#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:59:31 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180937 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/17/2201728.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201728_Fobs loop_ _publ_author_name 'Amini, Mostafa M.' 'Abadi, Shabnam Hossein' 'Mirzaee, Mahdi' 'L\"ugger, Thomas' 'Hahn, F. Ekkehardt' 'Ng, Seik Weng' _publ_section_title ; catena-Poly[\m-trifluoroacetato-O:O'-dimethylphenyltin(IV)] ; _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m650 _journal_page_last m652 _journal_volume 58 _journal_year 2002 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 6.6552 _cell_length_b 10.9949 _cell_length_c 17.0794 _exptl_crystal_F_000 656.00 _reflns_d_resolution_high 0.8098 _cod_data_source_file ya6139Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Triphenyltin trifluoroacetate in P212121' _shelx_refln_list_code 4 _shelx_f_calc_maximum 211.69 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4966.95 5176.20 95.56 o 4 0 0 3909.08 3940.18 105.29 o 6 0 0 123.82 145.69 14.47 o 8 0 0 3.84 3.22 7.71 o 1 1 0 995.00 1132.37 16.89 o 2 1 0 1434.56 1607.04 22.21 o 3 1 0 3373.61 3444.63 46.49 o 4 1 0 3798.79 3932.57 53.56 o 5 1 0 720.75 750.35 16.67 o 6 1 0 1158.67 1129.46 25.28 o 7 1 0 298.73 290.96 12.47 o 8 1 0 120.12 120.00 10.12 o 0 2 0 7972.28 8015.35 257.38 o 1 2 0 16766.19 16548.15 211.72 o 2 2 0 2902.16 3190.53 42.59 o 3 2 0 7031.82 7093.06 92.97 o 4 2 0 289.22 273.43 8.04 o 5 2 0 762.70 751.85 13.89 o 6 2 0 1.97 1.73 3.68 o 7 2 0 0.58 -4.11 4.11 o 8 2 0 0.58 -0.23 5.49 o 1 3 0 2483.00 2531.77 33.85 o 2 3 0 14.36 15.06 1.58 o 3 3 0 4645.09 4673.63 62.51 o 4 3 0 377.17 376.39 8.43 o 5 3 0 3477.99 3497.61 49.46 o 6 3 0 345.08 351.96 15.73 o 7 3 0 450.49 473.78 16.01 o 8 3 0 10.09 11.63 6.01 o 0 4 0 28590.39 23691.95 428.85 o 1 4 0 4189.85 4283.08 56.49 o 2 4 0 9857.80 9833.35 127.53 o 3 4 0 2094.01 2094.38 30.00 o 4 4 0 2160.81 2192.37 32.08 o 5 4 0 259.05 244.75 7.41 o 6 4 0 33.10 48.90 5.97 o 7 4 0 10.35 8.09 5.16 o 1 5 0 0.44 4.10 2.68 o 2 5 0 920.01 882.76 14.07 o 3 5 0 89.31 87.42 3.80 o 4 5 0 3298.22 3351.00 47.09 o 5 5 0 26.59 30.04 3.77 o 6 5 0 1023.55 1026.87 26.32 o 7 5 0 2.13 -2.81 4.78 o 0 6 0 16021.98 14889.73 271.72 o 1 6 0 4485.60 4629.44 68.03 o 2 6 0 4923.66 4823.33 64.65 o 