#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2201842.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201842_Fobs loop_ _publ_author_name 'Urs, Usha K.' 'Dharmaprakash, M. S.' 'Shivashankar, S. A.' 'Guru Row, T. N.' _publ_section_title ; Nitratotris(2,2,6,6-tetramethyl-3,5-heptadionato)hafnium(IV) ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1 _journal_page_last m2 _journal_volume 59 _journal_year 2003 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 79.683 _cell_angle_beta 75.336 _cell_angle_gamma 83.579 _cell_length_a 10.1563 _cell_length_b 10.5900 _cell_length_c 19.2766 _exptl_crystal_F_000 812.00 _reflns_d_resolution_high 0.7664 _[local]_cod_data_source_file cf6224Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' hfdpm_m in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 266.00 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas 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7 1 0 489.35 445.85 76.19 o 8 1 0 133.54 201.29 73.55 o 9 1 0 96.93 168.36 86.71 o 10 1 0 13.57 35.14 112.51 o 11 1 0 37.13 -50.79 125.52 o 12 1 0 14.17 174.13 209.30 o -12 2 0 269.21 360.29 179.34 o -11 2 0 820.16 906.00 207.22 o -10 2 0 1298.02 1133.54 211.93 o -9 2 0 2437.61 2331.13 256.62 o -8 2 0 4156.58 4078.56 309.86 o -7 2 0 3387.99 3166.97 159.54 o -6 2 0 4066.88 3700.16 157.66 o -5 2 0 1712.07 1597.12 101.49 o -4 2 0 64.87 15.67 47.58 o -3 2 0 320.33 380.22 57.62 o -2 2 0 423.12 444.82 58.35 o -1 2 0 9203.26 12220.71 223.65 o 0 2 0 1795.46 1141.61 385.80 o 1 2 0 134.31 52.31 35.54 o 2 2 0 624.74 438.52 43.61 o 3 2 0 4957.75 4060.49 117.63 o 4 2 0 5505.53 3694.09 960.04 o 5 2 0 4294.01 3821.29 257.27 o 6 2 0 3002.40 3081.88 142.64 o 7 2 0 3246.92 2974.27 155.38 o 8 2 0 3478.76 3264.34 175.04 o 9 2 0 915.96 858.43 109.50 o 10 2 0 247.29 343.75 133.77 o 11 2 0 65.06 79.84 126.78 o -11 3 0 307.25 361.82 172.36 o -10 3 0 970.20 1045.33 207.72 o -9 3 0 1200.83 1353.60 211.13 o -8 3 0 1771.48 1471.16 202.74 o -7 3 0 3600.43 3485.29 280.41 o -6 3 0 6239.82 6209.18 206.74 o -5 3 0 6971.17 7084.52 205.46 o -4 3 0 3684.19 3487.94 138.12 o -3 3 0 655.98 516.59 67.19 o -2 3 0 826.06 817.52 72.32 o -1 3 0 868.59 719.64 272.46 o 0 3 0 945.14 1005.04 330.25 o 1 3 0 374.89 540.58 54.17 o 2 3 0 182.02 150.46 40.10 o 3 3 0 2275.09 2088.49 90.94 o 4 3 0 10807.72 11602.74 229.50 o 5 3 0 6317.99 6312.57 188.77 o 6 3 0 3686.51 3588.00 157.84 o 7 3 0 1763.80 1658.62 443.67 o 8 3 0 1171.11 1334.79 123.90 o 9 3 0 1149.91 1167.61 145.65 o 10 3 0 408.90 676.08 167.45 o 11 3 0 267.73 397.03 156.99 o -11 4 0 96.92 44.84 131.83 o -10 4 0 370.97 372.06 