#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/17/2201791.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201791_Fobs loop_ _publ_author_name 'Clegg, William' 'Drummond, Allison M.' 'Liddle, Stephen T.' 'Mulvey, Robert E.' _publ_section_title ; A triclinic polymorph of octa-tert-butoxytetralithiumtetrasodium ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m64 _journal_page_last m66 _journal_volume 59 _journal_year 2003 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 82.560 _cell_angle_beta 89.492 _cell_angle_gamma 82.033 _cell_length_a 11.1917 _cell_length_b 21.0007 _cell_length_c 29.4496 _exptl_crystal_F_000 2304.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file bt6229Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' rem251 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 417.81 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 71.05 52.06 4.29 o 2 0 0 1282.09 1309.19 23.71 o 3 0 0 18417.69 18958.72 158.59 o 4 0 0 4345.44 3954.22 69.32 o 5 0 0 1674.68 1783.45 36.01 o 6 0 0 68.92 91.29 16.35 o 7 0 0 24.52 15.43 15.26 o 8 0 0 112.04 75.06 19.68 o 9 0 0 107.67 100.98 39.89 o 10 0 0 97.18 38.65 39.48 o 11 0 0 1.88 -15.79 46.12 o 12 0 0 4.65 27.01 45.71 o 13 0 0 38.77 9.56 48.62 o -13 1 0 49.93 60.67 50.70 o -12 1 0 1.31 -48.62 41.97 o -11 1 0 91.74 105.55 46.54 o -10 1 0 1.61 -8.31 38.23 o -9 1 0 109.29 86.02 38.23 o -8 1 0 527.17 485.72 31.21 o -7 1 0 892.21 1048.68 32.66 o -6 1 0 116.52 79.80 27.84 o -5 1 0 4797.92 4908.29 49.65 o -4 1 0 3630.21 4017.10 125.28 o -3 1 0 354.69 426.44 15.48 o -2 1 0 2439.16 2177.09 40.60 o -1 1 0 35096.45 35049.86 744.44 o 1 1 0 6790.90 5845.75 39.97 o 2 1 0 119.15 119.38 14.13 o 3 1 0 46876.77 50931.18 242.57 o 4 1 0 80.40 123.34 18.49 o 5 1 0 131.94 140.54 16.77 o 6 1 0 14371.91 15423.42 102.03 o 7 1 0 841.41 863.60 33.34 o 8 1 0 2063.69 2171.46 45.03 o 9 1 0 22.15 -4.16 34.90 o 10 1 0 22.34 32.41 44.88 o 11 1 0 26.44 33.66 46.12 o 12 1 0 98.61 87.26 48.62 o 13 1 0 67.49 28.67 48.20 o -12 2 0 43.74 55.68 51.11 o -11 2 0 48.08 28.67 41.97 o -10 2 0 0.50 22.02 39.48 o -9 2 0 5.87 -33.24 34.49 o -8 2 0 2058.88 1968.05 71.92 o -7 2 0 23.60 29.36 14.91 o -6 2 0 632.37 624.41 28.60 o -5 2 0 5.95 20.64 13.84 o -4 2 0 35.20 22.66 9.68 o -3 2 0 4690.68 4608.39 84.15 o -2 2 0 429.57 475.31 13.92 o -1 