3 6 0 1675.14 1696.97 27.84 o 4 6 0 1094.03 1095.32 25.72 o 5 6 0 203.63 220.43 7.44 o 6 6 0 49.38 56.34 6.34 o 7 6 0 2.00 4.79 5.21 o 1 7 0 3656.77 3881.02 58.20 o 2 7 0 48.19 46.81 2.94 o 3 7 0 1884.84 1903.24 29.67 o 4 7 0 155.47 141.54 5.70 o 5 7 0 1056.86 1066.70 21.48 o 6 7 0 31.61 30.83 7.04 o 7 7 0 234.01 237.42 20.35 o 0 8 0 269.67 311.44 41.10 o 1 8 0 6598.15 6605.47 97.46 o 2 8 0 752.78 745.91 15.20 o 3 8 0 1638.59 1591.94 27.86 o 4 8 0 15.85 20.93 3.75 o 5 8 0 278.20 285.12 10.04 o 6 8 0 18.24 18.08 6.31 o 1 9 0 31.10 39.32 4.84 o 2 9 0 554.68 574.97 15.28 o 3 9 0 692.17 683.44 33.14 o 4 9 0 513.83 502.95 15.01 o 5 9 0 388.97 384.43 12.13 o 6 9 0 228.18 255.79 14.32 o 0 10 0 2050.56 2031.65 55.61 o 1 10 0 0.10 -0.51 2.82 o 2 10 0 2671.99 2794.42 51.69 o 3 10 0 87.07 86.64 7.11 o 4 10 0 508.13 507.95 18.00 o 5 10 0 10.96 12.43 5.20 o 1 11 0 0.15 4.41 3.16 o 2 11 0 83.31 91.69 7.42 o 3 11 0 193.94 197.71 10.29 o 4 11 0 350.07 384.69 14.15 o 0 12 0 202.69 210.07 22.10 o 1 12 0 1425.85 1434.22 31.75 o 2 12 0 86.65 101.30 8.30 o 3 12 0 649.44 630.61 18.96 o 1 13 0 51.56 44.40 6.34 o 2 13 0 42.86 46.02 6.71 o 1 0 1 42973.57 27650.83 499.60 o 2 0 1 931.73 989.03 14.35 o 3 0 1 5727.64 5826.22 76.64 o 4 0 1 79.31 103.72 4.05 o 5 0 1 536.99 522.96 10.64 o 6 0 1 35.37 40.30 5.30 o 7 0 1 7.34 5.54 4.82 o 8 0 1 14.06 15.66 6.19 o -8 1 1 71.35 80.10 8.93 o -7 1 1 418.60 415.13 16.17 o -6 1 1 603.64 571.48 19.00 o -5 1 1 1272.96 1269.53 30.94 o -4 1 1 581.52 562.55 10.95 o -3 1 1 3484.97 3622.97 46.81 o -2 1 1 10402.59 10758.86 151.40 o -1 1 1 243.51 268.53 4.94 o 0 1 1 28.30 31.47 2.17 o 1 1 1 289.15 320.60 5.55 o 2 1 1 10386.54 10758.32 138.53 o 3 1 1 3254.37 3309.25 46.63 o 4 1 1 595.99 587.48 10.72 o 5 1 1 1269.40 1271.93 20.48 o 6 1 1 589.93 595.33 25.65 o 7 1 1 427.00 431.15 15.04 o 8 1 1 69.59 68.09 8.42 o -8 2 1 6.67 9.87 6.60 o -7 2 1 23.13 25.85 5.48 o -6 2 1 33.45 29.81 5.05 o -5 2 1 74.09 78.35 4.21 o -4 2 1 3868.69 3725.58 44.07 o -3 2 1 1205.97 1252.34 17.30 o -2 2 1 6882.68 7184.60 85.69 o -1 2 1 8871.69 9138.46 120.72 o 0 2 1 13712.43 12443.75 173.66 o 1 2 1 9403.70 9724.57 132.75 o 2 2 1 6849.05 7056.67 114.04 o 3 2 1 1250.75 1287.52 21.16 o 4 2 1 3875.75 3724.82 63.20 o 5 2 1 69.08 65.28 4.85 o 6 2 1 28.70 27.46 4.85 o 7 2 1 24.00 28.88 5.82 o 8 2 1 6.71 6.31 