#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/17/2201724.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201724_Fobs loop_ _publ_author_name 'Ravikumar, B.' 'Sridhar, B.' 'Rajaram, R. K.' _publ_section_title ; DL-Threoninium dihydrogen phosphate ; _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1185 _journal_page_last o1187 _journal_volume 58 _journal_year 2002 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.0590 _cell_length_b 19.5070 _cell_length_c 10.1015 _exptl_crystal_F_000 912.00 _reflns_d_resolution_high 0.8415 _[local]_cod_data_source_file ya6135Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' DL-THREONINE PHOSPHATE' _shelx_refln_list_code 4 _shelx_f_calc_maximum 258.23 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 66685.18 74442.25 689.96 o 4 0 0 8912.93 9708.45 67.66 o 6 0 0 1659.66 1613.42 21.50 o 8 0 0 197.47 195.16 11.61 o 10 0 0 574.91 566.10 20.56 o 2 1 0 9033.99 9946.23 98.65 o 4 1 0 3812.94 4315.51 30.69 o 6 1 0 1571.32 1604.81 15.10 o 8 1 0 624.59 552.24 11.48 o 10 1 0 75.49 70.26 7.79 o 0 2 0 11749.64 7416.30 75.43 o 2 2 0 571.59 570.38 8.05 o 4 2 0 1867.31 1775.86 17.88 o 6 2 0 478.14 435.30 12.53 o 8 2 0 200.00 184.50 10.95 o 10 2 0 2.16 -17.27 17.27 o 2 3 0 28080.42 35124.43 114.04 o 4 3 0 1510.56 1215.45 15.14 o 6 3 0 2.64 -0.66 10.79 o 8 3 0 732.62 701.08 18.09 o 10 3 0 424.59 412.15 18.45 o 0 4 0 45261.93 27880.71 280.12 o 2 4 0 9451.90 10196.22 58.24 o 4 4 0 989.95 1044.46 14.59 o 6 4 0 1305.36 1131.61 18.83 o 8 4 0 380.10 364.72 14.09 o 10 4 0 631.12 629.05 21.48 o 2 5 0 38126.55 46949.20 150.53 o 4 5 0 11868.32 13451.64 86.80 o 6 5 0 330.23 301.55 11.01 o 8 5 0 2.51 -10.57 11.56 o 10 5 0 1.18 -16.43 16.43 o 0 6 0 35742.39 36614.39 129.85 o 2 6 0 13569.52 14865.01 80.06 o 4 6 0 4591.87 4616.16 44.26 o 6 6 0 4757.48 4696.28 48.05 o 8 6 0 28.59 0.99 14.09 o 10 6 0 237.76 248.64 15.90 o 2 7 0 3253.93 3753.31 35.14 o 4 7 0 24.05 19.40 5.31 o 6 7 0 285.66 260.80 11.33 o 8 7 0 720.34 698.01 18.60 o 10 7 0 17.42 11.93 14.71 o 0 8 0 4020.19 4148.88 37.12 o 2 8 0 324.88 356.17 9.18 o 4 8 0 2564.22 2636.03 26.86 o 6 8 0 201.97 263.36 10.96 o 8 8 0 137.20 131.20 12.30 o 10 8 0 0.00 20.89 9.00 o 2 9 0 5656.96 5521.58 48.09 o 4 9 0 9119.39 9197.69 80.79 o 6 9 0 1290.54 1228.76 21.61 o 8 9 0 1765.33 1679.78 30.56 o 0 10 0 5040.60 4789.35 44.83 o 2 10 0 8479.97 9048.14 75.16 o 4 10 0 20.07 13.76 