#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:59:50 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180938 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/18/2201836.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201836_Fobs loop_ _publ_author_name 'Fleischer, Holger' 'Schollmeyer, Dieter' _publ_section_title ; Butanedithiol diacetate ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o845 _journal_page_last o847 _journal_volume 59 _journal_year 2003 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.942 _cell_angle_gamma 90.000 _cell_length_a 6.1998 _cell_length_b 8.0292 _cell_length_c 10.5650 _exptl_crystal_F_000 220.00 _reflns_d_resolution_high 0.8026 _cod_data_source_file bt6279Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' hfr444 in P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 65.90 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 46.56 29.74 5.07 o 2 0 0 2870.12 1970.04 334.28 o 3 0 0 2810.73 2106.86 439.51 o 4 0 0 194.07 148.75 31.80 o 5 0 0 104.63 99.91 23.58 o 6 0 0 41.65 39.66 7.35 o 7 0 0 64.89 71.52 18.42 o 1 1 0 2409.39 1891.16 381.09 o 2 1 0 2728.44 2189.36 507.75 o 3 1 0 417.45 369.29 75.30 o 4 1 0 19.24 13.69 2.91 o 5 1 0 239.83 219.02 49.24 o 6 1 0 11.18 14.26 2.95 o 7 1 0 2.68 2.42 2.00 o 0 2 0 2864.64 2346.41 31.12 o 1 2 0 0.38 1.58 0.93 o 2 2 0 161.30 142.07 26.67 o 3 2 0 732.96 705.53 132.98 o 4 2 0 19.93 22.46 7.46 o 5 2 0 8.09 5.57 2.32 o 6 2 0 115.84 110.65 14.07 o 7 2 0 30.58 28.68 5.07 o 1 3 0 45.67 44.71 1.58 o 2 3 0 2.64 1.61 1.48 o 3 3 0 10.94 8.68 2.43 o 4 3 0 9.01 9.91 1.60 o 5 3 0 0.09 1.70 2.87 o 6 3 0 0.25 -0.27 2.98 o 7 3 0 7.31 3.06 1.71 o 0 4 0 29.52 34.74 2.27 o 1 4 0 91.94 104.71 6.74 o 2 4 0 142.05 120.65 7.99 o 3 4 0 55.92 60.64 5.14 o 4 4 0 111.24 110.42 9.56 o 5 4 0 38.19 36.82 6.52 o 6 4 0 3.75 5.69 1.57 o 7 4 0 96.78 90.16 14.54 o 1 5 0 192.98 166.25 6.61 o 2 5 0 17.43 12.00 4.64 o 3 5 0 9.46 10.74 1.61 o 4 5 0 418.99 402.15 41.82 o 5 5 0 154.80 157.02 16.11 o 6 5 0 132.16 134.92 16.06 o 0 6 0 377.29 368.06 12.05 o 1 6 0 75.14 66.28 2.87 o 2 6 0 99.23 97.84 3.48 o 3 6 0 309.69 303.17 11.43 o 4 6 0 241.90 244.60 13.36 o 5 6 0 2.94 4.17 1.85 o 6 6 0 43.67 42.72 9.25 o 1 7 0 362.54 305.63 7.05 o 2 7 0 206.97 191.20 4.91 o 3 7 0 133.25 122.87 5.68 o 4 7 0 119.42 109.97 3.61 