#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/17/2201795.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201795_Fobs loop_ _publ_author_name 'Jones, Peter G.' 'Hopf, Henning' 'Hartig, Thorsten' 'D\"oring, Detlev' _publ_section_title ; Bis(\h^5^-pentamethylcyclopentadienyl)[bis-\h^5^-syn-[2.2](4,7)indenophanyl]diruthenium(II) ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m85 _journal_page_last m86 _journal_volume 59 _journal_year 2003 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.410 _cell_angle_gamma 90.000 _cell_length_a 8.6470 _cell_length_b 13.6040 _cell_length_c 28.9590 _exptl_crystal_F_000 1552.00 _reflns_d_resolution_high 0.8408 _[local]_cod_data_source_file bt62333sup2.hkl _[local]_cod_data_source_block 3 #BEGIN Tags that were not found in dictionaries: _shelx_title ' ruth in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 365.22 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 92227.82 85371.70 205.23 o 3 0 0 198.35 286.90 31.95 o 4 0 0 37662.67 35237.02 195.90 o 5 0 0 6133.89 5654.81 98.10 o 6 0 0 11578.98 11474.31 152.63 o 7 0 0 1418.67 1338.52 84.44 o 8 0 0 8195.21 7540.93 167.31 o 9 0 0 5872.87 5267.78 158.77 o 10 0 0 127.90 169.64 81.03 o 2 1 0 860.28 1022.02 85.70 o 3 1 0 69522.77 68665.36 163.62 o 4 1 0 401.95 171.03 29.32 o 5 1 0 9871.63 9483.81 85.68 o 6 1 0 3004.52 2898.41 62.64 o 7 1 0 23741.42 23178.59 468.92 o 8 1 0 11361.53 11431.55 143.37 o 9 1 0 1285.06 1323.71 114.36 o 10 1 0 3083.71 2763.25 107.43 o 1 2 0 2875.74 3017.18 82.12 o 2 2 0 72406.25 74646.36 1324.13 o 3 2 0 21059.05 21155.63 342.97 o 4 2 0 10866.84 9784.48 108.19 o 5 2 0 5448.57 4681.31 65.53 o 6 2 0 12337.13 12019.97 199.12 o 7 2 0 13079.94 13479.05 138.39 o 8 2 0 4629.22 4687.10 98.60 o 9 2 0 5014.55 5238.94 115.52 o 10 2 0 169.10 82.71 82.22 o 1 3 0 73847.32 73606.13 939.38 o 2 3 0 20113.10 21911.07 512.41 o 3 3 0 9672.82 8554.98 65.63 o 4 3 0 4921.90 4650.91 111.52 o 5 3 0 9562.08 8929.76 87.83 o 6 3 0 11148.43 11648.48 298.83 o 7 3 0 6056.84 6256.59 163.49 o 8 3 0 4073.27 4365.57 227.67 o 9 3 0 1785.40 1878.76 80.93 o 10 3 0 3694.81 3699.62 113.05 o 0 4 0 67744.21 71805.87 148.30 o 1 4 0 2406.64 2938.40 68.55 o 2 4 0 34067.28 33920.95 532.33 o 3 4 0 11628.25 12264.51 189.99 o 4 4 0 3329.51 