6.08 o -8 3 1 151.92 177.17 25.07 o -7 3 1 73.91 74.04 7.87 o -6 3 1 1250.86 1251.37 27.32 o -5 3 1 280.78 268.51 6.50 o -4 3 1 3257.46 3224.86 41.40 o -3 3 1 245.32 246.40 5.49 o -2 3 1 3709.76 3951.93 51.68 o -1 3 1 57.05 57.53 2.65 o 0 3 1 2022.73 2204.85 41.70 o 1 3 1 93.25 82.96 2.94 o 2 3 1 3620.56 3833.13 51.94 o 3 3 1 272.34 278.75 9.91 o 4 3 1 3311.00 3225.31 49.81 o 5 3 1 284.41 265.65 8.94 o 6 3 1 1231.93 1221.48 32.80 o 7 3 1 76.10 76.78 7.96 o 8 3 1 151.17 157.96 18.13 o -7 4 1 5.47 7.51 4.85 o -6 4 1 74.46 63.26 6.41 o -5 4 1 372.47 337.70 8.76 o -4 4 1 674.06 645.75 11.96 o -3 4 1 4488.54 4707.85 62.56 o -2 4 1 3194.56 3302.50 45.16 o -1 4 1 11258.41 11383.42 135.50 o 0 4 1 1282.44 1311.40 26.29 o 1 4 1 11331.03 11301.31 160.26 o 2 4 1 3294.18 3422.50 45.56 o 3 4 1 4402.94 4627.83 62.90 o 4 4 1 652.93 623.60 12.19 o 5 4 1 372.73 356.62 9.24 o 6 4 1 75.47 76.91 8.43 o 7 4 1 5.90 6.89 5.27 o -7 5 1 426.03 434.54 18.30 o -6 5 1 16.51 17.73 4.17 o -5 5 1 1771.36 1733.77 26.94 o -4 5 1 66.94 68.96 4.01 o -3 5 1 1490.99 1575.85 23.73 o -2 5 1 1044.36 1105.54 16.88 o -1 5 1 256.92 241.76 5.38 o 0 5 1 403.37 407.70 8.25 o 1 5 1 269.99 264.34 7.05 o 2 5 1 1061.48 1123.85 17.20 o 3 5 1 1521.03 1621.66 24.14 o 4 5 1 65.04 64.97 4.04 o 5 5 1 1751.46 1686.86 27.26 o 6 5 1 16.30 10.56 5.49 o 7 5 1 436.80 448.62 15.83 o -7 6 1 2.12 6.13 6.00 o -6 6 1 25.46 29.42 5.27 o -5 6 1 164.90 162.63 6.38 o -4 6 1 606.68 600.24 11.81 o -3 6 1 2236.22 2101.71 37.30 o -2 6 1 3006.68 3020.60 41.57 o -1 6 1 7938.10 8195.56 108.22 o 0 6 1 3719.73 3977.67 58.82 o 1 6 1 8035.41 8388.94 118.82 o 2 6 1 3029.74 3015.75 41.83 o 3 6 1 2230.10 2198.62 31.50 o 4 6 1 587.36 575.19 11.93 o 5 6 1 166.35 160.99 7.18 o 6 6 1 23.37 25.44 5.07 o 7 6 1 2.01 -0.84 4.95 o -7 7 1 31.75 37.00 7.86 o -6 7 1 543.30 561.85 19.91 o -5 7 1 64.20 78.65 5.78 o -4 7 1 1406.42 1397.65 25.26 o -3 7 1 143.39 149.24 6.07 o -2 7 1 2204.30 2204.50 41.34 o -1 7 1 685.06 684.05 13.52 o 0 7 1 5.96 6.29 1.91 o 1 7 1 702.35 706.67 11.86 o 2 7 1 2224.17 2204.16 69.43 o 3 7 1 136.76 129.64 5.44 o 4 7 1 1399.89 1385.43 24.66 o 5 7 1 68.61 71.73 5.83 o 6 7 1 523.19 527.95 19.34 o 7 7 1 31.96 33.62 10.37 o -6 8 1 40.46 48.14 7.71 o -5 8 1 71.74 70.51 5.86 o -4 8 1 385.84 383.77 10.71 o -3 8 1 249.26 251.21 10.39 o -2 8 1 3972.75 3988.68 