#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:59:50 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180938 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/18/2201827.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201827_Fobs loop_ _publ_author_name 'Simon, Monika' 'Csunderlik, Carol' 'Jones, Peter G.' 'Neda, Ion' 'Tarta-Micle, Andreea' _publ_section_title ; N,N'-Disuccinimidyl carbonate ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o683 _journal_page_last o685 _journal_volume 59 _journal_year 2003 _space_group_IT_number 43 _symmetry_space_group_name_Hall 'F 2 -2d' _symmetry_space_group_name_H-M 'F d d 2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 13.2389 _cell_length_b 14.6289 _cell_length_c 10.3595 _exptl_crystal_F_000 1056.00 _reflns_d_resolution_high 0.7114 _cod_data_source_file bt6267Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' carbe in Fdd2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 256.50 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' 'x+1/4, -y+1/4, z+1/4' '-x+1/4, y+1/4, z+1/4' 'x, y+1/2, z+1/2' '-x, -y+1/2, z+1/2' 'x+1/4, -y+3/4, z+3/4' '-x+1/4, y+3/4, z+3/4' 'x+1/2, y, z+1/2' '-x+1/2, -y, z+1/2' 'x+3/4, -y+1/4, z+3/4' '-x+3/4, y+1/4, z+3/4' 'x+1/2, y+1/2, z' '-x+1/2, -y+1/2, z' 'x+3/4, -y+3/4, z+1/4' '-x+3/4, y+3/4, z+1/4' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 8229.04 8901.70 93.94 o 8 0 0 3566.23 3158.82 72.04 o 12 0 0 18442.02 17719.02 227.68 o 16 0 0 686.61 661.54 53.73 o 2 2 0 6412.34 6355.55 42.34 o 4 2 0 1688.66 1927.94 16.34 o 6 2 0 1632.17 1534.36 20.98 o 8 2 0 3543.39 3817.16 36.44 o 10 2 0 35.78 24.10 10.40 o 12 2 0 4038.69 3745.66 70.36 o 14 2 0 244.34 262.78 32.04 o 16 2 0 6.80 19.09 17.03 o 18 2 0 62.75 65.78 22.26 o 0 4 0 9823.41 9806.07 304.34 o 2 4 0 451.53 503.86 8.91 o 4 4 0 1142.95 1332.85 14.86 o 6 4 0 363.85 445.62 10.86 o 8 4 0 1922.28 1913.45 34.64 o 10 4 0 7142.68 7345.61 147.07 o 12 4 0 2411.42 2370.87 100.90 o 14 4 0 81.47 76.51 16.74 o 16 4 0 752.97 768.92 40.81 o 18 4 0 161.07 171.57 23.20 o 2 6 0 18172.70 18981.21 223.54 o 4 6 0 1040.31 1087.93 22.12 o 6 6 0 839.57 793.41 14.44 o 8 6 0 1754.98 1607.08 27.28 o 10 6 0 7314.88 7499.65 75.84 o 12 6 0 1284.86 1297.52 47.55 o 14 6 0 19.83 22.15 10.76 o 16 6 0 0.21 -12.88 12.88 o 0 8 0 24262.04 26053.86 298.93 o 2 8 0 6639.29 7109.09 98.46 o 4 8 0 12917.72 13490.29 152.08 o 6 8 0 203.06 214.62 9.59 o 8 8 0 96.44 94.95 7.94 o 10 8 0 22.59 2.04 6.79 o 12 8 0 3608.64 3371.04 73.03 o 14 8 0 1253.66 1188.92 48.50 o 16 8 0 530.46 591.61 39.20 o 2 10 0 363.50 410.29 13.31 o 4 10 0 37.04 18.87 5.82 o 6 10 0 864.20 822.12 20.75 o 8 10 0 3053.04 2682.79 51.99 o 10 10 0 648.47 695.76 32.65 o 12 10 0 134.72 146.11 21.81 o 14 10 0 43.65 39.68 17.79 o 16 10 0 594.41 616.85 42.36 o 0 12 0 15.22 55.41 31.44 o 2 12 0 1559.19 1540.16 36.44 o 4 12 0 0.68 3.94 7.36 o 6 12 0 2227.54 2091.61 37.65 o 8 12 0 808.53 750.96 29.95 o 10 12 0 2253.22 2111.08 46.22 o 12 12 0 203.48 208.81 25.66 o 