#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2201852.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201852_Fobs loop_ _publ_author_name 'Urs, Usha K.' 'Dharmaprakash, M. S.' 'Shivashankar, S. A.' 'Guru Row, T. N.' _publ_section_title ; Tetrakis(tert-butyl 3-oxobutanoato)zirconium(IV) ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m83 _journal_page_last m84 _journal_volume 59 _journal_year 2003 _space_group_IT_number 88 _symmetry_space_group_name_Hall '-I 4ad' _symmetry_space_group_name_H-M 'I 41/a :2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 18.5695 _cell_length_b 18.5695 _cell_length_c 10.8176 _exptl_crystal_F_000 1520.00 _reflns_d_resolution_high 0.7691 _[local]_cod_data_source_file cf6235Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' zrtbuk_m in I4(1)/a' _shelx_refln_list_code 4 _shelx_f_calc_maximum 386.63 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-y+3/4, x+1/4, z+1/4' 'y+3/4, -x+3/4, z+3/4' 'x+1/2, y+1/2, z+1/2' '-x+1, -y+1/2, z+1' '-y+5/4, x+3/4, z+3/4' 'y+5/4, -x+5/4, z+5/4' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'y-3/4, -x-1/4, -z-1/4' '-y-3/4, x-3/4, -z-3/4' '-x+1/2, -y+1/2, -z+1/2' 'x, y+1/2, -z' 'y-1/4, -x+1/4, -z+1/4' '-y-1/4, x-1/4, -z-1/4' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 2 0 149479.41 151836.11 3925.58 o 2 2 0 24747.93 30044.88 571.20 o -2 4 0 25082.87 27737.63 384.31 o 0 4 0 18653.13 19308.67 374.01 o 2 4 0 68957.70 64734.69 7947.23 o 4 4 0 2059.59 1941.99 131.16 o -4 6 0 6684.73 6786.94 52.87 o -2 6 0 18326.21 19855.59 264.39 o 0 6 0 1807.63 1910.21 78.90 o 2 6 0 64.60 66.73 16.36 o 4 6 0 19309.47 22077.32 290.65 o 6 6 0 33306.34 36209.62 2594.89 o -6 8 0 27900.66 31871.01 489.48 o -4 8 0 20341.69 22336.03 207.92 o -2 8 0 467.96 397.68 37.98 o 0 8 0 1092.46 1032.51 28.86 o 2 8 0 4393.55 4211.69 73.83 o 4 8 0 14682.24 14019.36 1098.20 o 6 8 0 10355.99 10212.58 211.63 o 8 8 0 5327.03 4702.90 453.73 o -8 10 0 8140.84 8397.40 146.86 o -6 10 0 4486.34 4746.39 136.79 o -4 10 0 4.80 9.45 21.62 o -2 10 0 348.72 418.95 28.43 o 0 10 0 4106.13 4087.69 116.80 o 2 10 0 5710.23 4783.86 148.62 o 4 10 0 123.83 160.37 22.82 o 6 10 0 4815.06 5065.21 87.71 o 8 10 0 8143.67 8180.88 221.64 o 10 10 0 1042.86 950.29 53.76 o -10 12 0 224.92 233.45 45.79 o -8 12 0 2352.56 2309.26 101.35 o -6 12 0 557.40 647.25 75.04 o -4 12 0 24.91 24.73 32.34 o -2 12 0 3244.71 3080.07 64.27 o 0 12 0 2371.93 2515.91 91.06 o 2 12 0 563.61 532.76 30.85 o 4 12 0 3643.50 3358.06 77.78 o 6 12 0 