54.99 o -1 8 1 1062.57 1067.37 19.13 o 0 8 1 4200.67 4172.94 70.98 o 1 8 1 1034.31 1010.19 22.05 o 2 8 1 3884.84 3962.62 68.42 o 3 8 1 288.72 279.38 9.85 o 4 8 1 391.90 369.33 10.73 o 5 8 1 66.19 55.35 5.70 o 6 8 1 41.32 42.46 7.71 o -6 9 1 95.45 100.01 12.32 o -5 9 1 503.05 483.54 13.66 o -4 9 1 507.21 527.38 13.46 o -3 9 1 298.41 285.52 9.05 o -2 9 1 244.85 225.80 8.84 o -1 9 1 423.11 413.93 12.31 o 0 9 1 130.40 114.06 6.63 o 1 9 1 431.86 436.84 12.54 o 2 9 1 213.73 204.60 8.86 o 3 9 1 294.78 290.35 15.59 o 4 9 1 506.09 500.08 15.27 o 5 9 1 509.26 491.70 13.93 o 6 9 1 93.59 107.65 10.53 o -5 10 1 74.44 73.94 7.67 o -4 10 1 61.21 61.82 6.56 o -3 10 1 1402.90 1354.84 29.71 o -2 10 1 4.60 3.87 3.25 o -1 10 1 2718.71 2641.94 48.99 o 0 10 1 53.44 66.79 5.82 o 1 10 1 2665.19 2648.86 49.12 o 2 10 1 2.54 7.57 3.59 o 3 10 1 1420.90 1445.17 36.03 o 4 10 1 59.39 70.03 7.06 o 5 10 1 73.15 88.92 10.65 o -4 11 1 239.87 252.55 11.92 o -3 11 1 315.10 307.66 12.12 o -2 11 1 14.80 11.76 4.10 o -1 11 1 131.84 126.44 8.20 o 0 11 1 113.32 111.40 7.65 o 1 11 1 127.19 117.87 7.79 o 2 11 1 21.63 19.76 4.43 o 3 11 1 344.25 313.36 12.35 o 4 11 1 242.16 248.23 15.12 o -3 12 1 53.73 61.60 7.30 o -2 12 1 946.11 924.18 25.40 o -1 12 1 99.84 92.34 7.76 o 0 12 1 1204.15 1109.28 26.32 o 1 12 1 103.80 97.38 7.92 o 2 12 1 932.30 936.91 23.88 o 3 12 1 53.92 70.83 7.53 o -2 13 1 178.06 186.27 10.92 o -1 13 1 83.67 95.87 8.38 o 0 13 1 3.98 3.84 4.31 o 1 13 1 83.71 79.98 7.81 o 2 13 1 172.73 173.19 10.72 o 0 0 2 16151.71 14327.77 319.64 o 1 0 2 18877.42 17218.66 509.87 o 2 0 2 11348.69 11239.67 158.85 o 3 0 2 2366.10 2577.55 35.35 o 4 0 2 1743.90 1679.39 24.78 o 5 0 2 248.36 252.83 9.44 o 6 0 2 51.08 56.23 5.88 o 7 0 2 153.57 149.19 9.58 o 8 0 2 10.80 10.23 6.57 o -8 1 2 105.24 100.44 10.69 o -7 1 2 219.12 198.23 10.69 o -6 1 2 813.67 801.63 22.79 o -5 1 2 751.15 737.37 15.40 o -4 1 2 1386.93 1440.81 19.96 o -3 1 2 5419.92 5657.52 63.25 o -2 1 2 2875.14 2999.78 34.22 o -1 1 2 7387.29 7456.24 89.08 o 0 1 2 4321.78 4321.51 55.94 o 1 1 2 7518.50 7512.16 105.91 o 2 1 2 2879.69 2928.46 49.22 o 3 1 2 5327.34 5337.23 90.36 o 4 1 2 1401.41 1461.03 31.28 o 5 1 2 759.27 738.57 21.01 o 6 1 2 813.96 817.43 20.26 o 7 1 2 214.69 219.80 11.11 o 8 1 2 105.42 100.71 9.72 o -8 2 2 37.25 37.07 7.95 o -7 2 2 3.21 1.50 4.83 o -6 2 2 