#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2201709.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201709_Fobs loop_ _publ_author_name 'Gilardi, Richard' 'Flippen-Anderson, Judith L.' 'Evans, Robin' _publ_section_title ; cis-2,4,6,8-Tetranitro-1H,5H-2,4,6,8-tetraazabicyclo[3.3.0]octane, the energetic compound `bicyclo-HMX' ; _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o972 _journal_page_last o974 _journal_volume 58 _journal_year 2002 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 101.783 _cell_angle_gamma 90.000 _cell_length_a 8.5979 _cell_length_b 6.9495 _cell_length_c 8.9726 _exptl_crystal_F_000 300.00 _reflns_d_resolution_high 0.8390 _[local]_cod_data_source_file ya6116IIsup2.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' bchmxm in P2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 73.20 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 6 -6 0 0.80 1.38 0.45 o 1 -5 0 46.64 42.89 3.17 o 2 -5 0 21.00 23.04 1.09 o 6 -5 0 12.06 11.38 1.28 o 7 -5 0 0.44 0.38 0.34 o 0 -4 0 139.48 146.10 5.63 o 1 -4 0 102.97 100.80 4.11 o 2 -4 0 590.27 678.72 17.65 o 3 -4 0 17.01 15.24 0.80 o 4 -4 0 0.06 0.19 0.27 o 7 -4 0 7.73 9.10 1.11 o 8 -4 0 15.48 15.68 1.41 o 1 -3 0 21.05 19.85 1.41 o 2 -3 0 439.79 487.12 17.68 o 3 -3 0 267.23 283.84 11.20 o 4 -3 0 86.83 87.35 4.95 o 5 -3 0 0.21 0.40 0.28 o 7 -3 0 87.28 86.46 5.87 o 8 -3 0 49.32 49.13 3.53 o 9 -3 0 13.74 14.98 1.30 o 2 -2 0 1067.22 1072.48 49.66 o 3 -2 0 939.54 1020.75 25.67 o 4 -2 0 178.71 189.66 5.09 o 5 -2 0 227.30 238.85 6.35 o 6 -2 0 38.22 33.40 1.96 o 7 -2 0 74.95 80.06 5.29 o 8 -2 0 75.25 76.46 4.92 o 9 -2 0 9.63 9.61 1.03 o 1 -1 0 114.53 119.61 4.01 o 2 -1 0 2827.27 2525.69 62.87 o 3 -1 0 171.83 177.31 6.53 o 4 -1 0 34.27 34.41 0.93 o 5 -1 0 3.75 4.06 0.78 o 6 -1 0 72.21 67.36 2.64 o 7 -1 0 108.03 106.51 6.73 o 8 -1 0 152.66 144.96 9.08 o 9 -1 0 29.99 47.04 3.28 o 1 0 0 99.49 90.41 2.82 o 2 0 0 773.83 759.90 15.39 o 3 0 0 28.50 28.59 0.72 o 4 0 0 292.28 312.54 11.27 o 5 0 0 1.26 0.92 0.24 o 6 0 0 42.15 41.39 1.99 o 7 0 0 131.07 134.77 8.47 o 8 0 0 206.04 204.72 12.48 o 1 1 0 111.22 107.87 