2573.71 116.98 o 5 4 0 4654.59 4605.30 69.81 o 6 4 0 7473.01 7733.40 115.59 o 7 4 0 2725.69 2910.64 84.19 o 8 4 0 2246.18 2296.81 99.99 o 9 4 0 3209.54 3399.85 102.16 o 1 5 0 25665.20 27209.39 339.36 o 2 5 0 423.74 439.00 27.35 o 3 5 0 12004.75 11537.57 296.38 o 4 5 0 3377.85 3276.86 55.64 o 5 5 0 5265.23 5222.80 75.89 o 6 5 0 4713.34 4634.03 103.78 o 7 5 0 1217.41 1455.95 63.87 o 8 5 0 1470.10 1584.11 87.20 o 9 5 0 1181.87 1144.41 72.56 o 0 6 0 170.74 405.36 36.77 o 1 6 0 487.82 592.69 50.96 o 2 6 0 7921.57 7632.19 254.19 o 3 6 0 113.46 55.55 32.29 o 4 6 0 5196.07 5009.47 152.61 o 5 6 0 1582.72 1641.52 56.63 o 6 6 0 4175.75 4515.36 82.01 o 7 6 0 4283.28 4105.68 94.07 o 8 6 0 1608.52 1636.44 72.61 o 9 6 0 618.62 547.78 78.65 o 1 7 0 3517.01 3285.00 88.01 o 2 7 0 38.36 32.95 37.90 o 3 7 0 2321.21 2442.42 80.84 o 4 7 0 2113.99 2043.96 91.57 o 5 7 0 1498.92 1400.24 54.91 o 6 7 0 962.85 903.42 67.52 o 7 7 0 1210.66 1271.82 67.43 o 8 7 0 179.22 42.28 44.17 o 9 7 0 1066.05 1137.25 71.76 o 0 8 0 1753.51 1967.29 83.23 o 1 8 0 62.77 105.59 60.94 o 2 8 0 933.66 869.37 38.27 o 3 8 0 619.05 669.59 38.71 o 4 8 0 1894.14 1858.40 89.45 o 5 8 0 131.63 187.74 55.98 o 6 8 0 2045.03 2104.63 72.58 o 7 8 0 103.97 38.26 40.52 o 8 8 0 1175.09 1231.75 69.94 o 1 9 0 0.47 15.32 20.46 o 2 9 0 414.80 427.03 53.31 o 3 9 0 500.74 555.78 44.60 o 4 9 0 533.31 462.67 53.23 o 5 9 0 2125.14 2047.98 67.05 o 6 9 0 414.75 417.53 57.11 o 7 9 0 451.18 430.23 57.07 o 8 9 0 95.53 48.81 68.54 o 0 10 0 3599.28 3694.12 166.65 o 1 10 0 42.61 111.22 55.24 o 2 10 0 203.28 249.14 59.24 o 3 10 0 1026.27 1161.25 75.23 o 4 10 0 755.55 813.85 80.15 o 5 10 0 724.80 815.57 81.38 o 6 10 0 226.61 99.89 92.47 o 7 10 0 556.74 514.29 89.66 o 8 10 0 758.12 663.50 89.95 o 1 11 0 3202.45 3271.45 102.16 o 2 11 0 49.23 14.85 29.69 o 3 11 0 1328.01 1352.50 88.57 o 4 11 0 1246.39 1391.16 86.08 o 5 11 0 137.68 54.25 108.50 o 6 11 0 991.86 856.77 95.75 o 7 11 0 212.04 172.80 87.59 o 0 12 0 3195.33 3216.59 102.44 o 1 12 0 80.10 65.90 95.80 o 2 12 0 1611.38 1769.43 86.95 o 3 12 0 108.75 120.95 78.13 o 4 12 0 1057.22 1109.86 83.57 o 5 12 0 1040.47 1167.41 91.88 o 6 12 0 0.54 99.29 87.79 o 1 13 0 3843.60 3990.09 120.43 o 2 13 0 1038.21 970.76 86.29 o 3 13 0 980.35 992.77 81.57 o 4 13 