#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/16/2201665.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201665_Fobs loop_ _publ_author_name 'Cabort, Amel' 'Therrien, Bruno' 'Bernauer, Klaus' 'S\"uss-Fink, Georg' _publ_section_title ; [RuCl{2,6-bis(3,4-dihydro-2H-pyrrol-5-yl)pyridine}(PPh~3~)~2~]BF~4~ dichloromethane solvate ; _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m557 _journal_page_last m558 _journal_volume 58 _journal_year 2002 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 80.231 _cell_angle_beta 89.193 _cell_angle_gamma 67.943 _cell_length_a 10.3368 _cell_length_b 12.7939 _cell_length_c 19.1336 _exptl_crystal_F_000 1068.00 _reflns_d_resolution_high 0.8147 _[local]_cod_data_source_file wn6119Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' AC007' _shelx_refln_list_code 4 _shelx_f_calc_maximum 202.11 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 9982.11 9868.93 230.22 o 2 0 0 1591.54 1575.67 70.59 o 3 0 0 21170.15 24247.47 493.50 o 4 0 0 4370.69 4060.99 168.43 o 5 0 0 8677.04 8923.68 204.26 o 6 0 0 15041.28 16197.74 202.21 o 7 0 0 982.82 1009.22 45.97 o 8 0 0 1299.32 1315.50 59.90 o 9 0 0 7195.56 7630.75 104.43 o 10 0 0 335.06 274.40 77.81 o 11 0 0 37.12 57.15 74.53 o -11 1 0 123.46 83.98 84.32 o -10 1 0 235.34 218.07 65.87 o -9 1 0 1554.25 1685.59 66.55 o -8 1 0 831.24 866.77 51.76 o -7 1 0 241.21 275.88 31.41 o -6 1 0 266.86 231.79 37.63 o -5 1 0 654.50 681.75 39.10 o -4 1 0 871.79 926.94 42.53 o -3 1 0 2409.02 2399.14 59.00 o -2 1 0 7745.47 7781.55 145.90 o -1 1 0 1329.21 1344.53 56.47 o 1 1 0 7625.88 7532.58 305.11 o 3 1 0 13370.09 15907.21 228.37 o 4 1 0 6.26 3.05 34.00 o 5 1 0 782.07 760.47 51.89 o 6 1 0 9063.65 9629.89 222.18 o 7 1 0 485.00 524.22 49.23 o 8 1 0 588.38 572.34 70.65 o 9 1 0 4550.14 4478.75 133.61 o 10 1 0 579.89 559.09 62.92 o 11 1 0 47.53 26.90 80.12 o -10 2 0 238.01 271.24 66.97 o -9 2 0 100.36 73.05 54.28 o -8 2 0 662.79 664.74 42.56 o -7 2 0 2.76 10.24 44.16 o -6 2 0 39.36 48.12 25.34 o -5 2 0 4616.45 4686.05 63.70 o -4 2 0 34.91 15.33 28.21 o -3 2 0 389.22 338.80 38.37 o -2 2 0 6939.76 8184.84 595.89 o -1 2 0 7149.43 6996.74 96.29 o 0 2 0 108.18 88.49 35.11 o 1 2 0 620.67 663.23 47.09 o 2 2 0 5604.96 5559.77 134.65 o 3 2 0 9790.07 10688.02 225.10 o 4 2 0 8275.04 8331.90 653.23 o 5 2 0 725.95 693.28 61.02 o 6 2 0 2621.23 2267.09 92.15 o 7 2 0 131.55 96.39 42.64 o 8 2 0 1060.78 1026.44 66.04 o 9 2 0 5839.76 5593.73 348.63 o 10 2 0 470.21 447.80 81.20 o -10 3 0 14.71 -10.17 77.10 o -9 3 0 2.66 -4.40 52.84 o -8 3 0 865.16 951.88 44.16 o -7 3 0 55.64 50.14 36.18 o -6 3 0 558.69 593.56 30.76 o -5 3 0 2021.32 2195.39 46.59 o -4 3 0 217.83 238.31 29.03 o -3 3 0 139.26 188.92 37.28 o -2 3 0 6336.88 6494.53 74.18 o -1 3 0 4309.51 4504.66 64.43 o 0 3 0 921.80 1004.74 40.44 o 1 3 0 29804.62 29192.58 638.38 o 2 3 0 4200.39 4072.71 98.29 o 3 3 0 1877.02 1800.50 68.91 o 4 3 0 17.17 20.46 40.90 o -10 4 0 0.05 -25.01 64.92 o -9 4 0 783.64 772.83 68.78 o -8 4 0 1477.64 1498.89 61.90 o -7 4 0 557.99 533.25 40.06 o -6 4 0 800.98 781.13 63.99 o -5 4 0 2130.06 2002.76 48.14 o -4 4 0 0.53 15.76 29.70 o -3 4 0 9071.04 9204.30 84.47 o -2 4 0 2720.18 3295.06 155.12 o -1 4 0 1272.90 1159.67 39.79 o 0 4 0 13044.74 13844.65 104.95 o 1 4 0 32692.56 41613.02 188.57 o 2 4 0 