#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/18/2201825.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201825_Fobs loop_ _publ_author_name 'Fl\"orke, Ulrich' 'Suwarso, Wahyudi Priyono' 'Gani, Ratna Layla' 'Krohn, Karsten' 'Wang, Si' _publ_section_title ; Dasypogalactone--methanol--water (1/2/1) ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o638 _journal_page_last o640 _journal_volume 59 _journal_year 2003 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 8.8977 _cell_length_b 19.5245 _cell_length_c 21.4452 _exptl_crystal_F_000 1408.00 _reflns_d_resolution_high 0.7801 _[local]_cod_data_source_file bt6265Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' C30 H54 O9, 2 CH3OH, H2O in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 224.92 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 50587.46 53407.43 1412.96 o 4 0 0 602.34 567.53 122.94 o 6 0 0 10.19 37.35 87.30 o 8 0 0 884.32 1165.53 261.52 o 10 0 0 31.49 219.53 437.41 o 1 1 0 3326.02 3486.72 114.47 o 2 1 0 26450.14 26431.16 503.67 o 3 1 0 178.03 300.77 59.47 o 4 1 0 43.12 93.77 51.95 o 5 1 0 446.88 452.53 89.50 o 6 1 0 139.69 188.85 79.47 o 7 1 0 0.37 -37.42 82.67 o 8 1 0 79.79 112.57 99.40 o 9 1 0 18.05 130.18 237.98 o 10 1 0 13.39 -142.49 268.21 o 11 1 0 8.98 -163.44 405.32 o 0 2 0 58.98 159.23 54.19 o 1 2 0 22.27 75.05 29.50 o 2 2 0 32989.95 34426.88 606.67 o 3 2 0 2085.85 2146.25 112.68 o 4 2 0 2989.65 2932.66 148.84 o 5 2 0 120.14 168.04 64.98 o 6 2 0 5.63 76.24 68.16 o 7 2 0 0.52 19.54 80.90 o 8 2 0 1531.93 1940.21 277.21 o 9 2 0 64.60 114.95 156.24 o 10 2 0 96.89 4.34 289.84 o 11 2 0 15.39 296.68 522.52 o 1 3 0 1.61 37.44 30.99 o 2 3 0 80.19 69.47 38.76 o 3 3 0 5317.54 5267.22 171.01 o 4 3 0 2585.12 2548.99 143.44 o 5 3 0 47.41 121.00 63.22 o 6 3 0 35.07 -25.39 63.17 o 7 3 0 277.48 358.01 102.56 o 8 3 0 7.04 -47.49 123.22 o 9 3 0 269.32 352.43 192.22 o 10 3 0 0.01 116.81 414.29 o 11 3 0 23.82 405.71 492.56 o 0 4 0 8623.22 9160.89 338.56 o 1 4 0 9137.26 8772.24 249.19 o 2 4 0 990.42 1052.97 78.34 o 3 4 0 1789.11 1943.35 103.37 o 4 4 0 279.93 222.59 62.70 o 5 4 0 45.76 60.83 61.75 o 6 4 0 647.26 583.46 110.79 o 7 4 0 22.24 53.15 99.71 o 8 4 0 135.24 78.29 141.58 o 9 4 0 2.94 149.22 182.19 o 10 4 0 26.88 23.68 438.33 o 11 4 0 44.46 440.84 459.33 o 1 5 0 598.20 692.42 74.73 o 2 5 0 228.68 374.40 55.16 o 3 5 0 2116.62 1979.33 103.85 o 4 5 0 1282.27 1389.66 113.81 o 5 5 0 1391.62 1335.94 140.41 o 6 5 0 14.76 40.52 62.92 o 7 5 0 53.13 123.42 113.37 o 8 5 0 613.40 451.22 175.75 o 9 5 0 18.67 66.70 194.30 o 10 5 0 7.35 142.63 228.23 o 11 5 0 34.35 196.88 472.49 o 0 6 0 21293.48 22047.25 618.10 o 1 6 0 2311.90 