#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2201649.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201649_Fobs loop_ _publ_author_name 'Otieno, Tom' 'Pinkston, Andrea T.' 'Johnson, Natisha C.' 'Parkin, Sean' _publ_section_title ; Aquatetrakis(2-methylpyrazine-\kN)(nitrato-\kO)copper(II) nitrate ; _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m328 _journal_page_last m330 _journal_volume 58 _journal_year 2002 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 88.562 _cell_angle_beta 72.938 _cell_angle_gamma 86.242 _cell_length_a 8.4480 _cell_length_b 12.3090 _cell_length_c 12.8410 _exptl_crystal_F_000 602.00 _reflns_d_resolution_high .8410 _[local]_cod_data_source_file wn6100Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' K01165 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 144.03 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 4791.65 4464.49 85.13 o 2 0 0 167.51 193.74 8.23 o 3 0 0 40.64 41.73 4.07 o 4 0 0 70.01 40.98 9.30 o 5 0 0 47.24 60.08 3.12 o 6 0 0 87.74 82.29 3.32 o 7 0 0 40.28 39.31 5.38 o 8 0 0 28.81 22.34 6.22 o 9 0 0 19.43 8.70 7.94 o -9 1 0 182.86 198.24 17.19 o -8 1 0 35.39 33.50 3.93 o -7 1 0 3.01 16.18 6.83 o -6 1 0 728.59 740.51 16.41 o -5 1 0 2820.67 2945.82 54.72 o -4 1 0 22.20 42.55 1.70 o -3 1 0 2525.76 2476.60 40.99 o -2 1 0 2865.63 3341.85 64.26 o -1 1 0 1797.09 1836.04 31.55 o 0 1 0 277.58 141.44 2.50 o 1 1 0 1277.68 1714.43 30.78 o 2 1 0 185.59 116.49 7.50 o 3 1 0 973.49 779.92 15.93 o 4 1 0 991.04 1022.02 187.30 o 5 1 0 925.27 802.00 17.41 o 6 1 0 534.59 541.30 20.27 o 7 1 0 .71 1.88 1.88 o 8 1 0 80.20 87.02 5.43 o 9 1 0 271.64 250.80 19.30 o -9 2 0 56.05 61.58 9.39 o -8 2 0 401.86 338.30 14.16 o -7 2 0 1322.00 1403.08 51.67 o -6 2 0 296.10 339.04 10.14 o -5 2 0 44.88 96.59 33.45 o -4 2 0 1325.84 1340.49 22.06 o -3 2 0 396.26 454.66 7.96 o -2 2 0 13470.21 14914.00 266.66 o -1 2 0 31.38 26.81 .90 o 0 2 0 1609.62 1720.35 28.99 o 1 2 0 2828.98 2847.16 60.99 o 2 2 0 7390.84 7009.81 255.49 o 3 2 0 23.16 36.14 3.16 o 4 2 0 1610.59 1856.43 41.39 o 5 2 0 2.91 1.55 1.64 o 6 2 0 82.64 72.39 4.02 o 7 2 0 376.87 371.63 12.89 o 8 2 0 12.45 6.56 2.66 o 9 2 0 72.74 77.33 23.00 o -9 3 0 202.16 187.49 18.68 o -8 3 0 1.65 8.98 4.12 o -7 3 0 48.15 56.07 14.71 o -6 3 0 343.78 391.32 11.87 o -5 3 0 3869.17 4118.14 92.93 o -4 3 0 166.11 192.79 9.19 o -3 3 0 340.85 389.83 10.41 o -2 3 0 6.98 6.50 .71 