1.66 o 2 1 0 2834.26 2433.42 70.05 o 3 1 0 173.36 168.67 3.28 o 4 1 0 34.55 35.51 1.21 o 5 1 0 3.72 3.11 0.37 o 6 1 0 71.72 69.47 2.85 o 7 1 0 107.57 100.42 4.67 o 0 2 0 1069.27 1035.60 18.91 o 1 2 0 1946.77 1904.40 37.85 o 2 2 0 1067.48 1058.97 19.44 o 3 2 0 942.33 996.59 20.87 o 4 2 0 179.32 186.71 3.90 o 5 2 0 228.90 230.06 16.50 o 6 2 0 38.39 35.76 1.19 o 7 2 0 74.62 75.52 3.62 o 8 2 0 74.55 67.58 3.33 o 1 3 0 21.21 20.53 0.66 o 2 3 0 439.70 477.48 8.94 o 3 3 0 267.06 301.93 6.63 o 4 3 0 87.39 89.84 2.99 o 5 3 0 0.24 0.60 0.16 o 6 3 0 74.77 75.05 2.38 o 7 3 0 87.00 89.89 4.09 o 8 3 0 49.49 50.50 2.42 o 0 4 0 138.97 146.97 5.82 o 1 4 0 102.82 100.40 3.15 o 2 4 0 592.00 689.03 12.79 o 3 4 0 16.90 17.02 1.20 o 4 4 0 0.06 0.05 0.13 o 5 4 0 64.78 65.79 2.12 o 6 4 0 99.45 96.41 3.00 o 7 4 0 7.72 8.14 0.54 o 8 4 0 15.59 15.07 0.90 o 1 5 0 45.90 40.99 2.05 o 2 5 0 20.71 23.28 1.68 o 3 5 0 56.13 47.42 1.78 o 4 5 0 14.85 13.69 0.63 o 5 5 0 3.66 3.89 0.33 o 6 5 0 12.05 12.48 0.69 o 7 5 0 0.44 0.80 0.27 o 1 6 0 2.53 2.27 0.39 o 2 6 0 47.67 54.69 2.08 o 3 6 0 22.74 20.84 0.98 o 4 6 0 3.92 4.40 0.41 o 5 6 0 27.86 26.39 0.99 o 6 6 0 0.81 1.25 0.22 o 2 7 0 70.14 72.43 3.35 o 3 7 0 8.31 8.56 0.53 o 4 7 0 6.89 7.83 0.67 o 5 7 0 0.81 0.54 0.16 o -6 -6 1 25.44 25.60 2.04 o -8 -5 1 18.28 15.71 1.37 o -7 -5 1 7.13 7.44 0.93 o -2 -5 1 54.87 48.60 1.95 o -1 -5 1 129.64 132.97 5.39 o 0 -5 1 58.57 60.61 2.84 o 1 -5 1 67.75 71.62 3.26 o 2 -5 1 101.58 90.89 3.96 o 5 -5 1 25.54 24.77 2.08 o 6 -5 1 23.86 22.61 1.95 o 7 -5 1 5.52 4.77 0.69 o -8 -4 1 3.57 2.94 0.60 o -7 -4 1 10.83 9.37 1.14 o -4 -4 1 23.84 21.62 1.43 o -3 -4 1 97.95 99.40 4.54 o -1 -4 1 52.52 53.34 1.62 o 0 -4 1 189.60 191.12 7.07 o 1 -4 1 313.65 300.30 7.82 o 2 -4 1 331.61 337.27 8.92 o 3 -4 1 164.96 159.60 5.13 o 4 -4 1 154.08 153.21 5.57 o 6 -4 1 17.42 18.12 1.74 o 7 -4 1 27.33 25.62 2.12 o 8 -4 1 8.49 9.41 0.98 o -9 -3 1 4.22 3.08 0.56 o -8 -3 1 4.60 4.21 0.75 o -7 -3 1 22.29 23.76 2.05 o -5 -3 1 121.21 115.33 5.04 o -4 -3 1 1.06 0.73 0.33 o -3 -3 1 81.41 92.28 2.85 o -2 -3 1 732.91 796.44 28.92 o 0 -3 1 597.62 627.17 22.33 o 1 -3 1 202.08 