10.17 o 6 10 0 543.20 537.72 15.46 o 8 10 0 453.48 421.29 17.72 o 2 11 0 6152.61 6168.30 56.25 o 4 11 0 4521.71 4529.45 46.55 o 6 11 0 742.37 717.66 17.54 o 8 11 0 293.56 345.03 16.09 o 0 12 0 1366.36 1479.12 19.91 o 2 12 0 163.62 153.75 8.35 o 4 12 0 463.08 451.24 13.11 o 6 12 0 1268.37 1218.60 22.66 o 8 12 0 2.56 3.59 13.90 o 2 13 0 80.87 48.11 7.51 o 4 13 0 1173.19 1057.63 20.04 o 6 13 0 33.47 11.05 13.65 o 8 13 0 198.43 167.39 13.92 o 0 14 0 417.50 360.21 12.08 o 2 14 0 923.81 892.12 18.25 o 4 14 0 2493.18 2404.93 30.13 o 6 14 0 1004.51 1045.10 24.15 o 8 14 0 1.32 -2.63 14.45 o 2 15 0 8269.92 8070.26 76.44 o 4 15 0 1505.31 1488.99 24.99 o 6 15 0 3.37 -3.40 13.65 o 8 15 0 532.67 577.41 21.76 o 0 16 0 753.18 689.30 16.67 o 2 16 0 302.57 291.86 12.43 o 4 16 0 470.99 438.25 15.05 o 6 16 0 7.72 2.38 15.26 o 2 17 0 4.40 15.26 10.61 o 4 17 0 0.21 0.00 14.20 o 6 17 0 289.22 286.73 15.90 o 0 18 0 1541.73 1542.52 26.13 o 2 18 0 50.18 27.56 13.80 o 4 18 0 885.76 790.89 22.51 o 6 18 0 367.34 377.32 18.59 o 2 19 0 1499.09 1487.23 29.03 o 4 19 0 256.58 249.46 14.66 o 6 19 0 395.73 423.04 19.25 o 0 20 0 0.70 -1.13 10.50 o 2 20 0 0.03 6.99 12.40 o 4 20 0 681.93 711.51 22.51 o 2 21 0 756.67 745.74 22.49 o 4 21 0 479.61 527.43 20.43 o 0 22 0 12.49 21.48 11.89 o 2 22 0 26.88 27.63 14.23 o 1 1 1 954.08 1000.13 3.49 o 2 1 1 6758.28 7220.40 22.03 o 3 1 1 2593.89 2822.54 20.43 o 4 1 1 548.60 510.23 5.13 o 5 1 1 75.61 82.73 3.18 o 6 1 1 1023.87 1009.65 8.72 o 7 1 1 81.71 75.62 4.33 o 8 1 1 541.75 550.58 8.13 o 9 1 1 8.60 12.95 6.84 o 10 1 1 982.71 932.33 12.54 o 0 2 1 411.53 495.97 8.02 o 1 2 1 72.85 64.31 2.26 o 2 2 1 2918.61 2797.01 18.38 o 3 2 1 2492.32 2643.97 19.25 o 4 2 1 8.51 14.19 4.59 o 5 2 1 1317.78 1286.64 12.25 o 6 2 1 1940.86 1945.47 17.72 o 7 2 1 100.86 84.05 6.36 o 8 2 1 4572.40 4541.10 32.37 o 9 2 1 244.40 214.78 10.94 o 10 2 1 21.75 26.16 10.69 o 1 3 1 200.64 157.83 2.71 o 2 3 1 73.48 97.22 3.90 o 3 3 1 1015.30 1056.42 9.08 o 4 3 1 324.33 350.35 7.07 o 5 3 1 399.00 344.13 7.23 o 6 3 1 204.53 218.43 7.00 o 7 3 1 715.24 694.74 11.73 o 8 3 1 376.61 368.69 16.07 o 9 3 1 3.55 3.53 12.59 o 10 3 1 3.07 -2.13 10.58 o 0 4 1 11039.19 11645.73 131.82 o 1 4 1 226.31 280.83 6.86 o 2 4 1 5466.42 5762.45 31.21 o 3 4 1 916.69 952.75 8.99 o 4 4 1 481.44 428.78 14.48 o 5 4 1 2974.32 3166.79 30.89 o 6 4 1 1409.23 1372.35 18.03 o 7 4 1 48.59 45.20 18.04 o 8 4 1 507.86 