#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/17/2201739.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201739_Fobs loop_ _publ_author_name 'Doriguetto, Antonio C.' 'de Paula Silva, Carlos H. T.' 'Rando, Daniela G.' 'Ferreira, Elizabeth I.' 'Ellena, Javier A.' _publ_section_title ; 4-(2-Isonicotinoylhydrazino)-4-oxobutanoic acid ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o288 _journal_page_last o289 _journal_volume 59 _journal_year 2003 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 83.797 _cell_angle_beta 79.735 _cell_angle_gamma 81.035 _cell_length_a 4.8140 _cell_length_b 8.9168 _cell_length_c 12.4943 _exptl_crystal_F_000 248.00 _reflns_d_resolution_high 0.8410 _[local]_cod_data_source_file ac6028IIsup2.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' tomich in P -1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 36.59 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 85.16 69.76 2.91 o 3 0 0 165.75 171.50 4.78 o 4 0 0 6.01 5.74 0.41 o 5 0 0 6.43 6.78 0.70 o -5 1 0 32.57 33.67 2.24 o -4 1 0 0.49 0.42 0.25 o -3 1 0 47.43 65.99 2.06 o -2 1 0 378.44 439.46 21.43 o 1 1 0 528.84 441.61 19.83 o 2 1 0 26.99 25.64 0.83 o 3 1 0 52.00 48.19 2.31 o 4 1 0 6.39 6.67 0.56 o 5 1 0 77.65 87.73 5.11 o -5 2 0 1.32 0.50 0.49 o -4 2 0 248.37 269.11 10.08 o -3 2 0 35.03 41.27 1.66 o -2 2 0 0.01 0.06 0.17 o -1 2 0 17.86 17.07 0.70 o 0 2 0 7.38 5.28 0.30 o 1 2 0 523.81 528.33 12.16 o 2 2 0 565.92 521.97 15.01 o 3 2 0 67.27 63.99 1.54 o 4 2 0 4.64 4.77 0.52 o 5 2 0 2.40 2.20 0.65 o -5 3 0 55.03 44.46 7.53 o -4 3 0 71.89 86.12 4.31 o -3 3 0 5.26 5.65 0.51 o -2 3 0 436.77 500.96 21.27 o -1 3 0 35.64 46.83 2.25 o 0 3 0 212.24 185.79 6.16 o 1 3 0 345.33 297.03 10.56 o 2 3 0 182.03 177.54 5.96 o 3 3 0 15.77 12.88 0.89 o 4 3 0 96.34 102.71 4.30 o 5 3 0 89.95 81.61 31.09 o -4 4 0 36.25 36.00 4.25 o -3 4 0 228.23 250.01 9.65 o -2 4 0 1.80 2.14 0.36 o -1 4 0 330.92 348.27 11.02 o 0 4 0 5.34 3.59 0.33 o 1 4 0 80.02 71.73 2.68 o 2 4 0 89.82 83.46 3.13 o 3 4 0 12.69 10.96 0.60 o 4 4 0 331.07 380.65 14.32 o -4 5 0 7.50 4.52 1.14 o -3 5 0 2.10 2.65 0.45 o -2 5 0 9.04 8.09 0.48 o -1 5 0 33.06 34.30 1.37 o 