o -1 3 0 467.48 495.41 9.97 o 0 3 0 595.87 363.95 8.17 o 1 3 0 2525.80 2952.65 50.99 o 2 3 0 2967.94 3059.44 58.02 o 3 3 0 594.78 717.63 13.76 o 4 3 0 1327.69 1366.27 55.40 o 5 3 0 1887.96 1869.15 41.35 o 6 3 0 250.33 206.24 7.52 o 7 3 0 20.04 17.75 2.94 o 8 3 0 633.22 709.83 37.53 o 9 3 0 420.49 384.39 40.58 o -9 4 0 54.69 54.56 11.53 o -8 4 0 .84 6.13 5.26 o -7 4 0 130.24 145.97 29.25 o -6 4 0 307.92 344.37 13.43 o -5 4 0 136.64 167.13 19.75 o -4 4 0 455.55 425.78 15.44 o -3 4 0 778.20 899.76 66.51 o -2 4 0 30.13 18.80 1.02 o -1 4 0 1716.58 1828.55 41.12 o 0 4 0 2544.03 2361.21 43.65 o 1 4 0 168.11 191.29 3.68 o 2 4 0 549.07 698.09 12.36 o 3 4 0 1168.32 1137.93 19.69 o 4 4 0 847.20 905.64 25.51 o 5 4 0 196.00 197.85 6.46 o 6 4 0 383.16 361.53 23.35 o 7 4 0 349.92 308.47 12.97 o 8 4 0 234.88 224.01 14.42 o 9 4 0 289.36 271.09 29.00 o -8 5 0 15.75 34.91 16.29 o -7 5 0 8.71 17.27 12.25 o -6 5 0 914.50 973.47 39.58 o -5 5 0 1268.03 1444.74 49.83 o -4 5 0 540.69 601.18 20.48 o -3 5 0 61.60 59.76 2.26 o -2 5 0 356.70 356.53 7.50 o -1 5 0 84.63 136.98 14.18 o 0 5 0 232.80 196.78 4.03 o 1 5 0 2611.83 2836.99 66.16 o 2 5 0 538.93 600.35 11.66 o 3 5 0 2.19 4.78 1.38 o 4 5 0 360.96 288.82 9.15 o 5 5 0 792.55 821.28 25.76 o 6 5 0 214.77 217.72 8.88 o 7 5 0 65.46 64.19 7.08 o 8 5 0 189.94 212.50 19.57 o 9 5 0 57.18 54.63 9.20 o -8 6 0 190.61 184.28 21.38 o -7 6 0 72.35 52.72 5.49 o -6 6 0 155.53 146.49 9.56 o -5 6 0 247.09 307.50 14.24 o -4 6 0 436.53 477.02 15.72 o -3 6 0 153.57 214.51 213.76 o -2 6 0 204.40 186.03 5.14 o -1 6 0 579.12 538.17 88.65 o 0 6 0 5913.31 5859.10 105.20 o 1 6 0 1546.45 1775.74 52.42 o 2 6 0 192.95 224.69 7.25 o 3 6 0 895.72 1027.55 85.80 o 4 6 0 711.57 730.06 20.07 o 5 6 0 3.48 .10 7.77 o 6 6 0 518.75 560.74 19.21 o 7 6 0 5.41 2.31 6.08 o 8 6 0 26.95 30.56 8.13 o -8 7 0 14.95 8.52 7.34 o -7 7 0 77.66 83.47 10.35 o -6 7 0 2.68 7.38 6.06 o -5 7 0 396.54 409.88 18.43 o -4 7 0 209.38 220.77 18.41 o -3 7 0 31.41 38.37 12.11 o -2 7 0 1844.73 2039.00 45.88 o -1 7 0 774.39 869.96 29.03 o 0 7 0 38.92 46.05 2.11 o 1 7 0 1021.42 924.64 18.44 o 2 7 0 99.44 123.38 4.07 o 3 7 0 72.34 67.16 12.89 o 4 7 0 1404.31 1462.15 38.62 o 5 7 0 446.27 590.28 37.65 o 6 7 0 2.60 15.19 9.50 o 7 7 0 44.96 33.92 3.68 o 8 7 0 238.59 246.15 20.99 o -7 8 0 45.55 37.60 6.14 o -6 8 0 23.92 7.56 4.42 o -5 8 0 79.33 83.04 6.57 o -4 8 0 546.91 619.40 25.15 o -3 8 0 1026.74 