503.17 11.30 o 9 4 1 65.62 75.28 7.45 o 10 4 1 26.57 26.56 6.84 o 1 5 1 12682.71 13554.44 215.84 o 2 5 1 2076.58 1808.01 12.62 o 3 5 1 917.68 907.16 15.63 o 4 5 1 1010.99 892.56 21.54 o 5 5 1 321.92 338.15 13.30 o 6 5 1 571.77 582.98 10.21 o 7 5 1 43.59 67.39 9.95 o 8 5 1 2029.52 2020.62 20.73 o 9 5 1 6.34 -1.05 9.58 o 10 5 1 481.71 467.77 13.77 o 0 6 1 1709.09 1678.52 12.19 o 1 6 1 2996.88 2888.68 24.39 o 2 6 1 700.13 747.49 19.28 o 3 6 1 1603.17 1558.85 18.71 o 4 6 1 709.33 760.64 12.24 o 5 6 1 4.54 10.49 6.38 o 6 6 1 163.78 168.08 7.03 o 7 6 1 4.41 3.24 9.37 o 8 6 1 0.22 -8.46 9.05 o 9 6 1 19.10 29.81 18.39 o 10 6 1 3.40 20.37 9.64 o 1 7 1 5442.44 5769.38 24.48 o 2 7 1 1745.85 1847.20 21.31 o 3 7 1 333.30 388.43 6.83 o 4 7 1 6010.83 6034.03 94.84 o 5 7 1 212.06 231.47 22.82 o 6 7 1 915.49 892.53 12.53 o 7 7 1 277.06 288.65 12.04 o 8 7 1 87.83 98.48 6.96 o 9 7 1 8.79 0.47 10.71 o 10 7 1 483.25 495.15 14.36 o 0 8 1 12440.82 13394.67 62.28 o 1 8 1 512.45 520.15 5.17 o 2 8 1 646.03 575.10 7.94 o 3 8 1 81.39 62.87 4.29 o 4 8 1 28.10 20.06 4.66 o 5 8 1 756.52 717.69 10.60 o 6 8 1 4635.66 4519.30 32.19 o 7 8 1 16.83 13.99 6.06 o 8 8 1 543.93 516.52 12.86 o 9 8 1 8.22 22.73 9.42 o 10 8 1 1.59 14.28 10.62 o 1 9 1 1410.99 1517.68 8.68 o 2 9 1 565.26 568.48 8.23 o 3 9 1 1257.85 1270.93 24.74 o 4 9 1 5.85 -3.84 8.73 o 5 9 1 67.07 88.41 7.10 o 6 9 1 828.22 800.59 12.73 o 7 9 1 384.21 401.79 20.49 o 8 9 1 376.13 356.74 11.31 o 9 9 1 24.05 26.15 7.13 o 0 10 1 0.32 1.25 5.42 o 1 10 1 183.32 190.80 4.24 o 2 10 1 610.65 616.00 19.22 o 3 10 1 1130.85 1099.86 19.62 o 4 10 1 229.08 205.84 6.69 o 5 10 1 172.09 169.81 6.94 o 6 10 1 1709.33 1622.49 17.82 o 7 10 1 65.26 53.87 6.34 o 8 10 1 37.07 41.70 16.21 o 9 10 1 0.04 -1.79 22.10 o 1 11 1 70.29 68.95 3.18 o 2 11 1 102.70 103.58 5.10 o 3 11 1 242.90 221.72 6.90 o 4 11 1 2425.99 2372.10 19.22 o 5 11 1 1.01 5.57 10.39 o 6 11 1 239.71 227.79 8.19 o 7 11 1 1.15 0.79 17.95 o 8 11 1 573.06 559.16 13.99 o 9 11 1 0.05 -9.54 9.54 o 0 12 1 821.28 846.65 11.04 o 1 12 1 43.08 43.11 3.13 o 2 12 1 181.29 182.58 6.50 o 3 12 1 95.46 113.66 5.82 o 4 12 1 2832.66 2849.49 21.83 o 5 12 1 74.94 80.86 6.17 o 6 12 1 937.24 916.87 14.49 o 7 12 1 97.48 84.82 7.65 o 8 12 1 0.00 11.22 9.44 o 9 12 1 14.40 14.41 11.73 o 1 13 1 28.67 33.90 3.18 o 2 13 1 7.26 7.70 8.78 o 3 13 1 213.55 218.91 7.57 o 4 13 1 76.98 75.29 8.04 o 5 13 1 87.91 88.30 