0 1809.58 1910.59 95.62 o 5 13 0 7.54 16.43 32.87 o 6 13 0 1413.09 1457.81 101.91 o 0 14 0 1898.78 1896.58 91.77 o 1 14 0 1.95 15.71 31.42 o 2 14 0 1454.92 1639.37 87.76 o 3 14 0 1160.79 1170.16 87.19 o 4 14 0 154.15 145.72 77.28 o 5 14 0 1469.02 1365.82 103.09 o 1 15 0 1282.63 1363.60 85.22 o 2 15 0 188.23 213.46 71.25 o 3 15 0 775.71 695.41 79.91 o 0 16 0 1150.53 1111.19 87.64 o 1 16 0 26.98 37.84 75.67 o -10 1 1 82.74 118.40 81.01 o -9 1 1 3.62 45.90 49.43 o -8 1 1 323.09 449.04 81.22 o -7 1 1 4985.48 5041.57 189.42 o -6 1 1 376.38 355.50 40.54 o -5 1 1 308.02 298.78 53.26 o -4 1 1 2026.90 1969.49 41.25 o -3 1 1 3043.08 3287.36 42.28 o -2 1 1 1046.27 1168.21 26.43 o 2 1 1 421.93 462.29 24.32 o 3 1 1 761.30 837.94 31.07 o 4 1 1 1213.67 1159.66 35.27 o 5 1 1 290.26 291.11 32.28 o 6 1 1 68.21 84.99 43.44 o 7 1 1 275.32 295.86 59.22 o 8 1 1 105.01 72.46 91.00 o 9 1 1 75.90 19.61 27.73 o 10 1 1 19.21 50.38 54.25 o -10 2 1 132.77 201.92 61.61 o -9 2 1 797.97 927.67 80.88 o -8 2 1 964.93 997.12 66.06 o -7 2 1 2300.14 2304.11 79.34 o -6 2 1 3324.67 3269.28 70.18 o -5 2 1 3232.77 3269.36 55.98 o -4 2 1 9035.41 9806.78 130.16 o -3 2 1 1540.11 1505.73 70.38 o -2 2 1 5496.47 5802.96 46.48 o -1 2 1 3049.73 3288.53 30.51 o 0 2 1 60629.34 59490.09 594.65 o 1 2 1 8627.70 9439.07 81.89 o 2 2 1 1005.93 994.84 51.17 o 3 2 1 197.96 177.21 24.43 o 4 2 1 3692.16 4293.96 56.25 o 5 2 1 2007.80 1936.55 48.09 o 6 2 1 72.58 108.44 47.30 o 7 2 1 514.87 494.19 55.94 o 8 2 1 7.48 18.53 26.21 o 9 2 1 109.37 53.01 73.91 o 10 2 1 110.98 228.85 63.52 o -10 3 1 1885.06 1812.40 103.30 o -9 3 1 646.19 742.51 83.24 o -8 3 1 8931.56 8883.03 130.39 o -7 3 1 5873.61 5798.84 98.87 o -6 3 1 9687.00 9923.75 110.26 o -5 3 1 4195.67 4162.71 82.21 o -4 3 1 317.79 235.84 31.05 o -3 3 1 8553.54 8905.19 140.14 o -2 3 1 1381.54 1514.74 30.09 o -1 3 1 6.54 50.57 58.62 o 0 3 1 690.17 785.72 16.59 o 1 3 1 50.91 49.62 28.29 o 2 3 1 1678.06 1860.32 48.48 o 3 3 1 2237.99 2258.25 48.16 o 4 3 1 171.20 154.10 30.01 o 5 3 1 848.35 892.24 100.43 o 6 3 1 2605.01 2543.49 66.18 o 7 3 1 268.19 205.21 56.74 o 8 3 1 3325.41 3143.72 88.70 o 9 3 1 230.59 288.41 61.18 o 10 3 1 35.93 22.97 32.45 o -9 4 1 5293.81 5555.96 129.35 o -8 4 1 511.06 566.65 57.83 o -7 4 1 13739.56 13986.97 