298.60 307.73 19.36 o -5 2 2 905.75 906.40 18.01 o -4 2 2 843.91 842.60 12.12 o -3 2 2 6659.36 7253.17 86.33 o -2 2 2 2464.68 2518.20 31.13 o -1 2 2 19165.90 19066.09 209.69 o 0 2 2 1250.05 1315.35 17.92 o 1 2 2 19775.04 18696.77 345.28 o 2 2 2 2482.17 2472.96 37.56 o 3 2 2 6592.37 6983.83 103.08 o 4 2 2 825.91 831.03 18.20 o 5 2 2 922.19 918.93 18.44 o 6 2 2 295.18 308.79 11.50 o 7 2 2 3.35 4.54 4.66 o 8 2 2 36.79 38.25 7.35 o -7 3 2 395.95 410.20 18.98 o -6 3 2 112.63 103.49 6.36 o -5 3 2 1841.08 1843.72 29.77 o -4 3 2 725.44 779.80 17.74 o -3 3 2 5488.01 5917.10 72.77 o -2 3 2 5489.89 5557.41 66.93 o -1 3 2 119.90 122.10 3.02 o 0 3 2 1486.51 1315.40 18.26 o 1 3 2 72.96 75.89 3.05 o 2 3 2 5399.59 5473.90 79.93 o 3 3 2 5628.01 6040.11 87.21 o 4 3 2 691.51 734.58 15.29 o 5 3 2 1839.05 1786.91 35.26 o 6 3 2 123.52 119.86 9.21 o 7 3 2 391.00 380.69 14.39 o -7 4 2 78.86 96.17 9.24 o -6 4 2 164.10 157.89 8.74 o -5 4 2 511.27 480.52 14.16 o -4 4 2 1401.43 1362.87 21.06 o -3 4 2 2065.58 2020.50 28.32 o -2 4 2 5071.42 5217.94 68.31 o -1 4 2 4214.65 4343.08 58.18 o 0 4 2 12304.11 12581.15 177.28 o 1 4 2 4349.27 4482.75 58.38 o 2 4 2 5091.13 5152.61 68.86 o 3 4 2 1994.62 1946.64 28.92 o 4 4 2 1398.26 1338.94 23.84 o 5 4 2 516.79 517.29 11.56 o 6 4 2 170.75 164.90 9.02 o 7 4 2 81.55 96.09 8.90 o -7 5 2 2.96 1.45 6.09 o -6 5 2 829.36 823.78 18.46 o -5 5 2 111.03 116.95 6.90 o -4 5 2 1657.68 1619.29 24.36 o -3 5 2 2017.95 2151.35 31.24 o -2 5 2 953.95 908.47 14.17 o -1 5 2 2743.77 2704.41 40.33 o 0 5 2 134.17 134.13 5.85 o 1 5 2 2787.31 2708.30 40.84 o 2 5 2 935.64 904.59 14.67 o 3 5 2 2063.79 2244.23 32.07 o 4 5 2 1682.92 1574.48 48.68 o 5 5 2 108.31 112.66 5.72 o 6 5 2 841.12 816.85 24.27 o 7 5 2 3.11 1.48 5.04 o -7 6 2 58.18 71.32 11.30 o -6 6 2 48.14 56.87 6.25 o -5 6 2 398.20 377.69 10.51 o -4 6 2 585.65 569.46 11.18 o -3 6 2 1201.84 1196.65 18.67 o -2 6 2 5301.51 5500.47 67.99 o -1 6 2 3716.42 3776.21 52.65 o 0 6 2 6563.60 6701.32 108.13 o 1 6 2 3967.20 4072.90 58.38 o 2 6 2 5350.69 5569.15 81.20 o 3 6 2 1162.22 1166.92 19.13 o 4 6 2 555.74 512.92 12.46 o 5 6 2 405.79 395.11 10.16 o 6 6 2 49.73 62.40 6.67 o 7 6 2 59.14 67.51 8.07 o -6 7 2 66.00 71.22 11.14 o -5 7 2 930.80 932.85 29.12 o -4 7 2 243.26 235.31 12.17 o -3 7 2 1610.58 1568.26 24.64 o -2 7 2 1000.01 943.04 15.67 o -1 7 