1082.52 32.77 o -2 8 0 324.23 304.90 7.48 o -1 8 0 1296.69 1415.66 39.45 o 0 8 0 405.82 385.50 11.38 o 1 8 0 36.62 33.58 5.24 o 2 8 0 250.97 231.19 9.53 o 3 8 0 486.41 485.69 15.33 o 4 8 0 168.08 168.80 7.11 o 5 8 0 74.83 84.07 26.24 o 6 8 0 1.65 2.79 7.33 o 7 8 0 78.21 113.78 9.95 o 8 8 0 1.62 2.18 7.22 o -7 9 0 90.18 97.22 20.04 o -6 9 0 151.55 193.18 35.73 o -5 9 0 340.38 352.04 18.04 o -4 9 0 52.96 34.65 4.30 o -3 9 0 710.70 720.68 20.63 o -2 9 0 723.70 723.25 26.33 o -1 9 0 222.80 241.34 11.62 o 0 9 0 34.75 36.18 7.03 o 1 9 0 105.56 81.44 3.23 o 2 9 0 228.38 256.22 8.07 o 3 9 0 60.49 43.24 5.10 o 4 9 0 5.10 5.39 2.89 o 5 9 0 1421.03 1489.38 58.55 o 6 9 0 107.00 87.11 10.17 o 7 9 0 22.96 11.61 7.18 o -6 10 0 34.90 17.56 11.88 o -5 10 0 162.77 160.15 12.51 o -4 10 0 361.56 406.37 24.31 o -3 10 0 135.36 102.91 14.10 o -2 10 0 267.93 183.94 12.78 o -1 10 0 179.58 161.65 9.04 o 0 10 0 578.14 645.15 43.92 o 1 10 0 26.88 23.48 5.70 o 2 10 0 22.92 25.51 4.58 o 3 10 0 326.77 343.11 13.72 o 4 10 0 352.00 330.95 15.25 o 5 10 0 143.25 159.31 11.59 o 6 10 0 505.54 477.59 28.12 o 7 10 0 176.48 177.46 31.07 o -5 11 0 27.27 10.35 12.51 o -4 11 0 25.50 13.08 6.22 o -3 11 0 40.40 33.01 5.58 o -2 11 0 34.07 58.82 7.46 o -1 11 0 9.15 9.77 4.15 o 0 11 0 322.03 360.19 21.96 o 1 11 0 457.97 450.85 21.21 o 2 11 0 135.06 135.02 7.25 o 3 11 0 96.28 91.85 5.71 o 4 11 0 31.00 38.50 3.75 o 5 11 0 753.59 753.54 39.65 o 6 11 0 22.94 16.06 6.06 o -5 12 0 36.71 40.24 12.02 o -4 12 0 280.30 295.53 25.93 o -3 12 0 6.05 .43 5.44 o -2 12 0 137.08 120.29 18.90 o -1 12 0 321.86 306.20 20.45 o 0 12 0 523.05 560.13 31.87 o 1 12 0 2.61 2.64 5.08 o 2 12 0 38.69 54.05 16.96 o 3 12 0 94.60 103.23 9.64 o 4 12 0 .53 -.05 3.81 o 5 12 0 1.88 3.52 4.42 o -3 13 0 184.64 161.44 14.13 o -2 13 0 187.03 183.87 22.66 o -1 13 0 20.59 26.77 5.98 o 0 13 0 116.95 110.73 17.46 o 1 13 0 599.87 633.70 40.26 o 2 13 0 251.14 278.88 20.94 o 3 13 0 .21 9.94 8.23 o 4 13 0 186.54 191.63 18.13 o -2 14 0 19.83 19.64 7.21 o -1 14 0 190.65 142.61 15.14 o 0 14 0 149.38 181.55 20.72 o 1 14 0 .66 13.66 9.64 o 2 14 0 191.80 180.93 22.06 o 3 14 0 71.10 55.83 12.03 o -3 -14 1 63.15 81.77 15.33 o -2 -14 1 62.12 48.97 21.88 o -1 -14 1 504.52 453.28 39.88 o 0 -14 1 165.63 183.36 17.58 o 1 -14 1 26.57 18.15 7.91 o 2 -14 1 195.62 195.89 41.52 o -4 -13 1 1.77 19.01 7.68 o -3 -13 1 116.53 142.55 18.73 o -2 -13 1 211.15 201.15 