157.41 o -9 4 0 1186.60 1004.13 197.72 o -8 4 0 713.45 753.90 168.01 o -7 4 0 1902.14 2160.84 303.90 o -6 4 0 4755.81 4798.35 242.02 o -5 4 0 4181.97 4476.75 186.33 o -4 4 0 8058.53 8033.79 276.23 o -3 4 0 6342.37 6285.03 232.49 o -2 4 0 3757.56 3213.21 128.45 o -1 4 0 8948.58 9344.90 232.63 o 0 4 0 3462.54 2698.49 409.08 o 1 4 0 2236.36 2918.88 111.17 o 2 4 0 2866.53 3190.99 112.38 o 3 4 0 1609.17 2350.41 102.71 o 4 4 0 169.58 173.67 49.79 o 5 4 0 1465.80 1348.51 99.11 o 6 4 0 1624.12 1657.16 117.00 o 7 4 0 1697.27 1746.91 159.38 o 8 4 0 695.50 753.04 120.56 o 9 4 0 1305.50 1282.70 155.95 o 10 4 0 871.57 923.44 184.27 o 11 4 0 343.14 376.73 232.74 o -10 5 0 0.40 170.57 147.98 o -9 5 0 76.39 13.86 120.55 o -8 5 0 421.18 440.46 151.32 o -7 5 0 446.58 420.86 134.36 o -6 5 0 1937.35 1842.15 168.59 o -5 5 0 2871.33 3206.47 198.69 o -4 5 0 3894.91 4079.65 244.33 o -3 5 0 9912.87 10287.66 249.21 o -2 5 0 9485.28 8624.90 273.82 o -1 5 0 5765.15 5333.84 168.94 o 0 5 0 5799.21 5201.48 162.44 o 1 5 0 4334.15 4414.71 149.74 o 2 5 0 6145.87 5790.17 267.77 o 3 5 0 2604.11 2319.54 151.53 o 4 5 0 151.32 87.74 49.38 o 5 5 0 91.09 58.66 68.39 o 6 5 0 2.12 5.04 72.34 o 7 5 0 670.08 729.28 120.70 o 8 5 0 877.90 890.88 138.40 o 9 5 0 831.15 873.40 146.91 o 10 5 0 668.50 895.48 191.10 o 11 5 0 534.59 343.24 244.46 o 12 5 0 572.37 162.41 264.55 o -10 6 0 140.30 46.63 151.20 o -9 6 0 111.18 173.60 154.88 o -8 6 0 2.71 1.82 137.30 o -7 6 0 3.15 94.58 110.23 o -6 6 0 4.05 -52.87 87.64 o -5 6 0 203.79 123.50 86.71 o -4 6 0 1105.02 1087.47 132.41 o -3 6 0 3067.40 3029.61 154.78 o -2 6 0 8580.99 8466.29 237.46 o -1 6 0 8357.59 8262.06 226.84 o 0 6 0 7173.61 6957.60 203.69 o 1 6 0 7307.43 6675.65 198.43 o 2 6 0 3690.93 3998.41 152.44 o 3 6 0 3643.99 3484.52 137.95 o 4 6 0 2487.99 2504.00 242.12 o 5 6 0 1118.76 1141.09 132.45 o 6 6 0 75.35 121.70 87.61 o 7 6 0 89.22 106.49 86.61 o 8 6 0 102.75 51.79 114.67 o 9 6 0 133.52 72.25 126.09 o 10 6 0 116.26 183.33 144.21 o 11 6 0 158.00 185.85 239.43 o -9 7 0 514.83 508.65 177.68 o -8 7 0 363.04 363.68 152.27 o -7 7 0 239.71 307.33 136.14 o -6 7 0 54.43 72.02 111.80 o -5 7 0 3.55 20.92 80.64 o -4 7 0 69.89 129.46 86.48 o -3 7 0 275.14 266.78 82.30 o -2 7 0 1138.15 1057.86 109.09 o -1 7 0 2301.15 2263.02 140.95 o 0 7 0 2727.12 2800.69 150.97 o 1 7 0 2706.53 2530.81 141.67 o 2 7 0 3113.87 3257.03 197.50 o 3 7 0 5275.17 5431.16 257.96 o 4 7 0 3465.27 3513.15 247.13 o 5 7 0 1345.10 1343.64 154.67 o 6 7 0 457.25 509.21 116.76 o 7 7 0 55.50 225.71 133.95 o 8 7 0 74.49 176.75 123.72 o 9 7 0 50.12 21.17 122.70 o 10 7 0 4.36 76.59 163.25 o 