2155.12 106.49 o 2 6 0 8364.06 8425.15 200.13 o 3 6 0 4.85 24.76 36.10 o 4 6 0 732.74 748.16 86.42 o 5 6 0 827.55 899.76 116.84 o 6 6 0 47.85 82.24 99.16 o 7 6 0 204.60 125.86 113.27 o 8 6 0 77.42 -25.66 133.43 o 9 6 0 89.46 108.45 195.48 o 10 6 0 7.88 -79.32 200.49 o 11 6 0 33.31 78.39 448.93 o 1 7 0 698.54 851.03 102.17 o 2 7 0 2172.86 2143.03 148.60 o 3 7 0 2404.73 2318.01 117.67 o 4 7 0 1520.00 1676.93 117.25 o 5 7 0 5.64 45.13 56.87 o 6 7 0 51.94 122.38 102.37 o 7 7 0 1089.62 953.29 188.27 o 8 7 0 1344.86 1364.53 310.31 o 9 7 0 63.45 48.29 194.16 o 10 7 0 0.57 32.12 211.36 o 0 8 0 1141.86 1531.52 232.32 o 1 8 0 1333.04 1371.24 131.64 o 2 8 0 9492.93 9215.45 287.92 o 3 8 0 201.32 169.67 50.76 o 4 8 0 1058.54 1056.70 105.10 o 5 8 0 2312.10 2197.18 191.68 o 6 8 0 1009.45 933.15 181.98 o 7 8 0 1.99 -39.22 100.24 o 8 8 0 0.40 82.34 176.69 o 9 8 0 111.31 230.30 219.15 o 10 8 0 78.13 59.56 227.20 o 1 9 0 370.46 355.41 83.28 o 2 9 0 67.63 122.98 67.48 o 3 9 0 163.69 329.85 78.62 o 4 9 0 0.86 32.12 47.17 o 5 9 0 1241.05 1178.19 158.51 o 6 9 0 19.78 95.82 103.84 o 7 9 0 158.04 235.96 181.65 o 8 9 0 206.96 216.12 182.22 o 9 9 0 0.30 -0.72 190.83 o 10 9 0 184.29 111.43 231.63 o 0 10 0 1675.15 1344.91 249.13 o 1 10 0 678.23 676.50 110.81 o 2 10 0 240.59 211.25 69.33 o 3 10 0 2206.21 2307.44 176.07 o 4 10 0 384.23 281.19 109.66 o 5 10 0 0.78 -15.98 71.68 o 6 10 0 87.30 119.91 155.55 o 7 10 0 82.48 151.25 169.50 o 8 10 0 61.72 40.91 179.72 o 9 10 0 5.88 -8.72 200.64 o 10 10 0 33.60 -27.81 224.00 o 1 11 0 314.67 353.62 89.48 o 2 11 0 2.29 -5.20 53.32 o 3 11 0 165.43 226.12 82.49 o 4 11 0 162.17 232.30 94.63 o 5 11 0 272.48 291.83 101.58 o 6 11 0 154.26 188.50 122.60 o 7 11 0 28.46 12.19 179.36 o 8 11 0 445.67 374.42 247.58 o 9 11 0 131.08 10.49 190.82 o 10 11 0 156.97 221.15 255.58 o 0 12 0 226.95 346.90 170.60 o 1 12 0 509.66 506.03 111.46 o 2 12 0 389.05 426.75 91.50 o 3 12 0 131.27 109.46 79.59 o 4 12 0 328.74 251.53 97.14 o 5 12 0 91.66 141.34 120.43 o 6 12 0 631.96 685.77 264.93 o 7 12 0 212.82 58.35 152.56 o 8 12 0 0.02 57.22 186.81 o 9 12 0 20.81 -44.22 190.39 o 10 12 0 0.06 123.77 297.74 o 1 13 0 603.87 624.33 121.89 o 2 13 0 0.01 54.02 68.27 o 3 13 0 0.30 39.75 82.84 o 4 13 0 740.67 828.44 155.63 o 5 13 0 13.74 -23.61 143.61 o 6 13 0 618.72 412.71 217.73 o 7 13 0 15.96 97.04 165.35 o 8 13 0 0.62 53.07 194.51 o 9 13 0 18.08 -180.76 196.65 o 0 14 0 28.52 114.73 147.66 o 1 14 0 251.94 375.94 108.92 o 2 14 0 455.11 537.77 112.30 o 3 14 0 165.73 234.17 99.23 o 4 14 0 91.01 154.37 129.59 o 5 14 0 2.11 47.29 161.77 o 6 14 0 68.44 122.14 184.65 o 7 14 0 27.79 110.24 151.79 o 8 14 0 1.71 215.51 223.09 o 9 14 0 