12318.55 11424.20 918.18 o 8 12 0 8082.48 7617.95 201.63 o 10 12 0 165.58 145.59 37.38 o 12 12 0 691.83 666.51 62.23 o -12 14 0 3129.47 2988.35 186.76 o -10 14 0 222.08 191.97 46.87 o -8 14 0 1.07 -3.72 43.80 o -6 14 0 2940.38 3065.26 193.90 o -4 14 0 2304.74 2209.20 238.46 o -2 14 0 3942.87 3775.84 137.03 o 0 14 0 7471.43 6861.48 248.35 o 2 14 0 1752.50 1823.43 58.02 o 4 14 0 1461.63 1393.23 48.79 o 6 14 0 3071.38 2901.67 84.82 o 8 14 0 3954.06 3903.57 94.22 o 10 14 0 2362.79 3401.49 799.93 o 12 14 0 1090.03 1067.50 120.74 o 14 14 0 1464.69 1504.21 226.70 o -14 16 0 252.31 97.88 74.35 o -12 16 0 487.18 431.62 78.75 o -10 16 0 512.99 583.23 60.82 o -8 16 0 343.16 485.65 57.44 o -6 16 0 3236.82 3289.31 144.31 o -4 16 0 3126.44 2978.40 117.87 o -2 16 0 434.68 473.27 46.59 o 0 16 0 3332.67 3215.49 198.33 o 2 16 0 1361.37 1419.11 77.84 o 4 16 0 160.69 94.19 50.01 o 6 16 0 138.21 109.35 51.30 o 8 16 0 1380.86 1327.98 88.05 o 10 16 0 1111.68 1087.07 88.11 o 12 16 0 451.64 398.57 70.82 o 14 16 0 562.00 906.61 419.25 o 16 16 0 155.18 182.71 109.56 o -16 18 0 45.09 0.00 120.06 o -14 18 0 0.51 36.86 142.59 o -12 18 0 20.87 46.81 59.12 o -10 18 0 361.01 420.33 64.07 o -8 18 0 984.71 1148.14 70.12 o -6 18 0 961.15 1001.55 95.97 o -4 18 0 699.75 734.71 101.65 o -2 18 0 31.16 26.31 54.34 o 0 18 0 326.84 326.05 60.12 o 2 18 0 3843.19 3635.42 126.05 o 4 18 0 409.20 483.25 68.43 o 6 18 0 67.69 67.44 54.02 o 8 18 0 46.63 53.71 65.80 o 10 18 0 346.08 340.23 81.53 o 12 18 0 498.31 463.31 122.71 o 14 18 0 324.36 546.81 127.03 o -10 20 0 17.03 48.28 90.59 o -8 20 0 535.87 660.79 118.33 o -6 20 0 914.36 1075.42 152.73 o -4 20 0 421.75 470.07 86.64 o -2 20 0 299.02 282.01 63.18 o 0 20 0 714.07 756.68 73.15 o 2 20 0 2633.55 2670.78 123.76 o 4 20 0 937.76 3010.58 627.53 o 6 20 0 3.53 55.95 73.29 o 8 20 0 184.48 248.41 92.57 o 10 20 0 425.65 477.52 82.02 o 12 20 0 44.26 -20.50 156.18 o -8 22 0 154.62 97.59 204.50 o -6 22 0 389.58 360.45 85.75 o -4 22 0 268.27 256.29 122.44 o -2 22 0 378.71 1273.55 1531.13 o 0 22 0 457.98 517.34 87.32 o 2 22 0 314.60 540.78 248.13 o 4 22 0 408.43 444.94 112.10 o 6 22 0 207.92 224.43 80.47 o 8 22 0 104.00 259.93 96.56 o 2 24 0 23.69 -81.99 141.54 o 0 1 1 20679.86 21888.11 1362.22 o -1 2 1 52523.55 59426.20 861.19 o 1 2 1 5790.30 6621.55 240.84 o -2 3 1 2275.75 2849.96 136.08 o 0 3 1 15148.36 16924.86 191.22 o 2 3 1 33957.86 35342.22 1113.95 o -3 4 1 18185.83 18368.31 742.40 o -1 4 1 48522.12 54232.18 458.61 o 1 4 1 9578.40 10665.09 153.11 o 3 4 1 9141.18 