#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2201835.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201835_Fobs loop_ _publ_author_name 'Matthews, Melissa L.' 'Webster, Michael' _publ_section_title ; Tris(nitrato-\k^2^O,O')tris(triphenylphosphine oxide-\kO)terbium(III) acetone sesquisolvate ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m322 _journal_page_last m323 _journal_volume 59 _journal_year 2003 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 94.895 _cell_angle_gamma 90.000 _cell_length_a 11.0612 _cell_length_b 19.1798 _cell_length_c 27.6409 _exptl_crystal_F_000 2576.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file bt6278Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' [Tb(NO3)3(Ph3PO)3].1.5(Me2CO)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 496.76 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 6 0 0 100059.36 101444.35 6262.60 o 8 0 0 10974.27 10149.87 689.96 o 10 0 0 22724.89 26117.94 2165.91 o 12 0 0 2688.93 2708.96 507.59 o 2 1 0 167029.95 153752.55 16939.12 o 3 1 0 9621.05 8637.88 314.54 o 4 1 0 42871.18 41263.41 1726.20 o 5 1 0 16.02 0.00 254.71 o 6 1 0 17689.50 16154.10 814.06 o 7 1 0 840.95 898.91 136.47 o 8 1 0 17677.24 18012.92 968.82 o 9 1 0 15.27 180.54 180.54 o 10 1 0 404.33 419.87 147.32 o 11 1 0 13.11 -90.05 259.72 o 12 1 0 15074.68 16681.65 1569.93 o 13 1 0 136.74 178.39 252.29 o 2 2 0 515.91 358.90 358.90 o 3 2 0 3246.75 3278.82 160.82 o 4 2 0 31189.93 31558.06 1154.74 o 5 2 0 530.86 810.07 179.77 o 6 2 0 59387.76 60326.57 2610.36 o 7 2 0 1065.94 983.53 146.94 o 8 2 0 4227.60 4134.17 294.21 o 9 2 0 70.20 143.95 160.94 o 10 2 0 16507.20 17113.19 1131.57 o 11 2 0 52.47 215.24 160.94 o 12 2 0 2033.50 2381.57 359.25 o 13 2 0 284.24 536.09 253.53 o 2 3 0 70959.12 71304.26 3621.60 o 3 3 0 1769.83 2550.57 475.40 o 4 3 0 44022.53 40401.49 2191.02 o 5 3 0 9020.73 9622.24 508.70 o 6 3 0 26754.37 22400.16 2519.44 o 7 3 0 3183.15 3214.22 213.79 o 8 3 0 13563.21 14824.15 781.98 o 9 3 0 593.84 598.46 146.87 o 10 3 0 1801.36 1478.04 174.50 o 11 3 0 14.64 -79.88 174.34 o 12 3 0 8313.32 7655.31 927.36 o 2 4 0 130.83 359.73 207.03 o 3 4 0 188.06 449.10 179.30 o 4 4 0 43505.49 41521.70 2551.17 o 5 4 0 114.15 359.69 207.00 o 6 4 0 31573.92 30544.22 1608.14 o 7 4 0 911.65 539.39 179.36 o 8 4 0 5743.27 5769.62 644.21 o 9 4 0 120.52 268.89 179.26 o 10 4 0 6229.91 6235.41 556.45 o 11 4 0 476.79 159.70 174.32 o 12 4 0 773.56 1208.17 366.86 o 1 5 0 40964.27 44580.64 1978.29 o 2 5 0 64220.68 61581.58 2657.94 o 3 5 0 6404.51 7333.45 526.52 o 4 5 0 5270.02 5370.10 361.30 o 5 5 0 368.58 628.44 179.31 o 6 5 0 10588.63 9295.23 635.36 o 7 5 0 29.71 -89.63 179.25 o 8 5 0 15575.81 16576.65 896.19 o 9 5 0 3.14 179.25 253.50 o 10 5 0 501.62 478.89 227.01 o 