14 12 0 42.91 25.66 18.70 o 2 14 0 7094.40 6766.60 107.80 o 4 14 0 2959.68 2826.83 51.74 o 6 14 0 1986.82 1980.39 134.14 o 8 14 0 775.30 792.27 37.85 o 10 14 0 1346.47 1459.72 60.10 o 12 14 0 187.36 220.91 40.60 o 0 16 0 16.07 38.84 22.09 o 2 16 0 712.19 657.33 28.95 o 4 16 0 146.16 138.43 16.85 o 6 16 0 254.08 254.31 21.51 o 8 16 0 2.60 -1.65 14.15 o 10 16 0 259.90 301.62 32.33 o 2 18 0 7.25 2.34 11.89 o 4 18 0 599.17 661.67 31.79 o 6 18 0 89.71 93.47 22.59 o 8 18 0 611.42 740.39 44.04 o 0 20 0 269.39 305.69 47.37 o 2 20 0 61.07 76.62 18.92 o 4 20 0 796.11 809.65 37.96 o 1 1 1 13259.35 13189.68 102.83 o 3 1 1 1701.51 1818.52 10.86 o 5 1 1 5473.18 5659.60 25.41 o 7 1 1 2569.69 2772.58 31.14 o 9 1 1 486.50 534.65 17.06 o 11 1 1 1334.03 1383.91 29.34 o 13 1 1 2777.04 2674.04 44.17 o 15 1 1 737.01 758.23 26.99 o 17 1 1 990.90 1006.58 34.10 o 1 3 1 18518.97 17910.22 119.19 o 3 3 1 37930.34 38682.06 251.15 o 5 3 1 21788.39 22511.23 106.67 o 7 3 1 11110.18 12176.40 79.19 o 9 3 1 4527.69 4527.31 31.84 o 11 3 1 928.56 880.48 23.85 o 13 3 1 5653.48 5199.82 62.35 o 15 3 1 387.19 385.14 20.99 o 17 3 1 392.60 426.74 21.70 o 1 5 1 20085.92 20679.12 93.48 o 3 5 1 2063.72 2146.44 19.24 o 5 5 1 1615.89 1771.22 15.96 o 7 5 1 1881.27 2036.66 16.39 o 9 5 1 2819.36 2657.76 30.04 o 11 5 1 275.20 269.48 13.73 o 13 5 1 1556.68 1419.16 48.39 o 15 5 1 555.15 547.96 21.65 o 17 5 1 125.29 133.42 14.59 o 1 7 1 5698.88 5963.73 38.06 o 3 7 1 8271.61 8541.07 95.98 o 5 7 1 2271.29 2464.82 18.48 o 7 7 1 24.40 26.91 3.70 o 9 7 1 667.45 692.02 13.79 o 11 7 1 39.39 28.25 6.99 o 13 7 1 806.18 747.41 20.69 o 15 7 1 352.85 367.90 21.92 o 17 7 1 47.92 52.75 15.89 o 1 9 1 1246.71 1283.48 12.44 o 3 9 1 675.79 674.35 11.67 o 5 9 1 1842.88 2043.76 20.87 o 7 9 1 677.41 639.85 13.03 o 9 9 1 1704.72 1678.44 28.45 o 11 9 1 1780.65 1683.65 36.04 o 13 9 1 777.36 708.84 26.65 o 15 9 1 39.21 32.33 13.24 o 1 11 1 2795.63 2717.93 28.18 o 3 11 1 6255.52 6269.59 57.93 o 5 11 1 1361.30 1308.95 18.37 o 7 11 1 3780.97 3704.35 42.03 o 9 11 1 5481.09 5299.23 57.25 o 11 11 1 64.21 50.28 10.96 o 13 11 1 26.15 7.35 11.17 o 15 11 1 516.50 562.74 28.51 o 1 13 1 298.19 267.85 10.84 o 3 13 1 3457.12 3315.06 41.11 o 5 13 1 207.72 218.07 12.18 o 7 13 1 141.54 121.67 9.94 o 9 13 1 1475.18 1438.64 34.51 o 11 13 1 881.28 794.20 33.06 o 13 13 1 73.80 53.40 14.22 o 1 15 1 671.58 669.47 19.14 o 3 15 1 1183.61 1161.41 24.79 o 5 15 1 1.75 -0.55 6.97 o 7 15 1 28.64 35.71 8.47 o 9 15 1 379.28 377.44 24.69 o 11 15 1 49.18 19.50 16.04 o 1 17 1 890.05 850.63 23.25 o 3 17 1 13.98 8.35 7.89 o 5 17 1 196.63 199.75 14.27 o 7 17 1 1030.46 1006.22 26.53 o 9 17 1 147.37 157.30 18.26 o 1 19 1 532.46 496.18 26.02 o 3 19 1 289.77 289.52 18.22 o 5 19 1 105.19 94.16 13.34 o 7 19 1 74.74 67.23 15.98 o 2 0 2 30818.16 30897.12 251.35 o 6 0 2 17221.61 17414.57 238.71 o 10 0 2 3703.44 3871.59 103.69 o 14 0 2 2834.03 2599.53 65.30 o 18 0 2 1729.05 1946.08 73.44 o 0 2 2 65792.70 61917.37 1144.95 o 2 2 2 17094.61 17453.29 159.80 o 