40.28 57.84 o -13 2 2 37.47 66.02 35.83 o -12 2 2 107.52 74.63 20.17 o -11 2 2 58.80 36.06 17.89 o -10 2 2 9.92 0.67 17.36 o -9 2 2 100.74 51.51 16.74 o -8 2 2 3.14 -15.85 36.91 o -7 2 2 8.61 1.90 12.59 o -6 2 2 10.01 30.37 25.88 o -5 2 2 11.78 11.50 11.38 o -4 2 2 556.87 559.40 17.91 o -3 2 2 240.49 236.43 46.29 o -2 2 2 530.92 546.97 70.77 o -1 2 2 734.25 620.63 67.79 o 0 2 2 282.62 257.62 39.63 o 1 2 2 537.92 526.65 16.21 o 2 2 2 431.81 452.34 27.66 o 3 2 2 0.01 -22.13 11.07 o 4 2 2 326.30 304.84 23.69 o 5 2 2 662.02 652.91 21.41 o 6 2 2 166.13 191.65 49.92 o 7 2 2 191.39 196.94 52.70 o 8 2 2 12.08 19.42 16.45 o 9 2 2 478.53 455.89 25.29 o 10 2 2 404.38 420.67 25.64 o 11 2 2 72.63 32.38 37.76 o 12 2 2 15.01 10.46 19.54 o -12 3 2 13.16 65.51 47.65 o -11 3 2 321.90 350.75 56.93 o -10 3 2 617.94 575.49 69.50 o -9 3 2 105.75 102.88 18.43 o -8 3 2 49.79 47.10 20.91 o -7 3 2 584.45 593.40 24.57 o -6 3 2 314.18 336.95 23.22 o -5 3 2 156.10 164.31 15.07 o -4 3 2 144.47 108.45 14.32 o -3 3 2 1071.46 1090.48 44.97 o -2 3 2 8.33 32.42 22.05 o -1 3 2 0.59 -28.39 22.26 o 0 3 2 283.13 286.00 37.10 o 1 3 2 148.54 164.94 18.23 o 2 3 2 63.93 59.10 13.24 o 3 3 2 38.00 21.96 17.37 o 4 3 2 2038.22 2058.24 34.76 o 5 3 2 25.67 21.21 15.28 o 6 3 2 1.68 -8.30 27.23 o 7 3 2 2.28 -7.76 55.47 o 8 3 2 19.70 0.52 29.83 o 9 3 2 108.14 130.83 19.76 o 10 3 2 0.24 -19.81 17.97 o 11 3 2 28.26 -7.73 18.43 o 12 3 2 33.24 41.39 21.48 o -12 4 2 0.92 -36.63 18.31 o -11 4 2 6.09 -13.07 17.33 o -10 4 2 16.74 29.92 25.10 o -9 4 2 32.21 77.94 37.76 o -8 4 2 237.55 219.37 21.47 o -7 4 2 158.04 173.07 19.33 o -6 4 2 81.59 68.56 17.11 o -5 4 2 221.63 261.61 19.97 o -4 4 2 2.44 3.25 13.61 o -3 4 2 214.57 216.04 21.77 o -2 4 2 276.41 284.08 18.19 o -1 4 2 0.90 -9.74 43.98 o 0 4 2 128.86 127.45 21.02 o 1 4 2 57.30 86.62 26.87 o 2 4 2 23.36 0.06 13.57 o 3 4 2 0.06 -2.27 13.28 o 4 4 2 0.07 -7.58 14.55 o 5 4 2 175.66 160.75 21.81 o 6 4 2 257.42 259.85 23.92 o 7 4 2 5.45 12.06 31.79 o 8 4 2 10.18 26.55 18.51 o 9 4 2 70.29 36.31 42.08 o 10 4 2 145.01 79.04 25.10 o 11 4 2 100.35 142.15 41.11 o -10 5 2 38.18 39.32 27.64 o -9 5 2 40.62 56.42 17.94 o -8 5 2 403.36 387.22 26.61 o -7 5 2 1.13 9.24 35.03 o -6 5 2 1.67 29.10 15.90 o -5 5 2 122.67 89.36 53.61 o -4 5 2 128.92 129.81 18.17 o -3 5 2 105.97 114.43 16.99 o -2 5 2 6.65 -15.28 13.73 o -1 5 2 121.51 137.93 20.58 o 0 5 2 4.84 -28.40 14.20 o 1 5 2 0.17 -28.76 44.65 o 2 5 2 222.40 167.10 19.27 o 3 5 2 88.97 99.26 16.96 o 4 5 2 11.92 49.17 16.90 o 5 5 2 0.05 -27.10 17.15 o 6 5 2 27.66 7.67 35.35 o 7 5 2 0.04 5.78 25.39 