2 0 2466.88 2207.57 20.31 o 0 2 0 47973.48 47005.05 304.43 o 1 2 0 333.08 378.06 9.77 o 2 2 0 4673.23 4735.25 36.72 o 3 2 0 4181.19 4363.53 53.53 o 4 2 0 992.88 1045.65 25.37 o 5 2 0 4037.05 4316.80 48.94 o 6 2 0 11517.17 11731.99 86.15 o 7 2 0 3577.73 3564.00 50.23 o 8 2 0 48.05 50.83 19.46 o 9 2 0 3704.76 3850.83 78.18 o 10 2 0 1048.78 1097.64 70.65 o 11 2 0 91.39 93.08 44.05 o 12 2 0 30.36 20.78 51.53 o 13 2 0 46.59 41.14 49.86 o -12 3 0 10.03 -25.76 47.37 o -11 3 0 35.58 31.17 46.54 o -10 3 0 132.75 147.10 43.22 o -9 3 0 100.45 103.47 41.55 o -8 3 0 558.02 509.09 54.44 o -7 3 0 13.57 28.88 15.28 o -6 3 0 15.99 31.03 13.68 o -5 3 0 5141.42 5598.50 50.05 o -4 3 0 1635.92 1658.90 71.10 o -3 3 0 5193.11 5595.04 58.53 o -2 3 0 7380.80 6968.28 177.46 o -1 3 0 26927.47 24547.84 134.88 o 0 3 0 648.67 589.98 47.20 o 1 3 0 19.30 16.70 7.48 o 2 3 0 3938.75 3572.96 36.47 o 3 3 0 2851.63 3758.82 60.14 o 4 3 0 63.28 48.99 12.26 o 5 3 0 911.89 968.25 34.50 o 6 3 0 4635.47 4639.05 143.35 o 7 3 0 2675.47 2705.97 46.82 o 8 3 0 11348.09 11220.15 93.79 o 9 3 0 1712.69 1753.42 47.82 o 10 3 0 59.75 73.97 37.40 o 11 3 0 2.39 17.45 44.05 o 12 3 0 543.50 524.03 65.24 o 13 3 0 618.04 750.94 80.21 o -12 4 0 607.11 642.47 70.65 o -11 4 0 32.34 -20.78 42.38 o -10 4 0 419.85 476.24 63.17 o -9 4 0 156.70 179.52 46.96 o -8 4 0 4246.05 4073.08 91.50 o -7 4 0 207.40 224.40 36.57 o -6 4 0 13.66 10.54 13.13 o -5 4 0 580.94 632.80 25.86 o -4 4 0 68.58 82.29 16.21 o -3 4 0 7.29 16.50 8.01 o -2 4 0 251.32 126.46 10.72 o -1 4 0 14084.07 13194.48 75.24 o 0 4 0 4.02 20.04 12.26 o 1 4 0 4619.42 4590.74 36.31 o 2 4 0 47107.57 45571.76 276.69 o 3 4 0 473.17 560.03 23.90 o 4 4 0 8.65 2.70 12.34 o 5 4 0 4714.30 5285.85 84.49 o 6 4 0 5698.25 5685.72 60.88 o 7 4 0 260.28 267.30 21.58 o 8 4 0 0.26 17.28 19.20 o 9 4 0 1562.73 1505.90 47.35 o 10 4 0 77.56 136.34 26.91 o 11 4 0 1482.66 1361.64 76.89 o 12 4 0 0.01 -12.47 49.03 o 13 4 0 0.28 -29.50 50.28 o -12 5 0 160.28 199.05 54.44 o -11 5 0 194.18 178.27 51.11 o -10 5 0 130.47 120.92 42.80 o -9 5 0 1885.15 1858.94 76.49 o -8 5 0 33.49 24.52 34.07 o -7 5 0 89.78 96.82 34.49 o -6 5 0 1314.26 1460.42 41.78 o -5 5 0 958.28 1073.98 27.18 o -4 5 0 2837.60 2645.73 72.17 o -3 5 0 2430.33 2293.44 28.70 o -2 5 0 3502.38 3436.81 31.60 o -1 5 0 859.74 940.32 18.51 o 0 5 0 20258.88 