4 2 2 17025.10 17944.11 131.06 o 6 2 2 5239.74 5588.37 39.21 o 8 2 2 131.70 144.32 6.37 o 10 2 2 1632.75 1626.44 30.09 o 12 2 2 6080.67 5828.34 63.06 o 14 2 2 58.00 37.36 10.49 o 16 2 2 770.12 726.70 25.41 o 18 2 2 101.03 96.30 15.43 o 2 4 2 3966.38 4004.52 51.76 o 4 4 2 2311.00 2464.44 26.82 o 6 4 2 6537.11 7079.69 50.20 o 8 4 2 5528.35 5712.96 49.03 o 10 4 2 317.16 324.03 13.68 o 12 4 2 325.25 315.61 15.06 o 14 4 2 917.22 937.11 25.81 o 16 4 2 256.28 226.63 17.35 o 18 4 2 98.58 120.07 16.81 o 0 6 2 17563.23 18624.60 267.57 o 2 6 2 5131.26 5503.15 35.62 o 4 6 2 2826.15 2809.07 22.44 o 6 6 2 698.80 772.17 11.04 o 8 6 2 2268.17 2363.44 24.94 o 10 6 2 3629.46 3537.19 35.22 o 12 6 2 218.15 164.42 12.63 o 14 6 2 138.79 128.39 13.04 o 16 6 2 751.89 800.23 26.70 o 2 8 2 2062.14 2253.11 19.22 o 4 8 2 107.68 120.05 6.64 o 6 8 2 6775.85 6784.16 36.91 o 8 8 2 40.44 38.20 4.49 o 10 8 2 10.39 -2.14 5.30 o 12 8 2 42.61 29.08 9.46 o 14 8 2 89.50 81.56 13.59 o 16 8 2 122.70 124.50 17.29 o 0 10 2 3500.28 3853.50 33.12 o 2 10 2 4110.14 3893.92 32.40 o 4 10 2 2101.48 2239.98 28.04 o 6 10 2 182.42 172.92 8.46 o 8 10 2 720.96 673.92 14.57 o 10 10 2 2526.79 2379.95 32.88 o 12 10 2 234.65 198.36 16.80 o 14 10 2 210.67 198.06 18.99 o 16 10 2 466.16 477.41 27.95 o 2 12 2 2682.53 2579.14 40.20 o 4 12 2 335.68 323.03 13.21 o 6 12 2 928.97 872.87 18.12 o 8 12 2 323.82 290.30 11.56 o 10 12 2 2062.87 2075.87 37.56 o 12 12 2 409.70 407.40 22.38 o 14 12 2 216.67 241.72 21.37 o 0 14 2 4849.92 4565.40 139.09 o 2 14 2 1032.79 978.93 22.10 o 4 14 2 556.03 504.97 16.89 o 6 14 2 229.83 228.79 13.37 o 8 14 2 144.90 156.43 13.39 o 10 14 2 1296.43 1265.02 39.75 o 12 14 2 602.16 683.31 42.36 o 2 16 2 1451.37 1409.35 28.30 o 4 16 2 396.65 383.71 16.48 o 6 16 2 599.90 568.75 19.86 o 8 16 2 139.05 162.68 16.61 o 10 16 2 1009.39 1160.16 36.11 o 0 18 2 681.74 658.65 39.39 o 2 18 2 83.53 83.80 13.20 o 4 18 2 3.84 5.20 9.44 o 6 18 2 323.91 328.60 18.77 o 8 18 2 17.73 25.80 13.79 o 2 20 2 318.17 351.11 27.92 o 1 1 3 30678.74 30612.32 244.64 o 3 1 3 23956.82 25226.25 187.39 o 5 1 3 8611.74 8799.24 98.20 o 7 1 3 11234.22 12340.86 61.05 o 9 1 3 1207.83 1102.96 15.32 o 11 1 3 255.91 256.09 13.33 o 13 1 3 2708.18 2593.98 39.27 o 15 1 3 350.96 344.84 18.91 o 17 1 3 516.84 550.44 24.02 o 1 3 3 27760.84 28991.83 385.27 o 3 3 3 10856.04 11933.48 79.34 o 5 3 3 764.35 878.37 11.32 o 7 3 3 1122.81 1089.69 12.54 o 9 3 3 1870.56 1789.77 22.65 o 11 3 3 1808.86 1609.24 35.03 o 13 3 3 329.40 353.51 16.64 o 15 3 3 174.53 143.78 14.12 o 17 3 3 157.83 167.83 17.08 o 1 5 3 1546.05 1562.07 13.40 o 3 5 3 3084.35 3163.30 29.48 o 5 5 3 1671.38 1718.02 21.90 o 7 5 3 3021.64 3392.11 26.51 o 9 5 3 5100.86 5002.56 54.83 o 11 5 3 2569.94 2406.63 35.24 o 13 5 3 606.29 594.00 20.80 o 15 5 3 105.08 124.53 13.96 o 17 5 3 643.73 659.50 26.84 o 1 7 3 4540.32 4989.24 50.71 o 3 7 3 1767.69 1940.22 26.32 o 5 7 3 4065.34 4023.38 31.13 o 7 7 3 2302.38 2236.65 20.23 o 9 7 3 603.66 601.44 14.17 o 11 7 3 2661.81 2574.36 36.75 