6.26 o 6 13 1 231.67 244.39 10.09 o 7 13 1 57.70 55.70 7.11 o 8 13 1 468.13 517.93 13.64 o 0 14 1 1938.45 1895.11 30.95 o 1 14 1 134.66 140.35 6.97 o 2 14 1 27.25 36.94 8.49 o 3 14 1 475.25 488.67 30.70 o 4 14 1 936.84 919.49 15.60 o 5 14 1 126.38 130.33 8.82 o 6 14 1 714.26 715.94 14.76 o 7 14 1 2.49 8.43 9.17 o 8 14 1 18.70 35.79 8.58 o 1 15 1 270.03 305.76 6.07 o 2 15 1 1101.85 1067.09 14.44 o 3 15 1 0.61 -5.71 8.44 o 4 15 1 2.81 -0.33 14.58 o 5 15 1 37.05 40.04 13.12 o 6 15 1 326.92 301.08 10.34 o 7 15 1 12.36 8.73 9.16 o 8 15 1 4.81 0.64 9.62 o 0 16 1 89.26 100.55 11.92 o 1 16 1 27.62 23.13 4.46 o 2 16 1 11.86 -2.11 13.01 o 3 16 1 203.11 199.12 7.90 o 4 16 1 178.49 191.94 7.94 o 5 16 1 115.43 96.87 7.71 o 6 16 1 31.79 36.92 8.49 o 7 16 1 3.77 4.59 9.62 o 1 17 1 57.82 66.78 4.38 o 2 17 1 966.50 1009.85 15.10 o 3 17 1 0.02 -8.45 8.45 o 4 17 1 56.04 68.40 6.78 o 5 17 1 188.19 181.39 9.09 o 6 17 1 71.07 100.74 7.99 o 7 17 1 38.64 42.20 9.01 o 0 18 1 606.68 580.05 13.50 o 1 18 1 57.74 52.15 4.29 o 2 18 1 22.70 23.21 8.20 o 3 18 1 136.67 156.64 8.50 o 4 18 1 99.32 103.12 7.75 o 5 18 1 87.15 96.63 8.62 o 6 18 1 103.16 94.07 11.86 o 1 19 1 151.19 154.48 5.91 o 2 19 1 441.67 444.16 30.41 o 3 19 1 30.14 31.70 8.87 o 4 19 1 130.00 138.92 8.97 o 5 19 1 21.03 22.94 10.04 o 6 19 1 65.59 65.47 8.30 o 0 20 1 2362.59 2442.55 26.39 o 1 20 1 90.79 86.25 5.25 o 2 20 1 42.94 39.60 6.99 o 3 20 1 54.97 59.39 20.53 o 4 20 1 671.38 677.14 19.01 o 5 20 1 0.55 -11.01 15.59 o 1 21 1 30.76 40.83 5.18 o 2 21 1 871.46 883.52 17.63 o 3 21 1 0.21 8.03 8.94 o 4 21 1 83.32 112.10 8.08 o 0 22 1 74.35 90.99 14.40 o 1 22 1 1.59 5.76 8.90 o 2 22 1 343.18 391.48 18.77 o 3 22 1 59.39 62.29 8.07 o 1 23 1 10.25 -5.64 7.63 o 0 0 2 47961.68 38548.98 389.64 o 1 0 2 4180.30 4094.88 63.36 o 2 0 2 1520.55 1554.65 14.70 o 3 0 2 1.76 21.66 5.63 o 4 0 2 0.90 -2.67 8.82 o 5 0 2 4802.56 5153.91 49.43 o 6 0 2 81.77 36.47 8.27 o 7 0 2 3180.24 3158.94 33.35 o 8 0 2 181.61 151.80 11.21 o 9 0 2 2504.57 2348.34 36.19 o 10 0 2 345.34 308.73 16.97 o 1 1 2 6061.20 6462.98 39.90 o 2 1 2 15301.45 17437.14 158.37 o 3 1 2 67.61 97.13 7.69 o 4 1 2 124.53 107.71 4.64 o 5 1 2 49.15 69.21 4.70 o 6 1 2 25.19 32.44 10.65 o 7 1 2 0.05 3.37 8.45 o 8 1 2 790.45 823.92 20.80 o 9 1 2 3.62 13.83 10.26 o 10 1 2 229.03 222.14 10.86 o 0 2 2 1044.32 1044.44 10.86 o 1 2 2 248.15 193.71 4.20 o 2 2 2 3195.10 3285.93 28.55 o 