15.10 74.37 240.38 o 1 15 0 1141.77 1168.29 183.58 o 2 15 0 33.87 102.88 81.38 o 3 15 0 869.34 764.67 149.68 o 4 15 0 25.67 27.93 144.41 o 5 15 0 71.22 -15.23 165.04 o 6 15 0 123.93 306.28 216.65 o 7 15 0 173.67 149.54 166.14 o 8 15 0 43.93 142.43 197.88 o 9 15 0 4.00 -101.69 222.88 o 0 16 0 668.96 520.37 252.45 o 1 16 0 192.27 137.05 141.13 o 2 16 0 111.01 129.69 88.53 o 3 16 0 1.04 33.39 161.33 o 4 16 0 77.17 105.05 172.08 o 5 16 0 54.68 72.99 171.11 o 6 16 0 6.66 171.48 201.06 o 7 16 0 77.03 97.52 198.42 o 8 16 0 1.47 -18.69 205.77 o 1 17 0 107.59 159.36 172.84 o 2 17 0 1.88 -40.24 97.93 o 3 17 0 204.38 47.61 167.24 o 4 17 0 7.81 61.79 182.57 o 5 17 0 36.73 99.85 199.50 o 6 17 0 0.69 15.38 202.08 o 7 17 0 46.27 -179.24 204.58 o 8 17 0 15.21 124.18 239.17 o 0 18 0 97.12 -118.52 164.21 o 1 18 0 218.41 274.83 165.37 o 2 18 0 54.43 145.07 192.31 o 3 18 0 83.87 211.72 191.67 o 4 18 0 25.82 36.13 198.23 o 5 18 0 50.97 137.65 213.71 o 6 18 0 12.42 -8.23 224.43 o 7 18 0 0.01 -87.73 215.72 o 1 19 0 96.06 176.59 168.21 o 2 19 0 20.05 38.33 191.90 o 3 19 0 1.39 18.76 201.65 o 4 19 0 249.10 328.63 246.65 o 5 19 0 55.58 -1.30 217.00 o 6 19 0 33.93 132.15 240.84 o 7 19 0 10.40 177.83 271.63 o 0 20 0 140.36 163.70 200.01 o 1 20 0 206.06 73.22 201.82 o 2 20 0 11.34 98.50 215.47 o 3 20 0 12.51 -41.14 215.71 o 4 20 0 16.30 131.34 241.37 o 5 20 0 67.11 41.37 236.60 o 6 20 0 0.05 1.90 225.75 o 1 21 0 7.52 12.93 239.43 o 2 21 0 37.58 176.19 216.26 o 3 21 0 12.78 -54.87 205.19 o 4 21 0 21.00 142.48 262.17 o 5 21 0 33.68 -27.51 236.70 o 6 21 0 7.69 6.91 245.04 o 1 22 0 5.08 -15.19 252.05 o 2 22 0 177.71 367.42 265.00 o 3 22 0 28.97 -111.80 251.87 o 4 22 0 0.19 231.27 276.51 o 5 22 0 17.15 41.54 266.74 o 2 23 0 3.12 135.53 286.64 o 3 23 0 0.36 37.19 289.57 o 4 23 0 10.33 -41.46 265.14 o 3 24 0 60.95 173.55 296.36 o 1 0 1 2637.37 3581.66 156.39 o 2 0 1 1506.51 1627.36 89.11 o 3 0 1 5090.38 5108.22 166.74 o 4 0 1 3609.77 3598.92 162.69 o 5 0 1 1131.84 1238.14 136.20 o 6 0 1 19.63 32.35 64.68 o 7 0 1 6.78 -1.44 81.81 o 8 0 1 441.63 451.16 140.01 o 9 0 1 245.64 170.18 241.31 o 10 0 1 0.10 -113.54 274.81 o 11 0 1 0.21 73.65 427.89 o 0 1 1 25.50 21.26 11.02 o 1 1 1 17594.16 22431.34 665.47 o 2 1 1 29764.49 29624.49 400.68 o 3 1 1 1521.97 1459.30 73.03 o 4 1 1 6831.97 6732.04 154.52 o 5 1 1 130.29 234.96 50.66 o 6 1 1 1015.97 1081.84 100.17 o 7 1 1 197.32 224.59 70.31 o 8 1 1 51.56 5.26 83.76 o 9 1 1 74.62 8.82 129.07 o 10 1 1 164.87 160.90 213.94 o 11 1 1 11.69 466.32 541.02 o 0 2 1 306.51 364.61 41.86 o 1 2 1 3320.44 3450.23 88.59 o 2 2 1 7443.96 7621.26 129.87 o 3 2 1 598.25 708.37 58.90 o 4 2 1 3497.90 3442.89 112.65 o 5 2 1 