o 13 7 3 220.69 181.57 14.33 o 15 7 3 470.22 452.93 23.83 o 17 7 3 257.67 258.48 22.65 o 1 9 3 1046.61 1097.20 13.92 o 3 9 3 1475.86 1518.71 20.42 o 5 9 3 3706.24 3749.72 27.61 o 7 9 3 7639.16 7453.80 70.28 o 9 9 3 848.37 825.45 22.51 o 11 9 3 329.45 322.53 18.26 o 13 9 3 79.37 46.33 12.13 o 15 9 3 355.19 360.76 24.06 o 1 11 3 868.75 857.24 14.60 o 3 11 3 2181.48 2132.15 22.58 o 5 11 3 3372.07 3335.60 41.28 o 7 11 3 454.83 446.26 12.85 o 9 11 3 214.76 230.63 13.17 o 11 11 3 0.76 0.93 9.33 o 13 11 3 286.56 334.55 22.11 o 15 11 3 91.61 110.69 18.31 o 1 13 3 547.65 513.24 14.43 o 3 13 3 4804.92 4607.55 45.36 o 5 13 3 1300.47 1248.61 24.49 o 7 13 3 258.72 257.06 13.89 o 9 13 3 948.00 883.85 27.52 o 11 13 3 62.81 44.41 13.73 o 13 13 3 439.75 446.25 29.71 o 1 15 3 265.89 284.78 16.41 o 3 15 3 126.27 127.83 11.22 o 5 15 3 862.00 823.53 22.14 o 7 15 3 667.78 663.35 20.67 o 9 15 3 21.07 18.73 11.37 o 11 15 3 301.49 335.40 51.55 o 1 17 3 258.35 251.16 19.51 o 3 17 3 368.85 351.12 19.56 o 5 17 3 941.73 1023.41 26.60 o 7 17 3 386.97 437.08 21.34 o 9 17 3 117.56 141.11 18.50 o 1 19 3 278.60 308.02 23.10 o 3 19 3 12.01 1.20 11.41 o 5 19 3 449.87 446.98 23.88 o 0 0 4 830.41 873.76 21.80 o 4 0 4 9789.60 9955.84 101.96 o 8 0 4 3067.11 2955.07 28.75 o 12 0 4 2072.15 2030.21 42.32 o 16 0 4 119.80 104.32 21.81 o 2 2 4 7685.34 8018.19 55.67 o 4 2 4 3352.26 3504.70 24.00 o 6 2 4 6949.82 7336.34 87.32 o 8 2 4 538.93 525.64 10.73 o 10 2 4 3458.34 3338.69 83.71 o 12 2 4 157.98 138.87 11.80 o 14 2 4 370.16 371.37 18.13 o 16 2 4 1413.82 1497.83 35.46 o 0 4 4 1024.56 918.34 16.66 o 2 4 4 9894.90 10260.23 89.74 o 4 4 4 12695.25 12927.28 93.96 o 6 4 4 1779.79 1625.30 17.88 o 8 4 4 5115.71 5215.09 48.11 o 10 4 4 420.47 388.29 15.10 o 12 4 4 379.98 390.78 16.77 o 14 4 4 7.97 7.64 8.94 o 16 4 4 785.48 805.58 27.54 o 2 6 4 2712.75 2974.25 23.63 o 4 6 4 3249.22 3429.24 30.27 o 6 6 4 255.20 256.77 8.66 o 8 6 4 3235.03 3155.50 29.75 o 10 6 4 343.81 316.16 12.84 o 12 6 4 947.93 976.94 42.96 o 14 6 4 1155.39 1140.11 35.41 o 16 6 4 100.41 81.59 15.84 o 0 8 4 4244.81 3842.52 53.51 o 2 8 4 1955.10 1889.00 22.94 o 4 8 4 396.70 459.93 10.11 o 6 8 4 1647.60 1718.75 17.79 o 8 8 4 1533.83 1459.44 17.52 o 10 8 4 1615.12 1552.62 39.62 o 12 8 4 90.30 88.79 12.66 o 14 8 4 473.98 480.22 24.32 o 16 8 4 77.24 77.50 16.32 o 2 10 4 472.83 369.85 10.51 o 4 10 4 3941.47 3800.57 44.84 o 6 10 4 3637.34 3495.93 31.30 o 8 10 4 2169.12 2042.70 37.81 o 10 10 4 279.42 264.10 15.43 o 12 10 4 322.33 328.47 20.22 o 14 10 4 34.41 44.97 14.10 o 0 12 4 1106.28 911.97 36.17 o 2 12 4 92.04 70.59 7.92 o 4 12 4 304.86 321.89 12.35 o 6 12 4 224.73 212.81 11.40 o 8 12 4 366.81 322.47 13.56 o 10 12 4 739.37 726.87 21.13 o 12 12 4 621.45 675.46 27.89 o 14 12 4 61.49 46.85 15.58 o 2 14 4 698.58 659.60 21.44 o 4 14 4 196.03 188.56 12.22 o 6 14 4 34.41 26.18 7.96 o 8 14 4 256.39 264.45 16.91 o 10 14 4 850.63 884.20 30.67 o 12 14 4 594.78 596.16 40.35 o 0 16 4 2094.45 2139.02 113.84 o 2 16 4 1697.73 1679.33 