190.91 5.25 o 2 -3 1 236.37 231.57 6.22 o 3 -3 1 112.25 119.82 3.42 o 4 -3 1 0.92 1.19 0.28 o 5 -3 1 3.81 4.40 0.51 o 6 -3 1 10.64 10.09 1.24 o 7 -3 1 20.44 18.45 1.76 o 8 -3 1 0.00 0.06 0.31 o 9 -3 1 2.89 4.51 0.62 o -9 -2 1 4.02 3.38 0.63 o -8 -2 1 131.69 132.72 8.41 o -7 -2 1 81.28 80.70 5.38 o -6 -2 1 230.92 245.07 9.53 o -5 -2 1 26.44 28.42 1.61 o -4 -2 1 10.50 9.60 0.50 o -3 -2 1 273.45 265.02 8.97 o -2 -2 1 117.60 136.40 3.52 o -1 -2 1 681.77 693.50 17.49 o 1 -2 1 1286.00 1404.79 35.88 o 2 -2 1 1560.90 1755.15 42.37 o 3 -2 1 707.70 749.56 19.44 o 4 -2 1 49.30 48.63 1.64 o 5 -2 1 90.73 96.50 3.46 o 6 -2 1 37.40 33.04 2.64 o 7 -2 1 81.96 77.09 5.24 o 8 -2 1 14.86 12.34 1.32 o 9 -2 1 5.03 4.98 0.72 o -8 -1 1 108.22 107.16 6.85 o -7 -1 1 9.31 10.67 1.23 o -6 -1 1 38.22 36.36 1.37 o -5 -1 1 378.56 416.32 10.90 o -4 -1 1 353.43 396.24 10.22 o -3 -1 1 102.00 92.38 2.57 o -2 -1 1 607.03 581.96 12.18 o -1 -1 1 634.19 572.86 24.65 o 0 -1 1 1782.94 1564.02 53.42 o 1 -1 1 373.08 366.59 9.31 o 2 -1 1 296.27 287.03 7.20 o 3 -1 1 260.25 274.86 5.84 o 4 -1 1 26.19 30.50 1.57 o 5 -1 1 217.47 218.09 8.80 o 6 -1 1 49.02 50.95 2.72 o 7 -1 1 24.27 34.71 2.51 o 8 -1 1 98.18 101.78 6.61 o 9 -1 1 5.47 5.16 0.76 o -7 0 1 4.29 3.58 0.43 o -6 0 1 341.20 370.89 14.07 o -5 0 1 27.52 29.68 1.46 o -4 0 1 0.06 0.22 0.14 o -3 0 1 146.35 126.37 2.74 o -2 0 1 1498.15 1393.80 41.34 o -1 0 1 2573.64 2202.79 55.28 o 0 0 1 586.08 505.96 14.53 o 1 0 1 1398.66 1230.20 25.27 o 2 0 1 278.96 257.51 6.55 o 3 0 1 722.84 729.83 15.12 o 4 0 1 25.78 24.75 0.93 o 5 0 1 137.11 135.48 3.88 o 6 0 1 0.15 0.53 0.35 o 7 0 1 0.03 0.12 0.40 o 8 0 1 139.37 140.14 8.81 o 9 0 1 2.09 1.89 0.55 o -8 1 1 107.85 106.75 4.84 o -7 1 1 9.43 9.92 0.74 o -6 1 1 38.12 34.41 1.16 o -5 1 1 378.73 411.22 15.47 o -4 1 1 353.11 388.44 8.27 o -3 1 1 101.59 93.48 2.09 o -2 1 1 605.45 596.50 14.32 o -1 1 1 636.79 556.12 20.37 o 0 1 1 1790.75 1503.69 38.20 o 2 1 1 295.55 294.42 7.15 o 3 1 1 258.75 277.96 8.20 o 5 1 1 216.90 230.06 7.22 o 6 1 1 48.73 49.86 1.87 o 7 1 1 24.09 22.91 2.28 o -9 2 1 4.05 3.67 0.39 o -8 2 1 131.26 134.14 5.98 o -7 2 1 81.95 79.27 