11 5 0 6.08 -90.16 292.95 o 12 5 0 5180.91 4688.41 765.89 o 0 6 0 20553.68 15497.13 917.46 o 1 6 0 2466.64 2356.26 127.19 o 2 6 0 7824.89 7146.40 314.34 o 3 6 0 2657.41 2780.58 176.37 o 4 6 0 20241.93 21879.19 1231.58 o 5 6 0 885.13 898.93 179.38 o 6 6 0 9776.31 9156.43 834.56 o 7 6 0 1216.72 1051.48 258.44 o 8 6 0 5230.11 4485.11 520.06 o 9 6 0 144.55 153.66 198.88 o 10 6 0 6674.92 6234.98 1503.48 o 11 6 0 9.56 179.47 292.95 o 12 6 0 1673.66 2023.51 538.14 o 1 7 0 17954.68 15247.27 641.59 o 2 7 0 75569.56 74320.46 3319.88 o 3 7 0 4046.92 4574.95 325.60 o 4 7 0 8520.16 8894.52 541.84 o 5 7 0 242.71 119.52 207.02 o 6 7 0 144.22 89.63 179.27 o 7 7 0 759.14 718.04 254.60 o 8 7 0 2583.13 2278.73 359.90 o 9 7 0 713.98 719.29 179.32 o 10 7 0 93.74 89.74 292.96 o 11 7 0 53.47 -239.39 320.97 o 12 7 0 7231.04 7079.45 1049.16 o 0 8 0 43639.93 43994.73 3456.25 o 1 8 0 61.13 0.00 146.37 o 2 8 0 18504.46 19613.87 826.43 o 3 8 0 15826.52 15204.64 766.73 o 4 8 0 20186.47 19990.78 1081.71 o 5 8 0 143.59 358.54 179.27 o 6 8 0 9516.37 10514.89 939.58 o 7 8 0 733.66 409.90 198.95 o 8 8 0 2102.14 1016.96 414.45 o 9 8 0 842.22 659.14 226.84 o 10 8 0 11525.30 13940.96 1566.38 o 11 8 0 2.28 239.96 414.62 o 12 8 0 1450.08 1316.85 414.88 o 1 9 0 1447.82 1900.47 135.69 o 2 9 0 11059.18 10524.73 479.18 o 3 9 0 3171.04 3540.97 221.40 o 4 9 0 3840.89 3951.11 347.64 o 5 9 0 1558.78 1794.50 310.82 o 6 9 0 2003.70 2173.19 227.03 o 7 9 0 1639.00 1292.83 271.27 o 8 9 0 9701.11 8762.46 907.67 o 9 9 0 1181.79 1526.27 358.72 o 10 9 0 31.75 89.63 292.72 o 11 9 0 187.26 538.66 380.89 o 12 9 0 7550.52 8857.44 1383.89 o 0 10 0 15666.25 14217.20 805.65 o 1 10 0 206.28 462.77 135.53 o 2 10 0 1645.37 1889.13 178.51 o 3 10 0 447.73 478.17 207.05 o 4 10 0 12172.78 12814.58 886.54 o 5 10 0 89.26 268.89 179.26 o 6 10 0 8763.48 8767.43 701.68 o 7 10 0 1737.99 1714.55 230.21 o 8 10 0 90.24 51.22 221.78 o 9 10 0 84.53 -71.70 354.91 o 10 10 0 5882.70 6201.51 913.20 o 11 10 0 88.34 -239.01 239.01 o 1 11 0 1561.55 2214.30 152.79 o 2 11 0 6135.27 5863.68 305.85 o 3 11 0 2.30 268.88 179.25 o 4 11 0 4571.27 5152.10 317.28 o 5 11 0 16.05 358.50 206.98 o 6 11 0 7897.04 8264.71 820.35 o 7 11 0 147.96 239.02 226.75 o 8 11 0 4842.04 4784.25 609.66 o 9 11 0 1.63 0.00 413.96 o 10 11 0 6.99 119.50 413.96 o 11 11 0 257.58 239.03 414.01 o 0 12 0 8084.21 9009.68 519.40 o 1 12 0 1.86 179.25 146.36 o 2 12 0 1700.87 1739.05 206.29 o 3 12 0 5513.75 5805.27 309.26 o 4 12 0 4138.16 4580.64 380.29 o 5 12 0 334.86 119.52 225.38 o 6 12 0 7151.24 8280.63 870.54 o 7 12 0 1633.07 1434.04 271.24 o 8 12 0 646.87 418.39 226.81 o 9 12 0 277.51 178.41 379.69 o 10 12 0 3624.98 1756.11 937.82 o 11 12 0 255.48 50.73 688.84 o 1 13 0 4158.32 4367.02 264.43 o 2 13 0 7671.20 7690.19 570.30 o 