46.35 63.92 39.35 o 6 2 1 83.80 51.11 48.38 o 7 2 1 191.38 249.22 72.15 o 8 2 1 67.21 70.35 99.00 o 9 2 1 2.37 -43.94 109.84 o 10 2 1 30.29 -148.22 215.34 o 11 2 1 22.90 24.51 310.63 o 0 3 1 524.87 581.74 72.55 o 1 3 1 19334.25 18874.81 268.72 o 2 3 1 324.00 398.04 40.48 o 3 3 1 1167.24 1109.65 65.03 o 4 3 1 1233.50 1278.53 82.12 o 5 3 1 1486.36 1488.00 99.19 o 6 3 1 0.65 22.21 45.10 o 7 3 1 514.29 601.05 100.61 o 8 3 1 88.61 75.65 98.71 o 9 3 1 347.94 321.54 135.27 o 10 3 1 10.99 39.43 236.23 o 11 3 1 22.77 254.77 322.49 o 0 4 1 61.61 21.54 38.53 o 1 4 1 14827.22 14425.98 228.46 o 2 4 1 876.10 952.27 55.04 o 3 4 1 57.07 91.53 28.69 o 4 4 1 969.42 1080.71 79.49 o 5 4 1 414.06 412.20 60.50 o 6 4 1 538.05 452.65 70.47 o 7 4 1 169.71 152.82 86.67 o 8 4 1 97.34 83.30 95.70 o 9 4 1 105.28 73.11 123.44 o 10 4 1 237.72 318.06 226.51 o 11 4 1 28.36 -69.97 303.14 o 0 5 1 83.31 83.23 49.77 o 1 5 1 3360.43 3265.09 77.57 o 2 5 1 4601.61 4747.45 98.58 o 3 5 1 304.53 324.58 39.40 o 4 5 1 91.76 147.53 37.38 o 5 5 1 182.85 174.21 46.45 o 6 5 1 809.35 841.34 100.81 o 7 5 1 412.29 464.25 111.73 o 8 5 1 170.68 112.31 95.70 o 9 5 1 95.72 115.99 129.92 o 10 5 1 36.89 26.55 159.00 o 11 5 1 0.21 135.98 298.34 o 0 6 1 90.76 117.59 52.78 o 1 6 1 1234.75 1339.57 72.80 o 2 6 1 3557.17 3570.82 101.34 o 3 6 1 316.50 329.26 41.95 o 4 6 1 1369.22 1533.77 80.36 o 5 6 1 306.39 376.09 60.47 o 6 6 1 1774.57 1751.62 138.60 o 7 6 1 786.29 761.34 127.22 o 8 6 1 90.86 95.42 109.68 o 9 6 1 144.75 77.46 136.52 o 10 6 1 95.01 251.25 172.69 o 11 6 1 6.01 124.41 310.96 o 0 7 1 3743.49 3717.40 195.17 o 1 7 1 12452.59 12288.58 211.14 o 2 7 1 2760.30 2758.08 94.14 o 3 7 1 3507.49 3573.45 100.22 o 4 7 1 194.20 177.01 38.59 o 5 7 1 8.47 61.56 43.21 o 6 7 1 635.95 608.77 107.06 o 7 7 1 345.77 389.60 101.27 o 8 7 1 8.17 78.25 108.51 o 9 7 1 43.68 -0.75 132.56 o 10 7 1 63.30 147.85 170.31 o 0 8 1 697.41 656.39 113.65 o 1 8 1 118.95 156.49 46.22 o 2 8 1 1957.04 1985.11 105.28 o 3 8 1 1073.19 1173.80 85.25 o 4 8 1 1300.70 1391.02 82.07 o 5 8 1 41.73 50.22 47.76 o 6 8 1 603.38 527.39 102.54 o 7 8 1 49.28 -36.99 92.41 o 8 8 1 209.42 181.73 133.35 o 9 8 1 2.68 21.03 144.87 o 10 8 1 2.72 153.34 172.93 o 0 9 1 663.52 595.08 124.80 o 1 9 1 128.98 181.56 47.51 o 2 9 1 397.32 438.63 62.92 o 3 9 1 908.11 980.08 82.29 o 4 9 1 381.17 364.27 56.18 o 5 9 1 526.07 588.11 84.44 o 6 9 1 113.96 75.34 82.91 o 7 9 1 390.58 411.14 126.89 o 8 9 1 17.53 -77.67 107.08 o 9 9 1 106.13 122.13 149.20 o 10 9 1 16.15 -44.15 148.00 o 0 10 1 488.60 415.72 110.97 o 1 10 1 71.86 95.24 45.09 o 2 10 1 480.68 618.69 64.87 o 3 10 1 68.20 61.55 47.93 o 4 10 1 1500.18 1470.85 102.97 o 5 10 