3 2 2 207.78 292.60 8.59 o 4 2 2 174.88 170.89 7.44 o 5 2 2 122.44 136.45 7.95 o 6 2 2 703.07 698.16 15.35 o 7 2 2 7.60 4.83 12.22 o 8 2 2 249.63 236.05 12.17 o 9 2 2 230.72 223.09 14.11 o 10 2 2 1.45 -7.61 16.10 o 1 3 2 489.29 625.78 6.05 o 2 3 2 1720.02 1663.71 16.28 o 3 3 2 81.29 60.88 6.15 o 4 3 2 1372.48 1365.40 16.77 o 5 3 2 21.28 10.87 9.70 o 6 3 2 117.94 119.43 9.08 o 7 3 2 665.51 631.52 16.47 o 8 3 2 1375.10 1376.97 24.15 o 9 3 2 164.24 168.39 13.44 o 10 3 2 772.95 765.35 23.00 o 0 4 2 10999.06 11720.31 60.78 o 1 4 2 398.74 411.12 5.44 o 2 4 2 600.27 683.17 10.86 o 3 4 2 53.23 48.99 5.71 o 4 4 2 1368.21 1431.14 17.57 o 5 4 2 154.22 150.67 8.35 o 6 4 2 4.84 14.05 7.21 o 7 4 2 1343.48 1343.42 22.58 o 8 4 2 328.74 288.42 13.31 o 9 4 2 1199.97 1147.82 26.72 o 10 4 2 131.42 164.68 12.89 o 1 5 2 213.10 311.95 7.89 o 2 5 2 165.96 146.82 7.04 o 3 5 2 4368.79 4762.25 43.15 o 4 5 2 3722.44 3705.88 35.96 o 5 5 2 790.66 866.61 15.48 o 6 5 2 31.48 30.85 8.09 o 7 5 2 40.73 44.94 8.56 o 8 5 2 5.97 -6.95 13.68 o 9 5 2 14.63 -14.82 16.28 o 10 5 2 0.02 -14.38 15.07 o 0 6 2 4203.47 3626.51 32.02 o 1 6 2 43.32 76.53 4.15 o 2 6 2 4956.93 5047.15 48.91 o 3 6 2 144.47 132.12 7.37 o 4 6 2 599.08 541.00 12.30 o 5 6 2 246.61 236.66 9.72 o 6 6 2 1959.02 2004.22 25.64 o 7 6 2 472.37 470.70 14.72 o 8 6 2 26.55 24.37 13.39 o 9 6 2 767.07 749.52 21.98 o 10 6 2 52.45 70.63 11.49 o 1 7 2 68.97 92.08 7.80 o 2 7 2 468.65 455.43 10.23 o 3 7 2 1885.95 2027.69 21.37 o 4 7 2 660.86 670.33 13.74 o 5 7 2 186.35 185.02 9.67 o 6 7 2 142.76 155.48 9.93 o 7 7 2 768.19 780.01 18.54 o 8 7 2 581.71 555.39 18.80 o 9 7 2 70.99 82.06 10.76 o 10 7 2 181.68 170.00 15.12 o 0 8 2 18.77 6.81 7.72 o 1 8 2 192.92 205.93 6.45 o 2 8 2 272.31 229.73 8.55 o 3 8 2 257.90 296.10 9.43 o 4 8 2 842.43 879.07 15.97 o 5 8 2 57.69 40.48 7.06 o 6 8 2 700.73 698.00 17.36 o 7 8 2 80.34 64.28 9.26 o 8 8 2 0.50 1.06 12.62 o 9 8 2 7.89 21.92 15.77 o 1 9 2 1002.40 997.88 10.52 o 2 9 2 1679.04 1529.46 19.00 o 3 9 2 726.44 782.32 15.15 o 4 9 2 3487.42 3412.16 33.31 o 5 9 2 1497.59 1459.99 22.18 o 6 9 2 207.46 201.64 11.14 o 7 9 2 965.98 982.29 21.17 o 8 9 2 344.49 360.41 16.32 o 9 9 2 94.21 85.36 12.30 o 0 10 2 724.98 714.30 13.09 o 1 10 2 56.72 47.55 4.02 o 2 10 2 2252.37 2352.97 24.40 o 3 10 2 583.19 537.67 13.21 o 4 10 2 219.68 224.36 10.04 o 5 10 2 0.15 -11.09 12.07 o 6 10 2 276.31 262.47 12.28 o 7 10 2 553.55 