2 483.12 480.91 9.24 o 0 7 2 6347.11 6514.23 94.87 o 1 7 2 457.19 487.37 10.48 o 2 7 2 1004.20 941.15 27.16 o 3 7 2 1611.36 1636.15 27.55 o 4 7 2 227.55 229.76 10.03 o 5 7 2 914.61 909.10 23.25 o 6 7 2 69.53 71.13 8.90 o -6 8 2 101.21 107.55 11.73 o -5 8 2 188.53 190.18 9.88 o -4 8 2 218.40 218.25 7.31 o -3 8 2 1230.54 1210.79 19.92 o -2 8 2 680.63 647.54 14.00 o -1 8 2 3384.45 3460.06 59.86 o 0 8 2 1460.07 1464.16 27.76 o 1 8 2 3467.11 3571.64 61.09 o 2 8 2 725.68 698.42 16.66 o 3 8 2 1176.36 1149.46 25.23 o 4 8 2 204.46 202.38 8.30 o 5 8 2 199.28 185.85 8.60 o 6 8 2 99.21 112.73 10.42 o -6 9 2 213.08 212.66 17.63 o -5 9 2 222.70 257.38 11.10 o -4 9 2 550.82 566.98 14.00 o -3 9 2 402.02 389.41 14.11 o -2 9 2 485.09 452.85 13.05 o -1 9 2 624.51 650.98 16.27 o 0 9 2 246.22 243.07 9.08 o 1 9 2 633.08 646.25 16.36 o 2 9 2 460.90 451.02 13.33 o 3 9 2 384.52 363.63 12.20 o 4 9 2 543.89 539.89 16.21 o 5 9 2 220.58 230.22 11.39 o 6 9 2 224.57 237.64 22.71 o -5 10 2 145.11 159.91 20.17 o -4 10 2 317.26 344.15 12.48 o -3 10 2 117.42 122.79 7.88 o -2 10 2 2521.49 2552.15 47.66 o -1 10 2 36.11 35.95 4.78 o 0 10 2 2868.65 2733.10 57.19 o 1 10 2 31.62 40.48 4.91 o 2 10 2 2591.74 2545.40 48.07 o 3 10 2 122.01 115.41 10.15 o 4 10 2 307.17 292.01 12.22 o 5 10 2 146.77 160.30 10.29 o -4 11 2 296.96 321.92 12.94 o -3 11 2 184.47 192.81 10.01 o -2 11 2 430.54 395.27 13.40 o -1 11 2 188.83 200.15 9.69 o 0 11 2 52.09 55.23 6.52 o 1 11 2 196.88 210.12 10.00 o 2 11 2 451.03 429.19 14.07 o 3 11 2 173.06 190.94 10.35 o 4 11 2 306.94 312.34 13.18 o -3 12 2 351.05 353.44 13.75 o -2 12 2 47.29 50.71 6.33 o -1 12 2 801.39 770.63 20.72 o 0 12 2 178.61 173.00 9.76 o 1 12 2 810.97 791.81 21.01 o 2 12 2 46.98 54.00 6.56 o 3 12 2 358.16 362.34 13.93 o -2 13 2 135.24 137.95 9.76 o -1 13 2 82.24 79.47 8.37 o 0 13 2 211.38 212.02 11.37 o 1 13 2 85.68 83.53 8.05 o 2 13 2 136.92 138.69 9.89 o 1 0 3 19945.74 17957.73 398.35 o 2 0 3 2765.56 2919.25 48.22 o 3 0 3 5385.72 5378.93 78.49 o 4 0 3 1520.73 1546.78 26.06 o 5 0 3 275.83 272.40 8.72 o 6 0 3 266.56 276.38 9.62 o 7 0 3 7.21 7.16 4.96 o 8 0 3 102.51 110.54 11.18 o -8 1 3 33.13 48.07 8.73 o -7 1 3 272.37 280.09 12.29 o -6 1 3 471.90 465.95 12.61 o -5 1 3 1707.55 1736.53 29.66 o -4 1 3 1815.92 1874.62 28.35 o -3 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