1 103.35 114.50 56.77 o 6 10 1 593.07 585.37 110.99 o 7 10 1 257.59 73.25 104.92 o 8 10 1 81.89 58.83 125.42 o 9 10 1 7.37 20.33 127.41 o 10 10 1 39.78 142.85 153.24 o 0 11 1 6924.15 6620.11 324.60 o 1 11 1 114.81 209.46 54.80 o 2 11 1 1236.35 1332.69 91.60 o 3 11 1 203.41 255.15 62.44 o 4 11 1 489.04 577.99 83.05 o 5 11 1 273.81 319.09 81.54 o 6 11 1 74.96 88.87 93.40 o 7 11 1 33.66 -12.05 111.50 o 8 11 1 33.73 13.96 124.99 o 9 11 1 66.67 137.91 145.81 o 10 11 1 48.67 255.97 189.09 o 0 12 1 4.27 34.53 81.14 o 1 12 1 399.86 453.65 75.18 o 2 12 1 742.78 828.57 80.86 o 3 12 1 30.45 85.92 56.33 o 4 12 1 219.00 185.41 65.41 o 5 12 1 435.81 393.39 98.33 o 6 12 1 655.96 619.79 139.98 o 7 12 1 105.35 -4.11 107.64 o 8 12 1 311.37 209.17 144.61 o 9 12 1 13.17 17.94 133.88 o 10 12 1 3.87 -58.37 190.07 o 0 13 1 497.27 458.94 136.34 o 1 13 1 913.64 1019.01 107.84 o 2 13 1 502.02 492.92 69.33 o 3 13 1 248.78 288.00 75.68 o 4 13 1 243.15 283.60 82.88 o 5 13 1 44.60 60.87 95.27 o 6 13 1 1.60 -42.99 92.87 o 7 13 1 82.48 80.27 124.47 o 8 13 1 1.63 20.59 130.95 o 9 13 1 124.52 28.08 157.07 o 0 14 1 12.47 -40.95 81.45 o 1 14 1 654.81 539.93 88.75 o 2 14 1 828.57 903.95 93.98 o 3 14 1 61.42 83.14 64.27 o 4 14 1 20.78 16.00 82.19 o 5 14 1 55.89 143.67 114.61 o 6 14 1 32.79 21.43 106.82 o 7 14 1 10.89 49.88 111.83 o 8 14 1 9.87 27.91 131.71 o 9 14 1 17.92 -58.39 155.75 o 0 15 1 73.42 120.13 110.79 o 1 15 1 1048.50 1121.17 139.17 o 2 15 1 83.26 42.21 56.44 o 3 15 1 83.24 70.21 84.80 o 4 15 1 124.53 134.09 108.45 o 5 15 1 67.53 76.83 122.41 o 6 15 1 184.86 175.58 139.48 o 7 15 1 53.23 -35.21 116.15 o 8 15 1 32.37 42.93 147.89 o 9 15 1 20.78 -6.94 161.30 o 0 16 1 719.85 684.62 174.21 o 1 16 1 505.87 464.17 102.39 o 2 16 1 43.42 37.02 74.72 o 3 16 1 23.50 78.94 92.63 o 4 16 1 94.11 70.74 118.22 o 5 16 1 13.60 -33.65 122.30 o 6 16 1 63.26 46.30 138.81 o 7 16 1 7.41 45.64 133.91 o 8 16 1 46.36 65.31 154.25 o 0 17 1 392.57 568.95 181.90 o 1 17 1 208.31 212.45 85.94 o 2 17 1 82.37 91.38 104.36 o 3 17 1 23.42 88.00 122.48 o 4 17 1 90.15 187.88 139.36 o 5 17 1 54.21 28.89 138.15 o 6 17 1 0.31 30.71 150.96 o 7 17 1 17.85 90.78 161.20 o 8 17 1 6.91 -155.28 155.66 o 0 18 1 60.98 264.03 157.97 o 1 18 1 122.00 116.28 101.97 o 2 18 1 27.35 56.64 112.64 o 3 18 1 113.56 5.32 131.00 o 4 18 1 25.10 45.09 142.12 o 5 18 1 86.02 21.72 145.34 o 6 18 1 29.75 107.08 163.82 o 7 18 1 17.11 -49.10 161.94 o 0 19 1 11.99 168.43 149.84 o 1 19 1 134.44 191.10 119.20 o 2 19 1 227.15 302.40 155.25 o 3 19 1 65.07 72.41 141.01 o 4 19 1 0.14 70.08 150.17 o 5 19 1 64.50 94.20 159.83 o 6 19 1 19.81 -24.96 156.90 o 7 19 1 23.68 32.96 173.86 o 0 20 1 54.31 24.21 