#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:59:13 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180936 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/16/2201677.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201677_Fobs loop_ _publ_author_name 'Guo, Tengwen' 'Lai, Chian Sing' 'Tan, Xi Jie' 'Teo, Chin Seng' 'Tiekink, Edward R. T.' _publ_section_title ; Bis(diethyldithiocarbamato)(4,7-dimethyl-1,10-phenanthroline)cadmium(II) acetonitrile solvate ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m439 _journal_page_last m440 _journal_volume 58 _journal_year 2002 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 94.198 _cell_angle_gamma 90.000 _cell_length_a 10.9451 _cell_length_b 10.0886 _cell_length_c 28.4366 _exptl_crystal_F_000 1352.00 _reflns_d_resolution_high 0.7102 _cod_data_source_file ww6024Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Template texray.inf' _shelx_refln_list_code 4 _shelx_f_calc_maximum 401.30 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 4013.53 4416.72 126.00 o 2 0 0 29316.58 34014.21 925.93 o 3 0 0 14216.83 15985.85 447.48 o 4 0 0 21727.06 25020.78 694.67 o 5 0 0 55017.16 61647.38 1681.04 o 6 0 0 3609.88 4056.72 101.94 o 7 0 0 6859.62 7047.61 179.68 o 8 0 0 5016.69 4860.32 125.96 o 9 0 0 7356.60 7793.47 187.53 o 10 0 0 979.35 1124.59 61.30 o 11 0 0 2014.77 1901.18 78.74 o 12 0 0 2026.42 2022.06 119.99 o 13 0 0 46.41 2.71 43.30 o 14 0 0 130.15 193.97 57.14 o 15 0 0 28.88 48.72 43.00 o 1 1 0 3809.98 4391.58 62.00 o 2 1 0 2533.97 2932.88 55.08 o 3 1 0 11502.96 12660.64 209.45 o 4 1 0 602.39 625.96 27.95 o 5 1 0 1267.67 1289.84 39.40 o 6 1 0 101.05 137.14 18.94 o 7 1 0 693.92 646.80 33.50 o 8 1 0 177.52 167.33 32.79 o 9 1 0 2.84 -8.24 28.34 o 10 1 0 152.67 170.13 25.19 o 11 1 0 3.70 -10.15 25.57 o 12 1 0 718.51 784.16 57.51 o 13 1 0 236.29 326.03 44.74 o 14 1 0 305.04 326.39 52.18 o 15 1 0 92.93 169.22 35.58 o 0 2 0 1319.35 1339.21 39.32 o 1 2 0 1922.38 2241.00 46.01 o 2 2 0 250.26 220.78 13.97 o 3 2 0 3556.09 3684.02 72.36 o 4 2 0 7974.35 8166.15 143.84 o 5 2 0 17253.44 18050.05 301.20 o 6 2 0 263.05 288.38 23.53 o 7 2 0 8720.74 8825.80 186.52 o 8 2 0 201.00 152.16 25.90 o 9 2 0 377.69 323.41 33.19 o 10 2 0 4285.89 4295.06 102.55 o 11 2 0 0.10 -26.01 50.15 o 12 2 0 1627.35 1641.55 63.69 o 13 2 0 1212.49 1372.89 