o 5 7 0 59.94 59.73 5.53 o 0 8 0 216.95 175.51 6.77 o 1 8 0 10.65 7.60 2.95 o 2 8 0 2.05 2.89 1.78 o 3 8 0 153.09 144.91 7.84 o 4 8 0 39.35 39.54 2.20 o 1 9 0 2.13 -0.82 5.46 o 2 9 0 9.01 8.74 1.37 o 3 9 0 14.60 16.58 1.80 o 0 10 0 13.17 13.97 1.80 o -7 1 1 58.42 50.91 3.90 o -6 1 1 47.97 36.23 3.16 o -5 1 1 17.81 16.66 2.75 o -4 1 1 20.75 18.92 2.29 o -3 1 1 223.55 172.76 5.54 o -2 1 1 394.48 294.13 7.22 o -1 1 1 205.92 171.01 4.21 o 0 1 1 186.28 180.94 4.89 o 1 1 1 1223.24 1336.84 20.07 o 2 1 1 556.86 638.04 15.31 o 3 1 1 469.92 541.57 16.63 o 4 1 1 30.55 40.04 3.04 o 5 1 1 89.13 102.21 5.17 o 6 1 1 72.45 85.70 4.65 o 7 1 1 73.01 89.06 4.45 o -7 2 1 55.03 36.84 3.52 o -6 2 1 105.21 101.45 5.09 o -5 2 1 247.65 197.57 7.04 o -4 2 1 21.02 18.22 2.89 o -3 2 1 589.03 486.61 12.08 o -2 2 1 36.61 24.04 1.89 o -1 2 1 792.90 740.49 15.08 o 0 2 1 3438.36 2894.08 37.29 o 1 2 1 251.91 236.56 5.97 o 2 2 1 488.71 560.85 15.13 o 3 2 1 245.81 324.55 9.70 o 4 2 1 654.81 761.32 17.98 o 5 2 1 206.56 241.14 7.84 o 6 2 1 20.77 25.89 3.23 o 7 2 1 71.95 85.79 4.32 o -7 3 1 91.17 89.20 4.26 o -6 3 1 0.05 0.72 5.06 o -5 3 1 221.16 196.82 7.23 o -4 3 1 556.71 474.29 14.20 o -3 3 1 534.29 487.13 12.89 o -2 3 1 639.20 567.64 16.78 o -1 3 1 579.65 537.23 14.49 o 0 3 1 4342.98 3833.28 50.91 o 1 3 1 295.66 306.09 7.80 o 2 3 1 67.17 67.81 3.07 o 3 3 1 1473.85 1665.23 35.21 o 4 3 1 0.81 -2.72 4.82 o 5 3 1 45.15 54.41 3.75 o 6 3 1 169.79 210.47 6.80 o 7 3 1 32.88 35.41 2.61 o -7 4 1 40.58 37.56 2.49 o -6 4 1 151.05 125.55 5.39 o -5 4 1 145.25 127.12 5.85 o -4 4 1 7.09 3.12 4.55 o -3 4 1 614.28 557.62 15.02 o -2 4 1 794.59 739.44 21.35 o -1 4 1 175.51 177.02 5.62 o 0 4 1 339.30 304.52 8.63 o 1 4 1 1271.12 1146.86 25.49 o 2 4 1 212.00 196.32 6.53 o 3 4 1 1.52 3.28 3.88 o 4 4 1 401.34 430.97 14.35 o 5 4 1 88.63 114.28 5.44 o 6 4 1 0.07 -3.53 3.81 o -6 5 1 16.14 9.24 2.55 o -5 5 1 20.46 19.99 2.81 o -4 5 1 122.57 119.89 5.45 o -3 5 1 113.59 104.26 4.99 o -2 5 1 100.06 94.54 4.35 o -1 5 1 26.99 26.87 2.34 o 0 5 1 398.23 370.50 11.02 o 1 5 1 426.57 427.20 12.11 o 2 5 1 33.59 34.23 2.92 o 3 5 1 763.74 803.85 19.58 o 4 5 1 19.44 17.19 2.75 o 5 5 1 0.86 1.49 1.78 o 6 5 1 167.91 173.61 6.05 o -6 6 1 10.43 7.45 1.91 o -5 6 1 43.85 41.97 3.24 o -4 6 1 28.37 26.12 3.04 o -3 6 1 24.30 25.64 2.96 o -2 6 1 1.68 0.00 