189.29 o 1 20 1 9.64 -73.25 124.63 o 2 20 1 37.21 120.21 148.96 o 3 20 1 6.44 1.65 149.91 o 4 20 1 122.40 195.21 182.41 o 5 20 1 9.24 -73.70 154.32 o 6 20 1 15.26 7.49 173.23 o 0 21 1 13.37 150.90 212.95 o 1 21 1 21.35 183.11 195.43 o 2 21 1 53.33 27.33 159.15 o 3 21 1 27.70 52.75 169.20 o 4 21 1 8.59 129.46 178.77 o 5 21 1 6.77 151.82 179.03 o 6 21 1 54.50 50.85 171.40 o 1 22 1 64.24 79.10 269.58 o 2 22 1 1.60 -40.74 167.13 o 3 22 1 42.99 147.70 182.19 o 4 22 1 40.75 65.41 185.01 o 5 22 1 29.19 42.38 195.42 o 1 23 1 21.77 103.77 330.15 o 2 23 1 12.56 -12.80 253.08 o 3 23 1 22.02 175.62 194.70 o 4 23 1 74.12 228.50 205.09 o 2 24 1 18.27 149.32 364.14 o 3 24 1 27.98 -10.54 199.37 o 0 0 2 3103.37 3583.24 365.28 o 1 0 2 5527.92 5137.56 120.97 o 2 0 2 5957.36 6150.46 261.86 o 3 0 2 5606.28 6089.47 185.26 o 4 0 2 1350.13 1367.28 125.80 o 5 0 2 650.90 588.24 93.64 o 6 0 2 0.23 87.07 67.96 o 7 0 2 0.55 6.28 75.70 o 8 0 2 94.51 92.95 144.16 o 9 0 2 9.12 -109.77 206.99 o 10 0 2 0.10 22.67 284.95 o 11 0 2 70.88 382.67 501.68 o 0 1 2 348.15 336.91 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6 21 195.08 208.81 120.09 o 3 6 21 82.04 132.18 164.49 o 4 6 21 21.28 212.35 151.45 o 5 6 21 13.01 27.84 125.66 o 6 6 21 5.56 77.49 144.41 o 0 7 21 13.66 49.02 154.54 o 1 7 21 125.10 94.32 107.08 o 2 7 21 61.26 134.05 116.54 o 3 7 21 33.54 14.72 121.92 o 4 7 21 52.49 18.59 143.14 o 5 7 21 30.74 0.30 136.18 o 6 7 21 3.88 91.49 158.06 o 0 8 21 36.86 147.37 165.48 o 1 8 21 87.02 58.48 111.11 o 2 8 21 15.65 -56.08 110.85 o 3 8 21 92.58 68.78 106.48 o 4 8 21 12.40 46.35 139.96 o 5 8 21 14.74 90.44 170.34 o 6 8 21 1.80 122.66 150.36 o 0 9 21 43.27 76.83 169.09 o 1 9 21 27.91 -57.65 119.18 o 2 9 21 39.66 137.97 121.26 o 3 9 21 11.98 59.46 98.95 o 4 9 21 21.72 67.67 118.39 o 5 9 21 195.62 220.77 177.45 o 6 9 21 97.97 13.69 200.12 o 0 10 21 53.49 -43.29 159.64 o 1 10 21 5.99 11.21 127.00 o 2 10 21 58.79 196.20 120.27 o 3 10 21 42.17 107.59 105.09 o 4 10 21 55.91 21.34 110.50 o 5 10 21 5.36 -58.54 163.34 o 0 11 21 60.86 21.01 163.29 o 1 11 21 165.78 102.04 128.38 o 2 11 21 52.73 167.33 130.00 o 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149.05 o 6 6 22 28.08 186.72 162.52 o 0 7 22 0.19 22.67 165.32 o 1 7 22 15.11 179.90 117.92 o 2 7 22 38.68 222.04 129.64 o 3 7 22 4.38 81.29 160.96 o 4 7 22 16.37 96.72 159.61 o 5 7 22 3.42 78.92 188.59 o 6 7 22 8.65 187.90 184.02 o 0 8 22 3.47 116.22 176.25 o 1 8 22 9.59 -14.51 114.72 o 2 8 22 54.88 102.42 130.28 o 3 8 22 8.71 26.56 124.87 o 4 8 22 2.01 -40.84 150.88 o 5 8 22 97.87 173.08 179.30 o 0 9 22 45.79 138.46 178.07 o 1 9 22 9.56 160.97 131.13 o 2 9 22 10.57 57.57 127.32 o 3 