3.73 o -6 2 1 230.86 240.96 6.34 o -5 2 1 26.51 28.18 0.95 o -4 2 1 10.33 9.56 0.52 o -3 2 1 272.41 264.63 8.00 o -2 2 1 118.06 134.94 2.57 o -1 2 1 680.97 695.77 17.69 o 0 2 1 984.59 994.37 19.91 o 1 2 1 1285.53 1442.07 39.33 o 2 2 1 1558.11 1608.01 42.76 o 3 2 1 708.62 776.84 19.68 o 4 2 1 50.25 53.29 1.81 o 5 2 1 90.58 94.67 2.98 o 6 2 1 37.58 33.38 1.34 o -9 3 1 4.22 3.64 0.37 o -8 3 1 4.43 4.18 0.47 o -7 3 1 22.39 22.25 1.06 o -6 3 1 58.63 53.22 1.82 o -5 3 1 121.34 120.45 2.31 o -4 3 1 1.04 0.99 0.20 o -3 3 1 81.37 97.91 4.26 o -2 3 1 730.37 803.77 21.89 o -1 3 1 11.72 13.02 0.54 o 0 3 1 596.22 628.94 14.64 o 1 3 1 204.24 202.84 7.00 o 2 3 1 236.64 237.07 8.31 o 3 3 1 113.18 120.19 3.49 o 4 3 1 0.88 0.87 0.30 o 5 3 1 3.86 3.59 0.26 o 6 3 1 10.59 9.71 0.60 o 7 3 1 20.44 18.74 0.89 o -8 4 1 3.52 3.74 0.41 o -7 4 1 10.82 9.51 0.59 o -6 4 1 12.24 13.04 0.62 o -5 4 1 227.71 231.56 6.74 o -4 4 1 23.69 21.23 0.65 o -3 4 1 96.97 109.53 2.72 o -2 4 1 97.25 104.77 2.44 o -1 4 1 52.88 51.76 1.79 o 0 4 1 189.84 185.54 3.26 o 1 4 1 313.08 289.79 8.88 o 2 4 1 330.68 336.69 9.02 o 3 4 1 165.94 158.92 3.50 o 4 4 1 153.88 153.49 4.71 o 5 4 1 60.33 56.57 2.72 o 6 4 1 17.37 18.14 1.02 o 7 4 1 27.30 25.76 1.10 o 8 4 1 8.60 9.07 0.60 o -8 5 1 18.11 19.00 0.97 o -7 5 1 7.28 8.23 0.51 o -6 5 1 1.51 1.86 0.24 o -5 5 1 32.98 31.39 1.16 o -4 5 1 3.77 3.62 0.32 o -3 5 1 31.00 29.42 1.07 o -2 5 1 53.72 51.24 1.38 o -1 5 1 129.74 130.35 4.30 o 0 5 1 58.62 64.09 2.13 o 1 5 1 67.19 71.35 3.62 o 2 5 1 100.53 87.75 2.43 o 3 5 1 24.98 23.26 1.06 o 4 5 1 17.77 18.52 0.78 o 5 5 1 25.09 23.62 1.11 o 6 5 1 23.64 23.69 1.07 o 7 5 1 5.53 4.44 0.34 o -7 6 1 1.80 2.32 0.23 o -6 6 1 25.28 26.72 1.12 o -5 6 1 0.81 0.76 0.18 o -4 6 1 33.06 29.12 1.08 o -3 6 1 60.58 63.49 2.04 o -2 6 1 17.20 17.58 2.57 o -1 6 1 37.48 31.09 1.59 o 0 6 1 60.38 58.98 2.80 o 1 6 1 23.20 23.74 1.33 o 2 6 1 115.63 126.51 4.38 o 3 6 1 54.85 54.18 2.07 o 4 6 1 7.46 8.72 0.57 o 5 6 1 2.62 3.01 0.32 o 6 6 1 3.82 3.74 0.31 o -5 7 1 2.67 2.74 0.38 o -4 7 1 0.82 1.28 0.23 o -3 7 1 76.07 77.24 4.85 o 0 7 1 20.82 23.01 1.23 o 1 7 1 12.48 13.88 0.86 o 2 