11 7 0 13.13 -70.32 229.39 o -9 8 0 499.47 456.70 175.08 o -8 8 0 887.32 1088.53 209.70 o -7 8 0 1118.52 1043.21 243.62 o -6 8 0 981.61 893.77 180.94 o -5 8 0 655.11 802.81 167.32 o -4 8 0 317.38 438.02 111.42 o -3 8 0 126.56 153.91 91.16 o -2 8 0 4.12 23.35 68.91 o -1 8 0 17.22 -8.47 64.92 o 0 8 0 64.54 129.98 75.31 o 1 8 0 546.17 527.40 115.09 o 2 8 0 361.19 464.88 111.18 o 3 8 0 1093.18 1224.54 149.01 o 4 8 0 1676.77 1577.20 170.30 o 5 8 0 1298.22 1456.72 170.95 o 6 8 0 1197.16 1388.60 491.43 o 7 8 0 527.77 674.17 171.75 o 8 8 0 304.47 406.69 158.99 o 9 8 0 246.29 339.33 153.79 o 10 8 0 73.39 144.73 163.37 o -8 9 0 539.91 567.05 180.18 o -7 9 0 1327.26 1181.30 228.05 o -6 9 0 1899.13 1907.01 254.28 o -5 9 0 1451.27 1387.55 216.42 o -4 9 0 984.45 1021.48 152.48 o -3 9 0 878.99 957.85 144.07 o -2 9 0 714.99 854.59 131.45 o -1 9 0 635.95 758.56 131.93 o 0 9 0 371.69 258.40 106.05 o 1 9 0 26.10 12.90 87.96 o 2 9 0 530.00 494.42 125.56 o 3 9 0 685.94 683.00 129.83 o 4 9 0 478.68 495.81 125.85 o 5 9 0 430.14 528.29 161.99 o 6 9 0 854.97 1294.78 220.86 o 7 9 0 863.84 845.72 208.46 o 8 9 0 376.03 500.69 194.71 o 9 9 0 177.07 455.97 194.30 o -7 10 0 242.62 382.42 164.60 o -6 10 0 938.20 1062.76 464.64 o -5 10 0 1257.60 1377.41 224.42 o -4 10 0 670.76 770.20 280.46 o -3 10 0 543.70 714.05 136.06 o -2 10 0 770.71 567.25 155.52 o -1 10 0 1076.42 975.56 179.77 o 0 10 0 631.97 570.45 128.63 o 1 10 0 24.31 34.20 96.13 o 2 10 0 37.11 -11.70 94.95 o 3 10 0 16.80 118.64 127.51 o 4 10 0 5.03 139.12 133.83 o 5 10 0 61.25 110.05 134.36 o 6 10 0 273.60 338.22 264.55 o 7 10 0 317.30 439.92 182.15 o 8 10 0 206.79 574.92 206.67 o -6 11 0 176.52 169.61 150.09 o -5 11 0 360.96 346.59 194.23 o -4 11 0 336.61 438.68 207.62 o -3 11 0 394.12 480.05 155.67 o -2 11 0 571.63 684.14 176.93 o -1 11 0 849.39 707.31 171.07 o 0 11 0 781.16 706.17 169.89 o 1 11 0 267.73 417.47 131.30 o 2 11 0 102.59 201.94 141.16 o 3 11 0 100.85 218.04 147.20 o 4 11 0 43.77 -65.22 156.55 o 5 11 0 20.88 -9.13 132.86 o 6 11 0 1.43 53.71 155.20 o 7 11 0 25.70 53.55 169.63 o -4 12 0 60.71 -20.09 177.48 o -3 12 0 217.30 267.90 182.51 o -2 12 0 386.35 382.68 149.47 o -1 12 0 364.50 425.98 153.53 o 0 12 0 348.63 544.17 234.41 o 1 12 0 213.87 375.06 222.69 o 2 12 0 134.12 194.94 160.09 o 3 12 0 173.20 352.04 174.94 o 4 12 0 123.94 139.31 155.62 o 5 12 0 41.18 -107.66 143.35 o -2 13 0 42.64 -55.25 207.62 o -1 13 0 90.17 224.36 231.06 o 0 13 0 131.58 58.60 207.62 o 1 13 0 164.82 180.83 215.99 o 3 13 0 141.80 68.65 293.01 o -3 -13 1 7.01 25.12 281.29 o 0 -13 1 123.43 -66.97 209.30 o 1 -13 1 126.73 226.04 231.06 