9 22 2.59 8.15 121.59 o 4 9 22 20.85 48.21 173.61 o 5 9 22 8.67 127.19 190.88 o 0 10 22 344.47 311.18 199.92 o 1 10 22 15.22 23.15 129.73 o 2 10 22 14.94 236.83 135.96 o 3 10 22 11.80 130.27 127.66 o 4 10 22 70.74 170.88 140.72 o 5 10 22 20.47 163.84 185.23 o 0 11 22 18.03 176.92 211.99 o 1 11 22 40.66 7.84 124.07 o 2 11 22 188.51 179.01 134.89 o 3 11 22 20.54 31.13 118.60 o 4 11 22 46.95 -3.32 121.33 o 0 12 22 2.35 8.69 204.37 o 1 12 22 98.02 127.25 143.70 o 2 12 22 69.73 165.09 144.16 o 3 12 22 21.30 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9 23 17.16 -39.18 168.70 o 0 10 23 35.67 157.62 193.75 o 1 10 23 45.11 171.50 144.98 o 2 10 23 0.59 -2.61 132.59 o 3 10 23 25.37 -15.16 141.89 o 4 10 23 26.65 147.63 182.13 o 0 11 23 3.85 458.32 260.95 o 1 11 23 16.16 19.18 135.78 o 2 11 23 27.61 200.63 152.54 o 3 11 23 28.70 49.58 150.48 o 0 12 23 52.08 84.11 236.99 o 1 12 23 2.44 -47.97 138.87 o 2 12 23 60.40 142.55 149.86 o 3 12 23 22.69 64.58 151.99 o 0 13 23 21.46 102.90 270.49 o 1 13 23 150.47 249.76 196.85 o 0 0 24 18.42 135.48 355.85 o 1 0 24 8.26 80.70 263.59 o 2 0 24 64.41 41.39 428.20 o 3 0 24 0.29 -84.49 200.30 o 4 0 24 34.08 217.00 220.69 o 5 0 24 8.39 -102.21 230.46 o 0 1 24 1.48 36.54 254.09 o 1 1 24 37.42 -56.46 175.10 o 2 1 24 18.05 10.67 202.69 o 3 1 24 32.52 170.45 207.35 o 4 1 24 50.05 208.53 176.29 o 5 1 24 0.26 20.00 170.44 o 0 2 24 34.84 140.33 275.44 o 1 2 24 23.00 145.68 216.31 o 2 2 24 12.40 145.42 179.78 o 3 2 24 31.15 143.65 167.83 o 4 2 24 37.14 113.17 151.79 o 5 2 24 1.20 -79.44 166.48 o 0 3 24 12.59 71.31 262.92 o 1 3 24 4.71 30.55 165.47 o 2 3 24 28.35 36.67 150.33 o 3 3 24 36.91 8.99 173.94 o 4 3 24 8.92 158.25 162.88 o 5 3 24 22.26 40.53 184.85 o 0 4 24 59.49 -26.33 332.26 o 1 4 24 14.21 22.78 170.40 o 2 4 24 50.61 85.17 152.61 o 3 4 24 4.21 80.91 166.06 o 4 4 24 10.10 109.13 174.14 o 5 4 24 2.92 229.29 186.63 o 0 5 24 54.08 103.05 221.22 o 1 5 24 17.09 58.47 146.44 o 2 5 24 9.39 10.67 163.39 o 3 5 24 0.82 94.22 179.90 o 4 5 24 9.21 -82.56 175.47 o 5 5 24 23.85 45.68 215.13 o 0 6 24 83.15 188.84 189.76 o 1 6 24 64.63 83.40 163.10 o 2 6 24 12.88 -41.54 173.67 o 3 6 24 3.10 154.51 183.38 o 4 6 24 5.74 124.02 190.86 o 0 7 24 0.13 -133.42 174.38 o 1 7 24 12.20 73.91 143.84 o 2 7 24 16.33 82.93 168.09 o 3 7 24 3.13 67.34 172.28 o 4 7 24 18.17 39.92 189.33 o 0 8 24 20.89 146.90 192.84 o 1 8 24 22.80 155.53 138.74 o 2 8 24 9.17 142.12 198.13 o 3 8 24 3.55 -108.70 170.71 o 4 8 24 60.25 99.62 185.04 o 0 9 24 5.76 112.29 183.06 o 1 9 24 1.75 -21.96 137.17 o 2 9 24 5.84 62.87 168.90 o 3 9 24 14.34 58.98 178.70 o 0 10 24 1.11 175.49 197.33 o 1 10 24 6.02 145.90 149.77 o 2 10 24 