4.72 o -1 6 1 42.51 37.94 3.19 o 0 6 1 27.70 21.74 2.72 o 1 6 1 16.19 20.59 2.48 o 2 6 1 2.44 -2.21 4.59 o 3 6 1 121.77 118.95 5.61 o 4 6 1 63.25 59.13 4.39 o 5 6 1 91.26 93.74 5.40 o 6 6 1 0.05 1.91 1.13 o -5 7 1 1.76 0.86 3.55 o -4 7 1 97.02 90.14 4.51 o -3 7 1 31.56 29.66 3.20 o -2 7 1 2.69 4.06 2.01 o -1 7 1 155.16 133.71 5.83 o 0 7 1 14.71 12.07 2.34 o 1 7 1 47.36 42.29 3.24 o 2 7 1 0.32 0.00 3.26 o 3 7 1 0.07 0.00 3.57 o 4 7 1 4.14 0.00 3.64 o 5 7 1 1.84 2.87 1.44 o -4 8 1 0.85 0.44 3.41 o -3 8 1 101.49 92.12 4.61 o -2 8 1 32.10 33.77 2.88 o -1 8 1 8.97 5.34 2.18 o 0 8 1 36.95 38.22 3.27 o 1 8 1 139.78 127.18 5.57 o 2 8 1 1.79 3.40 1.87 o 3 8 1 1.92 1.02 1.99 o 4 8 1 114.96 117.48 5.08 o -3 9 1 0.86 3.38 1.27 o -2 9 1 5.01 3.43 4.01 o -1 9 1 163.13 150.17 6.09 o 0 9 1 93.58 85.27 4.84 o 1 9 1 1.36 0.57 3.72 o 2 9 1 45.73 46.30 3.40 o 3 9 1 90.45 85.19 3.70 o -7 0 2 14.68 12.13 2.38 o -6 0 2 135.72 119.81 5.61 o -5 0 2 1171.76 936.27 29.27 o -4 0 2 497.77 417.27 12.38 o -3 0 2 48.69 42.71 2.72 o -2 0 2 2428.38 1861.63 29.95 o -1 0 2 4140.79 4201.56 50.23 o 0 0 2 3538.86 3882.43 44.86 o 1 0 2 56.70 59.75 2.03 o 2 0 2 3.49 5.21 1.30 o 3 0 2 365.49 385.65 10.55 o 4 0 2 692.72 737.24 17.62 o 5 0 2 161.75 166.01 6.54 o 6 0 2 180.81 216.80 7.11 o 7 0 2 45.44 61.17 3.65 o -7 1 2 184.84 161.42 6.44 o -6 1 2 61.70 56.54 4.08 o -5 1 2 1.96 3.90 4.21 o -4 1 2 503.62 428.57 12.79 o -3 1 2 2084.41 1758.73 33.54 o -2 1 2 341.08 314.84 7.74 o -1 1 2 539.17 512.34 11.48 o 0 1 2 2787.70 2439.79 31.38 o 1 1 2 137.28 152.90 4.47 o 2 1 2 33.85 35.69 2.04 o 3 1 2 396.48 456.31 11.61 o 4 1 2 192.53 205.65 6.67 o 5 1 2 13.71 9.34 2.48 o 6 1 2 130.18 150.92 6.09 o 7 1 2 198.59 225.46 8.16 o -7 2 2 0.95 3.10 1.75 o -6 2 2 3.15 5.73 2.24 o -5 2 2 182.09 169.47 6.50 o -4 2 2 4.70 5.68 2.04 o -3 2 2 10.86 15.04 2.01 o -2 2 2 1775.27 1700.40 30.06 o -1 2 2 8.93 8.98 1.13 o 0 2 2 1426.95 1386.71 22.63 o 1 2 2 2184.41 2264.77 33.61 o 2 2 2 61.06 79.35 3.17 o 3 2 2 600.62 709.37 20.88 o 4 2 2 335.50 361.71 10.30 o 5 2 2 32.22 31.43 3.29 o 6 2 2 137.84 162.19 6.23 o 7 2 2 0.85 1.08 1.60 o -7 3 2 1.34 2.46 2.66 o -6 3 2 8.86 11.30 2.18 o -5 3 2 9.27 8.36 2.44 o -4 3 2 79.51 77.22 4.30 o -3 3 2 6.15 -1.59 3.56 o -2 3 2 113.56 106.01 3.84 o -1 3 2 51.34 54.88 2.52 o 0 3 2 4.05 3.98 1.09 o 1 3 2 