19996.89 106.61 o 1 5 0 78.46 120.27 10.58 o 2 5 0 1085.94 1029.49 21.37 o 3 5 0 2545.36 2469.93 31.75 o 4 5 0 1458.98 1467.91 33.05 o 5 5 0 7762.87 7947.05 69.38 o 6 5 0 132.85 121.81 19.32 o 7 5 0 1451.00 1660.37 41.28 o 8 5 0 1364.64 1399.31 43.19 o 9 5 0 0.12 -20.60 21.23 o 10 5 0 172.43 207.46 28.69 o 11 5 0 1.23 -6.23 40.31 o 12 5 0 47.45 52.36 45.71 o 13 5 0 492.96 494.52 65.24 o -12 6 0 2.50 2.91 53.19 o -11 6 0 0.32 16.21 43.22 o -10 6 0 2096.94 2014.41 83.14 o -9 6 0 39.92 84.35 41.97 o -8 6 0 489.92 529.86 55.69 o -7 6 0 1457.39 1379.61 61.94 o -6 6 0 624.35 624.27 26.52 o -5 6 0 391.72 385.57 23.78 o -4 6 0 1541.69 1399.83 28.89 o -3 6 0 14702.32 14401.27 112.62 o -2 6 0 88.33 31.54 9.38 o -1 6 0 25.28 6.25 8.37 o 0 6 0 2351.09 2900.77 282.31 o 1 6 0 9566.04 9713.40 92.32 o 2 6 0 574.89 441.71 18.86 o 3 6 0 0.54 -11.60 10.53 o 4 6 0 4238.08 4457.48 72.00 o 5 6 0 1.58 -0.10 16.58 o 6 6 0 1095.46 1067.51 35.56 o 7 6 0 46.00 96.95 20.17 o 8 6 0 2932.00 3101.23 73.39 o 9 6 0 583.78 532.24 38.48 o 10 6 0 196.79 227.79 28.72 o 11 6 0 2481.90 2678.85 90.63 o 12 6 0 74.05 118.84 51.11 o 13 6 0 162.45 189.90 57.34 o -12 7 0 11.99 16.21 50.28 o -11 7 0 3.79 10.80 44.88 o -10 7 0 277.18 300.03 54.02 o -9 7 0 4230.75 4232.20 103.96 o -8 7 0 206.07 277.59 43.63 o -7 7 0 152.62 113.03 34.07 o -6 7 0 178.96 195.72 34.91 o -5 7 0 52.50 88.27 13.84 o -4 7 0 5281.69 5026.31 111.34 o -3 7 0 7535.76 7222.63 98.54 o -2 7 0 12369.59 12853.65 115.89 o -1 7 0 319.50 288.91 18.99 o 0 7 0 4954.11 5194.67 43.65 o 1 7 0 337.29 550.63 20.43 o 2 7 0 206.08 206.90 32.21 o 3 7 0 2534.80 2703.82 38.90 o 4 7 0 272.82 310.25 21.42 o 5 7 0 2423.24 2530.86 44.00 o 6 7 0 910.99 893.80 35.55 o 7 7 0 41.04 39.42 18.19 o 8 7 0 459.70 443.03 35.99 o 9 7 0 2.95 12.43 23.00 o 10 7 0 199.44 177.12 29.10 o 11 7 0 12.95 5.64 28.10 o 12 7 0 245.30 260.55 56.10 o 13 7 0 305.15 322.88 59.01 o -11 8 0 37.85 73.13 53.19 o -10 8 0 90.97 101.39 44.05 o -9 8 0 2653.65 2599.58 86.89 o -8 8 0 34.32 20.78 36.15 o -7 8 0 196.70 230.21 39.48 o -6 8 0 694.02 728.13 56.11 o -5 8 0 2400.21 2407.31 82.54 o -4 8 0 4864.79 5131.54 70.95 o -3 8 0 1358.26 1388.01 31.96 o -2 8 0 2219.14 2074.49 34.64 o -1 8 0 1737.10 1608.80 58.01 o 0 8 0 1373.00 1216.97 53.22 o 1 8 0 2607.32 2705.22 34.93 o 2 8 0 147.45 132.29 22.02 o 3 