o 8 5 2 16.82 -33.91 17.70 o 9 5 2 5.69 -9.44 17.59 o -8 6 2 0.73 42.85 17.56 o -7 6 2 18.38 14.33 56.14 o -6 6 2 305.99 307.90 24.40 o -5 6 2 8.65 -10.17 21.35 o -4 6 2 59.61 94.22 17.20 o -3 6 2 164.24 110.26 20.46 o -2 6 2 9.23 38.52 16.87 o -1 6 2 19.20 10.46 20.96 o 0 6 2 27.07 14.07 26.42 o 1 6 2 0.16 -30.99 15.49 o 2 6 2 5.56 -31.02 15.51 o 3 6 2 2.06 -18.69 17.01 o 4 6 2 19.54 10.87 17.32 o 5 6 2 14.59 16.24 21.87 o 6 6 2 0.62 -24.34 17.09 o 7 6 2 5.45 17.75 18.77 o -5 7 2 5.88 51.86 18.90 o -4 7 2 13.57 9.76 18.01 o -3 7 2 28.69 43.63 34.12 o -2 7 2 51.75 27.56 31.80 o -1 7 2 4.82 14.09 43.90 o 0 7 2 27.97 11.54 17.70 o 1 7 2 30.59 36.68 26.47 o 2 7 2 5.99 6.34 49.92 o 3 7 2 3.55 22.41 18.37 o 4 7 2 8.26 46.10 19.23 o -13 0 3 28.78 29.95 36.71 o -11 0 3 296.87 311.10 23.50 o -9 0 3 652.86 615.66 65.43 o -7 0 3 226.95 229.43 17.83 o -5 0 3 311.17 267.12 15.08 o -3 0 3 706.06 731.69 29.47 o -1 0 3 1230.55 1209.73 17.37 o 1 0 3 41.85 31.74 12.44 o 3 0 3 372.72 306.61 23.07 o 5 0 3 34.30 36.46 13.04 o 7 0 3 1680.43 1837.12 99.43 o 9 0 3 89.69 200.79 61.74 o 11 0 3 0.12 9.54 17.24 o 13 0 3 14.59 78.16 57.48 o -14 1 3 55.03 57.33 20.35 o -13 1 3 551.31 504.63 51.89 o -12 1 3 625.52 635.96 29.77 o -11 1 3 39.25 12.36 33.07 o -10 1 3 16.36 -29.08 16.74 o -9 1 3 40.86 21.09 28.24 o -8 1 3 183.20 173.64 17.08 o -7 1 3 61.44 33.56 43.78 o -6 1 3 224.60 252.13 15.77 o -5 1 3 77.31 121.48 48.87 o -4 1 3 10.60 5.27 11.06 o -3 1 3 964.68 924.44 30.55 o -2 1 3 104.28 93.41 11.44 o -1 1 3 1904.64 1945.53 135.96 o 0 1 3 8650.93 7921.23 374.68 o 1 1 3 3098.61 3067.93 134.36 o 2 1 3 265.62 244.43 21.41 o 3 1 3 90.35 104.03 12.40 o 4 1 3 1200.65 1271.80 48.79 o 5 1 3 1128.11 1227.42 56.69 o 6 1 3 15.63 -15.22 18.94 o 7 1 3 24.79 35.97 14.19 o 8 1 3 282.35 276.25 23.07 o 9 1 3 114.01 139.59 19.25 o 10 1 3 112.53 101.18 19.83 o 11 1 3 25.18 72.39 55.56 o 12 1 3 8.44 -1.92 17.80 o -13 2 3 4.51 38.16 29.90 o -12 2 3 42.29 13.34 18.50 o -11 2 3 14.07 22.10 22.80 o -10 2 3 760.81 740.34 29.65 o -9 2 3 474.21 443.78 36.92 o -8 2 3 0.01 -11.83 30.21 o -7 2 3 1.37 -2.08 12.87 o -6 2 3 17.88 17.23 12.37 o -5 2 3 16.43 18.09 11.71 o -4 2 3 164.09 172.14 13.47 o -3 2 3 3589.89 3617.99 116.08 o -2 2 3 213.63 206.88 28.56 o -1 2 3 1018.67 1149.55 112.33 o 0 2 3 1801.58 1765.86 159.70 o 1 2 3 541.11 552.20 22.75 o 2 2 3 331.09 420.19 46.93 o 3 2 3 5.04 -3.03 10.92 o 4 2 3 20.40 25.78 12.31 o 5 2 3 0.88 23.47 26.25 o 6 2 3 565.39 613.25 27.26 o 7 2 3 3.53 -12.30 15.18 o 8 2 3 60.20 60.58 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