12.82 12.01 1.62 o 2 3 2 8.74 8.91 1.69 o 3 3 2 114.17 130.59 5.05 o 4 3 2 27.24 26.29 3.06 o 5 3 2 22.80 25.96 3.01 o 6 3 2 62.29 65.86 4.02 o 7 3 2 0.13 1.92 2.08 o -7 4 2 22.20 23.38 2.14 o -6 4 2 0.05 -3.67 3.67 o -5 4 2 4.04 -3.81 4.64 o -4 4 2 52.13 56.81 4.04 o -3 4 2 149.36 148.35 5.54 o -2 4 2 11.12 13.76 2.26 o -1 4 2 220.98 234.21 6.78 o 0 4 2 522.22 564.58 17.07 o 1 4 2 138.04 145.83 4.62 o 2 4 2 659.40 753.67 22.13 o 3 4 2 66.95 72.67 4.19 o 4 4 2 11.60 14.77 2.51 o 5 4 2 34.09 37.65 3.69 o 6 4 2 20.69 22.54 2.90 o -6 5 2 36.60 36.07 3.21 o -5 5 2 32.74 30.30 3.22 o -4 5 2 18.54 20.44 3.00 o -3 5 2 88.08 81.19 4.44 o -2 5 2 45.71 51.98 3.60 o -1 5 2 209.25 195.55 6.87 o 0 5 2 1094.69 1113.03 27.91 o 1 5 2 199.85 185.08 5.79 o 2 5 2 15.57 11.83 2.06 o 3 5 2 324.49 368.68 13.35 o 4 5 2 505.95 578.66 16.88 o 5 5 2 45.13 49.71 3.70 o 6 5 2 5.56 2.64 3.04 o -6 6 2 42.53 36.42 2.59 o -5 6 2 47.82 38.81 3.28 o -4 6 2 212.02 203.02 6.98 o -3 6 2 37.36 40.03 3.50 o -2 6 2 190.35 175.00 6.68 o -1 6 2 242.01 217.25 6.99 o 0 6 2 21.48 26.19 2.81 o 1 6 2 667.73 664.68 17.22 o 2 6 2 289.43 269.52 8.09 o 3 6 2 364.18 385.80 13.74 o 4 6 2 72.77 76.49 4.47 o 5 6 2 72.45 69.61 4.40 o -5 7 2 14.52 11.71 2.16 o -4 7 2 108.00 97.30 4.68 o -3 7 2 257.57 240.98 7.77 o -2 7 2 76.53 75.16 4.51 o -1 7 2 23.93 18.27 2.52 o 0 7 2 419.43 386.62 11.30 o 1 7 2 135.97 136.76 5.82 o 2 7 2 2.99 0.80 4.89 o 3 7 2 163.97 172.05 6.42 o 4 7 2 96.20 103.62 5.23 o 5 7 2 1.89 3.85 1.51 o -4 8 2 57.28 54.56 3.42 o -3 8 2 2.08 -1.70 3.81 o -2 8 2 86.66 84.14 4.50 o -1 8 2 89.70 83.51 4.64 o 0 8 2 6.72 -3.60 4.01 o 1 8 2 107.22 106.45 5.12 o 2 8 2 84.94 93.15 4.56 o 3 8 2 40.46 43.26 3.73 o 4 8 2 16.72 14.19 1.80 o -3 9 2 4.17 0.66 2.33 o -2 9 2 5.91 6.72 1.72 o -1 9 2 22.86 20.68 3.12 o 0 9 2 49.73 49.37 3.78 o 1 9 2 10.25 8.08 2.26 o 2 9 2 6.63 4.68 1.89 o 3 9 2 32.98 34.35 2.28 o -7 1 3 0.15 -0.50 4.04 o -6 1 3 11.04 12.95 2.69 o -5 1 3 0.81 2.18 2.22 o -4 1 3 2.51 0.82 1.97 o -3 1 3 642.51 578.41 18.20 o -2 1 3 187.53 171.18 4.96 o -1 1 3 315.83 417.63 11.25 o 0 1 3 880.81 985.35 17.92 o 1 1 3 1441.45 1556.91 25.94 o 2 1 3 184.81 220.59 7.07 o 3 1 3 194.19 235.20 7.16 o 4 1 3 198.89 228.15 7.06 o 5 1 3 2.09 0.00 4.59 o 6 1 3 60.40 65.90 3.93 o 7 1 3 12.98 12.89 2.10 o -7 2 3 82.10 78.28 4.34 o -6 