o 2 -13 1 130.06 267.78 162.57 o -5 -12 1 86.56 -43.53 269.57 o -4 -12 1 97.07 183.74 158.91 o -3 -12 1 49.95 198.50 162.51 o -2 -12 1 4.04 18.36 143.20 o -1 -12 1 48.67 83.72 194.23 o 0 -12 1 13.30 46.29 125.89 o 1 -12 1 8.70 131.27 132.46 o 2 -12 1 27.33 80.36 138.38 o 3 -12 1 63.44 85.17 133.98 o 4 -12 1 177.21 214.32 209.30 o -6 -11 1 245.93 475.51 196.66 o -5 -11 1 514.05 503.95 184.08 o -4 -11 1 455.55 325.83 197.57 o -3 -11 1 367.75 511.95 179.23 o -2 -11 1 313.31 415.50 165.21 o -1 -11 1 234.66 233.47 121.25 o 0 -11 1 202.63 317.38 137.84 o 1 -11 1 128.73 72.93 131.40 o 2 -11 1 36.90 187.22 128.19 o 3 -11 1 17.86 46.06 116.67 o 4 -11 1 19.57 267.90 177.48 o 5 -11 1 179.17 184.18 189.20 o 6 -11 1 183.04 157.07 166.01 o -8 -10 1 54.73 229.39 217.67 o -7 -10 1 154.06 109.61 188.37 o -6 -10 1 299.73 182.67 164.22 o -5 -10 1 603.73 586.99 179.43 o -4 -10 1 701.16 635.39 175.23 o -3 -10 1 943.64 896.22 166.25 o -2 -10 1 1470.34 1288.62 171.51 o -1 -10 1 1628.72 1540.99 178.64 o 0 -10 1 1457.41 1297.45 165.87 o 1 -10 1 725.57 765.73 179.16 o 2 -10 1 162.27 216.42 127.17 o 3 -10 1 81.14 291.89 134.28 o 4 -10 1 36.39 147.40 108.88 o 5 -10 1 11.74 38.93 120.60 o 6 -10 1 113.24 429.02 194.23 o 7 -10 1 142.22 129.34 146.45 o -9 -9 1 3.08 -29.65 172.10 o -8 -9 1 0.49 177.06 167.85 o -7 -9 1 19.73 83.96 140.47 o -6 -9 1 124.73 152.77 139.44 o -5 -9 1 460.13 446.07 156.85 o -4 -9 1 766.87 680.73 139.91 o -3 -9 1 804.73 886.84 146.86 o -2 -9 1 1068.41 1191.02 157.68 o -1 -9 1 1286.84 1497.17 164.57 o 0 -9 1 1633.40 1831.12 179.65 o 1 -9 1 1750.05 1766.41 178.17 o 2 -9 1 1418.34 1380.76 181.80 o 3 -9 1 987.79 1029.84 149.74 o 4 -9 1 383.26 408.15 120.11 o 5 -9 1 145.37 183.31 129.92 o 6 -9 1 63.82 -112.69 115.53 o 7 -9 1 9.59 124.69 126.52 o 8 -9 1 73.08 107.30 143.44 o -10 -8 1 87.52 144.00 222.69 o -9 -8 1 94.12 71.38 146.13 o -8 -8 1 145.47 160.08 136.56 o -7 -8 1 104.70 -16.74 115.06 o -6 -8 1 77.12 30.23 90.22 o -5 -8 1 3.46 4.67 84.24 o -4 -8 1 87.41 94.56 98.06 o -3 -8 1 479.46 626.99 127.14 o -2 -8 1 1683.43 1800.09 169.12 o -1 -8 1 1826.71 2122.47 182.35 o 0 -8 1 2296.40 2148.45 176.79 o 1 -8 1 3505.41 3521.03 185.63 o 2 -8 1 3148.89 3277.04 184.29 o 3 -8 1 3097.09 2835.99 208.73 o 4 -8 1 1681.35 1587.66 170.15 o 5 -8 1 651.43 750.45 134.55 o 6 -8 1 770.15 568.62 162.53 o 7 -8 1 531.52 593.22 165.33 o 8 -8 1 63.80 97.14 125.92 o 9 -8 1 10.32 27.93 130.40 o -10 -7 1 255.81 279.09 168.27 o -9 -7 1 376.66 513.94 170.44 o -8 -7 1 466.68 580.56 168.71 o -7 -7 1 358.93 351.95 114.47 o -6 -7 1 902.46 887.67 138.46 o -5 -7 1 1079.13 1014.07 139.12 o -4 -7 