32.67 o -1 -13 1 103.34 120.05 16.05 o 0 -13 1 368.04 359.71 35.59 o 1 -13 1 66.28 53.98 7.59 o 2 -13 1 2.66 13.55 6.57 o 3 -13 1 24.36 36.76 19.93 o -5 -12 1 688.51 691.13 45.15 o -4 -12 1 116.63 98.95 12.06 o -3 -12 1 141.48 142.38 19.10 o -2 -12 1 6.89 -3.46 17.92 o -1 -12 1 54.45 49.75 7.35 o 0 -12 1 155.05 133.64 36.20 o 1 -12 1 9.40 8.89 4.26 o 2 -12 1 262.99 276.81 23.53 o 3 -12 1 420.62 413.47 25.64 o 4 -12 1 31.25 36.49 11.13 o 5 -12 1 103.72 90.60 18.48 o -6 -11 1 314.89 294.00 24.53 o -5 -11 1 123.62 126.96 8.15 o -4 -11 1 421.73 442.52 20.10 o -3 -11 1 384.49 374.97 21.91 o -2 -11 1 42.38 47.48 5.10 o -1 -11 1 2.34 1.80 2.54 o 0 -11 1 40.16 41.31 4.57 o 1 -11 1 507.57 579.55 37.11 o 2 -11 1 199.15 176.86 10.89 o 3 -11 1 41.37 35.08 13.63 o 4 -11 1 154.73 194.83 39.48 o 5 -11 1 152.49 131.92 14.86 o 6 -11 1 28.27 29.18 26.57 o -7 -10 1 32.91 19.99 7.22 o -6 -10 1 46.51 42.58 16.05 o -5 -10 1 526.74 542.75 22.47 o -4 -10 1 835.67 823.24 33.19 o -3 -10 1 1.50 -.82 2.66 o -2 -10 1 105.79 88.78 4.36 o -1 -10 1 430.32 437.30 14.21 o 0 -10 1 1.71 5.13 3.45 o 1 -10 1 10.47 10.88 3.37 o 2 -10 1 221.86 212.15 22.27 o 3 -10 1 77.20 32.65 9.63 o 4 -10 1 4.03 12.14 6.19 o 5 -10 1 3.41 12.04 4.98 o 6 -10 1 91.90 112.36 13.72 o -7 -9 1 49.40 43.75 10.16 o -6 -9 1 300.17 270.84 16.25 o -5 -9 1 296.07 282.07 14.08 o -4 -9 1 186.29 226.56 12.88 o -3 -9 1 417.13 472.32 19.48 o -2 -9 1 889.16 884.34 29.71 o -1 -9 1 17.18 21.59 2.10 o 0 -9 1 234.29 240.71 7.72 o 1 -9 1 151.84 112.71 4.03 o 2 -9 1 8.35 7.06 1.66 o 3 -9 1 519.94 527.71 18.81 o 4 -9 1 336.95 302.85 13.72 o 5 -9 1 357.88 375.67 43.70 o 6 -9 1 84.58 100.08 16.04 o 7 -9 1 57.32 58.41 13.48 o -8 -8 1 46.91 57.59 22.57 o -7 -8 1 33.21 51.49 20.23 o -6 -8 1 85.15 99.83 9.10 o -5 -8 1 61.29 56.65 4.23 o -4 -8 1 179.19 169.72 24.57 o -3 -8 1 59.96 55.67 3.57 o -2 -8 1 315.69 333.45 19.00 o -1 -8 1 2551.60 2720.68 66.46 o 0 -8 1 136.56 119.25 3.77 o 1 -8 1 53.14 34.96 4.12 o 2 -8 1 393.38 342.44 8.89 o 3 -8 1 2252.32 2393.47 70.67 o 4 -8 1 94.03 111.68 13.44 o 5 -8 1 411.14 394.71 22.51 o 6 -8 1 111.63 85.02 7.43 o 7 -8 1 16.71 7.26 5.01 o -8 -7 1 5.34 10.94 19.34 o -7 -7 1 47.47 48.67 6.64 o -6 -7 1 71.71 63.28 7.07 o -5 -7 1 267.81 268.42 10.69 o -4 -7 1 601.30 767.45 69.03 o -3 -7 1 1047.96 1044.21 28.93 o -2 -7 1 158.50 120.31 4.43 o -1 -7 1 34.64 15.20 1.26 o 0 -7 1 538.49 571.90 37.94 o 1 -7 1 329.88 