#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/17/2201751.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201751_Fobs loop_ _publ_author_name 'Shi, He-Ping' 'Liu, Dian-Sheng' 'Huang, Shu-Ping' _publ_section_title ; [(1-tert-Butyl-2-phenylvinylamino)(dimethylamino)dimethylsilyl-\k^2^N,N'] (N,N,N',N'-tetramethylenediamine-\k^2^N,N')lithium(I) ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m339 _journal_page_last m341 _journal_volume 59 _journal_year 2003 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 97.674 _cell_angle_gamma 90.000 _cell_length_a 14.8188 _cell_length_b 9.4142 _cell_length_c 18.6351 _exptl_crystal_F_000 880.00 _reflns_d_resolution_high 0.8406 _[local]_cod_data_source_file ac6040Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' HS0267P in P2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 160.01 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 -11 0 176.75 197.67 64.43 o 2 -11 0 43.69 118.85 48.95 o 3 -11 0 4.10 23.15 33.15 o 0 -10 0 34.92 40.66 41.44 o 1 -10 0 44.55 61.15 39.25 o 2 -10 0 64.88 86.64 44.88 o 3 -10 0 18.31 25.49 36.91 o 4 -10 0 25.30 65.06 43.16 o 5 -10 0 100.07 94.93 47.23 o 6 -10 0 16.97 36.59 40.19 o 7 -10 0 0.31 13.92 33.94 o 1 -9 0 152.18 151.32 39.88 o 2 -9 0 136.81 157.01 57.86 o 3 -9 0 43.12 28.93 33.78 o 4 -9 0 80.20 99.77 45.51 o 5 -9 0 304.54 395.19 80.23 o 6 -9 0 17.61 14.54 28.31 o 7 -9 0 35.11 50.98 36.75 o 8 -9 0 175.91 219.41 67.25 o 9 -9 0 10.26 28.93 35.03 o 10 -9 0 73.22 131.21 56.92 o 0 -8 0 193.56 135.90 45.82 o 1 -8 0 404.94 421.24 53.95 o 2 -8 0 257.34 243.65 59.74 o 3 -8 0 283.58 276.65 65.06 o 4 -8 0 313.38 277.27 64.43 o 5 -8 0 13.71 50.04 33.78 o 6 -8 0 0.45 -15.95 23.46 o 7 -8 0 78.33 85.54 42.85 o 8 -8 0 24.60 41.44 38.16 o 9 -8 0 14.15 31.28 34.87 o 10 -8 0 85.77 131.52 54.27 o 11 -8 0 8.51 18.45 30.34 o 12 -8 0 97.05 123.54 56.77 o 1 -7 0 301.33 316.50 42.63 o 2 -7 0 387.16 332.67 43.10 o 3 -7 0 190.15 194.70 50.83 o 4 -7 0 162.63 117.60 43.94 o 5 -7 0 16.11 4.54 26.12 o 6 -7 0 777.70 703.89 80.69 o 7 -7 0 46.48 44.26 34.87 o 8 -7 0 294.26 176.25 54.42 o 9 -7 0 113.24 125.42 49.26 o 10 -7 0 35.08 78.82 47.54 o 11 -7 0 40.67 50.04 38.78 o 12 -7 0 84.54 114.79 53.64 o 13 -7 0 16.62 36.59 38.47 o 0 -6 0 788.78 720.47 68.81 