10442.21 298.06 o -4 5 1 1695.26 1845.35 86.16 o -2 5 1 3326.65 3681.38 107.40 o 0 5 1 780.24 764.82 18.79 o 2 5 1 12892.74 13716.68 444.66 o 4 5 1 12537.09 12859.91 494.65 o -5 6 1 29843.49 30720.90 1593.91 o -3 6 1 1554.82 1371.00 63.10 o -1 6 1 175.50 265.95 19.64 o 1 6 1 361.02 431.51 30.92 o 3 6 1 3213.31 3103.97 60.34 o 5 6 1 5479.36 5485.32 150.36 o -6 7 1 45.04 45.63 15.19 o -4 7 1 452.81 552.06 22.15 o -2 7 1 3321.58 3857.33 36.96 o 0 7 1 952.46 1008.58 17.30 o 2 7 1 7282.80 7157.03 98.92 o 4 7 1 11177.46 12137.00 184.31 o 6 7 1 13405.62 15019.96 228.17 o -7 8 1 4859.97 4448.19 172.33 o -5 8 1 18833.89 21248.98 220.51 o -3 8 1 329.20 246.82 16.26 o -1 8 1 9663.26 10979.00 125.54 o 1 8 1 53.51 59.68 13.27 o 3 8 1 2501.67 2512.86 45.15 o 5 8 1 13169.37 13132.72 349.66 o 7 8 1 11071.15 11594.12 258.06 o -8 9 1 1109.42 930.56 57.88 o -6 9 1 119.82 70.56 19.40 o -4 9 1 1984.26 1973.37 31.09 o -2 9 1 12901.15 14325.58 368.86 o 0 9 1 861.33 768.53 18.23 o 2 9 1 1811.13 1848.53 36.87 o 4 9 1 8916.76 8820.16 314.41 o 6 9 1 1760.62 1592.28 61.52 o 8 9 1 596.23 573.62 24.06 o -9 10 1 486.67 556.47 32.52 o -7 10 1 0.94 13.07 19.04 o -5 10 1 4153.32 3998.47 99.28 o -3 10 1 10566.57 10944.83 420.14 o -1 10 1 248.27 197.87 16.87 o 1 10 1 51.05 60.83 13.86 o 3 10 1 1085.16 1036.82 22.49 o 5 10 1 3575.80 3654.42 75.21 o 7 10 1 9173.66 9255.61 195.64 o 9 10 1 3659.40 3317.73 165.44 o -10 11 1 402.30 365.42 28.11 o -8 11 1 355.64 336.55 26.36 o -6 11 1 3075.47 3158.84 73.14 o -4 11 1 3015.23 3581.13 332.69 o -2 11 1 2218.36 2041.51 31.04 o 0 11 1 1093.25 1039.56 23.31 o 2 11 1 1309.64 1161.45 26.92 o 4 11 1 4776.83 4443.17 86.87 o 6 11 1 1888.40 1882.27 37.51 o 8 11 1 1031.38 949.90 26.85 o 10 11 1 1886.04 1672.91 88.48 o -11 12 1 1078.82 1193.00 48.06 o -9 12 1 807.75 874.19 36.67 o -7 12 1 49.21 126.26 32.56 o -5 12 1 387.91 412.41 35.91 o -3 12 1 4998.60 4610.39 269.17 o -1 12 1 3758.41 3705.91 65.97 o 1 12 1 1014.33 883.85 27.40 o 3 12 1 876.54 745.19 24.79 o 5 12 1 291.44 240.55 18.80 o 7 12 1 1136.83 1133.06 30.12 o 9 12 1 2580.08 2339.09 57.38 o 11 12 1 719.51 669.38 34.76 o -12 13 1 211.10 179.70 36.21 o -10 13 1 693.25 717.93 37.93 o -8 13 1 781.32 761.59 37.49 o -6 13 1 1182.15 1121.49 37.30 o -4 13 1 1711.06 1524.51 67.56 o -2 13 1 1294.88 1256.74 36.04 o 0 13 1 1362.13 1301.14 31.58 o 2 13 1 537.41 517.18 25.21 o 4 13 1 1352.73 1279.06 30.10 o 6 13 1 1522.41 1363.25 32.73 o 8 13 1 729.73 696.01 34.34 o 10 13 1 1547.79 1501.39 65.53 o 12 13 1 1084.88 