144.33 o -6 4 1 3034.53 3271.12 70.20 o -5 4 1 6606.22 6587.97 80.04 o -4 4 1 304.49 96.41 30.35 o -3 4 1 13400.30 14064.43 280.83 o -2 4 1 19848.88 19457.43 412.99 o -1 4 1 2979.00 3271.72 55.07 o 0 4 1 19628.04 21125.99 136.30 o 1 4 1 735.45 762.54 26.43 o 2 4 1 6990.14 6887.78 208.30 o 3 4 1 12125.40 12557.33 220.39 o 4 4 1 19.15 9.24 13.07 o 5 4 1 4965.96 5061.85 78.53 o 6 4 1 35.34 56.35 72.12 o 7 4 1 1946.22 1922.76 71.55 o 8 4 1 49.87 46.09 49.14 o 9 4 1 124.72 56.61 55.32 o -9 5 1 276.01 293.66 62.07 o -8 5 1 6457.89 6677.05 117.68 o -7 5 1 1650.97 1800.52 67.08 o -6 5 1 15524.17 15192.66 137.30 o -5 5 1 4584.80 4533.95 70.23 o -4 5 1 1079.44 910.24 37.89 o -3 5 1 2553.06 1885.80 42.82 o -2 5 1 78.48 79.22 30.30 o -1 5 1 30439.65 31858.73 944.09 o 0 5 1 129.40 173.30 25.28 o 1 5 1 20616.73 21965.88 340.56 o 2 5 1 1191.01 1290.80 39.65 o 3 5 1 789.57 677.05 53.74 o 4 5 1 4661.86 4458.24 62.05 o 5 5 1 1609.19 1694.69 51.99 o 6 5 1 2192.75 2399.72 66.03 o 7 5 1 84.69 24.74 32.34 o 8 5 1 869.54 871.04 66.24 o 9 5 1 302.93 268.78 81.85 o -9 6 1 7720.46 7414.61 192.62 o -8 6 1 506.28 560.18 57.58 o -7 6 1 12625.69 12590.06 155.36 o -6 6 1 1022.23 1060.78 86.48 o -5 6 1 10303.36 10896.73 209.46 o -4 6 1 10331.15 9824.62 90.72 o -3 6 1 1109.75 912.45 34.65 o -2 6 1 14646.46 13428.35 466.21 o -1 6 1 1084.95 1259.09 34.99 o 0 6 1 18089.84 17971.61 66.58 o 1 6 1 89.89 177.81 27.79 o 2 6 1 6903.70 6874.30 171.37 o 3 6 1 1809.75 1851.19 92.27 o 4 6 1 1770.46 1489.98 47.65 o 5 6 1 3380.97 3611.36 135.56 o 6 6 1 88.85 44.70 62.94 o 7 6 1 1533.26 1527.96 69.19 o 8 6 1 106.35 84.94 82.52 o 9 6 1 273.78 219.33 68.87 o -9 7 1 228.59 276.81 81.20 o -8 7 1 8913.97 9055.89 137.74 o -7 7 1 627.62 785.82 59.02 o -6 7 1 18800.10 19339.13 162.80 o -5 7 1 3693.12 3987.62 75.71 o -4 7 1 5000.43 5078.00 139.40 o -3 7 1 12215.06 11653.78 138.68 o -2 7 1 63.93 71.69 34.80 o -1 7 1 11143.89 10330.61 490.64 o 0 7 1 133.59 150.91 22.21 o 1 7 1 7376.82 6673.02 249.23 o 2 7 1 1836.44 1767.22 42.62 o 3 7 1 4246.37 4119.72 167.52 o 4 7 1 864.08 879.74 43.56 o 5 7 1 1009.77 1076.87 50.74 o 6 7 1 3473.95 3614.89 188.51 o 7 7 1 194.66 223.16 61.44 o 8 7 1 820.23 812.79 209.09 o 9 7 1 44.87 66.80 61.91 o -8 8 1 595.90 731.32 152.19 o -7 8 1 12995.44 