35.53 o 4 16 4 238.34 229.26 16.72 o 6 16 4 6.41 -0.99 8.64 o 8 16 4 133.42 147.41 17.18 o 10 16 4 99.04 90.65 17.15 o 2 18 4 600.96 621.28 28.29 o 4 18 4 64.54 61.75 12.89 o 6 18 4 205.39 222.72 18.85 o 1 1 5 8167.11 8602.37 149.03 o 3 1 5 4424.66 4890.80 55.80 o 5 1 5 6357.41 6799.06 37.67 o 7 1 5 280.69 248.59 7.63 o 9 1 5 130.53 139.55 6.84 o 11 1 5 150.47 142.40 10.06 o 13 1 5 890.16 817.22 28.22 o 15 1 5 1884.20 1890.60 43.60 o 17 1 5 701.07 726.71 31.39 o 1 3 5 1669.99 1604.80 24.04 o 3 3 5 4272.15 4694.22 60.94 o 5 3 5 7018.66 7156.54 74.71 o 7 3 5 1068.16 1146.62 14.05 o 9 3 5 160.29 173.36 9.04 o 11 3 5 623.20 617.53 21.11 o 13 3 5 11.26 4.32 8.14 o 15 3 5 247.60 236.97 19.51 o 17 3 5 710.60 738.91 32.04 o 1 5 5 443.43 481.63 12.04 o 3 5 5 3662.72 3738.34 48.12 o 5 5 5 5121.51 5504.36 66.75 o 7 5 5 1118.62 1005.17 15.64 o 9 5 5 2166.90 2095.29 28.75 o 11 5 5 493.02 406.72 16.67 o 13 5 5 211.77 219.81 15.55 o 15 5 5 58.66 46.40 11.89 o 1 7 5 2235.86 2246.38 19.16 o 3 7 5 4816.62 4732.79 67.27 o 5 7 5 1499.49 1399.02 18.28 o 7 7 5 1223.92 1258.52 18.10 o 9 7 5 436.70 453.18 12.66 o 11 7 5 2332.15 2185.21 35.63 o 13 7 5 976.99 946.61 31.28 o 15 7 5 42.23 29.75 13.21 o 1 9 5 1870.39 1864.39 30.55 o 3 9 5 595.32 593.56 12.88 o 5 9 5 692.99 673.49 14.26 o 7 9 5 354.99 356.05 10.93 o 9 9 5 687.53 695.94 18.86 o 11 9 5 107.25 96.08 12.96 o 13 9 5 4.32 4.02 10.11 o 15 9 5 137.65 140.50 18.02 o 1 11 5 2277.85 2183.77 29.51 o 3 11 5 537.99 521.42 14.76 o 5 11 5 134.43 121.47 8.33 o 7 11 5 658.45 698.64 16.33 o 9 11 5 106.55 109.63 10.79 o 11 11 5 237.53 263.37 19.55 o 13 11 5 49.41 28.08 13.10 o 1 13 5 2399.15 2184.32 49.90 o 3 13 5 134.20 101.88 11.17 o 5 13 5 500.60 524.64 17.70 o 7 13 5 304.49 304.43 15.58 o 9 13 5 200.82 183.05 14.97 o 11 13 5 461.11 445.11 27.86 o 1 15 5 300.98 276.72 21.37 o 3 15 5 807.85 827.29 25.36 o 5 15 5 59.12 52.26 10.64 o 7 15 5 60.25 49.35 11.41 o 9 15 5 643.08 676.90 28.55 o 11 15 5 37.45 40.02 21.25 o 1 17 5 8.38 3.42 11.30 o 3 17 5 349.78 376.31 21.06 o 5 17 5 151.88 147.13 15.83 o 7 17 5 97.39 104.36 17.67 o 1 19 5 303.04 343.90 25.02 o 3 19 5 22.68 10.53 14.38 o 2 0 6 7262.83 7290.42 244.76 o 6 0 6 1280.67 1310.51 22.44 o 10 0 6 3773.62 3399.63 97.12 o 14 0 6 426.98 361.13 29.83 o 0 2 6 8045.22 8361.05 188.04 o 2 2 6 5161.08 5200.72 73.25 o 4 2 6 423.59 423.27 10.85 o 6 2 6 464.09 461.09 13.25 o 8 2 6 3734.08 3582.62 46.27 o 10 2 6 543.04 497.89 17.26 o 12 2 6 176.97 123.97 13.64 o 14 2 6 544.03 559.99 28.87 o 16 2 6 92.72 99.06 16.45 o 2 4 6 7288.16 7782.19 112.18 o 4 4 6 1338.02 1425.14 21.51 o 6 4 6 11119.04 10969.87 159.53 o 8 4 6 454.73 497.75 12.41 o 10 4 6 2423.15 2221.37 34.26 o 12 4 6 815.70 868.90 24.41 o 14 4 6 535.89 555.15 25.15 o 16 4 6 275.34 303.74 23.54 o 0 6 6 4696.97 4595.65 60.68 o 2 6 6 734.59 786.60 16.56 o 4 6 6 2128.11 2185.17 26.07 o 6 6 6 656.12 653.18 13.84 o 8 6 6 2026.47 1960.56 22.20 o 10 6 6 787.68 761.87 19.50 o 12 6 6 39.02 21.91 9.07 o 14 6 6 1079.14 1090.98 29.90 o 