152.17 o 14 2 0 303.81 415.96 48.04 o 15 2 0 90.15 221.12 36.49 o 1 3 0 1511.19 1873.31 47.02 o 2 3 0 485.83 528.62 25.68 o 3 3 0 10450.72 10887.94 155.38 o 4 3 0 3476.37 3290.00 58.91 o 5 3 0 3642.39 3584.20 64.87 o 6 3 0 11154.91 11233.56 200.28 o 7 3 0 2221.85 2107.30 61.39 o 8 3 0 5766.31 5620.40 178.58 o 9 3 0 2.07 -17.96 24.39 o 10 3 0 28.96 -11.50 24.24 o 11 3 0 1771.27 1805.71 66.53 o 12 3 0 9.33 -29.17 29.17 o 13 3 0 904.54 1103.82 68.13 o 14 3 0 65.59 96.87 33.26 o 15 3 0 447.72 627.03 85.56 o 0 4 0 1622.96 1486.57 54.19 o 1 4 0 24.39 18.67 16.24 o 2 4 0 140.70 190.30 20.66 o 3 4 0 492.51 475.59 26.80 o 4 4 0 2349.84 2662.57 64.04 o 5 4 0 89.69 85.61 17.42 o 6 4 0 367.46 355.97 24.10 o 7 4 0 592.51 478.77 28.51 o 8 4 0 493.52 440.63 29.32 o 9 4 0 67.81 96.57 22.92 o 10 4 0 23.23 44.41 22.21 o 11 4 0 707.17 811.59 40.75 o 12 4 0 25.27 20.31 23.54 o 13 4 0 377.19 389.50 34.18 o 14 4 0 31.59 52.65 25.34 o 1 5 0 15990.69 16578.00 280.56 o 2 5 0 2475.00 2490.55 62.43 o 3 5 0 5315.18 5391.32 108.62 o 4 5 0 1750.25 1591.40 51.11 o 5 5 0 301.57 324.90 28.96 o 6 5 0 3769.63 3384.95 175.97 o 7 5 0 617.95 595.20 32.26 o 8 5 0 1832.75 1864.27 61.68 o 9 5 0 1584.13 1436.67 48.59 o 10 5 0 1279.51 1217.61 46.83 o 11 5 0 1598.27 1576.57 54.40 o 12 5 0 121.03 41.14 28.17 o 13 5 0 787.17 797.76 44.39 o 14 5 0 66.98 171.09 31.40 o 0 6 0 10205.66 10209.86 315.76 o 1 6 0 163.06 168.15 24.73 o 2 6 0 9013.52 9011.39 167.73 o 3 6 0 3561.69 3630.66 86.33 o 4 6 0 92.65 110.55 25.90 o 5 6 0 1671.51 1721.18 58.63 o 6 6 0 231.57 219.66 30.59 o 7 6 0 772.10 785.04 44.76 o 8 6 0 2570.65 2373.97 74.85 o 9 6 0 825.09 787.20 47.59 o 10 6 0 1010.04 945.88 44.58 o 11 6 0 11.44 44.00 25.45 o 12 6 0 419.57 419.33 61.37 o 13 6 0 16.58 89.13 45.02 o 1 7 0 5411.23 5541.70 118.64 o 2 7 0 2976.08 2838.80 77.41 o 3 7 0 502.63 504.32 37.27 o 4 7 0 5668.42 5477.24 120.44 o 5 7 0 2180.67 2077.87 75.39 o 6 7 0 5441.42 5267.66 120.45 o 7 7 0 748.73 737.02 46.57 o 8 7 0 598.97 596.26 44.13 o 9 7 0 381.76 381.86 39.74 o 10 7 0 114.02 95.18 31.85 o 11 7 0 1054.07 1113.26 59.32 o 12 7 0 283.54 335.92 72.44 o 13 7 0 234.75 292.88 56.49 o 0 8 0 370.73 331.70 56.84 o 1 8 0 299.94 308.97 39.39 o 2 8 0 7332.43 7278.63 151.47 o 3 8 0 5104.21 4707.72 111.61 o 4 8 0 230.84 232.36 34.68 o 5 8 0 3145.50 3047.23 86.90 o 6 8 0 208.73 