7 1 1.20 1.32 0.28 o 3 7 1 34.32 35.64 1.41 o 4 7 1 0.21 0.03 0.14 o 5 7 1 4.15 5.58 0.35 o -7 -6 2 5.73 5.59 0.67 o 0 -5 2 55.92 52.26 1.81 o 1 -5 2 10.26 10.46 0.98 o 5 -5 2 16.94 14.93 1.49 o 6 -5 2 1.29 1.09 0.45 o 7 -5 2 6.60 7.01 0.81 o -8 -4 2 17.61 18.56 1.62 o -4 -4 2 84.59 72.54 3.48 o -3 -4 2 82.13 81.33 3.80 o -2 -4 2 271.55 303.15 11.21 o -1 -4 2 57.88 58.43 1.81 o 0 -4 2 90.69 94.65 2.77 o 1 -4 2 109.60 105.35 4.25 o 2 -4 2 10.38 9.47 0.59 o 3 -4 2 108.55 101.65 4.81 o 4 -4 2 7.12 8.09 1.05 o 5 -4 2 3.61 3.08 0.74 o 6 -4 2 23.02 17.33 1.71 o 7 -4 2 5.79 5.74 0.82 o 8 -4 2 0.84 1.04 0.37 o -9 -3 2 4.06 4.67 0.65 o -8 -3 2 24.34 22.08 1.96 o -6 -3 2 380.27 372.94 16.07 o -5 -3 2 139.55 132.79 4.10 o -4 -3 2 139.02 138.20 5.11 o -3 -3 2 64.32 65.48 3.54 o -2 -3 2 68.10 76.69 3.26 o -1 -3 2 694.56 750.29 19.18 o 0 -3 2 988.58 1123.78 27.86 o 1 -3 2 5.34 7.04 0.40 o 2 -3 2 515.80 575.64 14.94 o 3 -3 2 260.72 300.92 7.96 o 4 -3 2 156.01 147.09 3.87 o 5 -3 2 36.86 31.30 2.40 o 6 -3 2 0.11 -0.24 0.34 o 7 -3 2 66.06 64.28 4.36 o 8 -3 2 3.99 3.07 0.60 o -9 -2 2 14.88 17.09 1.39 o -8 -2 2 304.53 313.99 18.82 o -7 -2 2 28.19 26.98 1.52 o -6 -2 2 22.46 20.08 0.88 o -5 -2 2 184.24 175.51 4.83 o -4 -2 2 77.20 74.01 3.38 o -3 -2 2 1130.76 1311.36 32.85 o -2 -2 2 426.16 459.49 11.94 o -1 -2 2 54.82 57.24 1.29 o 0 -2 2 1841.20 1890.32 47.95 o 1 -2 2 178.36 191.91 4.95 o 2 -2 2 439.70 476.22 19.33 o 3 -2 2 369.56 429.15 11.19 o 4 -2 2 332.48 349.79 9.30 o 5 -2 2 65.84 65.58 3.66 o 6 -2 2 3.11 2.42 0.70 o 7 -2 2 14.72 15.15 1.57 o 8 -2 2 4.69 4.11 0.74 o 9 -2 2 4.72 4.72 0.65 o -8 -1 2 59.29 53.53 2.63 o -7 -1 2 36.35 33.41 1.44 o -6 -1 2 17.27 19.42 0.70 o -5 -1 2 367.58 399.75 10.50 o -4 -1 2 132.74 129.12 3.59 o -3 -1 2 391.67 424.41 8.71 o -2 -1 2 1059.63 1095.63 31.98 o -1 -1 2 1576.68 1654.15 40.55 o 0 -1 2 5356.27 3957.29 269.40 o 1 -1 2 1241.32 1346.59 33.57 o 2 -1 2 387.62 379.15 7.95 o 3 -1 2 72.51 72.72 2.11 o 4 -1 2 146.77 151.73 4.19 o 5 -1 2 157.75 168.00 9.99 o 6 -1 2 72.42 74.50 5.05 o 7 -1 2 40.45 42.11 3.26 o 8 -1 2 36.86 39.35 2.93 o 9 -1 2 6.08 5.70 0.75 o -8 0 2 0.02 