2 3 3.59 6.00 2.22 o -5 2 3 38.01 30.51 3.41 o -4 2 3 389.36 335.59 9.75 o -3 2 3 108.00 84.89 3.82 o -2 2 3 229.31 231.20 7.47 o -1 2 3 1529.44 1415.55 25.31 o 0 2 3 1493.68 1396.35 24.35 o 1 2 3 40.60 42.21 2.24 o 2 2 3 391.64 469.18 11.25 o 3 2 3 698.22 832.98 23.88 o 4 2 3 176.12 189.00 6.57 o 5 2 3 18.06 20.21 2.70 o 6 2 3 61.25 73.97 4.18 o 7 2 3 34.39 38.02 2.55 o -7 3 3 32.13 28.06 2.62 o -6 3 3 154.01 144.53 5.85 o -5 3 3 351.72 342.12 10.65 o -4 3 3 14.63 17.31 2.40 o -3 3 3 334.12 316.88 10.57 o -2 3 3 763.85 698.76 19.73 o -1 3 3 136.80 131.73 3.96 o 0 3 3 49.59 42.46 2.53 o 1 3 3 1867.45 1851.44 33.50 o 2 3 3 41.85 39.51 2.94 o 3 3 3 53.53 61.83 3.79 o 4 3 3 851.81 977.99 30.50 o 5 3 3 56.00 62.61 4.15 o 6 3 3 35.01 40.88 3.07 o -7 4 3 206.12 183.39 6.16 o -6 4 3 1.38 3.99 1.78 o -5 4 3 7.63 4.79 2.68 o -4 4 3 537.41 488.31 15.41 o -3 4 3 255.47 244.37 8.06 o -2 4 3 38.29 36.08 2.83 o -1 4 3 184.97 168.03 5.06 o 0 4 3 1271.68 1220.94 27.51 o 1 4 3 156.91 186.19 6.32 o 2 4 3 21.00 20.41 2.53 o 3 4 3 842.52 916.35 28.16 o 4 4 3 0.35 -3.06 3.42 o 5 4 3 33.21 33.60 3.26 o 6 4 3 167.15 200.81 6.68 o -6 5 3 6.23 4.00 2.15 o -5 5 3 100.42 94.27 4.81 o -4 5 3 57.40 48.59 3.86 o -3 5 3 37.45 33.90 3.44 o -2 5 3 717.32 715.39 17.66 o -1 5 3 26.69 28.08 2.51 o 0 5 3 7.02 3.05 3.61 o 1 5 3 991.53 984.55 27.67 o 2 5 3 46.22 48.74 3.73 o 3 5 3 27.77 35.38 3.13 o 4 5 3 135.94 152.84 6.31 o 5 5 3 30.19 33.91 2.90 o 6 5 3 2.76 6.27 1.40 o -6 6 3 1.85 2.06 2.18 o -5 6 3 0.19 -3.66 3.66 o -4 6 3 2.87 -0.72 3.90 o -3 6 3 17.32 0.00 6.52 o -2 6 3 99.40 94.03 4.93 o -1 6 3 176.80 171.37 6.34 o 0 6 3 156.92 148.17 5.79 o 1 6 3 0.27 0.76 3.30 o 2 6 3 8.62 6.98 2.39 o 3 6 3 104.79 107.79 5.10 o 4 6 3 10.27 13.29 2.15 o 5 6 3 15.60 18.72 2.26 o -5 7 3 6.68 2.71 3.44 o -4 7 3 33.86 36.12 2.93 o -3 7 3 28.90 21.93 2.67 o -2 7 3 1.15 0.20 1.96 o -1 7 3 95.11 97.97 5.00 o 0 7 3 5.95 8.22 2.13 o 1 7 3 16.49 14.28 2.74 o 2 7 3 2.01 0.79 3.96 o 3 7 3 17.40 18.18 2.55 o 4 7 3 9.45 10.84 2.13 o 5 7 3 21.71 22.51 1.94 o -4 8 3 84.38 86.77 3.93 o -3 8 3 31.36 29.15 3.18 o -2 8 3 9.84 12.81 2.14 o -1 8 3 35.08 38.63 3.33 o 0 8 3 188.09 186.53 6.68 o 1 8 3 7.13 2.16 4.82 o 2 8 3 6.78 0.66 3.98 o 3 8 3 120.11 134.56 5.64 o 4 8 3 19.55 23.19 2.05 o -3 9 3 118.88 122.25 4.23 o -2 9 3 42.91 47.82 