12882.58 153.01 o -6 8 1 2156.15 2416.14 71.15 o -5 8 1 9310.74 9644.88 112.18 o -4 8 1 4177.17 4455.34 74.81 o -3 8 1 3674.97 3600.76 62.14 o -2 8 1 10073.32 9901.32 219.77 o -1 8 1 434.35 523.48 38.13 o 0 8 1 6118.20 5441.35 136.61 o 1 8 1 37.13 26.83 30.89 o 2 8 1 6901.94 6828.40 208.98 o 3 8 1 1134.18 1110.90 45.38 o 4 8 1 719.57 791.90 106.30 o 5 8 1 1592.01 1653.68 58.82 o 6 8 1 1091.26 1101.26 60.23 o 7 8 1 1307.33 1305.63 68.70 o 8 8 1 29.95 27.25 35.89 o -8 9 1 4096.67 4238.74 104.37 o -7 9 1 982.44 1016.21 64.67 o -6 9 1 8081.36 8549.36 120.05 o -5 9 1 1539.95 1658.25 66.96 o -4 9 1 12176.80 12121.12 433.00 o -3 9 1 10459.48 10692.58 399.62 o -2 9 1 312.07 374.29 35.21 o -1 9 1 16436.34 16772.54 920.13 o 0 9 1 728.76 673.04 29.22 o 1 9 1 9859.09 10026.27 479.31 o 2 9 1 140.96 224.61 36.81 o 3 9 1 2302.25 2332.21 140.95 o 4 9 1 1879.85 1954.38 105.40 o 5 9 1 1072.64 968.61 56.97 o 6 9 1 841.44 887.50 59.79 o 7 9 1 27.69 27.46 33.76 o 8 9 1 92.73 29.51 37.02 o -8 10 1 757.84 737.85 85.59 o -7 10 1 4020.55 4327.81 141.27 o -6 10 1 1311.50 1577.40 94.85 o -5 10 1 6102.93 6578.64 146.50 o -4 10 1 12587.96 13007.87 185.40 o -3 10 1 1062.25 1136.09 70.35 o -2 10 1 10884.07 11698.97 158.46 o -1 10 1 2596.39 2740.52 88.25 o 0 10 1 10000.13 9590.66 267.72 o 1 10 1 1227.96 1140.83 69.82 o 2 10 1 792.07 879.24 66.05 o 3 10 1 2549.94 2902.54 97.31 o 4 10 1 5372.63 5411.50 129.92 o 5 10 1 837.60 872.11 81.20 o 6 10 1 864.23 897.78 89.00 o 7 10 1 36.03 17.51 35.02 o 8 10 1 248.98 239.11 79.44 o -7 11 1 395.46 365.41 87.47 o -6 11 1 3320.34 3402.45 124.09 o -5 11 1 1865.88 1673.68 98.52 o -4 11 1 4798.70 5115.95 132.06 o -3 11 1 12541.53 12121.67 178.97 o -2 11 1 2701.34 2809.23 99.99 o -1 11 1 10319.30 10790.44 158.44 o 0 11 1 3498.45 3529.86 72.93 o 1 11 1 2238.85 2692.40 94.76 o 2 11 1 1991.97 1985.88 88.54 o 3 11 1 2172.87 2335.41 93.11 o 4 11 1 504.08 324.07 83.09 o 5 11 1 1029.74 1004.19 86.49 o 6 11 1 9.80 18.44 36.89 o 7 11 1 609.04 574.68 87.56 o -6 12 1 188.43 18.36 36.72 o -5 12 1 2872.66 2906.86 114.69 o -4 12 1 1231.25 1183.24 88.36 o -3 12 1 3355.05 3366.25 110.62 o -2 12 1 5181.15 5323.28 127.39 o -1 12 1 2789.04 3281.79 104.62 o 0 12 1 3485.17 3484.28 158.07 o 1 12 1 3114.41 3372.08 109.55 o 2 12 1 1620.29 