o 1 -6 0 372.18 353.41 41.13 o 2 -6 0 199.91 174.10 30.03 o 3 -6 0 284.58 259.60 50.67 o 4 -6 0 1694.53 1481.75 99.15 o 5 -6 0 103.23 154.20 46.13 o 6 -6 0 588.97 551.26 67.71 o 7 -6 0 127.72 126.83 45.04 o 8 -6 0 305.46 270.86 62.24 o 9 -6 0 58.24 82.10 43.01 o 10 -6 0 8.10 9.70 27.37 o 11 -6 0 43.69 63.49 39.72 o 12 -6 0 186.05 165.14 58.33 o 13 -6 0 116.87 147.47 55.20 o 14 -6 0 51.42 143.87 59.74 o 1 -5 0 748.17 814.91 46.72 o 2 -5 0 554.34 571.29 44.65 o 3 -5 0 61.41 50.36 25.33 o 4 -5 0 749.58 710.93 65.99 o 5 -5 0 523.84 437.41 59.74 o 6 -5 0 137.93 176.09 43.48 o 7 -5 0 164.92 177.18 44.10 o 8 -5 0 319.43 338.11 59.27 o 9 -5 0 37.93 30.34 26.27 o 10 -5 0 390.50 415.05 70.37 o 11 -5 0 2.30 0.63 25.80 o 12 -5 0 18.96 2.66 24.08 o 13 -5 0 59.90 86.64 47.38 o 14 -5 0 52.79 99.46 49.26 o 0 -4 0 4668.88 4573.96 135.74 o 1 -4 0 612.80 560.80 34.51 o 2 -4 0 102.40 93.08 18.66 o 3 -4 0 773.06 667.30 55.67 o 4 -4 0 162.10 145.44 15.64 o 5 -4 0 908.79 897.81 34.09 o 6 -4 0 19.78 29.40 10.95 o 7 -4 0 1143.31 1135.51 47.07 o 8 -4 0 385.98 441.01 62.55 o 9 -4 0 1106.01 1078.12 89.14 o 10 -4 0 152.51 147.94 47.07 o 11 -4 0 322.92 372.04 67.09 o 12 -4 0 11.41 17.52 29.56 o 13 -4 0 17.77 28.62 35.66 o 14 -4 0 98.55 149.82 55.99 o 1 -3 0 4743.95 4635.07 83.19 o 2 -3 0 588.68 490.89 40.97 o 3 -3 0 87.26 95.08 11.42 o 4 -3 0 50.85 53.48 10.17 o 5 -3 0 738.85 800.54 33.78 o 6 -3 0 462.27 431.62 28.31 o 7 -3 0 975.76 888.74 69.59 o 8 -3 0 261.18 264.29 47.07 o 9 -3 0 103.45 115.57 35.97 o 10 -3 0 197.29 155.13 45.35 o 11 -3 0 1816.31 1891.95 121.36 o 12 -3 0 32.25 30.96 33.31 o 13 -3 0 408.28 522.01 79.44 o 14 -3 0 150.08 179.22 56.30 o 0 -2 0 2875.33 2654.95 72.88 o 1 -2 0 3611.32 3255.85 160.69 o 2 -2 0 750.77 702.95 20.02 o 3 -2 0 2685.53 2695.61 46.92 o 4 -2 0 1686.77 1648.46 70.69 o 5 -2 0 329.82 294.63 35.66 o 1 -1 0 15737.75 15458.07 142.62 o 2 -1 0 3636.52 3671.62 75.06 o 13 -1 0 7.23 23.46 23.77 o 14 -1 0 77.51 94.93 38.78 o 15 -1 0 40.59 66.15 35.81 o 1 0 0 0.74 2.19 1.88 o 2 0 0 11264.54 11256.46 116.04 o 3 0 0 2336.25 2341.56 60.99 o 4 0 0 203.85 223.63 24.87 o 5 0 0 637.35 638.83 42.07 o 6 0 0 2306.96 2343.28 87.42 o 7 0 0 905.60 924.24 60.99 o 8 0 0 14.19 13.29 16.26 o 9 0 0 2737.23 2868.89 118.38 o 10 0 0 178.59 207.21 