301.92 6.54 o 2 -7 1 89.35 108.74 11.83 o 3 -7 1 1244.08 1233.32 35.13 o 4 -7 1 1453.86 1405.49 80.80 o 5 -7 1 705.33 674.02 25.06 o 6 -7 1 36.40 51.34 5.98 o 7 -7 1 20.96 18.19 5.06 o 8 -7 1 91.56 101.84 20.19 o -8 -6 1 216.40 191.91 17.58 o -7 -6 1 41.16 34.31 10.88 o -6 -6 1 5.36 7.96 3.23 o -5 -6 1 887.91 823.72 31.02 o -4 -6 1 836.42 874.90 27.45 o -3 -6 1 47.21 51.94 4.88 o -2 -6 1 594.92 525.54 10.44 o -1 -6 1 3585.33 3627.29 61.45 o 0 -6 1 1592.18 1806.33 36.94 o 1 -6 1 26.24 35.73 1.82 o 2 -6 1 117.92 77.38 5.89 o 3 -6 1 1521.93 1541.64 38.72 o 4 -6 1 .30 5.26 2.45 o 5 -6 1 398.98 362.77 12.73 o 6 -6 1 360.50 369.15 26.41 o 7 -6 1 5.53 5.59 3.69 o 8 -6 1 34.14 27.51 8.65 o -8 -5 1 6.91 14.99 6.13 o -7 -5 1 6.37 5.65 2.13 o -6 -5 1 397.77 392.68 12.12 o -5 -5 1 126.47 115.92 4.01 o -4 -5 1 1.31 4.60 2.01 o -3 -5 1 791.49 857.97 17.65 o -2 -5 1 851.34 842.93 15.69 o -1 -5 1 331.03 338.63 8.80 o 0 -5 1 4783.89 4977.54 98.13 o 1 -5 1 212.53 250.53 4.76 o 2 -5 1 159.57 182.17 4.71 o 3 -5 1 966.98 832.96 16.10 o 4 -5 1 1823.88 1782.77 47.75 o 5 -5 1 258.83 243.68 14.30 o 6 -5 1 6.20 21.91 15.50 o 7 -5 1 64.10 56.56 5.18 o 8 -5 1 19.99 19.29 5.10 o -9 -4 1 1.50 17.66 8.25 o -8 -4 1 355.07 355.05 23.37 o -7 -4 1 133.93 151.78 6.87 o -6 -4 1 92.12 100.70 7.31 o -5 -4 1 903.38 863.31 27.25 o -4 -4 1 988.34 1124.93 28.62 o -3 -4 1 164.62 156.63 4.26 o -2 -4 1 3117.70 3269.58 59.56 o -1 -4 1 4606.19 4211.15 77.37 o 0 -4 1 1.84 4.04 .60 o 1 -4 1 443.36 532.69 10.70 o 2 -4 1 281.35 208.34 29.67 o 3 -4 1 709.76 911.57 17.48 o 4 -4 1 237.03 287.78 10.77 o 5 -4 1 692.47 690.16 21.62 o 6 -4 1 146.83 150.93 14.52 o 7 -4 1 94.13 102.95 6.37 o 8 -4 1 80.76 98.54 12.27 o 9 -4 1 129.20 141.47 21.21 o -9 -3 1 187.27 197.34 22.23 o -8 -3 1 23.99 28.99 10.95 o -7 -3 1 567.09 623.96 41.63 o -6 -3 1 1621.06 1734.63 47.89 o -5 -3 1 86.92 92.24 3.43 o -4 -3 1 1.90 6.78 2.63 o -3 -3 1 141.78 109.95 3.35 o -2 -3 1 1944.80 2055.85 40.03 o -1 -3 1 .55 3.99 1.01 o 0 -3 1 10077.43 9757.06 161.90 o 1 -3 1 4602.82 4368.21 91.67 o 2 -3 1 149.44 174.29 3.55 o 3 -3 1 1013.01 803.73 15.53 o 4 -3 1 2615.29 2765.71 55.45 o 5 -3 1 1362.45 1318.24 27.27 o 6 -3 1 277.33 311.19 19.44 o 7 -3 1 713.60 726.94 26.26 o 8 -3 1 537.76 531.46 32.68 o 9 -3 1 .03 18.55 7.74 o -9 -2 1 315.27 277.20 19.16 o -8 -2 1 98.93 99.09 23.73 o -7 -2 1 182.42 133.32 9.48 o -6 -2 1 234.73 197.15 6.27 o -5 -2 1 