1355.75 206.21 o -13 14 1 158.93 176.45 43.45 o -11 14 1 260.15 239.02 34.64 o -9 14 1 364.28 490.70 36.26 o -7 14 1 57.12 47.96 33.61 o -5 14 1 12.15 22.40 37.32 o -3 14 1 461.36 396.93 33.17 o -1 14 1 2951.51 2875.95 49.21 o 1 14 1 3154.46 2987.89 66.49 o 3 14 1 1716.37 1640.83 40.96 o 5 14 1 567.31 530.76 35.16 o 7 14 1 48.80 23.64 25.60 o 9 14 1 151.15 117.12 35.11 o 11 14 1 525.46 534.88 41.98 o 13 14 1 341.49 395.87 44.99 o -14 15 1 358.06 431.76 56.91 o -12 15 1 509.70 597.99 59.57 o -10 15 1 767.40 765.46 42.50 o -8 15 1 745.58 772.09 39.82 o -6 15 1 418.43 424.43 36.89 o -4 15 1 1125.80 1094.21 76.06 o -2 15 1 1477.57 1625.61 81.13 o 0 15 1 1139.47 1506.80 252.35 o 2 15 1 395.94 408.83 32.47 o 4 15 1 1.89 9.21 29.16 o 6 15 1 0.62 20.13 21.66 o 8 15 1 409.92 392.66 36.76 o 10 15 1 1505.23 1384.64 57.32 o 12 15 1 965.22 1012.73 78.63 o 14 15 1 187.91 459.12 162.64 o -15 16 1 87.70 112.64 63.91 o -13 16 1 37.85 67.24 45.83 o -11 16 1 5.81 -3.52 35.32 o -9 16 1 39.87 76.33 34.86 o -7 16 1 354.00 621.78 112.25 o -5 16 1 593.67 583.40 40.93 o -3 16 1 305.45 343.43 39.32 o -1 16 1 375.70 385.94 35.97 o 1 16 1 1870.29 1869.73 49.60 o 3 16 1 2662.43 2503.38 59.29 o 5 16 1 1227.65 1224.26 44.68 o 7 16 1 310.94 535.92 108.64 o 9 16 1 96.79 56.82 34.92 o 11 16 1 249.11 199.19 46.43 o 13 16 1 222.87 227.95 49.98 o 15 16 1 100.03 129.02 59.18 o -16 17 1 110.30 138.33 61.05 o -14 17 1 45.70 227.44 153.77 o -12 17 1 35.86 63.68 47.29 o -10 17 1 270.57 286.14 43.26 o -8 17 1 830.83 913.05 60.22 o -6 17 1 504.89 524.30 46.74 o -4 17 1 651.59 607.10 45.32 o -2 17 1 1843.76 1859.79 52.14 o 0 17 1 794.59 732.77 41.24 o 2 17 1 64.94 68.36 37.94 o 4 17 1 331.18 277.71 36.10 o 6 17 1 53.19 19.71 60.34 o 8 17 1 828.39 906.41 57.36 o 10 17 1 716.99 767.35 67.25 o 12 17 1 394.49 490.00 88.32 o 14 17 1 213.95 227.54 88.54 o 16 17 1 52.74 42.90 65.01 o -15 18 1 50.05 -11.83 74.80 o -13 18 1 187.23 315.98 82.87 o -11 18 1 102.78 103.89 43.60 o -9 18 1 173.97 150.84 42.63 o -7 18 1 539.13 603.43 52.02 o -5 18 1 411.86 457.19 53.00 o -3 18 1 88.31 127.90 36.93 o -1 18 1 171.24 168.38 35.90 o 1 18 1 1260.84 1283.75 76.91 o 3 18 1 1924.28 1932.42 58.06 o 5 18 1 499.69 533.74 43.96 o 7 18 1 191.17 239.54 48.94 o 9 18 1 280.82 303.41 50.80 o 11 18 1 72.13 16.72 69.08 o 13 18 1 14.64 -25.54 71.85 o 15 18 1 16.69 54.05 86.25 o -14 19 1 25.32 69.64 99.08 o -12 19 1 3.42 50.40 58.60 o -10 19 1 341.60 409.26 91.91 o -8 19 1 503.86 518.76 64.35 o -6 19 1 313.56 366.09 44.89 o -4 19 