41.13 o 11 0 0 70.85 54.58 26.74 o 12 0 0 23.12 0.31 16.11 o 13 0 0 11.56 26.74 24.71 o 14 0 0 91.45 121.36 42.22 o 15 0 0 22.20 26.27 24.71 o 1 1 0 15658.05 15760.21 533.35 o 2 1 0 3614.00 3547.84 50.90 o 3 1 0 7605.80 7743.34 86.64 o 4 1 0 2362.33 2382.71 61.69 o 5 1 0 1798.23 1768.07 115.33 o 6 1 0 1192.92 1191.04 45.23 o 7 1 0 514.19 470.51 31.32 o 8 1 0 1167.68 1142.32 50.76 o 9 1 0 187.74 181.80 25.86 o 10 1 0 356.08 408.97 36.64 o 11 1 0 199.65 149.56 26.70 o 12 1 0 145.69 141.84 40.66 o 13 1 0 6.67 31.28 26.59 o 14 1 0 78.93 106.97 41.44 o 15 1 0 41.53 71.47 33.62 o 16 1 0 74.23 103.37 43.16 o 0 2 0 2860.19 2913.46 77.10 o 1 2 0 3584.17 3456.69 60.40 o 2 2 0 749.68 665.96 38.47 o 3 2 0 2678.76 2663.66 58.90 o 4 2 0 1691.99 1717.13 59.90 o 5 2 0 325.48 328.67 26.05 o 6 2 0 385.57 414.58 32.92 o 7 2 0 596.22 551.52 35.24 o 8 2 0 161.36 163.11 24.66 o 9 2 0 211.42 240.07 31.36 o 10 2 0 182.24 228.17 41.75 o 11 2 0 156.74 129.26 25.88 o 12 2 0 664.89 664.13 51.09 o 13 2 0 50.26 61.89 24.08 o 14 2 0 126.40 146.81 34.73 o 15 2 0 36.11 52.55 32.06 o 16 2 0 53.72 80.54 41.29 o 17 2 0 3.17 -7.04 24.08 o 1 3 0 4746.86 4818.24 86.45 o 2 3 0 569.64 550.02 31.51 o 3 3 0 85.53 70.54 16.23 o 4 3 0 49.03 53.12 14.92 o 5 3 0 734.70 778.76 41.11 o 6 3 0 461.73 422.77 32.45 o 7 3 0 987.18 974.96 49.83 o 8 3 0 264.27 300.53 33.65 o 9 3 0 104.28 113.99 29.87 o 10 3 0 198.44 182.48 29.71 o 11 3 0 1809.46 1658.19 105.87 o 12 3 0 31.62 46.33 22.08 o 13 3 0 405.59 390.37 51.61 o 14 3 0 149.01 138.09 49.57 o 15 3 0 39.96 46.13 35.50 o 16 3 0 57.18 88.51 45.98 o 0 4 0 4663.08 4628.23 137.78 o 1 4 0 606.27 585.49 36.50 o 2 4 0 102.09 125.26 22.10 o 3 4 0 779.93 708.46 41.30 o 4 4 0 155.33 159.67 24.61 o 5 4 0 906.32 852.49 46.63 o 6 4 0 20.37 25.69 14.94 o 7 4 0 1140.08 1010.76 54.73 o 8 4 0 385.46 415.77 41.09 o 9 4 0 1098.56 1004.99 59.05 o 10 4 0 150.16 153.60 30.50 o 11 4 0 320.08 285.76 40.36 o 12 4 0 10.56 2.78 19.21 o 13 4 0 16.92 24.87 30.50 o 14 4 0 98.92 148.25 53.80 o 15 4 0 13.43 11.73 25.33 o 16 4 0 61.24 116.19 52.08 o 1 5 0 765.42 780.95 77.88 o 2 5 0 553.81 587.78 42.01 o 3 5 0 61.57 53.28 19.24 o 4 5 0 742.82 799.92 64.67 o 5 5 0 527.63 447.71 38.27 o 6 5 0 139.18 156.69 28.43 o 7 5 0 164.57 178.48 31.65 o 8 5 0 317.47 