199.59 36.69 o 7 8 0 3723.66 3566.35 97.72 o 8 8 0 303.00 287.64 37.99 o 9 8 0 710.93 732.20 49.98 o 10 8 0 913.84 889.13 54.75 o 11 8 0 44.80 25.74 29.97 o 12 8 0 955.82 1018.19 59.37 o 1 9 0 1381.60 1211.04 65.71 o 2 9 0 48.90 56.41 32.77 o 3 9 0 127.01 84.72 31.48 o 4 9 0 29.70 34.11 32.65 o 5 9 0 13.18 6.58 28.10 o 6 9 0 50.65 24.64 28.20 o 7 9 0 418.06 372.17 40.87 o 8 9 0 48.19 0.89 29.87 o 9 9 0 16.96 -18.86 28.77 o 10 9 0 42.85 38.32 31.70 o 11 9 0 2.69 21.08 30.21 o 0 10 0 901.23 954.20 89.31 o 1 10 0 57.71 43.13 33.80 o 2 10 0 2526.69 2424.81 94.07 o 3 10 0 626.46 624.49 69.62 o 4 10 0 283.08 230.48 38.67 o 5 10 0 670.11 723.03 51.80 o 6 10 0 39.68 26.41 29.66 o 7 10 0 1397.73 1327.30 65.23 o 8 10 0 208.26 256.53 42.25 o 9 10 0 553.28 603.37 52.00 o 10 10 0 502.99 459.43 50.80 o 1 11 0 1450.36 1439.62 115.63 o 2 11 0 13.29 -19.69 32.63 o 3 11 0 297.39 351.94 49.38 o 4 11 0 554.69 620.64 57.50 o 5 11 0 89.11 110.63 39.91 o 6 11 0 826.18 877.57 59.90 o 7 11 0 41.83 98.94 35.46 o 8 11 0 463.67 512.99 50.78 o 9 11 0 532.62 648.09 52.97 o 0 12 0 81.99 72.47 58.94 o 1 12 0 27.88 51.45 38.92 o 2 12 0 814.19 832.84 66.57 o 3 12 0 230.20 230.39 47.61 o 4 12 0 63.61 119.15 43.89 o 5 12 0 128.29 169.44 43.49 o 6 12 0 1.19 -3.67 34.14 o 7 12 0 243.20 215.32 42.50 o 8 12 0 25.33 83.38 37.30 o 1 13 0 1916.02 2061.60 101.52 o 2 13 0 474.20 572.34 62.73 o 3 13 0 172.00 263.55 53.88 o 4 13 0 1789.55 1877.43 159.53 o 5 13 0 19.34 39.06 61.95 o 6 13 0 694.01 858.39 89.16 o 0 14 0 338.09 468.23 85.10 o 1 14 0 18.10 34.98 43.91 o 2 14 0 121.40 127.34 45.90 o -14 1 1 1607.27 1839.69 144.50 o -13 1 1 102.85 144.51 36.27 o -12 1 1 1853.28 1865.54 67.36 o -11 1 1 2030.06 2044.05 57.97 o -10 1 1 1292.58 1290.30 45.68 o -9 1 1 14667.64 14907.22 229.74 o -8 1 1 1276.59 1246.22 46.98 o -7 1 1 5883.47 5862.39 115.57 o -6 1 1 2977.75 3010.65 67.87 o -5 1 1 12150.44 13042.49 221.19 o -4 1 1 26827.53 28436.92 458.49 o -3 1 1 650.70 712.49 26.50 o -2 1 1 14668.60 16820.14 239.05 o -1 1 1 3625.45 4246.96 69.41 o 0 1 1 68273.32 76440.98 1230.49 o 1 1 1 4265.83 5007.35 74.63 o 2 1 1 1306.10 1389.18 29.01 o 3 1 1 21370.74 22913.77 370.21 o 4 1 1 9956.18 11436.84 193.62 o 5 1 1 14873.75 15683.96 263.11 o 6 1 1 5997.21 6027.54 115.34 o 7 1 1 4366.01 4450.37 94.25 o 8 1 1 6991.14 7307.42 122.45 o 9 1 1 248.28 