3.18 o -1 9 3 70.91 67.29 4.21 o 0 9 3 54.45 50.10 3.67 o 1 9 3 83.44 87.06 4.47 o 2 9 3 59.16 60.75 3.44 o -7 0 4 274.08 258.35 7.71 o -6 0 4 301.20 278.96 8.40 o -5 0 4 381.53 346.97 10.82 o -4 0 4 103.30 99.76 4.62 o -3 0 4 237.24 220.14 6.82 o -2 0 4 524.80 541.73 15.79 o -1 0 4 618.09 588.37 14.71 o 0 0 4 46.45 44.66 2.04 o 1 0 4 1856.57 2050.31 33.53 o 2 0 4 1421.18 1724.27 32.89 o 3 0 4 239.84 294.72 10.18 o 4 0 4 2224.26 2354.19 48.64 o 5 0 4 1.60 2.41 3.68 o 6 0 4 1.17 1.30 2.91 o 7 0 4 245.37 251.98 7.47 o -7 1 4 108.78 98.56 4.84 o -6 1 4 61.04 58.20 4.08 o -5 1 4 137.31 124.34 5.67 o -4 1 4 862.20 790.40 18.84 o -3 1 4 0.00 1.08 2.02 o -2 1 4 55.91 60.28 2.78 o -1 1 4 392.77 469.00 13.24 o 0 1 4 12.36 9.52 1.29 o 1 1 4 1982.77 2177.98 35.39 o 2 1 4 382.13 402.20 10.71 o 3 1 4 792.61 852.85 24.89 o 4 1 4 321.04 376.62 12.97 o 5 1 4 163.07 171.75 6.69 o 6 1 4 362.29 389.18 12.65 o 7 1 4 5.31 7.63 1.40 o -7 2 4 117.97 113.66 4.81 o -6 2 4 16.25 18.31 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10.97 2.02 o -1 2 11 4.24 -2.56 4.24 o 0 2 11 354.21 331.38 11.55 o 1 2 11 93.01 79.25 4.11 o 2 2 11 8.93 7.56 1.85 o 3 2 11 16.20 10.78 1.81 o -4 3 11 69.95 59.03 3.37 o -3 3 11 0.36 1.43 2.47 o -2 3 11 182.73 231.09 7.38 o -1 3 11 91.39 118.12 4.88 o 0 3 11 51.78 48.31 3.60 o 1 3 11 206.99 187.37 6.82 o 2 3 11 87.05 85.22 4.07 o -3 4 11 137.51 146.24 5.23 o -2 4 11 11.78 18.11 2.20 o -1 4 11 13.57 15.42 2.50 o 0 4 11 205.78 205.76 6.83 o 1 4 11 50.73 47.83 3.20 o 2 4 11 2.21 1.60 2.70 o -2 5 11 154.02 156.27 5.02 o -1 5 11 38.92 40.00 3.04 o 0 5 11 66.44 64.69 3.28 o 1 5 11 83.42 76.75 3.39 o -3 0 12 79.85 86.27 4.10 o -2 0 12 72.21 64.49 3.82 o -1 0 12 0.85 0.53 1.91 o 0 0 12 170.76 168.24 6.09 o 1 0 12 542.67 487.22 12.74 o 2 0 12 112.29 91.96 4.00 o -3 1 12 60.23 65.46 3.50 o -2 1 12 75.73 74.51 4.13 o -1 1 12 89.75 84.03 4.34 o 0 1 12 256.50 232.61 7.26 o 1 1 12 5.13 0.92 2.34 o 2 1 12 84.94 68.84 3.61 o -3 2 12 6.95 10.06 1.69 o -2 2 12 98.53 112.68 4.67 o -1 2 12 0.11 1.44 1.86 o 0 2 12 1.39 3.32 1.47 o 1 2 12 135.35 124.37 4.93 o 2 2 12 8.37 6.19 1.40 o -2 3 12 6.65 9.08 1.61 o -1 3 12 0.03 1.22 1.86 o 0 3 12 16.38 16.99 2.15 o 1 3 12 19.80 17.20 1.99 o -1 4 12 105.46 110.34 4.30 o 0 4 12 4.35 3.70 1.38 o -1 1 13 5.06 4.87 1.29 o 0 1 13 1.04 1.67 1.81 o