0 5 0 12.98 14.70 0.59 o 1 5 0 611.39 593.04 14.72 o 2 5 0 526.13 530.30 29.93 o 3 5 0 137.88 134.68 5.00 o 4 5 0 145.20 141.69 11.08 o 5 5 0 18.18 21.23 3.21 o -4 6 0 1.17 -0.01 0.99 o -3 6 0 3.11 2.52 0.44 o -2 6 0 20.39 20.94 1.02 o -1 6 0 103.68 101.13 6.97 o 0 6 0 334.94 350.20 16.77 o 1 6 0 6.46 3.61 0.35 o 2 6 0 5.98 6.71 0.53 o 3 6 0 3.31 4.21 0.40 o 4 6 0 6.74 8.97 1.50 o 5 6 0 33.19 23.70 3.28 o -3 7 0 31.42 20.64 2.45 o -2 7 0 157.20 164.85 7.45 o -1 7 0 101.73 110.67 4.89 o 0 7 0 78.06 73.98 2.94 o 1 7 0 0.35 0.45 0.29 o 2 7 0 0.64 0.69 0.20 o 3 7 0 1.28 0.84 0.31 o 4 7 0 9.11 10.82 1.80 o -3 8 0 157.57 160.42 41.27 o -2 8 0 0.01 0.28 0.54 o -1 8 0 112.93 118.48 7.69 o 0 8 0 30.62 32.10 2.92 o 1 8 0 152.60 174.52 7.96 o 2 8 0 0.95 -0.01 0.68 o 3 8 0 0.91 3.35 0.89 o 4 8 0 0.72 1.48 1.16 o -2 9 0 1.56 1.13 0.80 o -1 9 0 169.13 190.03 12.90 o 0 9 0 211.49 257.69 18.57 o 1 9 0 14.86 12.85 1.54 o 2 9 0 74.41 75.81 6.01 o 3 9 0 10.46 9.17 1.76 o -1 10 0 3.69 3.22 0.80 o 0 10 0 6.68 7.11 1.10 o 1 10 0 3.03 4.95 2.19 o 2 10 0 6.54 6.19 1.40 o -2 -10 1 3.88 2.11 1.53 o -1 -10 1 16.42 15.49 3.78 o 0 -10 1 8.57 10.53 1.47 o -3 -9 1 8.81 4.85 1.52 o -2 -9 1 9.79 13.53 1.48 o -1 -9 1 7.47 6.87 0.90 o 0 -9 1 12.34 11.15 1.16 o 1 -9 1 17.89 15.93 3.72 o 2 -9 1 1.47 1.38 0.68 o -4 -8 1 11.11 6.51 1.10 o -3 -8 1 6.60 8.29 1.41 o -2 -8 1 113.80 121.41 4.38 o -1 -8 1 5.89 5.64 0.59 o 0 -8 1 7.39 7.60 0.59 o 1 -8 1 57.90 57.66 3.87 o 2 -8 1 23.05 24.60 1.48 o 3 -8 1 114.38 117.65 13.30 o -4 -7 1 5.36 5.04 0.83 o -3 -7 1 13.43 14.53 0.70 o -2 -7 1 4.06 4.75 0.41 o -1 -7 1 2.25 2.59 0.35 o 0 -7 1 88.50 90.79 2.94 o 1 -7 1 413.60 500.11 28.69 o 2 -7 1 297.35 366.57 15.41 o 3 -7 1 54.94 52.81 2.87 o -4 -6 1 0.02 -0.08 0.60 o -3 -6 1 3.17 3.84 0.41 o -2 -6 1 1.19 1.01 0.24 o -1 -6 1 306.91 340.24 17.64 o 0 -6 1 299.66 308.83 12.09 o 1 -6 1 91.96 110.02 3.08 o 2 -6 1 0.28 0.72 0.31 o 3 -6 1 3.10 2.85 0.42 o 4 -6 1 23.32 16.36 9.73 o -5 -5 1 0.10 -0.16 0.57 o -4 -5 1 0.42 -0.32 0.62 o -3 -5 1 0.16 0.13 0.19 o -2 -5 1 6.88 5.54 0.31 o -1 -5 1 80.93 87.25 3.17 o 0 -5 1 404.91 398.02 16.47 o 1 -5 1 0.18 1.08 0.30 o 2 -5 1 98.73 110.35 