#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2201819.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201819_Fobs loop_ _publ_author_name 'Nockemann, Peter' 'Meyer, Gerd' _publ_section_title ; Bis(tetrabutylammonium) decaiodotetramercurate(II), (Bu~4~N)~2~[Hg~4~I~10~] ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m236 _journal_page_last m238 _journal_volume 59 _journal_year 2003 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 114.327 _cell_angle_beta 104.183 _cell_angle_gamma 90.178 _cell_length_a 11.6809 _cell_length_b 15.7701 _cell_length_c 18.2876 _exptl_crystal_F_000 2256.00 _reflns_d_resolution_high 0.8107 _[local]_cod_data_source_file bt6259Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' BUI31 P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 985.88 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 40475.13 37986.07 2385.68 o 2 0 0 91499.24 85913.87 2872.35 o 3 0 0 388.45 1614.81 1249.83 o 4 0 0 4690.63 4156.43 1081.95 o 5 0 0 36374.41 32708.29 1989.02 o 6 0 0 222.89 160.20 1346.56 o 7 0 0 25565.65 25031.60 1676.56 o 8 0 0 973.05 1032.78 925.00 o 9 0 0 49756.64 50463.33 1908.92 o 10 0 0 4802.56 4596.78 944.93 o 11 0 0 1348.60 1558.73 1123.83 o 12 0 0 49.04 -362.75 1061.66 o 13 0 0 1743.85 2102.69 1193.32 o -13 1 0 4947.81 4501.77 1194.21 o -12 1 0 14770.11 14797.10 1180.18 o -11 1 0 716.35 387.34 1034.28 o -10 1 0 1218.88 1656.78 946.23 o -9 1 0 20022.86 19795.35 1066.84 o -8 1 0 1100.85 1977.34 976.79 o -7 1 0 370.95 -611.77 896.02 o -6 1 0 22794.74 22657.64 997.86 o -5 1 0 1028.78 1354.69 933.47 o -4 1 0 39.87 -197.48 1104.50 o -3 1 0 9289.20 9016.01 1154.09 o -2 1 0 15840.58 15663.80 1184.53 o -1 1 0 468339.38 505600.97 15336.95 o 1 1 0 617610.75 776614.81 17200.54 o 2 1 0 2443.79 1780.37 1454.70 o 3 1 0 4816.76 4552.77 1258.18 o 4 1 0 11.58 165.60 1049.56 o 5 1 0 5284.67 5096.39 1013.67 o 6 1 0 130516.56 119660.70 4676.47 o 7 1 0 12418.46 12235.69 1234.61 o 8 1 0 40998.97 41895.56 4888.88 o 9 1 0 1901.75 2145.87 1004.96 o 10 1 0 15310.33 16211.00 1024.95 o 11 1 0 3663.70 3804.23 1057.78 o 12 1 0 884.95 1235.10 1201.14 o 13 1 0 1256.77 1629.72 1182.98 o -13 2 0 7100.32 7399.81 1280.35 o -12 2 0 16688.98 17619.65 1179.35 o -11 2 0 9884.21 9704.12 1110.16 o -10 2 0 1924.85 2340.86 1020.37 o -9 2 0 956.62 1213.42 1006.12 o -8 2 0 4670.38 5250.14 1004.75 o -7 2 0 9233.70 10541.19 1102.17 o -6 2 0 147.88 812.99 1005.96 o -5 2 0 7057.35 7426.03 1207.32 o -4 2 0 37535.77 35021.90 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114904.66 2144.74 o 0 3 0 868.20 28.94 2040.28 o 1 3 0 128705.89 129331.52 2858.97 o 2 3 0 67314.41 69315.45 2431.96 o 3 3 0 91150.58 85839.57 4521.65 o 4 3 0 166.15 418.03 1129.95 o 5 3 0 14663.82 13837.35 1083.17 o 6 3 0 6332.73 6132.33 1145.33 o 7 3 0 56.81 132.34 965.60 o 8 3 0 5826.86 5133.11 1016.74 o 9 3 0 606.82 854.78 990.72 o 10 3 0 3499.07 3605.44 962.57 o 11 3 0 2623.49 3306.38 1222.11 o 12 3 0 5608.15 5294.38 1147.41 o 13 3 0 3818.91 5522.61 1209.12 o -13 4 0 7979.15 8454.68 1352.46 o -12 4 0 12856.29 15136.80 1295.98 o -11 4 0 3039.11 3708.07 1222.80 o -10 4 0 138.86 -449.59 1222.45 o -9 4 0 6407.02 6587.69 1198.02 o -8 4 0 1001.44 920.12 1146.53 o -7 4 0 53.69 789.42 1401.31 o -6 4 0 3088.88 3323.76 1151.97 o -5 4 0 1736.22 2537.37 1109.75 o -4 4 0 126781.85 126819.45 9209.56 o -3 4 0 61387.33 