28.90 16.91 155.84 o 3 10 24 34.55 86.93 203.32 o 0 11 24 87.85 3.07 222.65 o 1 11 24 4.34 69.83 146.96 o 2 11 24 2.90 56.65 155.32 o 0 12 24 322.57 339.58 309.28 o 1 12 24 1.45 87.03 185.58 o 1 0 25 3.72 -44.22 264.22 o 2 0 25 3.33 277.78 455.04 o 3 0 25 0.13 -94.47 426.75 o 4 0 25 0.53 21.31 242.89 o 0 1 25 20.61 270.22 278.05 o 1 1 25 28.00 -14.92 227.46 o 2 1 25 78.95 -45.39 291.65 o 3 1 25 9.69 166.72 232.54 o 4 1 25 27.41 264.26 184.86 o 0 2 25 12.84 -49.53 266.41 o 1 2 25 36.49 60.60 227.85 o 2 2 25 4.86 -89.54 299.59 o 3 2 25 15.56 40.81 218.55 o 4 2 25 40.12 -62.52 171.01 o 0 3 25 1.10 -187.15 337.57 o 1 3 25 10.64 -44.63 220.11 o 2 3 25 34.18 76.69 181.18 o 3 3 25 21.87 39.59 178.85 o 4 3 25 95.33 159.18 194.12 o 0 4 25 112.44 224.45 388.64 o 1 4 25 70.14 150.79 190.86 o 2 4 25 28.42 35.66 183.23 o 3 4 25 7.77 191.62 190.71 o 4 4 25 25.28 167.80 200.39 o 0 5 25 3.42 159.60 386.07 o 1 5 25 147.59 23.93 194.99 o 2 5 25 1.18 19.48 177.56 o 3 5 25 37.63 86.97 183.11 o 4 5 25 27.55 107.44 198.03 o 0 6 25 43.94 134.26 247.14 o 1 6 25 22.31 113.19 167.10 o 2 6 25 1.28 -76.43 179.35 o 3 6 25 5.53 17.43 179.73 o 0 7 25 70.07 -183.73 226.44 o 1 7 25 60.17 49.70 167.73 o 2 7 25 15.03 -10.49 170.71 o 3 7 25 15.81 39.08 190.80 o 0 8 25 5.46 143.49 196.39 o 1 8 25 57.33 73.80 177.48 o 2 8 25 0.09 -97.34 201.41 o 3 8 25 2.08 146.25 234.99 o 0 9 25 1.51 76.50 194.05 o 1 9 25 8.83 -66.50 164.10 o 2 9 25 29.54 -39.71 213.71 o 0 10 25 23.81 276.98 205.96 o 1 10 25 68.44 66.05 168.82 o 0 0 26 103.31 3.11 404.35 o 1 0 26 22.11 -36.68 394.07 o 2 0 26 19.73 59.40 396.63 o 3 0 26 110.73 0.66 443.35 o 0 1 26 0.12 12.27 272.38 o 1 1 26 58.40 -72.13 216.07 o 2 1 26 3.39 148.23 303.88 o 3 1 26 2.30 -276.96 276.96 o 0 2 26 2.83 36.01 379.68 o 1 2 26 8.61 106.05 227.68 o 2 2 26 26.58 -71.11 287.62 o 3 2 26 60.06 124.57 217.50 o 0 3 26 12.23 -173.37 347.37 o 1 3 26 117.19 78.44 225.25 o 2 3 26 67.45 74.58 215.59 o 3 3 26 7.37 -98.61 211.86 o 0 4 26 41.78 -49.91 351.85 o 1 4 26 64.65 235.52 228.59 o 2 4 26 8.48 -95.58 211.61 o 3 4 26 46.88 -61.92 184.81 o 0 5 26 190.56 138.65 377.69 o 1 5 26 14.46 -132.55 220.13 o 2 5 26 49.98 49.07 211.11 o 0 6 26 41.12 -90.25 316.93 o 1 6 26 51.77 83.30 190.72 o 2 6 26 30.49 234.28 188.65 o 0 7 26 7.67 -1.09 331.93 o 1 7 26 28.49 -179.92 182.47 o 0 8 26 13.37 -143.26 216.57 o 1 0 27 142.29 256.55 421.72 o 2 0 27 42.19 43.29 431.60 o 0 1 27 37.71 49.58 331.56 o 1 1 27 94.92 354.40 322.79 o 2 1 27 16.23 95.83 297.94 o 0 2 27 13.48 -43.67 324.64 o 1 2 27 85.15 165.86 223.18 o 0 3 27 10.67 305.58 398.28 o 1 3 27 0.21 -119.42 206.58 o 0 4 27 148.87 197.28 360.77 o 1 4 27 14.35 45.03 239.90 o