511.90 16.85 o 8 10 2 189.59 181.34 13.52 o 9 10 2 140.84 127.79 12.63 o 1 11 2 1771.31 1811.27 18.04 o 2 11 2 1.31 12.77 8.31 o 3 11 2 53.07 55.53 7.28 o 4 11 2 4.95 5.31 11.27 o 5 11 2 343.38 358.63 13.39 o 6 11 2 567.21 546.36 16.42 o 7 11 2 636.11 626.74 19.69 o 8 11 2 0.03 21.40 13.98 o 9 11 2 98.28 96.57 13.07 o 0 12 2 1258.49 1197.13 18.36 o 1 12 2 229.14 227.84 15.07 o 2 12 2 393.18 416.77 12.30 o 3 12 2 489.93 504.90 13.89 o 4 12 2 326.16 297.72 12.03 o 5 12 2 2332.45 2314.39 30.13 o 6 12 2 1573.64 1594.31 26.99 o 7 12 2 41.32 47.98 9.81 o 8 12 2 355.33 397.23 17.49 o 9 12 2 67.25 69.76 11.31 o 1 13 2 471.66 432.76 9.05 o 2 13 2 11.01 -3.70 10.76 o 3 13 2 22.57 13.61 12.22 o 4 13 2 446.89 459.58 14.79 o 5 13 2 283.50 246.45 12.02 o 6 13 2 2.23 18.15 11.63 o 7 13 2 146.83 128.31 12.82 o 8 13 2 155.80 162.73 13.33 o 0 14 2 320.90 319.90 11.52 o 1 14 2 14.57 4.29 8.51 o 2 14 2 866.98 873.44 18.31 o 3 14 2 515.98 519.26 15.17 o 4 14 2 714.23 686.98 17.87 o 5 14 2 1081.10 1054.06 22.48 o 6 14 2 128.21 127.57 12.34 o 7 14 2 11.10 7.35 15.59 o 8 14 2 69.15 59.62 12.48 o 1 15 2 480.57 498.49 10.40 o 2 15 2 2470.23 2393.99 30.03 o 3 15 2 319.26 289.91 12.61 o 4 15 2 396.80 378.81 14.34 o 5 15 2 1534.81 1510.86 27.08 o 6 15 2 116.85 133.74 12.34 o 7 15 2 407.80 362.98 17.57 o 8 15 2 155.01 201.90 14.87 o 0 16 2 1999.46 2125.25 28.54 o 1 16 2 546.94 543.17 11.06 o 2 16 2 12.97 42.04 7.03 o 3 16 2 274.53 290.27 12.83 o 4 16 2 606.13 523.60 16.71 o 5 16 2 16.85 20.42 9.37 o 6 16 2 496.90 499.62 19.70 o 7 16 2 63.40 89.81 11.09 o 1 17 2 273.49 252.66 8.55 o 2 17 2 4.42 18.48 10.98 o 3 17 2 696.92 717.38 18.56 o 4 17 2 10.54 25.98 8.20 o 5 17 2 27.81 32.53 9.29 o 6 17 2 0.35 -15.91 15.91 o 7 17 2 30.00 16.91 15.41 o 0 18 2 691.32 716.06 18.71 o 1 18 2 315.15 302.98 11.86 o 2 18 2 0.04 -6.22 12.70 o 3 18 2 552.68 565.34 19.24 o 4 18 2 252.55 234.98 13.81 o 5 18 2 138.15 120.32 13.03 o 6 18 2 425.74 478.76 20.06 o 1 19 2 15.08 23.19 10.29 o 2 19 2 886.45 845.76 22.92 o 3 19 2 486.69 452.65 18.02 o 4 19 2 188.80 202.29 13.77 o 5 19 2 128.75 117.34 12.41 o 0 20 2 129.50 142.72 12.12 o 1 20 2 90.85 102.99 7.81 o 2 20 2 25.49 27.08 14.67 o 3 20 2 375.73 363.98 16.98 o 4 20 2 13.49 36.81 8.31 o 5 20 2 97.40 69.11 12.34 o 1 21 2 194.54 187.70 10.38 o 2 21 2 154.24 157.31 13.22 o 3 21 2 19.93 22.10 14.53 o 4 21 2 417.02 438.05 19.32 o 0 22 2 419.41 454.88 