5284.78 5583.07 87.03 o 3 4 0 2130.31 2128.03 55.38 o 4 4 0 9083.42 8309.87 119.78 o 5 4 0 681.55 622.49 61.90 o -9 5 0 2500.28 2523.84 86.14 o -8 5 0 409.99 460.13 66.24 o -7 5 0 347.06 323.77 40.90 o -6 5 0 3060.29 3106.38 83.45 o -5 5 0 924.39 930.04 35.12 o -4 5 0 17.80 13.69 37.24 o -3 5 0 6195.64 6401.61 101.36 o -2 5 0 4131.56 4084.16 57.53 o -1 5 0 58.83 55.15 31.20 o 0 5 0 12405.31 12682.24 250.34 o 1 5 0 27542.74 33019.40 1091.95 o 2 5 0 92.66 129.36 30.23 o 3 5 0 2655.53 2412.53 70.65 o 4 5 0 7981.00 7629.17 162.28 o 5 5 0 1.32 6.65 31.49 o 6 5 0 6308.73 6169.14 167.40 o -8 6 0 330.62 360.36 55.24 o -7 6 0 520.54 504.24 56.83 o -6 6 0 227.19 235.06 54.28 o -5 6 0 386.84 402.19 39.00 o -4 6 0 252.88 238.63 27.14 o -3 6 0 3624.92 3553.96 47.42 o -2 6 0 1244.92 1267.25 44.87 o -1 6 0 4378.01 4233.49 57.14 o 0 6 0 734.95 549.87 32.96 o 1 6 0 5616.15 5140.92 377.81 o 2 6 0 13.23 24.12 29.91 o 3 6 0 721.83 613.76 49.66 o 4 6 0 10422.25 10222.55 172.52 o 5 6 0 3010.02 2891.02 100.34 o 6 6 0 6006.54 5631.10 175.08 o 7 6 0 10735.58 10903.20 288.22 o -8 7 0 22.94 2.72 63.58 o -7 7 0 11.43 11.75 45.97 o -6 7 0 980.33 961.78 49.20 o -5 7 0 422.04 494.25 39.09 o 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363.59 391.27 27.87 o 1 9 0 1216.48 1289.82 41.92 o 2 9 0 157.30 155.38 25.69 o 3 9 0 655.46 667.28 39.01 o 4 9 0 1924.18 1867.12 47.04 o 5 9 0 489.51 523.66 30.76 o 6 9 0 45.92 38.93 35.11 o 7 9 0 4454.15 4675.95 180.71 o 8 9 0 647.62 655.17 50.54 o 9 9 0 319.45 308.12 77.83 o -5 10 0 537.04 486.06 56.83 o -4 10 0 9.25 -25.58 65.49 o -3 10 0 937.71 916.78 50.68 o -2 10 0 2970.09 3126.00 52.22 o -1 10 0 1044.11 1042.85 39.74 o 0 10 0 42.83 267.93 63.48 o 1 10 0 2347.14 2335.32 44.15 o 2 10 0 180.69 207.61 36.36 o 3 10 0 751.71 776.54 44.87 o 4 10 0 970.11 1003.65 41.99 o 5 10 0 1753.58 1796.72 55.01 o 6 10 0 971.78 976.72 47.10 o 7 10 0 4014.50 3840.14 64.73 o 8 10 0 1054.35 1077.73 61.10 o 9 10 0 197.37 220.96 54.07 o 10 10 0 1350.52 37.88 74.74 o -4 11 0 11.00 47.60 75.63 o -3 11 0 336.23 304.74 66.22 o -2 11 0 2886.83 3037.15 65.53 o -1 11 0 214.83 157.23 55.01 o 0 11 0 254.92 312.16 49.15 o 1 11 0 1633.97 1467.27 77.30 o 2 11 0 1240.47 1375.92 59.38 o 3 11 0 1317.48 1351.27 49.66 o 4 11 0 4008.28 3784.73 97.27 o 5 11 0 1633.03 1595.63 46.74 o 6 11 0 111.19 67.69 48.63 o 7 11 0 4228.44 4340.00 101.87 o 8 11 0 2594.91 2630.95 70.56 o 9 11 0 91.13 48.16 53.76 o 10 11 0 1491.34 1471.45 96.94 o -3 12 0 68.41 39.93 54.30 o -2 12 0 127.05 104.51 52.46 o -1 12 0 144.00 28.23 45.97 o 0 12 0 4.24 84.17 53.56 o 1 12 0 31.22 20.64 43.16 o 2 12 0 13.30 13.56 43.70 o 3 12 0 857.07 893.10 47.53 o 4 12 0 710.70 707.58 55.73 o 5 12 0 583.87 670.44 55.01 o 6 12 0 60.92 24.78 53.56 o 7 12 0 730.00 745.47 57.55 o 8 12 0 508.95 503.73 56.46 o 9 12 0 14.98 9.21 63.27 o 10 12 0 495.05 533.19 85.10 o -2 13 0 159.70 155.33 62.61 o -1 13 0 94.42 69.13 62.40 o 0 13 0 0.97 38.61 44.49 o 1 13 0 103.68 100.67 51.70 o 2 13 0 75.95 79.13 43.56 o 3 13 0 23.67 21.23 51.73 o 4 13 0 77.22 33.26 42.42 o 5 13 0 72.13 73.28 42.95 o 6 13 0 45.47 51.32 43.00 o 7 13 0 724.96 777.00 55.77 o 8 13 0 175.33 179.61 64.77 o 9 13 0 148.88 166.31 75.65 o 10 13 0 491.37 495.96 78.75 o 0 14 0 9.95 -21.82 75.93 o 1 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