8 0 843.66 900.93 32.34 o 4 8 0 36398.08 37329.86 383.98 o 5 8 0 3189.03 3477.49 50.63 o 6 8 0 350.31 333.88 26.62 o 7 8 0 755.45 779.14 36.72 o 8 8 0 40.68 47.39 21.89 o 9 8 0 28.70 -21.21 23.16 o 10 8 0 248.66 217.32 30.26 o 11 8 0 1.58 14.34 27.62 o 12 8 0 101.48 106.79 52.36 o 13 8 0 4.34 -43.22 52.77 o -11 9 0 565.75 578.06 76.46 o -10 9 0 24.80 -5.82 44.88 o -9 9 0 473.34 499.51 67.74 o -8 9 0 778.76 775.50 67.74 o -7 9 0 0.25 14.96 36.57 o -6 9 0 300.26 262.63 35.74 o -5 9 0 2789.13 2719.36 38.23 o -4 9 0 4314.91 4120.79 94.23 o -3 9 0 12424.32 12525.10 159.96 o -2 9 0 2157.21 2172.73 36.74 o -1 9 0 11173.86 11839.92 79.50 o 0 9 0 661.77 637.25 28.16 o 1 9 0 1501.39 1500.66 34.24 o 2 9 0 96.12 58.32 19.95 o 3 9 0 5.48 -8.99 16.44 o 4 9 0 2490.12 2383.80 44.23 o 5 9 0 4833.89 5250.86 61.19 o 6 9 0 3764.32 3846.76 54.88 o 7 9 0 162.09 149.02 29.50 o 8 9 0 408.45 440.91 36.73 o 9 9 0 311.47 279.12 30.03 o 10 9 0 34.37 44.05 27.44 o 11 9 0 385.13 360.07 36.36 o 12 9 0 5.25 -3.32 44.88 o -11 10 0 83.58 97.65 50.28 o -10 10 0 304.15 362.78 57.76 o -9 10 0 197.76 179.93 45.71 o -8 10 0 1441.46 1418.18 73.57 o -7 10 0 0.36 1.66 35.32 o -6 10 0 1174.98 1075.67 58.19 o -5 10 0 232.61 219.83 32.00 o -4 10 0 2424.22 2266.32 55.92 o -3 10 0 63.77 94.41 15.96 o -2 10 0 2436.07 2282.06 70.90 o -1 10 0 3020.03 2984.90 71.96 o 0 10 0 1964.08 2053.74 37.88 o 1 10 0 515.93 450.18 29.35 o 2 10 0 954.07 948.61 44.06 o 3 10 0 12783.90 13493.03 128.08 o 4 10 0 2130.75 2325.87 42.90 o 5 10 0 0.14 16.11 17.74 o 6 10 0 2090.87 2099.85 45.21 o 7 10 0 408.67 452.01 36.44 o 8 10 0 91.40 81.13 25.42 o 9 10 0 87.87 102.38 26.73 o 10 10 0 12.60 0.37 26.73 o 11 10 0 158.84 117.46 31.14 o 12 10 0 66.16 65.01 33.60 o -10 11 0 100.50 93.91 48.20 o -9 11 0 182.67 192.40 47.37 o -8 11 0 43.18 36.15 41.55 o -7 11 0 1176.93 1086.45 63.59 o -6 11 0 922.89 853.25 56.11 o -5 11 0 981.39 1002.49 52.78 o -4 11 0 1861.16 1788.14 89.59 o -3 11 0 839.53 826.88 29.51 o -2 11 0 475.61 519.92 27.32 o -1 11 0 7628.57 7391.98 63.59 o 0 11 0 4876.95 5188.57 112.78 o 1 11 0 104.27 110.52 18.26 o 2 11 0 12614.06 12732.37 142.04 o 3 11 0 5883.93 5842.94 60.56 o 4 11 0 74.07 91.70 18.98 o 5 11 0 244.89 243.16 41.97 o 6 11 0 100.26 113.61 20.88 o 7 11 0 1513.98 1511.87 48.63 o 8 11 0 63.62 62.18 24.82 o 9 11 0 15.17 12.05 