326.93 46.45 o 9 5 0 37.76 33.37 21.77 o 10 5 0 383.36 399.14 47.38 o 11 5 0 2.28 2.50 17.96 o 12 5 0 18.31 45.98 35.34 o 13 5 0 59.73 63.81 38.63 o 14 5 0 52.93 96.96 46.76 o 15 5 0 30.55 22.21 36.75 o 0 6 0 800.07 754.40 71.00 o 1 6 0 370.45 419.32 58.88 o 2 6 0 200.48 184.79 31.57 o 3 6 0 287.22 282.64 38.03 o 4 6 0 1700.89 1504.97 96.96 o 5 6 0 105.98 125.63 28.48 o 6 6 0 589.60 649.34 51.46 o 7 6 0 126.78 125.61 31.57 o 8 6 0 303.03 316.30 45.92 o 9 6 0 57.00 76.25 29.07 o 10 6 0 7.80 12.98 22.00 o 11 6 0 43.72 73.97 43.16 o 12 6 0 183.14 179.06 58.64 o 13 6 0 116.58 169.68 59.43 o 14 6 0 52.02 101.65 50.36 o 1 7 0 304.59 237.02 38.62 o 2 7 0 386.10 297.68 43.56 o 3 7 0 189.12 197.88 36.80 o 4 7 0 161.08 161.36 36.27 o 5 7 0 15.99 26.99 22.83 o 6 7 0 776.29 694.30 57.20 o 7 7 0 45.70 90.87 30.73 o 8 7 0 295.58 286.05 45.16 o 9 7 0 113.26 106.28 34.14 o 10 7 0 35.97 88.98 50.04 o 11 7 0 42.12 53.80 42.38 o 12 7 0 83.83 74.91 49.26 o 13 7 0 15.87 26.12 37.38 o 0 8 0 192.87 187.66 56.30 o 1 8 0 402.07 420.99 52.07 o 2 8 0 254.75 228.43 42.54 o 3 8 0 281.16 322.32 48.36 o 4 8 0 310.74 295.81 46.82 o 5 8 0 13.39 45.13 27.29 o 6 8 0 0.26 0.30 21.34 o 7 8 0 77.07 76.77 31.89 o 8 8 0 23.17 18.72 24.60 o 9 8 0 14.02 27.68 39.25 o 10 8 0 86.17 131.99 61.15 o 11 8 0 8.44 5.00 38.16 o 12 8 0 99.61 158.26 63.65 o 1 9 0 148.37 149.44 40.56 o 2 9 0 136.26 149.61 39.86 o 3 9 0 41.88 48.96 30.35 o 4 9 0 79.59 106.97 37.98 o 5 9 0 302.34 293.58 51.97 o 6 9 0 18.42 27.76 27.83 o 7 9 0 34.68 27.16 30.26 o 8 9 0 176.30 212.53 77.25 o 9 9 0 10.45 -0.47 35.66 o 10 9 0 74.12 89.77 55.83 o 0 10 0 37.01 47.07 45.51 o 1 10 0 44.46 82.23 36.48 o 2 10 0 65.68 57.09 33.56 o 3 10 0 18.29 43.77 33.17 o 4 10 0 25.21 72.89 37.31 o 5 10 0 101.09 100.58 40.14 o 6 10 0 17.67 74.58 38.63 o 7 10 0 0.30 13.45 39.41 o 1 11 0 176.92 163.67 47.71 o 2 11 0 44.11 89.61 38.47 o 3 11 0 3.88 34.52 32.03 o -3 -11 1 34.08 41.75 37.38 o -2 -11 1 8.06 76.00 34.87 o -1 -11 1 1.70 48.79 41.44 o 0 -11 1 5.14 98.52 46.60 o 1 -11 1 16.73 33.00 34.40 o 2 -11 1 67.93 132.77 50.51 o 3 -11 1 46.41 39.10 38.63 o -7 -10 1 11.36 20.17 32.22 o -6 -10 1 106.21 208.62 69.90 o -5 -10 1 0.76 -10.48 26.59 o -4 -10 1 48.04 42.85 36.59 o -3 -10 1 13.30 23.46 35.81 o -2 -10 1 297.66 349.21 