0.19 0.21 o -7 0 2 29.09 30.67 1.61 o -6 0 2 0.01 -0.11 0.17 o -5 0 2 145.65 139.53 3.92 o -4 0 2 69.44 89.07 2.68 o -3 0 2 1323.76 1289.01 46.35 o -2 0 2 1418.13 1215.54 30.55 o -1 0 2 71.40 72.76 1.58 o 0 0 2 1335.19 1335.84 33.47 o 1 0 2 334.44 342.26 7.13 o 2 0 2 2769.60 2959.88 60.77 o 3 0 2 681.92 773.05 19.60 o 4 0 2 405.16 406.82 10.69 o 5 0 2 31.54 32.44 1.88 o 6 0 2 27.30 28.77 1.48 o 7 0 2 175.63 172.17 10.74 o 8 0 2 28.14 27.01 2.26 o 9 0 2 2.17 1.32 0.45 o -9 1 2 12.79 12.24 0.79 o -8 1 2 59.65 57.10 2.70 o -7 1 2 36.37 34.01 1.76 o -6 1 2 17.50 18.40 0.73 o -5 1 2 368.40 397.43 14.92 o -4 1 2 133.02 130.20 3.58 o -3 1 2 392.33 409.55 8.72 o -2 1 2 1063.42 1114.37 22.85 o -1 1 2 1576.88 1595.94 33.28 o 0 1 2 5358.93 3735.72 95.94 o 1 1 2 1245.60 1328.19 27.52 o 2 1 2 388.77 382.36 7.99 o 3 1 2 73.14 73.23 2.17 o 4 1 2 147.33 152.89 4.29 o 5 1 2 157.88 159.05 8.79 o 6 1 2 72.15 74.84 5.08 o 7 1 2 40.67 44.24 3.30 o 8 1 2 36.47 37.04 2.87 o -9 2 2 14.82 12.42 0.87 o -8 2 2 304.10 316.50 13.62 o -7 2 2 28.22 31.60 3.06 o -6 2 2 22.77 20.68 0.81 o -5 2 2 182.38 170.29 4.81 o -4 2 2 77.75 75.92 4.03 o -3 2 2 1131.47 1262.44 32.48 o -2 2 2 425.42 444.61 9.44 o -1 2 2 55.33 57.30 1.61 o 0 2 2 1842.30 1926.05 67.27 o 1 2 2 178.68 187.11 4.07 o 2 2 2 442.49 476.56 12.40 o 3 2 2 370.26 435.66 11.38 o 4 2 2 331.47 356.36 9.48 o 5 2 2 66.26 61.83 1.73 o 6 2 2 3.13 1.46 0.65 o -9 3 2 4.10 4.24 0.41 o -8 3 2 23.92 25.07 1.37 o -7 3 2 54.40 58.25 2.28 o -6 3 2 380.14 379.43 10.81 o -5 3 2 140.56 137.52 2.77 o -4 3 2 138.24 136.01 3.92 o -3 3 2 63.93 62.67 1.99 o -2 3 2 68.05 81.29 3.49 o -1 3 2 694.18 763.35 19.34 o 0 3 2 988.02 1088.94 28.40 o 1 3 2 5.42 7.09 0.75 o 2 3 2 516.46 592.67 21.36 o 3 3 2 260.82 297.56 8.10 o 4 3 2 154.89 150.85 3.85 o 5 3 2 36.82 32.22 1.34 o 6 3 2 0.10 0.24 0.20 o 7 3 2 65.86 60.52 3.62 o -8 4 2 17.74 18.97 1.09 o -7 4 2 34.04 35.66 1.26 o -6 4 2 149.56 151.02 4.53 o -5 4 2 8.97 8.84 0.48 o -4 4 2 84.24 76.05 1.68 o -3 4 2 82.94 85.47 2.67 o -2 4 2 272.98 296.55 8.31 o -1 4 2 57.46 56.85 1.98 o 0 4 2 90.55 94.81 2.29 o 1 4 2 108.11 100.35 3.05 o 2 4 2 10.57 