25.56 o 10 11 0 760.21 673.31 44.81 o 11 11 0 285.72 273.78 35.20 o 12 11 0 376.75 437.71 40.98 o -10 12 0 21.82 36.15 47.79 o -9 12 0 26.08 52.77 47.37 o -8 12 0 384.95 485.37 53.61 o -7 12 0 209.63 270.94 45.71 o -6 12 0 0.07 13.30 33.24 o -5 12 0 448.05 347.42 37.82 o -4 12 0 1044.82 1040.59 32.43 o -3 12 0 768.99 783.79 30.04 o -2 12 0 6.36 -6.10 14.95 o -1 12 0 1802.90 1895.35 91.05 o 0 12 0 1528.27 1513.46 35.61 o 1 12 0 275.98 264.27 23.29 o 2 12 0 7758.76 7864.28 164.91 o 3 12 0 1378.86 1393.35 36.95 o 4 12 0 190.06 236.05 65.87 o 5 12 0 3159.21 3413.32 53.23 o 6 12 0 7.17 17.31 20.07 o 7 12 0 321.76 355.85 28.76 o 8 12 0 2054.23 2067.06 52.59 o 9 12 0 5836.54 5830.31 80.10 o 10 12 0 105.21 84.52 30.25 o 11 12 0 43.82 32.97 31.70 o 12 12 0 387.62 455.59 42.44 o -10 13 0 5.93 8.31 49.03 o -9 13 0 1.04 2.91 43.63 o -8 13 0 502.46 467.51 54.02 o -7 13 0 176.81 213.59 42.80 o -6 13 0 134.78 116.35 36.98 o -5 13 0 156.11 144.61 34.49 o -4 13 0 581.03 501.61 45.71 o -3 13 0 33.61 15.39 16.80 o -2 13 0 330.34 382.16 29.07 o -1 13 0 94.27 77.22 17.39 o 0 13 0 440.12 468.54 28.36 o 1 13 0 262.76 359.61 29.36 o 2 13 0 86.14 76.98 17.95 o 3 13 0 555.58 551.81 32.13 o 4 13 0 374.46 320.70 32.62 o 5 13 0 302.59 313.45 26.39 o 6 13 0 181.29 171.00 24.26 o 7 13 0 19.06 27.28 24.65 o 8 13 0 3443.32 3457.22 64.23 o 9 13 0 828.00 800.65 45.09 o 10 13 0 0.07 -3.94 29.40 o 11 13 0 7.78 -14.03 30.85 o 12 13 0 239.26 287.39 39.52 o -9 14 0 37.53 33.24 45.71 o -8 14 0 371.87 401.84 52.36 o -7 14 0 8.03 60.25 40.31 o -6 14 0 4278.37 4082.94 93.15 o -5 14 0 169.30 170.37 36.98 o -4 14 0 190.86 156.66 33.66 o -3 14 0 20.01 33.74 19.04 o -2 14 0 29.74 15.37 17.77 o -1 14 0 470.97 488.46 30.16 o 0 14 0 1383.00 1303.97 46.97 o 1 14 0 46.71 41.62 18.04 o 2 14 0 420.87 494.42 38.03 o 3 14 0 220.88 235.90 26.18 o 4 14 0 1006.17 913.26 41.77 o 5 14 0 6.83 1.10 21.29 o 6 14 0 161.45 149.71 24.67 o 7 14 0 420.19 331.34 29.90 o 8 14 0 139.33 114.90 28.04 o 9 14 0 1236.69 1282.38 51.13 o 10 14 0 1.32 -4.65 28.89 o 11 14 0 256.56 303.79 38.92 o -9 15 0 80.52 145.44 52.77 o -8 15 0 280.66 347.82 51.94 o -7 15 0 4.87 13.30 37.81 o -6 15 0 989.65 1021.56 61.09 o -5 15 0 95.57 79.37 35.74 o -4 15 0 370.89 360.71 48.21 o -3 15 0 72.77 67.11 21.29 o -2 15 0 1514.01 1385.62 38.79 o -1 15 0 5.55 10.05 20.36 