1802.51 88.61 o 3 12 1 1851.31 1794.85 92.68 o 4 12 1 793.29 918.95 79.70 o 5 12 1 574.72 671.80 82.71 o 6 12 1 1726.11 1686.84 104.68 o -6 13 1 2181.97 2209.15 112.25 o -5 13 1 124.67 124.06 80.25 o -4 13 1 2193.04 2166.90 97.16 o -3 13 1 52.03 70.04 93.21 o -2 13 1 3095.68 3277.19 110.29 o -1 13 1 3011.54 3002.86 111.07 o 0 13 1 1469.04 1598.20 62.07 o 1 13 1 494.02 539.63 76.46 o 2 13 1 4392.10 4635.44 128.44 o 3 13 1 1727.37 1742.52 90.48 o 4 13 1 633.53 774.27 84.32 o 5 13 1 895.39 1054.41 83.41 o 6 13 1 1139.33 1083.94 102.41 o -5 14 1 2025.48 1969.81 106.89 o -4 14 1 113.75 121.39 75.40 o -3 14 1 1529.83 1417.48 89.16 o -2 14 1 180.27 231.72 74.85 o -1 14 1 2197.85 2216.70 103.94 o 0 14 1 240.76 275.54 50.71 o 1 14 1 3240.48 3242.82 114.28 o 2 14 1 882.04 1018.23 78.77 o 3 14 1 1922.61 1912.34 100.05 o 4 14 1 926.16 862.06 86.03 o 5 14 1 1740.42 1680.25 106.94 o -3 15 1 0.08 15.79 31.58 o -2 15 1 1875.50 1829.02 97.85 o -1 15 1 0.28 15.79 31.58 o 0 15 1 2393.75 2422.87 75.43 o 1 15 1 57.34 79.58 85.40 o 2 15 1 3232.31 3256.55 115.67 o 3 15 1 485.53 446.16 73.76 o -1 16 1 2312.99 2135.26 105.72 o 0 16 1 45.45 31.01 31.56 o 1 16 1 2644.81 2774.24 114.16 o -10 0 2 49.82 81.74 101.25 o -9 0 2 4811.17 4597.26 155.12 o -8 0 2 2026.45 1927.29 102.20 o -7 0 2 2902.74 2806.04 109.50 o -6 0 2 3306.32 3256.55 89.33 o -5 0 2 8270.36 7698.59 109.17 o -4 0 2 2149.19 2309.30 59.79 o -3 0 2 5375.43 4793.90 66.70 o -2 0 2 7969.46 7600.29 68.23 o 2 0 2 32.76 133.63 31.32 o 3 0 2 13568.47 12374.87 102.70 o 4 0 2 2415.05 1862.64 58.90 o 5 0 2 1.81 9.61 19.23 o 6 0 2 4097.22 4375.48 102.22 o 7 0 2 1410.44 1456.28 85.01 o 8 0 2 4214.31 3969.83 135.30 o 9 0 2 4360.75 4306.72 146.19 o 10 0 2 1255.19 1298.44 113.54 o -10 1 2 3704.66 3525.99 105.22 o -9 1 2 113.14 139.03 65.04 o -8 1 2 10250.91 10337.92 136.34 o -7 1 2 5323.23 5522.22 94.89 o -6 1 2 2484.91 2413.91 114.81 o -5 1 2 3328.19 3333.33 55.69 o -4 1 2 1424.34 1373.08 76.14 o -3 1 2 649.30 643.99 31.51 o -2 1 2 1653.71 1644.81 37.84 o -1 1 2 153.72 179.24 46.65 o 1 1 2 525.24 521.24 26.34 o 2 1 2 1437.51 1451.73 28.35 o 3 1 2 5307.94 5263.24 49.92 o 4 1 2 102.45 148.38 28.52 o 5 1 2 98.62 99.88 41.46 o 6 1 2 520.94 415.99 43.38 o 7 1 2 5410.92 5528.55 94.94 o 8 1 2 1262.51 1452.60 