3 13 0 1159.68 1145.08 158.30 o 4 13 0 5191.34 5206.45 374.70 o 5 13 0 4504.57 4683.64 1093.15 o 6 13 0 10812.02 12249.33 1135.36 o 7 13 0 136.40 417.71 361.74 o 8 13 0 4704.37 4480.12 671.71 o 9 13 0 639.41 260.80 307.38 o 10 13 0 447.33 -358.57 358.57 o 0 14 0 40283.69 40802.72 2661.78 o 1 14 0 6776.11 6879.58 399.16 o 2 14 0 42.08 51.22 135.50 o 3 14 0 7754.04 7332.18 462.18 o 4 14 0 2683.86 2764.01 223.62 o 5 14 0 317.00 307.34 221.80 o 6 14 0 10816.35 10201.99 1024.86 o 7 14 0 1949.10 2166.66 436.12 o 8 14 0 2739.06 3582.10 585.72 o 9 14 0 325.29 -504.63 504.63 o 10 14 0 6457.30 6750.47 1193.87 o 1 15 0 8239.35 8272.91 401.58 o 2 15 0 8745.71 8696.60 543.94 o 3 15 0 1290.64 1630.40 199.71 o 4 15 0 341.13 143.43 169.03 o 5 15 0 1183.36 1210.82 240.38 o 6 15 0 3442.23 3384.62 516.86 o 7 15 0 10.97 894.53 536.03 o 8 15 0 10312.61 11285.96 1635.93 o 9 15 0 3557.45 3221.17 714.66 o 0 16 0 13133.86 13871.68 1415.26 o 1 16 0 4216.69 4103.99 312.22 o 2 16 0 2089.67 2333.47 268.81 o 3 16 0 1877.02 1497.80 179.49 o 4 16 0 4485.12 4889.21 438.71 o 5 16 0 384.83 438.21 206.83 o 6 16 0 4039.56 4625.29 681.33 o 7 16 0 2831.87 3670.41 1789.69 o 8 16 0 1651.72 1609.27 504.93 o 9 16 0 69.16 358.51 594.03 o 1 17 0 408.63 469.78 187.36 o 2 17 0 10183.85 10747.66 710.65 o 3 17 0 9.99 59.75 152.87 o 4 17 0 6419.13 5957.95 516.61 o 5 17 0 114.81 239.01 225.34 o 6 17 0 2109.29 1563.93 1042.85 o 7 17 0 5.51 0.00 358.50 o 8 17 0 4735.60 5089.10 1117.09 o 0 18 0 10503.89 11315.26 1001.24 o 1 18 0 1703.37 1558.66 174.25 o 2 18 0 661.24 559.69 239.86 o 3 18 0 596.38 940.07 201.59 o 4 18 0 7762.20 7121.61 759.38 o 5 18 0 4.08 571.67 238.87 o 6 18 0 5187.01 3683.74 759.84 o 7 18 0 2317.68 3370.33 1071.42 o 8 18 0 1258.02 713.93 504.83 o 1 19 0 213.14 0.00 169.06 o 2 19 0 9373.25 9412.41 752.25 o 3 19 0 127.18 65.93 214.30 o 4 19 0 5632.59 4767.47 496.98 o 5 19 0 563.97 627.32 316.09 o 6 19 0 3770.27 4740.29 894.28 o 7 19 0 17.60 -356.78 504.56 o 0 20 0 8884.26 8780.25 1165.37 o 1 20 0 1558.94 1544.97 254.14 o 2 20 0 468.74 494.30 220.57 o 3 20 0 12.89 -179.68 192.15 o 4 20 0 3719.80 4056.76 741.18 o 5 20 0 1220.78 897.13 294.26 o 6 20 0 7411.46 7440.98 1119.95 o 1 21 0 1462.84 1114.86 253.97 o 2 21 0 11258.47 12550.87 1024.36 o 3 21 0 13.62 -102.71 199.44 o 4 21 0 3801.44 6176.88 1253.35 o 5 21 0 1052.62 719.88 294.23 o 0 22 0 11708.95 13291.06 1732.02 o 1 22 0 1198.54 1180.44 341.12 o 2 22 0 30.10 -124.05 196.12 o 3 22 0 73.49 358.51 507.01 o -11 0 1 9693.78 9777.00 1811.33 o -9 0 1 4.94 90.05 180.11 o -7 0 1 175.59 239.03 207.01 o -5 0 1 85773.30 87930.55 5372.65 o -3 0 1 168761.27 183166.33 13086.31 o 3 0 1 56439.43 53982.38 2925.99 o 5 0 1 24868.18 24816.48 1418.43 o 7 0 1 4562.45 4864.93 415.83 o 9 0 1 44707.12 47271.19 