16 6 6 112.15 112.14 21.23 o 2 8 6 101.16 96.77 7.29 o 4 8 6 4466.45 4426.40 47.36 o 6 8 6 1121.62 1088.72 18.06 o 8 8 6 2557.41 2495.15 34.40 o 10 8 6 507.64 455.97 18.27 o 12 8 6 1211.85 1255.30 34.08 o 14 8 6 10.37 21.16 14.60 o 0 10 6 3898.28 3641.00 68.80 o 2 10 6 97.01 76.40 8.25 o 4 10 6 3621.85 3598.59 68.85 o 6 10 6 1428.07 1412.51 21.74 o 8 10 6 1454.50 1420.27 22.72 o 10 10 6 138.09 127.52 12.69 o 12 10 6 408.03 439.93 23.51 o 14 10 6 323.27 325.70 24.07 o 2 12 6 248.15 231.46 14.43 o 4 12 6 1349.56 1331.90 25.92 o 6 12 6 665.40 688.54 19.98 o 8 12 6 1125.28 1232.16 26.54 o 10 12 6 33.48 28.77 10.08 o 12 12 6 169.62 163.84 18.04 o 0 14 6 108.57 96.54 18.24 o 2 14 6 13.23 3.90 9.61 o 4 14 6 867.01 864.65 25.69 o 6 14 6 30.22 21.07 9.97 o 8 14 6 23.49 19.38 14.01 o 10 14 6 16.89 23.72 13.60 o 2 16 6 833.33 853.45 31.06 o 4 16 6 289.72 320.46 19.65 o 6 16 6 5.16 5.06 11.19 o 8 16 6 393.67 450.59 30.01 o 0 18 6 374.16 435.44 37.25 o 2 18 6 865.83 902.81 34.42 o 4 18 6 757.76 865.46 30.49 o 1 1 7 486.34 492.13 13.54 o 3 1 7 4038.53 3842.95 60.99 o 5 1 7 3094.23 3078.91 36.49 o 7 1 7 3832.99 3587.15 46.71 o 9 1 7 425.72 433.46 12.58 o 11 1 7 1.04 4.04 8.13 o 13 1 7 158.17 176.76 17.09 o 15 1 7 120.78 115.26 16.68 o 1 3 7 486.64 505.62 15.33 o 3 3 7 2083.95 2074.07 32.23 o 5 3 7 335.74 383.49 11.67 o 7 3 7 905.33 814.35 16.21 o 9 3 7 146.35 137.40 8.54 o 11 3 7 132.04 143.46 14.42 o 13 3 7 185.16 158.94 16.06 o 15 3 7 748.52 833.19 32.25 o 1 5 7 756.16 775.66 41.08 o 3 5 7 561.36 592.62 16.93 o 5 5 7 7246.93 7196.93 120.18 o 7 5 7 565.01 541.76 13.58 o 9 5 7 3.02 1.00 5.28 o 11 5 7 154.45 147.55 12.78 o 13 5 7 368.26 346.02 21.95 o 15 5 7 750.08 794.50 31.83 o 1 7 7 1241.39 1274.64 24.87 o 3 7 7 3345.15 3264.87 83.56 o 5 7 7 2972.73 3058.70 32.01 o 7 7 7 6313.59 6221.50 56.36 o 9 7 7 924.90 1027.43 21.06 o 11 7 7 471.63 455.80 21.78 o 13 7 7 264.18 256.31 19.98 o 15 7 7 626.83 658.06 44.18 o 1 9 7 787.91 748.97 20.71 o 3 9 7 240.95 226.00 12.35 o 5 9 7 1532.76 1395.76 25.74 o 7 9 7 258.57 261.51 11.56 o 9 9 7 782.67 834.63 20.18 o 11 9 7 304.73 365.83 24.50 o 13 9 7 773.85 806.57 31.38 o 1 11 7 69.91 63.37 10.56 o 3 11 7 1074.98 1004.03 22.93 o 5 11 7 472.13 461.71 15.57 o 7 11 7 12.64 8.31 6.96 o 9 11 7 31.82 23.57 8.96 o 11 11 7 72.33 86.97 15.19 o 1 13 7 172.19 139.84 14.71 o 3 13 7 627.00 676.40 23.15 o 5 13 7 616.58 622.06 22.62 o 7 13 7 603.08 614.62 23.14 o 9 13 7 675.71 775.21 29.83 o 11 13 7 82.00 107.21 27.07 o 1 15 7 383.12 402.01 22.78 o 3 15 7 526.79 551.87 25.95 o 5 15 7 402.74 408.05 21.37 o 7 15 7 137.68 127.29 20.11 o 9 15 7 246.29 247.70 25.50 o 1 17 7 545.46 548.71 28.14 o 3 17 7 272.23 286.30 23.70 o 5 17 7 38.86 38.82 13.51 o 0 0 8 1058.36 1182.17 51.74 o 4 0 8 8683.57 8636.31 303.06 o 8 0 8 885.62 827.85 27.32 o 12 0 8 215.63 232.78 26.74 o 2 2 8 627.30 632.57 17.67 o 4 2 8 140.82 126.43 9.25 o 6 2 8 5445.60 5211.16 67.16 o 8 2 8 726.48 693.50 17.93 o 10 2 8 183.99 200.18 14.21 o 12 2 8 63.98 50.17 12.24 