3.96 o 3 -5 1 9.18 9.60 0.63 o 4 -5 1 2.62 2.07 1.02 o -4 -4 1 174.57 165.60 10.79 o -3 -4 1 330.50 327.01 11.94 o -2 -4 1 65.10 68.10 2.02 o -1 -4 1 131.64 120.34 4.96 o 0 -4 1 69.32 70.23 2.85 o 1 -4 1 44.39 48.08 1.53 o 2 -4 1 312.23 349.55 18.18 o 3 -4 1 7.52 7.07 0.68 o 4 -4 1 0.39 0.38 0.65 o -5 -3 1 93.07 110.89 12.06 o -4 -3 1 104.14 90.98 6.26 o -3 -3 1 7.99 7.29 0.48 o -2 -3 1 204.14 185.04 5.56 o -1 -3 1 76.23 72.89 2.59 o 0 -3 1 720.00 604.75 25.84 o 1 -3 1 146.41 156.86 5.11 o 2 -3 1 44.66 40.77 1.85 o 3 -3 1 4.48 5.01 1.02 o 4 -3 1 9.08 6.84 0.87 o 5 -3 1 5.42 5.56 2.40 o -5 -2 1 29.68 32.59 2.14 o -4 -2 1 244.61 279.99 10.34 o -3 -2 1 0.92 0.71 0.24 o -2 -2 1 346.41 327.45 17.12 o -1 -2 1 89.23 75.06 2.46 o 0 -2 1 28.31 29.14 1.32 o 1 -2 1 17.48 15.62 0.61 o 2 -2 1 502.52 513.56 30.94 o 3 -2 1 12.09 11.61 0.67 o 4 -2 1 230.42 234.51 9.05 o 5 -2 1 154.11 156.60 13.95 o -5 -1 1 8.84 9.33 0.70 o -4 -1 1 1.17 1.11 0.25 o -3 -1 1 56.16 48.12 1.49 o -2 -1 1 29.78 30.75 0.76 o -1 -1 1 73.27 67.49 2.34 o 0 -1 1 39.86 33.00 2.82 o 1 -1 1 193.64 187.70 6.31 o 2 -1 1 229.27 246.96 8.55 o 3 -1 1 508.73 591.09 16.51 o 4 -1 1 15.41 14.21 0.60 o 5 -1 1 6.48 7.92 0.64 o -5 0 1 38.77 43.89 2.77 o -4 0 1 17.00 19.02 0.73 o -3 0 1 76.29 77.92 2.58 o -1 0 1 531.09 421.63 61.88 o 1 0 1 43.86 31.05 1.24 o 2 0 1 0.02 0.10 0.24 o 3 0 1 23.45 28.06 0.87 o 4 0 1 6.55 5.62 0.42 o 5 0 1 94.46 107.29 5.65 o -5 1 1 7.99 7.24 0.73 o -4 1 1 16.26 14.77 0.90 o -3 1 1 0.01 0.17 0.22 o -2 1 1 255.07 249.04 6.59 o -1 1 1 16.81 12.98 0.52 o 0 1 1 53.04 23.89 34.40 o 1 1 1 142.73 121.15 3.19 o 2 1 1 0.00 1.13 0.20 o 3 1 1 4.39 4.82 0.42 o 4 1 1 28.66 32.38 1.63 o 5 1 1 24.67 25.84 1.83 o -5 2 1 70.82 77.36 5.81 o -4 2 1 0.82 0.71 0.40 o -3 2 1 41.80 50.24 2.84 o -2 2 1 0.00 0.12 0.20 o -1 2 1 39.64 37.44 2.21 o 0 2 1 72.29 68.80 6.27 o 2 2 1 0.09 0.32 0.14 o 3 2 1 154.65 162.37 5.19 o 4 2 1 68.74 69.65 2.56 o 5 2 1 9.63 10.86 1.06 o -5 3 1 3.88 3.50 0.77 o -4 3 1 8.67 10.52 0.60 o -3 3 1 0.13 0.20 0.22 o -2 3 1 185.93 210.43 7.16 o -1 3 1 392.51 438.08 49.58 o 0 3 1 340.37 332.69 11.39 o 1 3 1 103.90 108.85 3.89 o 2 3 1 60.29 54.24 1.86 