247.36 25.31 o 10 1 1 3265.98 3270.10 73.14 o 11 1 1 249.41 252.19 32.08 o 12 1 1 1358.70 1350.33 70.69 o 13 1 1 2185.13 2408.48 97.15 o 14 1 1 5.35 47.67 31.88 o 15 1 1 355.48 568.41 53.98 o -15 2 1 375.86 505.77 48.27 o -14 2 1 474.46 617.43 53.60 o -13 2 1 242.33 318.81 45.05 o -12 2 1 181.62 227.16 38.11 o -11 2 1 123.03 67.29 28.01 o -10 2 1 177.96 197.75 42.84 o -9 2 1 304.38 311.78 31.97 o -8 2 1 1046.15 1052.41 45.25 o -7 2 1 258.30 229.90 29.73 o -6 2 1 982.31 1049.97 39.35 o -5 2 1 2381.91 2281.85 45.62 o -4 2 1 1872.98 1874.52 37.79 o -3 2 1 3131.31 3282.53 54.57 o -2 2 1 2903.20 3294.98 53.06 o -1 2 1 497.68 575.98 18.51 o 0 2 1 7379.75 8521.72 124.69 o 1 2 1 5817.48 6407.55 97.10 o 2 2 1 1905.38 1888.70 33.36 o 3 2 1 79.89 50.26 14.82 o 4 2 1 2883.79 3249.09 68.25 o 5 2 1 2451.49 2933.55 66.29 o 6 2 1 9002.76 9316.13 168.50 o 7 2 1 2675.72 2827.89 70.60 o 8 2 1 1352.02 1256.85 73.40 o 9 2 1 1486.38 1283.42 53.48 o 10 2 1 650.72 571.49 39.85 o 11 2 1 1207.03 1258.31 55.63 o 12 2 1 406.99 464.20 48.50 o 13 2 1 778.30 835.96 63.37 o 14 2 1 347.73 410.89 50.29 o 15 2 1 0.61 73.80 34.13 o -15 3 1 11.53 78.79 45.71 o -14 3 1 304.48 435.69 48.74 o -13 3 1 301.32 343.18 44.49 o -12 3 1 36.41 31.32 33.04 o -11 3 1 261.89 319.09 36.12 o -10 3 1 534.14 495.14 38.40 o -9 3 1 333.43 347.45 41.42 o -8 3 1 532.92 550.54 36.67 o -7 3 1 68.53 59.29 21.62 o -6 3 1 24.57 44.24 18.80 o -5 3 1 5900.68 5966.66 95.39 o -4 3 1 8195.04 8814.82 130.09 o -3 3 1 6.73 15.65 14.25 o -2 3 1 134.64 111.42 12.33 o -1 3 1 134.88 137.73 13.83 o 0 3 1 2317.35 2437.95 46.76 o 1 3 1 14583.60 15736.51 228.48 o 2 3 1 51.68 67.76 16.26 o 3 3 1 1703.53 1589.59 36.10 o 4 3 1 13.86 8.89 12.93 o 5 3 1 1496.19 1692.09 49.29 o 6 3 1 569.35 561.66 32.32 o 7 3 1 435.34 476.42 33.06 o 8 3 1 940.95 935.88 48.06 o 9 3 1 1233.82 1141.38 52.35 o 10 3 1 924.77 840.12 47.27 o 11 3 1 443.38 476.67 40.98 o 12 3 1 654.15 711.19 47.13 o 13 3 1 256.07 315.36 45.65 o 14 3 1 46.40 102.34 34.38 o -14 4 1 93.39 183.00 30.15 o -13 4 1 174.77 124.98 29.82 o -12 4 1 1023.12 883.03 43.24 o -11 4 1 73.75 68.32 24.18 o -10 4 1 1112.45 1069.03 43.35 o -9 4 1 215.21 226.57 26.13 o -8 4 1 3882.69 3667.79 75.03 o -7 4 1 70.30 76.02 19.82 o -6 4 1 5063.79 5165.56 89.60 o -5 4 1 40.80 31.95 15.39 o -4 4 1 6.16 32.94 17.21 o -3 4 1 10879.74 11241.11 