1 410.50 438.93 74.35 o -2 19 1 418.48 500.28 169.05 o 0 19 1 2.79 28.09 39.66 o 2 19 1 8.22 14.30 38.83 o 4 19 1 604.03 713.53 47.74 o 6 19 1 1209.72 1145.05 58.82 o 8 19 1 221.78 150.08 50.66 o 10 19 1 8.29 18.72 73.45 o 12 19 1 53.09 12.28 70.40 o 14 19 1 109.99 -11.60 101.12 o -13 20 1 122.53 93.71 129.83 o -11 20 1 231.54 369.13 58.01 o -9 20 1 87.32 27.24 49.61 o -7 20 1 175.03 206.08 50.21 o -5 20 1 250.10 303.49 50.75 o -3 20 1 138.26 192.20 52.69 o -1 20 1 206.14 372.31 199.90 o 1 20 1 299.32 335.77 72.70 o 3 20 1 223.88 185.41 48.75 o 5 20 1 24.92 135.85 45.50 o 7 20 1 3.78 35.45 49.81 o 9 20 1 188.32 220.19 56.47 o 11 20 1 151.66 191.76 75.76 o 13 20 1 7.39 60.52 295.77 o -10 21 1 78.31 15.32 69.14 o -8 21 1 28.13 89.68 51.87 o -6 21 1 29.68 82.79 55.72 o -4 21 1 71.12 -2.89 48.50 o -2 21 1 86.32 186.60 74.27 o 0 21 1 209.03 207.92 72.01 o 2 21 1 663.13 754.62 76.77 o 4 21 1 921.28 941.52 65.24 o 6 21 1 289.51 292.90 62.86 o 8 21 1 3.00 72.16 67.42 o 10 21 1 24.15 12.25 77.70 o -9 22 1 117.01 56.87 95.45 o -7 22 1 107.15 107.36 66.50 o -5 22 1 264.50 316.89 59.96 o -3 22 1 58.39 212.96 315.49 o -1 22 1 3.56 155.41 287.48 o 1 22 1 70.37 39.21 48.38 o 3 22 1 92.87 131.86 49.63 o 5 22 1 36.91 129.83 109.53 o 7 22 1 11.01 146.06 158.39 o 9 22 1 60.04 148.52 81.31 o -6 23 1 24.61 -157.16 157.16 o -4 23 1 80.30 -65.40 157.16 o -2 23 1 211.48 307.91 72.64 o 0 23 1 214.38 2932.31 2326.17 o 2 23 1 99.13 229.01 125.23 o 4 23 1 50.28 183.97 153.71 o 6 23 1 29.37 177.33 120.06 o 1 1 2 577.80 431.65 26.96 o 0 2 2 20585.50 24181.70 377.90 o 2 2 2 74251.51 82597.66 744.31 o -1 3 2 28783.85 31810.53 554.56 o 1 3 2 12586.09 13580.37 472.52 o 3 3 2 30954.27 33486.74 945.74 o -2 4 2 9171.78 10448.95 133.03 o 0 4 2 3991.52 3500.44 119.98 o 2 4 2 8382.10 9747.02 136.29 o 4 4 2 572.45 485.36 16.95 o -3 5 2 956.23 1175.23 29.09 o -1 5 2 17408.34 17998.20 213.67 o 1 5 2 8426.02 8757.36 266.93 o 3 5 2 18833.88 20063.47 314.72 o 5 5 2 9463.47 8878.36 312.53 o -4 6 2 5611.66 5313.25 316.73 o -2 6 2 1226.75 1089.41 34.00 o 0 6 2 2437.37 2169.19 27.31 o 2 6 2 11295.96 11152.73 399.64 o 4 6 2 4732.00 5006.91 86.54 o 6 6 2 8972.08 9788.76 198.03 o -5 7 2 1914.74 2029.72 45.41 o -3 7 2 180.49 176.24 20.08 o -1 7 2 6561.73 6958.05 99.78 o 1 7 2 6912.56 6618.86 89.73 o 3 7 2 14855.96 14647.14 870.42 o 5 7 2 28032.85 30014.70 508.51 o 7 7 2 4521.90 4652.77 154.13 o -6 8 2 93.43 78.07 26.39 o -4 8 2 129.91 105.48 15.57 o -2 8 2 75.17 98.72 15.40 o 0 8 2 151.40 185.92 16.56 o 