o 14 2 8 408.99 441.80 25.04 o 0 4 8 4895.54 4913.07 153.24 o 2 4 8 1047.67 981.32 22.33 o 4 4 8 403.33 414.51 14.21 o 6 4 8 1252.43 1209.65 20.71 o 8 4 8 543.38 542.67 15.07 o 10 4 8 25.96 28.23 8.53 o 12 4 8 1701.78 1845.27 42.39 o 14 4 8 11.75 14.44 12.75 o 2 6 8 160.46 167.68 11.88 o 4 6 8 2566.17 2525.22 36.49 o 6 6 8 5546.47 5505.72 86.93 o 8 6 8 1300.99 1326.51 30.99 o 10 6 8 501.46 478.18 17.81 o 12 6 8 133.09 134.48 16.17 o 14 6 8 14.47 15.43 15.47 o 0 8 8 712.70 671.71 32.63 o 2 8 8 206.70 173.97 12.32 o 4 8 8 1171.54 1130.90 24.10 o 6 8 8 32.70 28.61 6.38 o 8 8 8 2014.13 2115.13 30.35 o 10 8 8 577.12 590.67 22.28 o 12 8 8 196.77 192.30 18.87 o 2 10 8 771.37 758.95 22.49 o 4 10 8 379.88 367.39 15.64 o 6 10 8 115.50 116.82 10.28 o 8 10 8 137.26 144.86 12.79 o 10 10 8 572.98 647.92 27.26 o 12 10 8 364.22 373.36 25.06 o 0 12 8 354.31 311.08 27.02 o 2 12 8 1357.07 1278.09 30.02 o 4 12 8 418.64 418.65 17.54 o 6 12 8 190.75 184.31 13.95 o 8 12 8 152.34 132.52 14.45 o 10 12 8 275.25 287.25 25.81 o 2 14 8 979.36 1061.01 34.01 o 4 14 8 210.97 240.94 20.33 o 6 14 8 148.06 161.04 15.95 o 8 14 8 127.52 139.73 20.87 o 0 16 8 225.51 230.63 30.67 o 2 16 8 331.28 396.25 26.52 o 4 16 8 452.81 464.47 26.89 o 1 1 9 125.78 101.81 11.17 o 3 1 9 1469.70 1450.20 33.31 o 5 1 9 112.25 89.72 9.10 o 7 1 9 670.81 664.62 18.72 o 9 1 9 4.60 9.30 8.31 o 11 1 9 654.92 666.87 26.85 o 13 1 9 811.03 910.91 33.22 o 1 3 9 3040.08 2850.32 53.31 o 3 3 9 308.83 330.19 13.93 o 5 3 9 1636.25 1700.52 27.99 o 7 3 9 3021.43 2872.15 36.63 o 9 3 9 777.99 797.54 21.35 o 11 3 9 89.26 101.11 14.37 o 13 3 9 493.34 564.24 27.34 o 1 5 9 1657.87 1491.46 28.97 o 3 5 9 1930.30 1772.22 43.96 o 5 5 9 1897.97 1803.17 40.25 o 7 5 9 2422.12 2436.19 46.99 o 9 5 9 513.59 513.72 18.30 o 11 5 9 5.15 -4.23 10.08 o 13 5 9 2285.34 2492.94 63.24 o 1 7 9 1089.98 1013.11 32.86 o 3 7 9 57.51 65.36 10.04 o 5 7 9 1267.57 1265.50 34.44 o 7 7 9 1876.26 1914.54 28.73 o 9 7 9 240.86 225.36 16.04 o 11 7 9 23.60 4.32 13.53 o 13 7 9 20.24 45.69 17.84 o 1 9 9 652.70 608.59 23.71 o 3 9 9 3750.08 3644.99 81.97 o 5 9 9 1910.73 1990.95 38.48 o 7 9 9 253.63 250.77 14.14 o 9 9 9 2095.88 2275.93 43.02 o 11 9 9 174.16 181.99 28.29 o 1 11 9 54.50 50.81 11.75 o 3 11 9 440.43 410.79 19.39 o 5 11 9 988.29 1127.48 27.02 o 7 11 9 822.36 908.89 29.16 o 9 11 9 52.26 50.65 12.92 o 1 13 9 167.37 166.52 17.56 o 3 13 9 148.85 131.62 16.38 o 5 13 9 16.81 14.02 11.78 o 7 13 9 418.60 440.29 25.49 o 1 15 9 35.17 18.52 13.52 o 3 15 9 37.44 46.84 15.22 o 5 15 9 338.57 373.49 30.39 o 2 0 10 472.98 385.46 27.00 o 6 0 10 2755.95 2528.52 50.91 o 10 0 10 158.21 199.80 26.27 o 0 2 10 8620.06 8073.76 358.43 o 2 2 10 988.52 942.36 24.36 o 4 2 10 65.16 51.80 8.80 o 6 2 10 108.23 107.25 10.86 o 8 2 10 55.68 40.47 9.21 o 10 2 10 134.23 138.53 16.41 o 12 2 10 1336.12 1447.29 41.07 o 2 4 10 985.03 918.85 24.46 o 4 4 10 789.43 814.78 23.45 o 6 4 10 408.09 412.84 16.49 o 8 4 10 281.53 286.12 16.25 o 10 4 10 38.99 44.35 11.47 o 12 4 10 51.05 