195.24 o -2 4 1 791.19 742.29 35.56 o -1 4 1 24013.69 26251.58 427.18 o 0 4 1 11218.54 11712.63 199.74 o 1 4 1 7770.86 8017.88 142.82 o 2 4 1 16875.40 17764.60 296.19 o 3 4 1 239.66 305.40 23.92 o 4 4 1 6820.76 6763.68 106.47 o 5 4 1 4680.06 4795.78 83.07 o 6 4 1 1451.72 1393.03 41.56 o 7 4 1 4393.76 3927.38 76.57 o 8 4 1 50.25 45.57 21.24 o 9 4 1 2442.97 2257.19 58.85 o 10 4 1 0.08 0.25 20.80 o 11 4 1 1919.38 1831.78 60.68 o 12 4 1 93.80 67.25 24.26 o 13 4 1 618.13 574.83 43.34 o 14 4 1 437.21 484.36 40.97 o -14 5 1 32.37 113.27 24.41 o -13 5 1 12.61 21.63 35.80 o -12 5 1 141.10 103.47 27.42 o -11 5 1 439.34 400.30 35.55 o -10 5 1 98.24 88.73 24.68 o -9 5 1 32.21 27.40 21.17 o -8 5 1 401.27 334.82 28.81 o -7 5 1 2351.03 2166.15 55.31 o -6 5 1 219.58 255.41 28.16 o -5 5 1 2.45 36.60 21.00 o -4 5 1 174.21 217.83 24.63 o -3 5 1 518.51 503.71 29.87 o -2 5 1 14151.33 14667.26 251.27 o -1 5 1 2993.73 3120.77 71.20 o 0 5 1 1188.40 1189.26 42.05 o 1 5 1 6930.46 7537.81 140.06 o 2 5 1 1126.52 1202.35 44.00 o 3 5 1 2794.47 2645.69 66.44 o 4 5 1 1498.86 1460.23 48.97 o 5 5 1 135.20 162.28 34.14 o 6 5 1 1739.49 1651.02 46.85 o 7 5 1 1664.42 1504.35 47.17 o 8 5 1 2.48 26.20 20.99 o 9 5 1 7.24 13.13 21.66 o 10 5 1 398.61 385.95 32.65 o 11 5 1 189.43 170.49 29.37 o 12 5 1 30.94 34.00 27.95 o 13 5 1 103.62 104.72 27.04 o 14 5 1 44.71 127.00 27.31 o -13 6 1 741.66 852.84 98.38 o -12 6 1 191.06 184.33 30.82 o -11 6 1 1486.68 1434.94 52.86 o -10 6 1 1812.92 1795.25 68.46 o -9 6 1 15.48 37.14 27.52 o -8 6 1 4533.76 4314.34 105.32 o -7 6 1 2575.79 2228.75 70.16 o -6 6 1 2649.71 2476.49 72.19 o -5 6 1 9863.68 9592.80 186.69 o -4 6 1 75.82 80.23 24.99 o -3 6 1 13896.82 13993.00 246.23 o -2 6 1 984.93 988.14 43.45 o -1 6 1 4354.71 4269.85 93.54 o 0 6 1 3867.16 3935.65 106.76 o 1 6 1 620.89 661.86 36.07 o 2 6 1 8022.35 8346.21 157.89 o 3 6 1 100.07 118.71 24.64 o 4 6 1 7784.85 7621.13 149.57 o 5 6 1 839.02 763.89 42.07 o 6 6 1 3884.18 3711.74 171.58 o 7 6 1 3553.29 3341.46 89.11 o 8 6 1 218.67 226.54 33.21 o 9 6 1 2968.47 2807.11 69.71 o 10 6 1 52.33 57.01 25.18 o 11 6 1 897.82 916.85 45.83 o 12 6 1 1096.21 1077.93 50.19 o 13 6 1 8.62 8.61 23.61 o -13 7 1 39.63 71.73 46.39 o -12 7 1 1007.54 1007.32 57.55 o -11 7 1 789.21 752.43 127.73 o -10 7 1 62.09 37.80 30.35 o -9 7 1 1055.88 989.97 66.99 o -8 7 1 