117.39 o 9 1 2 1913.95 2033.07 83.12 o 10 1 2 1737.26 1683.11 84.00 o -10 2 2 80.27 158.10 63.19 o -9 2 2 5477.15 5854.48 308.32 o -8 2 2 9.45 24.86 32.33 o -7 2 2 14154.65 14362.00 142.00 o -6 2 2 318.97 286.15 43.08 o -5 2 2 2393.93 2410.27 50.51 o -4 2 2 731.96 626.87 34.43 o -3 2 2 3096.29 3019.34 41.71 o -2 2 2 13323.18 13308.97 191.00 o -1 2 2 806.81 864.18 40.05 o 0 2 2 4979.27 5587.30 73.93 o 1 2 2 0.74 30.60 26.12 o 2 2 2 999.71 974.86 27.69 o 3 2 2 1053.99 1079.10 71.96 o 4 2 2 4561.26 4114.65 55.06 o 5 2 2 1604.27 1633.73 93.08 o 6 2 2 6499.43 6560.31 99.97 o 7 2 2 258.40 256.08 50.68 o 8 2 2 3071.14 3158.80 87.73 o 9 2 2 2847.18 2746.67 98.74 o 10 2 2 1008.74 1055.14 79.07 o -10 3 2 4714.99 4580.52 124.23 o -9 3 2 12.64 18.10 25.59 o -8 3 2 5459.57 5560.99 112.15 o -7 3 2 39.87 16.91 23.90 o -6 3 2 7356.91 7625.22 112.16 o -5 3 2 30.65 10.50 14.84 o -4 3 2 1012.25 860.84 35.58 o -3 3 2 1940.40 2433.36 43.55 o -2 3 2 928.84 970.16 27.16 o -1 3 2 3605.76 3773.13 37.91 o 0 3 2 1267.09 1376.68 19.45 o 1 3 2 200.12 228.38 55.17 o 2 3 2 4500.62 4475.97 129.51 o 3 3 2 3258.07 3368.74 45.43 o 4 3 2 114.52 84.73 40.42 o 5 3 2 2630.04 2816.35 96.33 o 6 3 2 2240.56 2149.37 59.52 o 7 3 2 1971.03 2077.31 71.31 o 8 3 2 1242.55 1471.30 69.57 o 9 3 2 1039.69 1034.43 122.41 o 10 3 2 2146.15 2243.02 89.75 o -9 4 2 4442.96 4494.55 111.31 o -8 4 2 42.44 17.09 24.17 o -7 4 2 2421.47 2500.54 78.01 o -6 4 2 364.09 398.05 46.33 o -5 4 2 4361.11 4297.00 66.96 o -4 4 2 589.71 691.59 33.76 o -3 4 2 765.91 648.22 32.40 o -2 4 2 693.46 736.03 29.25 o -1 4 2 6089.09 6312.62 50.16 o 0 4 2 4076.41 4070.71 29.28 o 1 4 2 2792.59 2866.44 79.50 o 2 4 2 3612.95 3626.56 119.07 o 3 4 2 1014.42 889.60 79.51 o 4 4 2 1085.80 1135.26 38.49 o 5 4 2 636.32 707.38 39.81 o 6 4 2 661.33 679.41 88.29 o 7 4 2 3254.82 3281.92 92.48 o 8 4 2 231.09 285.18 60.02 o 9 4 2 1871.39 2047.82 83.47 o -9 5 2 828.87 889.16 68.45 o -8 5 2 1741.55 1854.57 100.35 o -7 5 2 1697.02 1649.69 67.14 o -6 5 2 3132.53 3006.16 73.14 o -5 5 2 405.38 417.78 42.26 o -4 5 2 2899.41 2738.18 56.18 o -3 5 2 16.80 58.73 66.85 o -2 5 2 3124.23 3187.92 45.26 o -1 5 2 853.23 1014.37 47.27 o 0 5 2 5169.89 5136.25 81.59 o 1 5 2 2844.35 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