3765.12 o 11 0 1 18.86 179.25 541.20 o 13 0 1 5215.46 6076.82 1430.25 o -13 1 1 3334.24 3105.53 362.46 o -12 1 1 9.61 0.00 207.48 o -11 1 1 6.63 238.62 226.06 o -10 1 1 1020.57 898.29 187.89 o -9 1 1 14413.68 14979.04 910.65 o -8 1 1 21.95 214.83 160.63 o -7 1 1 1920.70 1820.00 169.36 o -6 1 1 528.40 873.69 135.56 o -5 1 1 43213.54 44442.47 2014.51 o -4 1 1 488.90 659.60 146.45 o -3 1 1 153102.19 157925.77 6524.64 o -2 1 1 1172.11 722.47 359.51 o 2 1 1 1536.30 2319.05 230.87 o 3 1 1 20786.90 19580.30 850.26 o 4 1 1 3250.50 3467.09 154.88 o 5 1 1 53399.45 53114.23 2277.89 o 6 1 1 2174.88 2695.30 211.85 o 7 1 1 32547.71 32960.06 1383.86 o 8 1 1 25.52 60.04 147.06 o 9 1 1 2140.83 1937.34 293.52 o 10 1 1 833.24 629.79 180.18 o 11 1 1 17461.24 18858.79 1730.71 o 12 1 1 45.27 477.98 206.97 o -13 2 1 609.23 178.43 252.34 o -12 2 1 11.63 72.11 239.13 o -11 2 1 8675.41 8902.61 647.37 o -10 2 1 19.06 -160.94 160.94 o -9 2 1 1689.32 2110.19 247.59 o -8 2 1 874.29 1004.64 161.44 o -7 2 1 4597.46 4157.80 180.38 o -6 2 1 746.35 1034.87 160.43 o -5 2 1 50214.88 49146.96 2230.98 o -4 2 1 3083.83 3044.23 161.44 o -3 2 1 45566.73 43090.31 1979.52 o -2 2 1 371.08 358.79 358.79 o 1 2 1 659.95 3565.70 420.33 o 2 2 1 4411.27 4239.64 242.46 o 3 2 1 62861.19 57704.34 2464.30 o 4 2 1 7203.22 6846.68 344.50 o 5 2 1 48287.34 48210.54 2020.70 o 6 2 1 4473.44 4406.79 296.31 o 7 2 1 8493.05 8786.31 507.93 o 8 2 1 3143.56 3202.92 210.04 o 9 2 1 39876.25 42601.96 2357.80 o 10 2 1 924.32 1014.18 157.43 o 11 2 1 142.82 -90.06 180.12 o 12 2 1 669.33 791.42 239.20 o 13 2 1 5568.52 7535.77 1437.36 o -13 3 1 2074.88 2348.07 507.44 o -12 3 1 807.47 287.18 239.21 o -11 3 1 100.82 215.51 160.63 o -10 3 1 1013.98 1283.02 229.70 o -9 3 1 25095.99 27491.05 1934.08 o -8 3 1 67.78 90.06 180.11 o -7 3 1 1340.79 1666.78 156.61 o -6 3 1 5.06 -89.63 179.25 o -5 3 1 17334.54 17063.08 1109.77 o -4 3 1 4858.19 4287.03 261.48 o -3 3 1 40039.81 38543.89 1742.88 o -2 3 1 4047.24 4377.13 270.40 o -1 3 1 22576.13 15593.44 2807.87 o 1 3 1 86660.70 59040.81 13135.19 o 2 3 1 37.86 179.26 253.52 o 3 3 1 15662.28 14788.15 740.56 o 4 3 1 4815.02 4331.10 241.72 o 5 3 1 85888.45 86739.53 3631.41 o 6 3 1 325.42 478.13 207.04 o 7 3 1 31191.38 31560.50 1424.47 o 8 3 1 4567.65 5161.53 376.20 o 9 3 1 1211.79 830.14 191.67 o 10 3 1 3205.44 2964.57 254.38 o 11 3 1 12708.87 12979.03 1147.62 o 12 3 1 0.03 0.00 179.68 o -12 4 1 134.12 0.29 259.82 o -11 4 1 6039.50 5682.05 392.58 o -10 4 1 0.46 -119.88 207.64 o -9 4 1 836.14 628.51 179.32 o -8 4 1 2165.76 1991.90 227.04 o -7 4 1 33011.79 35923.89 2133.49 o -6 4 1 1881.78 2004.15 160.02 o -5 4 1 19461.40 18592.29 979.91 o -4 4 1 0.22 0.00 179.25 o -3 4 1 1033.35 841.36 207.27 o -2 4 1 12256.53 10997.94 609.59 o -1 4 1 61920.00 