83.97 16.32 o 0 6 10 3497.13 2979.21 69.09 o 2 6 10 304.82 279.13 16.01 o 4 6 10 1923.83 1871.06 35.15 o 6 6 10 251.49 239.77 15.37 o 8 6 10 37.83 45.38 9.14 o 10 6 10 1140.27 1233.75 32.40 o 12 6 10 1638.70 1825.51 53.92 o 2 8 10 834.16 797.28 27.45 o 4 8 10 222.61 237.12 16.10 o 6 8 10 417.28 388.65 19.15 o 8 8 10 697.44 718.68 25.30 o 10 8 10 1145.31 1257.08 47.51 o 0 10 10 328.67 327.62 29.17 o 2 10 10 94.26 92.89 14.35 o 4 10 10 8.82 12.01 9.88 o 6 10 10 669.08 670.44 22.45 o 8 10 10 34.80 47.94 11.20 o 10 10 10 33.26 40.76 18.13 o 2 12 10 252.47 244.38 20.77 o 4 12 10 613.58 634.11 25.18 o 6 12 10 1082.71 1155.15 32.92 o 8 12 10 10.28 6.62 14.10 o 0 14 10 603.95 704.75 44.03 o 2 14 10 204.11 216.95 21.09 o 4 14 10 289.12 331.49 25.51 o 1 1 11 134.19 108.45 13.67 o 3 1 11 1457.86 1344.74 30.67 o 5 1 11 358.18 382.72 19.94 o 7 1 11 17.86 15.56 8.82 o 9 1 11 261.65 265.75 20.69 o 11 1 11 74.65 64.81 15.22 o 1 3 11 1441.29 1330.55 33.86 o 3 3 11 2.78 -0.39 8.13 o 5 3 11 639.31 604.63 20.28 o 7 3 11 134.64 143.36 13.14 o 9 3 11 286.58 320.78 22.23 o 11 3 11 368.45 437.55 26.57 o 1 5 11 248.63 242.07 18.29 o 3 5 11 469.07 484.54 26.16 o 5 5 11 525.65 546.38 21.67 o 7 5 11 53.73 51.12 10.36 o 9 5 11 465.37 523.60 23.39 o 11 5 11 25.81 33.85 15.16 o 1 7 11 710.63 699.38 31.25 o 3 7 11 399.37 390.55 19.41 o 5 7 11 519.68 539.98 22.44 o 7 7 11 874.22 883.54 27.89 o 9 7 11 982.95 1071.83 35.58 o 1 9 11 93.99 91.33 17.23 o 3 9 11 1101.52 1138.64 40.20 o 5 9 11 38.23 34.34 12.80 o 7 9 11 412.00 423.28 20.31 o 9 9 11 767.72 812.84 33.21 o 1 11 11 14.96 24.55 12.66 o 3 11 11 552.73 584.55 27.81 o 5 11 11 80.61 76.75 14.11 o 7 11 11 27.25 35.88 16.25 o 1 13 11 45.84 33.24 14.30 o 3 13 11 177.13 163.08 20.08 o 0 0 12 483.31 463.71 46.57 o 4 0 12 1813.56 1835.68 62.47 o 8 0 12 433.77 450.27 29.61 o 2 2 12 13.62 11.39 10.56 o 4 2 12 279.64 275.13 18.23 o 6 2 12 124.44 148.97 14.01 o 8 2 12 240.50 278.68 17.73 o 10 2 12 235.67 311.20 27.62 o 0 4 12 6314.50 5933.70 170.96 o 2 4 12 259.88 220.68 18.72 o 4 4 12 472.19 446.75 20.86 o 6 4 12 198.89 215.61 15.91 o 8 4 12 43.94 42.56 12.81 o 2 6 12 315.18 273.41 23.78 o 4 6 12 107.80 106.55 13.52 o 6 6 12 634.96 671.04 25.78 o 8 6 12 432.35 442.18 23.61 o 0 8 12 206.52 232.17 30.25 o 2 8 12 448.77 477.99 25.21 o 4 8 12 150.58 165.68 16.95 o 6 8 12 128.04 145.00 16.80 o 2 10 12 799.19 819.83 38.26 o 4 10 12 765.82 786.62 32.61 o 1 1 13 1295.54 1234.54 40.56 o 3 1 13 528.47 459.82 25.21 o 5 1 13 2.95 -0.64 11.31 o 7 1 13 50.36 52.33 12.83 o 1 3 13 146.14 133.81 17.51 o 3 3 13 340.31 379.96 29.81 o 5 3 13 69.49 82.89 14.15 o 7 3 13 157.60 132.51 14.85 o 1 5 13 146.46 141.50 16.72 o 3 5 13 22.49 22.15 12.66 o 5 5 13 0.80 -4.00 11.43 o 7 5 13 89.60 93.59 16.29 o 1 7 13 107.75 105.60 17.20 o 3 7 13 853.09 874.45 38.91 o 5 7 13 67.54 55.93 13.99 o 1 9 13 94.75 78.91 17.32 o 2 0 14 74.16 77.24 22.65 o 0 2 14 135.83 166.31 27.83 o 2 2 14 614.32 591.32 29.84 o 4 2 14 78.55 52.48 15.96 o 2 4 14 727.35 749.65 33.08 o