908.11 863.40 22.18 o -4 -2 1 177.53 274.28 6.74 o -3 -2 1 182.68 266.59 8.74 o -2 -2 1 242.09 216.37 4.98 o -1 -2 1 11312.29 9695.44 202.00 o 0 -2 1 1265.42 1373.58 21.70 o 1 -2 1 261.96 325.01 8.17 o 2 -2 1 138.75 200.96 4.42 o 3 -2 1 711.48 660.44 11.80 o 4 -2 1 41.68 45.91 1.85 o 5 -2 1 1770.79 1858.94 38.89 o 6 -2 1 922.77 1063.21 40.54 o 7 -2 1 1.07 15.02 2.38 o 8 -2 1 445.45 478.17 22.84 o 9 -2 1 379.67 388.47 25.59 o -9 -1 1 43.29 38.80 5.57 o -8 -1 1 74.06 81.78 9.45 o -7 -1 1 234.09 234.57 10.17 o -6 -1 1 556.73 621.23 17.73 o -5 -1 1 .29 4.43 3.02 o -4 -1 1 111.77 120.58 3.29 o -3 -1 1 1682.44 1154.19 58.95 o -2 -1 1 25.71 47.38 1.48 o -1 -1 1 1721.49 1589.79 30.51 o 0 -1 1 6861.32 6704.56 117.19 o 1 -1 1 1012.58 869.68 20.09 o 2 -1 1 239.31 224.77 4.18 o 3 -1 1 5940.29 5927.15 107.17 o 4 -1 1 2305.02 2182.91 37.18 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14 306.16 280.91 16.92 o 3 0 14 41.50 58.47 12.28 o 4 0 14 243.80 218.45 21.78 o 5 0 14 3.14 15.59 11.46 o 6 0 14 96.24 84.73 10.56 o -1 1 14 115.00 103.51 12.36 o 0 1 14 307.46 314.83 42.79 o 1 1 14 166.75 186.20 15.33 o 2 1 14 138.65 148.32 10.80 o 3 1 14 50.66 57.26 9.30 o 4 1 14 9.87 34.95 12.45 o 5 1 14 204.25 214.22 19.01 o 6 1 14 20.15 19.89 10.90 o 0 2 14 165.49 183.73 29.66 o 1 2 14 146.00 147.08 12.47 o 2 2 14 51.26 53.66 6.74 o 3 2 14 18.50 21.69 8.45 o 4 2 14 2.58 6.49 6.64 o 5 2 14 47.42 58.16 31.22 o 6 2 14 35.61 38.56 11.39 o 0 3 14 87.01 118.10 14.55 o 1 3 14 71.68 64.54 7.89 o 2 3 14 66.47 55.98 5.86 o 3 3 14 34.75 33.67 6.96 o 4 3 14 203.86 209.19 18.34 o 5 3 14 276.63 268.08 28.94 o 6 3 14 96.64 109.66 17.24 o 0 4 14 69.32 61.97 7.76 o 1 4 14 70.24 99.82 13.62 o 2 4 14 16.19 25.04 5.74 o 3 4 14 97.22 95.37 10.89 o 4 4 14 11.44 11.60 7.27 o 5 4 14 14.48 28.92 7.85 o 1 5 14 172.84 194.88 18.28 o 2 5 14 52.07 35.76 24.64 o 3 5 14 247.19 185.52 42.81 o 4 5 14 337.86 350.79 39.76 o 5 5 14 104.50 98.55 12.89 o 2 6 14 356.16 413.10 38.46 o 3 6 14 157.32 140.04 16.22 o 2 -2 15 38.06 37.04 6.86 o 3 -2 15 5.31 4.06 11.03 o 2 -1 15 167.04 190.14 21.45 o 3 -1 15 91.19 100.52 16.16 o 4 -1 15 285.50 306.89 34.75 o 2 0 15 71.88 58.90 10.59 o 3 0 15 98.32 87.35 13.14 o 4 0 15 92.71 86.75 14.11 o 2 1 15 98.36 94.80 14.43 o 3 1 15 164.11 147.44 17.59 o 4 1 15 75.67 66.90 9.99 o 2 2 15 36.96 28.36 8.13 o 3 2 15 .63 6.08 9.25 o 4 2 15 56.29 59.45 9.41 o 3 3 15 97.35 82.68 11.88 o