55798.83 2703.93 o 0 4 1 4793.59 4776.84 218.40 o 1 4 1 83.07 986.04 179.28 o 2 4 1 34053.55 32502.31 1441.11 o 3 4 1 71579.98 69270.48 3579.63 o 4 4 1 5500.76 5707.62 201.29 o 5 4 1 18807.83 17987.86 816.18 o 6 4 1 2848.65 2665.36 215.02 o 7 4 1 6002.14 6275.59 365.55 o 8 4 1 874.49 638.83 173.99 o 9 4 1 13305.89 14434.37 1045.64 o 10 4 1 182.40 268.90 179.27 o 11 4 1 555.60 717.88 271.44 o 12 4 1 173.76 360.25 292.97 o -12 5 1 1276.03 1319.65 414.86 o -11 5 1 4.41 359.19 239.13 o -10 5 1 13.06 239.00 206.98 o -9 5 1 20685.51 20691.00 1334.82 o -8 5 1 621.60 667.90 208.05 o -7 5 1 4159.16 4496.15 468.52 o -6 5 1 38.55 179.26 206.99 o -5 5 1 10047.84 9658.66 636.52 o -4 5 1 1746.45 2252.91 286.00 o -3 5 1 44486.87 42602.52 2574.74 o -2 5 1 1913.89 1441.39 207.55 o -1 5 1 40083.26 39061.46 2076.93 o 0 5 1 15824.87 20079.42 840.32 o 1 5 1 934.53 933.52 160.57 o 2 5 1 11843.41 12000.21 521.58 o 3 5 1 118.54 0.00 207.01 o 4 5 1 10306.42 11353.17 725.35 o 5 5 1 28033.01 27614.26 1588.80 o 6 5 1 838.43 1078.49 207.11 o 7 5 1 21196.49 20027.74 968.81 o 8 5 1 3219.40 3380.71 408.29 o 9 5 1 85.53 179.26 179.26 o 10 5 1 58.77 270.39 233.79 o 11 5 1 9718.67 10091.61 763.39 o 12 5 1 162.47 0.00 539.51 o -12 6 1 98.04 360.24 718.76 o -11 6 1 9959.36 10877.49 1731.32 o -10 6 1 2057.39 901.06 359.73 o -9 6 1 127.54 307.52 207.49 o -8 6 1 53.42 153.51 198.94 o -7 6 1 29299.11 28152.46 2030.16 o -6 6 1 500.46 628.47 181.42 o -5 6 1 25553.00 26191.38 1561.88 o -4 6 1 3182.62 2826.87 328.32 o -3 6 1 16061.37 16145.35 919.45 o -2 6 1 3315.61 3198.75 150.19 o -1 6 1 46356.25 46908.02 2343.31 o 0 6 1 45.55 89.63 179.26 o 1 6 1 41026.94 43003.15 1988.93 o 2 6 1 15567.05 15869.89 727.64 o 3 6 1 81471.60 81572.70 3844.69 o 4 6 1 2413.84 2834.52 199.32 o 5 6 1 137.95 239.03 225.36 o 6 6 1 1714.66 1482.79 179.48 o 7 6 1 272.11 268.92 179.28 o 8 6 1 2.86 90.49 181.85 o 9 6 1 36164.69 38187.30 3276.02 o 10 6 1 4206.07 3478.45 423.15 o 11 6 1 79.13 239.01 206.99 o 12 6 1 107.85 239.39 360.24 o -12 7 1 1242.80 816.84 401.72 o -11 7 1 33.33 358.51 358.51 o -10 7 1 25.30 -73.49 356.14 o -9 7 1 16408.07 17155.35 1531.08 o -8 7 1 3313.83 3551.30 423.57 o -7 7 1 34.98 179.25 179.25 o -6 7 1 2484.46 2242.40 271.48 o -5 7 1 10273.32 10631.52 724.15 o -4 7 1 35.65 0.00 206.99 o -3 7 1 115846.98 121570.74 6725.35 o -2 7 1 2209.61 2419.64 146.22 o -1 7 1 20131.14 20426.90 833.24 o 0 7 1 1278.55 818.31 156.75 o 1 7 1 34303.52 31121.46 1282.46 o 2 7 1 1114.78 1114.89 147.00 o 3 7 1 14687.65 15033.14 689.08 o 4 7 1 2358.28 2415.32 209.46 o 5 7 1 2247.35 1959.81 259.19 o 6 7 1 611.76 448.32 179.33 o 7 7 1 2324.21 2557.87 271.59 o 8 7 1 56.04 -73.49 356.14 o 9 7 1 670.37 418.73 226.93 o 10 7 1 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