1 118.74 239.15 91.55 o -3 -7 1 52.72 106.64 91.51 o -2 -7 1 45.88 44.11 79.58 o -1 -7 1 691.42 670.01 111.07 o 0 -7 1 1055.20 952.53 100.04 o 1 -7 1 4430.02 2980.93 675.80 o 2 -7 1 5257.81 4939.70 202.68 o 3 -7 1 3457.42 3532.26 214.19 o 4 -7 1 3283.00 3187.80 216.46 o 5 -7 1 1207.93 1299.35 156.85 o 6 -7 1 397.62 460.69 140.86 o 7 -7 1 724.97 693.33 170.20 o 8 -7 1 669.26 783.09 187.27 o 9 -7 1 313.36 560.30 186.51 o -11 -6 1 196.56 -25.12 202.60 o -10 -6 1 373.06 532.45 254.50 o -9 -6 1 654.83 787.01 189.03 o -8 -6 1 1715.62 1398.33 167.72 o -7 -6 1 2316.48 2365.27 199.95 o -6 -6 1 2109.50 2028.07 179.55 o -5 -6 1 2364.81 2187.20 175.69 o -4 -6 1 2274.81 2166.98 167.41 o -3 -6 1 3176.73 2719.28 187.09 o -2 -6 1 2120.58 2332.02 114.73 o -1 -6 1 135.09 109.52 59.69 o 0 -6 1 108.48 163.96 63.85 o 1 -6 1 219.63 48.09 52.20 o 2 -6 1 1438.86 1629.47 117.58 o 3 -6 1 2348.96 2280.97 140.47 o 4 -6 1 1950.75 2056.62 169.77 o 5 -6 1 1772.84 1559.94 157.57 o 6 -6 1 632.08 713.08 125.50 o 7 -6 1 1051.99 1115.95 189.21 o 8 -6 1 1902.40 1716.96 239.47 o 9 -6 1 1334.73 1249.72 228.58 o 10 -6 1 727.19 902.22 217.81 o -11 -5 1 3.78 -100.46 219.34 o -10 -5 1 41.37 291.34 224.36 o -9 -5 1 420.79 534.27 127.94 o -8 -5 1 2136.19 2096.14 192.96 o -7 -5 1 4333.24 4173.94 246.74 o -6 -5 1 4208.69 4091.32 230.92 o -5 -5 1 4569.17 4130.55 218.88 o -4 -5 1 5687.27 5552.81 239.48 o -3 -5 1 7845.77 7949.58 271.10 o -2 -5 1 5789.95 5860.47 187.59 o -1 -5 1 4983.57 4663.75 150.03 o 0 -5 1 2940.46 2663.66 120.76 o 1 -5 1 269.50 142.27 102.49 o 2 -5 1 321.00 364.84 73.95 o 3 -5 1 338.95 421.88 78.73 o 4 -5 1 1100.99 1314.75 107.78 o 5 -5 1 688.92 799.24 120.06 o 6 -5 1 845.15 846.28 132.96 o 7 -5 1 1421.14 1338.27 196.27 o 8 -5 1 1957.88 1790.91 236.36 o 9 -5 1 1610.10 1612.19 241.95 o 10 -5 1 1250.95 1283.37 230.00 o 11 -5 1 522.55 569.28 281.29 o -11 -4 1 182.74 93.76 210.97 o -10 -4 1 13.63 89.95 126.42 o -9 -4 1 154.29 174.21 101.16 o -8 -4 1 1769.68 1729.05 170.00 o -7 -4 1 3033.71 3004.03 209.61 o -6 -4 1 2550.87 2346.55 136.38 o -5 -4 1 2838.02 2508.06 126.06 o -4 -4 1 5459.68 5832.25 229.58 o -3 -4 1 13709.40 14890.14 501.23 o -2 -4 1 15937.60 15846.97 677.41 o -1 -4 1 6037.32 6289.05 150.63 o 0 -4 1 4711.36 5004.37 140.29 o 1 -4 1 6857.56 6999.66 208.41 o 2 -4 1 5191.35 5673.54 162.65 o 3 -4 1 1769.56 1771.09 108.63 o 4 -4 1 57.33 36.88 56.99 o 5 -4 1 53.29 39.43 53.06 o 6 -4 1 103.78 145.55 85.70 o 7 -4 1 832.27 918.72 138.22 o 8 -4 1 1516.02 1632.98 221.99 o 9 -4 1 632.28 624.04 163.97 o 10 -4 1 605.06 567.14 176.84 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