o 3 3 1 2.97 3.42 0.25 o 4 3 1 7.08 10.78 0.78 o -3 4 1 20.73 26.02 1.20 o -2 4 1 76.22 91.74 3.51 o -1 4 1 36.46 33.49 1.30 o 0 4 1 17.89 18.05 1.31 o 1 4 1 40.41 33.57 1.11 o 2 4 1 124.67 128.88 4.36 o 3 4 1 21.57 20.33 0.72 o 4 4 1 135.28 143.48 11.92 o -4 5 1 0.33 -1.30 0.93 o -3 5 1 111.05 116.63 4.19 o -2 5 1 35.55 38.54 1.81 o -1 5 1 199.70 205.56 7.77 o 0 5 1 0.90 1.93 0.29 o 1 5 1 109.63 97.51 3.35 o 2 5 1 68.69 62.61 2.24 o 3 5 1 17.44 17.46 0.63 o 4 5 1 49.91 50.00 2.36 o -4 6 1 0.10 0.04 0.52 o -3 6 1 0.05 -0.60 0.76 o -2 6 1 88.44 95.03 4.38 o -1 6 1 2.58 1.32 0.30 o 0 6 1 170.60 160.91 5.37 o 1 6 1 0.00 0.33 0.35 o 2 6 1 20.20 19.96 0.84 o 3 6 1 20.47 20.78 1.04 o 4 6 1 201.90 231.68 14.73 o 5 6 1 5.94 4.15 0.94 o -3 7 1 0.80 0.84 0.50 o -2 7 1 75.78 78.31 3.90 o -1 7 1 22.27 25.17 1.03 o 0 7 1 19.56 21.90 0.96 o 1 7 1 81.64 83.12 3.27 o 2 7 1 65.61 56.08 2.26 o 3 7 1 13.47 13.89 0.95 o 4 7 1 0.77 0.88 0.88 o -3 8 1 1.61 0.54 0.77 o -2 8 1 0.02 -0.11 0.85 o -1 8 1 31.35 28.84 1.52 o 0 8 1 187.04 186.68 10.97 o 1 8 1 33.74 37.25 1.86 o 2 8 1 29.90 28.11 1.32 o 3 8 1 10.99 9.54 1.47 o 4 8 1 1.44 1.22 0.87 o -2 9 1 18.93 18.78 1.68 o -1 9 1 46.78 54.66 2.68 o 0 9 1 49.85 71.73 9.79 o 1 9 1 1.31 3.17 1.00 o 2 9 1 16.59 15.54 2.42 o 3 9 1 1.40 0.51 0.84 o -1 10 1 34.71 34.14 3.28 o 0 10 1 63.19 60.91 9.74 o 1 10 1 14.31 16.78 2.76 o 2 10 1 54.51 52.43 5.42 o -1 -10 2 62.26 74.92 6.19 o 0 -10 2 0.35 1.37 1.10 o -3 -9 2 6.81 6.11 1.32 o -2 -9 2 40.47 45.28 8.91 o -1 -9 2 43.46 52.51 10.33 o 0 -9 2 0.23 1.79 0.76 o 1 -9 2 29.11 28.11 2.80 o 2 -9 2 0.58 0.46 0.65 o -3 -8 2 8.99 10.19 1.96 o -2 -8 2 12.68 13.79 0.70 o -1 -8 2 2.64 3.09 0.37 o 0 -8 2 1.28 1.34 0.47 o 1 -8 2 22.54 20.40 1.36 o 2 -8 2 6.68 5.64 0.89 o -4 -7 2 29.16 34.45 3.77 o -3 -7 2 0.49 0.48 0.30 o -2 -7 2 15.71 16.04 0.56 o -1 -7 2 110.24 114.91 4.06 o 0 -7 2 6.30 7.58 0.68 o 1 -7 2 202.00 216.94 11.01 o 2 -7 2 268.53 317.16 23.73 o 3 -7 2 16.36 13.02 1.75 o -4 -6 2 1.38 2.56 0.82 o -3 -6 2 16.28 14.19 0.70 o -2 -6 2 44.14 40.20 1.10 o -1 -6 2 304.01 343.76 15.63 o 0 -6 2 30.02 41.76 1.48 o 1 -6 2 125.89 129.53 4.39 o 2 -6 2 206.13 231.04 7.28 