2 8 2 9562.12 10022.37 128.49 o 4 8 2 4873.61 4186.96 134.11 o 6 8 2 208.80 223.45 17.21 o 8 8 2 2.65 1278.74 380.25 o -7 9 2 1309.14 1250.47 53.03 o -5 9 2 7172.18 6852.91 227.72 o -3 9 2 8557.95 8924.12 88.10 o -1 9 2 5052.48 5248.79 138.48 o 1 9 2 6946.47 6766.48 66.40 o 3 9 2 6108.42 6397.22 116.63 o 5 9 2 14329.64 14478.65 359.83 o 7 9 2 7250.73 6284.94 331.52 o 9 9 2 1870.24 1934.50 65.78 o -8 10 2 51.08 68.57 27.26 o -6 10 2 1366.22 1353.98 28.49 o -4 10 2 801.57 825.50 22.24 o -2 10 2 1829.00 2084.55 36.30 o 0 10 2 28.26 0.53 13.63 o 2 10 2 235.23 225.16 20.52 o 4 10 2 144.97 141.72 12.78 o 6 10 2 1134.47 1089.95 24.69 o 8 10 2 406.23 357.63 39.76 o 10 10 2 76.58 78.25 26.40 o -9 11 2 2167.19 1890.79 129.05 o -7 11 2 785.92 833.92 29.64 o -5 11 2 2727.43 2770.51 112.37 o -3 11 2 14139.33 14848.27 235.53 o -1 11 2 11124.88 11270.59 134.57 o 1 11 2 7824.52 7930.03 130.77 o 3 11 2 2833.70 2690.92 104.10 o 5 11 2 1005.83 945.01 24.54 o 7 11 2 1270.69 1104.59 37.41 o 9 11 2 1098.19 1053.12 50.70 o 11 11 2 2194.24 2009.54 119.97 o -10 12 2 1805.29 1683.03 63.28 o -8 12 2 5.12 37.59 37.82 o -6 12 2 889.44 868.85 49.70 o -4 12 2 0.37 -20.87 20.87 o -2 12 2 7.47 15.20 18.39 o 0 12 2 175.25 179.16 18.89 o 2 12 2 3.48 6.23 16.77 o 4 12 2 89.07 65.73 18.11 o 6 12 2 114.29 102.61 20.34 o 8 12 2 128.16 95.78 21.63 o 10 12 2 66.31 58.04 22.95 o 12 12 2 6.63 15.85 38.72 o -11 13 2 908.07 1342.28 189.49 o -9 13 2 748.82 1192.02 204.30 o -7 13 2 914.55 935.92 39.45 o -5 13 2 1792.46 1658.54 44.54 o -3 13 2 8672.56 8838.91 207.17 o -1 13 2 7702.11 8142.71 192.94 o 1 13 2 3258.83 3189.13 71.10 o 3 13 2 1181.17 1159.16 34.11 o 5 13 2 117.51 74.11 24.14 o 7 13 2 19.07 30.53 26.25 o 9 13 2 984.82 971.82 37.49 o 11 13 2 1892.54 1990.10 85.96 o 13 13 2 826.74 867.02 55.16 o -12 14 2 0.77 27.23 35.42 o -10 14 2 404.61 602.48 103.18 o -8 14 2 88.39 140.75 41.06 o -6 14 2 22.95 2.79 20.78 o -4 14 2 2251.69 2289.23 92.15 o -2 14 2 572.41 555.09 35.35 o 0 14 2 838.11 789.28 35.51 o 2 14 2 7.19 -3.45 23.55 o 4 14 2 34.58 28.41 24.93 o 6 14 2 251.67 185.26 27.99 o 8 14 2 228.20 242.45 30.49 o 10 14 2 306.57 292.12 34.41 o 12 14 2 557.70 518.82 45.33 o 14 14 2 3.79 -29.20 40.80 o -13 15 2 101.31 123.29 45.08 o -11 15 2 283.08 322.62 48.29 o -9 15 2 1103.88 1064.06 45.57 o -7 15 2 1504.05 1701.13 74.75 o -5 15 2 378.05 405.75 38.98 o -3 15 2 947.63 759.28 83.81 o -1 15 2 3336.14 3428.39 61.48 o 1 15 2 1819.39 1762.93 49.86 o 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