80.54 o -1 -10 1 37.35 29.09 38.00 o 0 -10 1 30.39 37.46 28.25 o 1 -10 1 140.46 150.31 40.83 o 2 -10 1 7.09 13.61 28.62 o 3 -10 1 295.26 277.27 74.91 o 4 -10 1 35.03 50.98 40.03 o 5 -10 1 51.65 96.02 49.73 o 6 -10 1 3.40 10.01 30.81 o 7 -10 1 164.16 201.89 64.59 o -10 -9 1 19.55 43.16 37.06 o -9 -9 1 6.70 14.54 34.87 o -8 -9 1 19.52 33.31 34.87 o -7 -9 1 186.93 240.99 69.12 o -6 -9 1 19.15 23.93 28.77 o -5 -9 1 35.14 41.91 35.34 o -4 -9 1 7.03 22.83 30.81 o -3 -9 1 125.80 140.43 52.39 o -2 -9 1 59.59 57.86 37.38 o -1 -9 1 5.63 14.86 30.65 o 0 -9 1 62.20 77.58 36.59 o 1 -9 1 70.05 67.21 29.24 o 2 -9 1 340.10 408.32 78.66 o 3 -9 1 58.83 68.81 38.47 o 4 -9 1 69.45 76.47 40.66 o 5 -9 1 2.99 10.79 28.15 o 6 -9 1 135.21 148.10 54.11 o 7 -9 1 4.43 16.73 28.15 o 8 -9 1 49.98 71.47 42.07 o 9 -9 1 6.54 50.20 39.10 o 10 -9 1 4.97 18.77 37.69 o -12 -8 1 15.70 83.20 48.17 o -11 -8 1 35.11 33.94 31.75 o -10 -8 1 4.91 37.38 31.28 o -9 -8 1 140.60 146.53 54.42 o -8 -8 1 34.73 40.03 35.03 o -7 -8 1 46.30 46.29 37.53 o -6 -8 1 85.13 85.70 44.88 o -5 -8 1 513.27 503.87 81.79 o -4 -8 1 109.12 102.28 45.51 o -3 -8 1 10.56 24.24 31.75 o -2 -8 1 252.70 201.11 58.18 o -1 -8 1 176.94 181.44 38.24 o 0 -8 1 43.60 32.71 21.84 o 1 -8 1 393.48 367.26 48.16 o 2 -8 1 31.85 33.80 23.65 o 3 -8 1 190.13 147.47 49.26 o 4 -8 1 101.69 96.65 42.38 o 5 -8 1 80.44 144.03 51.92 o 6 -8 1 54.37 51.14 36.59 o 7 -8 1 91.43 113.07 49.42 o 8 -8 1 52.52 52.86 36.91 o 9 -8 1 48.11 39.88 36.59 o 10 -8 1 134.18 173.90 57.55 o 11 -8 1 13.47 31.90 35.03 o 12 -8 1 6.10 12.51 29.40 o -13 -7 1 78.51 130.27 55.83 o -12 -7 1 56.74 25.49 32.37 o -11 -7 1 20.92 54.89 38.78 o -10 -7 1 154.15 220.97 66.62 o -9 -7 1 194.14 172.96 57.08 o -8 -7 1 368.06 466.34 78.97 o -7 -7 1 316.05 289.47 65.06 o -6 -7 1 81.78 78.35 40.50 o -5 -7 1 129.52 120.10 45.04 o -4 -7 1 453.72 461.65 72.56 o -3 -7 1 374.56 360.47 64.43 o -2 -7 1 17.96 -1.25 22.21 o -1 -7 1 200.78 218.89 36.74 o 0 -7 1 35.13 39.58 20.95 o 1 -7 1 83.09 62.07 23.73 o 2 -7 1 190.62 161.77 33.41 o 3 -7 1 1.96 8.91 23.93 o 4 -7 1 203.38 274.30 58.80 o 5 -7 1 600.12 599.11 81.95 o 6 -7 1 201.21 189.07 53.80 o 7 -7 1 54.07 10.48 25.49 o 8 -7 1 106.56 87.73 42.22 o 9 -7 1 62.07 83.67 40.97 o 10 -7 1 25.92 37.53 32.37 o 11 -7 1 110.94 