o 3 -6 2 13.34 14.31 0.88 o 4 -6 2 18.81 14.78 2.28 o -5 -5 2 1.15 2.00 0.62 o -4 -5 2 13.55 11.71 3.56 o -3 -5 2 17.37 19.24 1.22 o -2 -5 2 78.34 80.38 3.58 o -1 -5 2 70.70 69.87 3.50 o 0 -5 2 0.80 0.42 0.31 o 1 -5 2 49.43 58.60 2.00 o 2 -5 2 101.20 118.28 5.43 o 3 -5 2 152.65 182.58 7.46 o 4 -5 2 1.87 1.41 0.85 o -5 -4 2 6.88 6.56 0.84 o -4 -4 2 1.32 1.15 0.26 o -3 -4 2 4.56 4.45 0.69 o -2 -4 2 0.05 0.09 0.15 o -1 -4 2 6.51 5.91 0.33 o 1 -4 2 9.29 13.68 0.78 o 2 -4 2 10.13 7.94 0.66 o 3 -4 2 16.94 17.14 1.01 o 4 -4 2 1.27 1.21 0.81 o -5 -3 2 4.64 3.97 0.80 o -4 -3 2 22.52 21.34 1.41 o -3 -3 2 221.95 211.30 9.94 o -2 -3 2 641.63 624.45 19.36 o 0 -3 2 143.20 156.65 6.26 o 1 -3 2 569.76 536.51 22.86 o 2 -3 2 57.23 56.92 2.64 o 3 -3 2 93.58 106.85 4.23 o 4 -3 2 3.86 4.33 0.53 o 5 -3 2 43.49 29.80 5.63 o -5 -2 2 65.03 82.66 4.37 o -4 -2 2 771.91 756.08 53.67 o -3 -2 2 15.67 17.46 0.62 o -2 -2 2 15.60 14.28 0.80 o -1 -2 2 13.41 10.93 0.46 o 0 -2 2 371.15 340.58 11.04 o 1 -2 2 47.62 49.70 2.39 o 2 -2 2 5.41 7.15 0.49 o 3 -2 2 282.12 302.84 24.83 o 4 -2 2 16.72 19.19 0.81 o 5 -2 2 0.16 0.84 0.78 o -5 -1 2 40.14 56.12 6.75 o -4 -1 2 200.66 207.60 9.72 o -3 -1 2 0.47 0.69 0.14 o -2 -1 2 64.13 54.66 2.21 o -1 -1 2 0.02 0.14 0.07 o 2 -1 2 369.38 411.05 11.36 o 3 -1 2 13.77 16.91 0.62 o 4 -1 2 1.31 1.81 0.27 o 5 -1 2 51.95 51.11 3.63 o -5 0 2 3.08 2.10 0.52 o -4 0 2 0.31 0.13 0.25 o -3 0 2 89.78 95.87 3.51 o -2 0 2 135.50 129.92 3.72 o -1 0 2 34.30 44.72 1.41 o 0 0 2 0.09 0.13 0.09 o 1 0 2 3.59 3.13 0.16 o 2 0 2 10.92 9.97 0.48 o 3 0 2 133.42 141.55 3.43 o 4 0 2 92.09 80.15 3.40 o 5 0 2 8.71 8.57 0.72 o -5 1 2 38.06 41.83 3.08 o -4 1 2 116.21 133.65 6.74 o -3 1 2 5.05 4.77 0.48 o -2 1 2 86.29 97.77 2.99 o -1 1 2 95.08 85.30 3.64 o 1 1 2 7.10 5.35 0.23 o 2 1 2 260.97 258.14 7.50 o 3 1 2 233.97 277.91 10.25 o 4 1 2 109.97 101.40 3.42 o 5 1 2 18.54 20.68 1.68 o -5 2 2 10.79 8.34 0.96 o -4 2 2 20.44 21.85 1.20 o -3 2 2 2.83 2.60 0.48 o -2 2 2 360.17 378.22 19.25 o -1 2 2 458.29 420.23 13.18 o 3 2 2 2.78 2.21 0.23 o 4 2 2 17.28 19.84 1.01 o 5 2 2 6.95 2.41 0.99 o -4 3 2 56.32 52.96 3.91 o -3 3 2 40.26 38.24 1.23 o -2 3 2 185.27 242.48 