346.21 307.64 36.24 o -7 7 1 3894.06 3585.88 94.62 o -6 7 1 13613.84 13388.74 247.10 o -5 7 1 69.43 104.88 28.92 o -4 7 1 7042.26 6905.94 142.13 o -3 7 1 0.14 1.24 23.77 o -2 7 1 11767.47 11720.64 268.58 o -1 7 1 1986.44 1991.78 63.19 o 0 7 1 342.75 422.76 38.25 o 1 7 1 2103.27 2184.85 76.63 o 2 7 1 121.60 172.43 28.67 o 3 7 1 5716.81 5429.71 277.25 o 4 7 1 10.41 9.10 25.76 o 5 7 1 10187.59 10350.33 198.71 o 6 7 1 457.42 494.48 40.28 o 7 7 1 2635.09 2412.15 76.75 o 8 7 1 944.44 904.06 51.04 o 9 7 1 967.67 958.06 53.82 o 10 7 1 1537.16 1547.38 66.74 o 11 7 1 502.64 506.36 103.12 o 12 7 1 104.74 93.67 67.45 o 13 7 1 249.41 319.24 40.08 o -12 8 1 50.49 209.64 44.31 o -11 8 1 82.50 159.53 43.84 o -10 8 1 632.24 680.97 50.76 o -9 8 1 36.10 70.74 31.18 o -8 8 1 637.50 588.44 58.46 o -7 8 1 415.57 339.31 50.87 o -6 8 1 1205.07 1137.47 54.76 o -5 8 1 53.89 70.53 29.15 o -4 8 1 539.10 496.79 40.99 o -3 8 1 850.45 807.47 46.87 o -2 8 1 295.88 312.66 35.31 o -1 8 1 4077.32 3906.34 114.37 o 0 8 1 853.19 852.99 54.97 o 1 8 1 1887.68 1777.85 73.43 o 2 8 1 4346.55 4229.18 104.08 o 3 8 1 100.35 85.29 29.61 o 4 8 1 190.58 244.05 42.63 o 5 8 1 425.15 445.19 40.36 o 6 8 1 253.74 300.19 36.59 o 7 8 1 1165.45 1127.83 55.96 o 8 8 1 157.99 175.59 34.78 o 9 8 1 109.85 124.32 33.28 o 10 8 1 31.80 32.40 32.94 o 11 8 1 70.16 49.65 31.07 o 12 8 1 7.86 59.70 31.49 o -11 9 1 915.86 919.76 57.05 o -10 9 1 89.39 124.02 34.50 o -9 9 1 477.82 540.32 47.38 o -8 9 1 78.71 46.69 29.07 o -7 9 1 1335.55 1241.62 71.11 o -6 9 1 573.93 641.41 47.43 o -5 9 1 437.25 474.28 42.81 o -4 9 1 471.88 425.64 40.66 o -3 9 1 269.30 274.68 36.46 o -2 9 1 5967.55 5929.88 133.97 o -1 9 1 816.81 788.46 55.39 o 0 9 1 3230.87 3119.66 103.98 o 1 9 1 4539.41 4139.13 124.05 o 2 9 1 2713.44 2620.78 94.63 o 3 9 1 4585.54 4425.49 111.99 o 4 9 1 28.54 15.60 33.82 o 5 9 1 1817.39 1636.74 67.46 o 6 9 1 571.71 514.25 44.28 o 7 9 1 396.50 357.68 60.99 o 8 9 1 754.16 736.95 51.40 o 9 9 1 34.71 38.21 31.06 o 10 9 1 1286.64 1247.61 64.87 o 11 9 1 4.56 35.13 34.25 o -10 10 1 169.54 183.54 41.91 o -9 10 1 3.45 -1.60 28.00 o -8 10 1 116.98 107.64 34.77 o -7 10 1 75.64 83.49 33.63 o -6 10 1 295.34 308.53 55.28 o -5 10 1 25.15 -9.05 29.67 o -4 10 1 78.56 82.65 32.63 o -3 10 1 315.05 264.10 38.35 o -2 10 1 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