62617.56 3618.04 o -2 4 0 207.50 -40.65 1561.48 o -1 4 0 1292.27 1464.46 1644.99 o 0 4 0 86858.20 84120.13 2363.15 o 1 4 0 34.93 -151.03 1975.20 o 2 4 0 190066.67 202969.59 6837.21 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2151.95 1552.94 1011.38 o 7 5 0 18399.70 18881.54 1041.77 o 8 5 0 13985.42 12879.37 1048.74 o 9 5 0 11042.15 11177.81 1024.25 o 10 5 0 2882.38 3382.41 1022.96 o 11 5 0 171.98 648.46 1089.09 o 12 5 0 1483.08 2800.68 1594.93 o -13 6 0 2016.04 1229.99 1417.82 o -12 6 0 3197.42 4310.65 1337.02 o -11 6 0 280.25 658.72 1354.75 o -10 6 0 696.92 2563.27 1275.10 o -9 6 0 2235.95 2333.30 1548.99 o -8 6 0 3498.88 3759.79 1345.43 o -7 6 0 2077.57 1988.89 1432.42 o -6 6 0 2743.30 3132.74 1086.86 o -5 6 0 45672.16 45701.99 3562.07 o -4 6 0 15090.10 15639.26 1326.28 o -3 6 0 31134.80 32095.51 3286.05 o -2 6 0 9144.53 9992.62 1415.54 o -1 6 0 10675.84 10410.05 1296.70 o 0 6 0 6719.96 7033.03 1157.40 o 1 6 0 45.14 356.64 1539.93 o 2 6 0 132585.98 131037.88 1806.78 o 3 6 0 114700.26 120071.39 2395.80 o 4 6 0 1011.00 333.37 1033.08 o 5 6 0 341.77 150.59 1010.34 o 6 6 0 2030.27 2969.75 1000.01 o 7 6 0 493.01 1777.59 1102.38 o 8 6 0 8474.80 7890.48 1028.50 o 9 6 0 24150.12 24362.90 1319.65 o 10 6 0 3219.58 4027.28 1099.11 o 11 6 0 18.47 527.55 1067.27 o 12 6 0 1034.13 368.32 1133.64 o -13 7 0 1102.75 -114.02 1488.16 o -12 7 0 100.77 385.84 1444.88 o -11 7 0 3263.70 4156.05 1423.84 o -10 7 0 3024.80 3824.13 1724.15 o -9 7 0 59.95 255.10 1247.06 o -8 7 0 13304.43 15128.04 1523.23 o -7 7 0 3895.02 3962.70 1315.11 o -6 7 0 74555.36 79663.39 5413.40 o -5 7 0 14897.62 15020.90 1337.73 o -4 7 0 8238.12 7350.29 1247.32 o -3 7 0 7941.15 9721.31 1584.59 o -2 7 0 18.90 618.74 1306.05 o -1 7 0 2001.81 4614.21 1169.63 o 0 7 0 1074.10 2296.59 1144.42 o 1 7 0 147535.27 144499.83 1969.90 o 2 7 0 342.24 892.97 1498.25 o 3 7 0 24579.81 25057.07 1602.24 o 4 7 0 27563.69 26647.13 1600.27 o 5 7 0 3858.67 4301.03 1037.23 o 6 7 0 174.18 1044.39 1070.68 o 7 7 0 3046.33 3944.05 1012.19 o 8 7 0 17608.81 20012.11 1319.58 o 9 7 0 6.00 550.66 1042.47 o 10 7 0 14.27 655.95 1058.91 o 11 7 0 139.44 -698.65 1164.69 o 12 7 0 488.20 1867.47 1152.75 o -13 8 0 552.60 614.81 1672.03 o -12 8 0 222.22 682.50 1544.30 o -11 8 0 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1226.70 o -1 13 0 2137.23 2502.37 968.30 o 0 13 0 3623.39 3456.96 824.99 o 1 13 0 3227.47 4004.66 826.54 o 2 13 0 865.57 949.28 830.03 o 3 13 0 44692.82 43854.81 1835.22 o 4 13 0 15220.19 14862.27 878.40 o 5 13 0 4677.52 5282.72 856.86 o 6 13 0 2193.41 1379.54 897.50 o 7 13 0 1275.85 -18.04 888.14 o 8 13 0 22.32 -184.14 1134.35 o -9 14 0 11853.03 12568.63 2038.23 o -8 14 0 26.48 595.22 1737.78 o -7 14 0 657.93 1430.33 1419.28 o -6 14 0 191.04 363.15 1600.80 o -5 14 0 23.95 269.03 1247.23 o -4 14 0 104.79 311.25 1184.66 o -3 14 0 24211.49 23013.32 1112.81 o -2 14 0 20684.78 20102.25 1029.46 o -1 14 0 3261.88 3170.98 964.25 o 0 14 0 35.87 298.00 961.38 o 1 14 0 328.62 294.42 852.11 o 2 14 0 17754.43 16870.32 983.43 o 3 14 0 5234.19 4962.25 867.00 o 4 14 0 10440.76 11478.61 882.68 o 5 14 0 353.57 367.57 874.08 o 6 14 0 1.78 128.36 826.01 o 7 14 0 621.38 828.73 1138.06 o -8 15 0 6715.18 5366.27 2910.80 o -7 15 0 1043.42 668.74 1517.14 o -6 15 0 1105.55 574.74 1039.97 o -5 15 0 94.53 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