191.57 61.30 o 12 -7 1 19.00 42.38 35.03 o 13 -7 1 12.54 64.90 43.32 o -14 -6 1 4.82 14.39 32.06 o -13 -6 1 9.76 21.27 28.15 o -12 -6 1 5.32 -3.60 28.31 o -11 -6 1 155.70 126.52 49.73 o -10 -6 1 100.56 88.04 42.85 o -9 -6 1 13.02 13.45 25.65 o -8 -6 1 195.66 205.49 54.73 o -7 -6 1 147.97 125.26 45.51 o -6 -6 1 199.45 175.31 47.54 o -5 -6 1 256.02 265.23 53.80 o -4 -6 1 225.64 288.84 55.67 o -3 -6 1 126.26 121.98 38.78 o -2 -6 1 460.16 335.76 55.36 o -1 -6 1 637.84 590.88 43.79 o 0 -6 1 65.23 95.88 23.86 o 1 -6 1 311.23 380.93 40.80 o 2 -6 1 639.36 688.53 48.24 o 3 -6 1 252.14 235.05 48.64 o 4 -6 1 40.85 73.03 33.94 o 5 -6 1 58.00 48.32 27.99 o 6 -6 1 137.70 175.31 48.01 o 7 -6 1 145.27 147.00 43.79 o 8 -6 1 211.71 205.80 52.86 o 9 -6 1 292.05 351.40 67.56 o 10 -6 1 210.65 185.79 55.99 o 11 -6 1 67.38 85.07 41.91 o 12 -6 1 365.88 387.37 76.47 o 13 -6 1 8.38 11.26 29.71 o -15 -5 1 10.67 4.22 30.65 o -14 -5 1 1.36 -7.04 21.89 o -13 -5 1 6.89 3.75 29.40 o -12 -5 1 293.56 267.42 66.62 o -11 -5 1 65.20 71.00 40.97 o -10 -5 1 460.57 469.00 75.06 o -9 -5 1 242.51 241.30 55.83 o -8 -5 1 310.15 354.68 61.93 o -7 -5 1 491.25 401.44 62.24 o -6 -5 1 125.71 129.80 40.97 o -5 -5 1 41.69 35.19 24.55 o -4 -5 1 305.78 269.76 47.70 o -3 -5 1 2418.46 2454.16 47.85 o -2 -5 1 112.49 127.61 14.70 o -1 -5 1 1927.53 1961.90 70.70 o 0 -5 1 163.54 201.87 28.41 o 1 -5 1 27.14 37.10 15.17 o 2 -5 1 410.51 393.19 34.49 o 3 -5 1 64.62 68.34 28.93 o 4 -5 1 62.36 69.59 29.40 o 5 -5 1 110.47 91.33 34.56 o 6 -5 1 1614.83 1660.03 104.00 o 7 -5 1 671.65 526.24 62.24 o 8 -5 1 162.97 129.02 41.13 o 9 -5 1 880.64 915.01 85.39 o 10 -5 1 47.48 40.66 31.12 o 11 -5 1 133.44 184.69 53.33 o 12 -5 1 61.42 51.76 38.47 o 13 -5 1 39.14 81.01 43.32 o -15 -4 1 103.06 150.44 59.11 o -14 -4 1 192.46 227.70 65.37 o -13 -4 1 43.55 86.79 46.60 o -12 -4 1 263.72 281.34 66.46 o -11 -4 1 37.64 49.73 35.97 o -10 -4 1 105.77 99.30 41.29 o -9 -4 1 570.11 546.57 65.06 o -8 -4 1 413.07 454.93 35.34 o -7 -4 1 162.82 185.63 23.61 o -6 -4 1 922.01 841.35 38.78 o -5 -4 1 970.02 992.42 38.63 o -4 -4 1 1038.64 1096.89 37.06 o -3 -4 1 152.58 146.85 14.54 o -2 -4 1 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20.46 114.63 55.52 o -2 1 22 5.98 29.56 41.75 o -1 1 22 47.84 62.08 44.26 o