11.10 o -1 3 2 449.02 528.54 70.34 o 1 3 2 201.82 205.89 7.09 o 2 3 2 62.69 60.88 1.91 o 3 3 2 0.20 0.20 0.13 o 4 3 2 6.05 6.28 0.52 o -3 4 2 8.08 5.29 0.32 o -2 4 2 0.27 0.39 0.23 o -1 4 2 11.10 10.34 1.00 o 0 4 2 13.25 13.08 0.84 o 1 4 2 143.61 159.65 4.06 o 2 4 2 155.95 135.84 5.09 o 3 4 2 1.64 1.59 0.10 o 4 4 2 7.43 9.05 0.44 o -4 5 2 104.04 138.21 16.02 o -3 5 2 1.61 2.88 0.31 o -2 5 2 9.43 13.63 0.74 o -1 5 2 265.38 293.97 8.57 o 0 5 2 71.96 69.79 2.26 o 1 5 2 9.72 11.61 0.65 o 2 5 2 638.66 629.93 27.70 o 3 5 2 8.36 10.31 0.56 o 4 5 2 0.72 0.52 0.31 o -4 6 2 23.83 14.53 1.75 o -3 6 2 199.14 216.22 13.79 o -2 6 2 5.32 3.44 0.38 o -1 6 2 56.46 63.61 2.14 o 0 6 2 21.12 28.23 1.88 o 1 6 2 2.63 2.44 0.39 o 2 6 2 13.87 17.40 1.00 o 3 6 2 7.30 5.92 0.45 o 4 6 2 142.82 171.67 5.04 o 5 6 2 31.67 20.57 4.60 o -3 7 2 0.01 -0.36 0.89 o -2 7 2 70.30 80.55 3.50 o -1 7 2 23.13 21.62 0.87 o 0 7 2 13.88 15.68 1.06 o 1 7 2 16.41 17.25 0.92 o 2 7 2 226.13 244.07 14.94 o 3 7 2 54.43 54.04 2.24 o 4 7 2 132.89 173.23 15.07 o -2 8 2 2.82 1.97 0.72 o -1 8 2 50.64 54.14 2.39 o 0 8 2 7.74 6.31 0.63 o 1 8 2 1.95 3.58 0.44 o 2 8 2 2.78 2.43 0.49 o 3 8 2 1.65 1.47 0.66 o 4 8 2 10.67 9.10 1.48 o -2 9 2 29.84 25.98 3.42 o -1 9 2 45.06 46.07 2.28 o 0 9 2 131.04 133.75 22.90 o 1 9 2 0.09 0.78 1.00 o 2 9 2 3.61 2.30 1.27 o 3 9 2 0.81 0.58 0.94 o 0 10 2 20.82 21.40 2.09 o 1 10 2 7.63 11.25 1.84 o 2 10 2 2.37 2.87 1.32 o -1 -10 3 35.75 36.52 2.57 o 0 -10 3 17.79 22.37 2.46 o -2 -9 3 23.65 18.09 3.51 o -1 -9 3 181.66 204.75 24.72 o 0 -9 3 4.79 6.05 1.05 o 1 -9 3 5.76 5.70 1.05 o -2 -8 3 141.65 197.94 27.81 o -1 -8 3 16.13 14.87 0.77 o 0 -8 3 0.76 0.86 0.42 o 1 -8 3 87.62 89.84 8.67 o 2 -8 3 2.72 1.89 0.70 o -4 -7 3 17.17 14.21 1.78 o -3 -7 3 29.80 29.39 2.54 o -2 -7 3 35.91 33.23 1.91 o -1 -7 3 3.07 3.38 0.53 o 0 -7 3 15.75 16.34 0.75 o 1 -7 3 74.02 67.18 3.13 o 2 -7 3 11.68 13.13 0.71 o 3 -7 3 1.79 1.14 1.29 o -4 -6 3 31.79 39.51 4.99 o -3 -6 3 0.07 0.01 0.29 o -2 -6 3 70.10 72.66 4.84 o -1 -6 3 17.27 17.01 0.85 o 0 -6 3 3.09 2.76 0.40 o 1 -6 3 0.31 1.65 0.42 o 2 -6 3 2.22 2.72 0.39 o 3 -6 3 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