18.37 o 1 22 2 0.99 6.74 7.01 o 2 22 2 114.96 116.78 13.25 o 1 1 3 1336.81 1308.87 6.56 o 2 1 3 4146.59 3943.31 34.30 o 3 1 3 1564.59 1755.46 18.33 o 4 1 3 1111.62 1054.24 11.01 o 5 1 3 146.21 131.55 5.70 o 6 1 3 0.18 5.78 8.13 o 7 1 3 0.57 -8.35 12.60 o 8 1 3 850.19 850.06 14.27 o 9 1 3 22.24 29.80 7.81 o 10 1 3 41.17 52.54 7.77 o 0 2 3 29577.16 34245.25 119.69 o 1 2 3 83.72 82.57 4.01 o 2 2 3 32.92 1.72 7.98 o 3 2 3 60.89 94.28 6.30 o 4 2 3 4459.04 4600.67 45.83 o 5 2 3 452.61 399.03 11.28 o 6 2 3 4112.89 4231.57 42.21 o 7 2 3 45.11 46.81 8.97 o 8 2 3 394.26 372.91 14.45 o 9 2 3 2.03 -4.54 12.84 o 10 2 3 883.38 955.02 26.51 o 1 3 3 139.67 154.20 4.51 o 2 3 3 15.30 25.73 5.27 o 3 3 3 1595.91 1654.79 17.65 o 4 3 3 2196.68 2291.05 23.33 o 5 3 3 51.17 52.85 6.77 o 6 3 3 883.19 867.73 17.91 o 7 3 3 1040.44 961.89 20.09 o 8 3 3 165.49 157.75 11.21 o 9 3 3 120.00 109.29 12.01 o 10 3 3 12.19 -17.45 17.45 o 0 4 3 5512.09 4909.83 42.48 o 1 4 3 3472.44 3545.24 104.55 o 2 4 3 2027.13 1907.26 19.03 o 3 4 3 922.35 868.85 13.58 o 4 4 3 4722.04 4766.13 48.19 o 5 4 3 1823.70 1805.90 22.69 o 6 4 3 3350.93 3511.52 36.44 o 7 4 3 431.07 473.50 15.41 o 8 4 3 105.93 92.26 10.36 o 9 4 3 1.28 1.13 15.07 o 10 4 3 212.50 233.22 14.76 o 1 5 3 6092.74 6104.98 69.50 o 2 5 3 10057.38 10494.47 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9 7 4 38.46 53.21 10.94 o 0 8 4 375.76 434.96 10.62 o 1 8 4 403.08 402.94 7.52 o 2 8 4 402.16 376.71 10.62 o 3 8 4 1241.00 1295.26 19.54 o 4 8 4 14.58 15.88 6.73 o 5 8 4 152.44 160.36 10.84 o 6 8 4 487.77 486.69 16.30 o 7 8 4 38.21 48.34 9.37 o 8 8 4 141.83 159.47 13.40 o 9 8 4 33.42 23.57 17.56 o 1 9 4 355.54 322.73 7.29 o 2 9 4 11.91 15.73 9.51 o 3 9 4 5.64 11.20 9.62 o 4 9 4 465.97 453.91 14.07 o 5 9 4 355.25 366.46 14.09 o 6 9 4 6.10 3.99 12.11 o 7 9 4 43.04 37.99 9.81 o 8 9 4 27.59 29.09 15.15 o 9 9 4 1.32 16.17 9.37 o 0 10 4 1089.36 1057.85 17.00 o 1 10 4 254.60 245.83 15.88 o 2 10 4 796.03 771.43 15.73 o 3 10 4 586.01 603.83 15.04 o 4 10 4 959.68 931.33 18.87 o 5 10 4 10.45 7.43 12.73 o 6 10 4 889.35 894.53 21.27 o 7 10 4 297.03 291.73 15.61 o 8 10 4 42.11 49.62 10.76 o 9 10 4 197.85 228.47 14.91 o 1 11 4 1627.71 1592.56 30.35 o 2 11 4 122.99 122.91 8.86 o 3 11 4 28.70 31.21 7.32 o 4 11 4 702.13 704.68 17.25 o 5 11 4 3.84 -0.99 13.39 o 6 11 4 182.63 205.38 12.16 o 7 11 4 69.24 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