o 0 15 0 435.29 459.92 32.30 o 1 15 0 3865.97 3834.27 66.13 o 2 15 0 571.93 606.78 34.05 o 3 15 0 317.45 277.48 39.06 o 4 15 0 93.09 113.33 22.94 o 5 15 0 3355.14 3169.32 56.31 o 6 15 0 0.01 -4.28 24.28 o 7 15 0 496.72 481.87 38.35 o 8 15 0 817.48 765.99 44.53 o 9 15 0 93.88 101.93 30.82 o 10 15 0 105.55 99.99 33.23 o 11 15 0 78.30 96.94 35.08 o -8 16 0 480.14 477.07 63.58 o -7 16 0 353.95 371.51 49.45 o -6 16 0 466.03 444.24 54.85 o -5 16 0 191.20 265.12 41.97 o -4 16 0 65.26 69.81 34.91 o -3 16 0 1188.11 1161.69 56.94 o -2 16 0 67.78 54.66 21.29 o -1 16 0 758.76 657.08 41.77 o 0 16 0 489.07 531.52 65.87 o 1 16 0 131.79 108.04 34.91 o 2 16 0 178.30 176.67 23.66 o 3 16 0 359.29 391.79 32.31 o 4 16 0 166.42 173.84 25.89 o 5 16 0 18.77 36.40 23.86 o 6 16 0 175.10 133.28 26.45 o 7 16 0 568.76 640.24 43.06 o 8 16 0 436.35 388.44 74.39 o 9 16 0 807.36 874.85 49.70 o 10 16 0 58.00 67.58 32.89 o 11 16 0 140.72 129.03 37.82 o -8 17 0 34.93 57.76 46.54 o -7 17 0 282.75 296.29 49.45 o -6 17 0 88.88 54.44 41.14 o -5 17 0 39.53 39.89 37.40 o -4 17 0 1014.06 1012.42 61.93 o -3 17 0 1048.72 1079.35 58.60 o -2 17 0 286.08 267.27 26.30 o -1 17 0 160.17 169.25 24.07 o 0 17 0 1365.21 1445.12 41.90 o 1 17 0 681.25 650.40 58.60 o 2 17 0 1935.39 1752.08 45.93 o 3 17 0 135.08 112.99 24.65 o 4 17 0 206.30 170.91 26.26 o 5 17 0 20.47 5.06 24.75 o 6 17 0 112.92 137.02 28.62 o 7 17 0 182.38 210.38 37.81 o 8 17 0 256.88 240.80 32.81 o 9 17 0 2.41 13.67 31.00 o 10 17 0 434.32 444.94 44.36 o -1 18 0 372.52 391.04 42.39 o 0 18 0 72.01 83.11 35.74 o 1 18 0 211.40 275.09 36.15 o 2 18 0 803.32 789.30 41.14 o 3 18 0 139.44 161.04 26.75 o 4 18 0 332.86 356.10 31.61 o 5 18 0 164.60 173.67 28.65 o 6 18 0 738.39 720.09 44.88 o 7 18 0 24.84 12.47 43.63 o 8 18 0 7.26 0.42 45.29 o 9 18 0 296.35 256.81 54.85 o 10 18 0 19.76 -6.65 53.60 o -1 19 0 1176.60 1241.46 65.67 o 0 19 0 2858.41 3083.65 87.31 o 1 19 0 49.09 71.06 38.23 o 2 19 0 125.20 131.73 41.97 o 3 19 0 1155.44 1162.49 73.15 o 4 19 0 334.98 329.95 50.28 o 5 19 0 328.50 325.38 50.70 o 6 19 0 895.93 792.54 69.82 o 7 19 0 418.88 389.38 57.76 o 8 19 0 9.71 -33.66 44.05 o 9 19 0 45.20 54.44 50.70 o -1 20 0 1161.90 1258.49 70.24 o 0 20 0 4.95 37.40 37.40 o 1 20 0 40.65 53.19 41.14 o 2 20 0 159.72 104.72 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