8.75 0.63 o 3 4 2 108.35 99.52 2.35 o 4 4 2 7.15 7.30 0.51 o 5 4 2 3.43 3.07 0.36 o 6 4 2 22.85 19.62 0.91 o 7 4 2 5.85 5.68 0.40 o -8 5 2 10.60 11.63 0.71 o -7 5 2 6.53 7.06 0.46 o -6 5 2 35.98 35.65 1.48 o -5 5 2 92.23 89.68 2.81 o -4 5 2 27.39 26.80 0.91 o -3 5 2 66.56 62.60 2.52 o -2 5 2 42.54 40.42 0.97 o -1 5 2 53.68 48.74 1.28 o 0 5 2 55.60 53.19 2.61 o 1 5 2 10.39 10.00 0.56 o 2 5 2 44.60 42.57 1.38 o 3 5 2 3.19 2.83 0.34 o 4 5 2 9.40 9.84 0.61 o 5 5 2 17.17 16.73 0.94 o 6 5 2 1.31 1.04 0.21 o 7 5 2 6.64 7.46 0.41 o -7 6 2 5.62 5.84 0.36 o -6 6 2 8.40 9.76 0.66 o -5 6 2 4.76 4.47 0.33 o -4 6 2 45.39 50.63 1.94 o -3 6 2 109.45 103.07 3.13 o -2 6 2 74.32 74.97 2.35 o -1 6 2 47.52 43.58 2.13 o 0 6 2 38.53 37.96 1.92 o 1 6 2 31.04 32.64 1.71 o 2 6 2 104.18 105.09 5.44 o 3 6 2 11.33 13.08 0.71 o 4 6 2 4.15 4.45 0.39 o 5 6 2 12.50 14.74 0.72 o 6 6 2 9.03 8.37 0.45 o -5 7 2 5.00 5.83 0.66 o -4 7 2 30.36 32.03 2.08 o -3 7 2 3.79 4.76 0.74 o -1 7 2 33.15 31.82 1.59 o 0 7 2 47.17 41.47 2.01 o 1 7 2 2.20 2.18 0.32 o 2 7 2 8.43 9.95 0.69 o 3 7 2 1.65 1.52 0.23 o 4 7 2 5.17 6.37 0.39 o -8 -5 3 6.14 6.05 0.71 o -1 -5 3 25.11 25.26 1.64 o 0 -5 3 109.13 101.30 3.08 o -8 -4 3 2.52 2.24 0.53 o -6 -4 3 52.27 46.07 2.25 o -4 -4 3 66.05 57.14 2.95 o -3 -4 3 181.43 171.01 6.80 o -2 -4 3 30.28 33.44 1.72 o -1 -4 3 69.96 71.96 2.21 o 0 -4 3 46.39 41.67 1.46 o 1 -4 3 7.30 7.67 0.76 o 2 -4 3 5.41 5.36 0.72 o 3 -4 3 40.53 40.90 2.21 o 5 -4 3 12.84 12.58 1.32 o 6 -4 3 15.16 15.22 1.47 o 7 -4 3 4.63 6.78 0.81 o -9 -3 3 23.79 24.71 1.83 o -8 -3 3 11.71 11.55 1.26 o -7 -3 3 23.48 23.53 1.25 o -6 -3 3 5.74 5.53 0.50 o -5 -3 3 52.91 48.32 1.72 o -4 -3 3 3.44 3.42 0.55 o -3 -3 3 707.01 794.29 29.41 o -2 -3 3 81.74 84.15 2.42 o -1 -3 3 136.23 122.86 3.41 o 0 -3 3 181.90 191.75 7.26 o 1 -3 3 173.75 197.65 7.12 o 2 -3 3 119.78 121.88 4.87 o 3 -3 3 99.62 101.80 3.45 o 4 -3 3 24.75 23.17 0.96 o 5 -3 3 46.61 45.07 3.34 o 6 -3 3 28.18 25.80 2.19 o 7 -3 3 9.32 9.29 1.10 o 8 -3 3 4.32 5.02 0.70 o -8 -2 3 66.41 68.35 2.63 o -7 -2 3 52.61 50.77 2.47 o -6 -2 3 8.64 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