#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/18/2201854.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201854_Fobs loop_ _publ_author_name 'Li, Xiao-Fang' 'Feng, Ya-Qing' 'Gu, Yun-Feng' _publ_section_title ; 3-(2,6-Dichlorophenyl)-8-ethyl-4-phenyl-1-oxa-6-thia-2,8-diazaspiro[4.4]non-2-ene-7,9-dione ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o330 _journal_page_last o331 _journal_volume 59 _journal_year 2003 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 10.0339 _cell_length_b 12.5618 _cell_length_c 30.2202 _exptl_crystal_F_000 1728.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file cf6237Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 030121F in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 246.46 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 10571.86 11507.14 240.86 o 4 0 0 13716.89 14360.58 299.32 o 6 0 0 380.06 468.52 28.28 o 8 0 0 1077.45 1027.62 81.35 o 2 1 0 4698.03 5255.65 122.65 o 4 1 0 2271.35 2090.12 37.07 o 6 1 0 54.79 24.41 27.24 o 8 1 0 686.73 742.31 51.03 o 0 2 0 44088.86 42781.13 850.31 o 2 2 0 15063.90 15744.66 234.06 o 4 2 0 11843.81 12062.08 199.26 o 6 2 0 3.95 -11.80 22.38 o 8 2 0 1055.70 1132.48 88.97 o 10 2 0 14.03 -15.25 59.74 o 2 3 0 14770.04 14955.95 316.48 o 4 3 0 3393.87 3506.94 83.66 o 6 3 0 34.33 30.84 27.33 o 8 3 0 1.06 -69.91 53.38 o 10 3 0 435.86 387.02 76.90 o 0 4 0 13939.35 13725.07 305.68 o 2 4 0 2617.12 2398.10 49.18 o 4 4 0 17502.68 18320.96 233.30 o 6 4 0 4.41 -8.12 28.59 o 8 4 0 1395.03 1390.01 65.80 o 10 4 0 2.78 -99.14 66.09 o 2 5 0 4860.11 5188.33 86.66 o 4 5 0 24529.13 24495.71 388.84 o 6 5 0 798.73 717.19 49.15 o 8 5 0 1721.90 1570.67 72.10 o 10 5 0 9.35 50.21 61.64 o 0 6 0 2453.55 2068.75 102.63 o 2 6 0 1485.16 1360.04 47.62 o 4 6 0 843.14 736.70 33.52 o 6 6 0 1.27 13.73 32.95 o 8 6 0 126.91 136.51 37.53 o 10 6 0 20.16 19.07 64.82 o 2 7 0 2902.24 2759.38 80.44 o 4 7 0 646.95 616.37 34.27 o 6 7 0 81.15 43.71 36.37 o 8 7 0 696.40 705.88 58.27 o 10 7 0 232.71 373.04 81.98 o 0 8 0 392.62 367.78 44.80 o 2 8 0 278.29 289.26 24.22 o 4 8 0 3261.67 3217.99 76.86 o 6 8 0 1694.62 1520.01 76.55 o 8 8 0 31.69 92.10 41.94 o 10 8 0 1.46 99.14 73.72 o 2 9 0 18.81 -10.50 30.04 o 4 9 0 734.05 638.90 50.98 o 6 9 0 15.29 34.65 38.26 o 8 9 0 400.79 380.73 108.35 o 0 10 0 220.84 141.16 38.58 o 2 10 0 3.23 38.14 30.86 o 4 10 0 20.13 7.80 49.25 o 6 10 0 58.21 43.16 63.87 o 8 10 0 381.64 409.52 61.64 o 2 11 0 143.66 168.10 31.95 o 4 11 0 689.75 704.97 93.74 o 6 11 0 34.08 79.89 44.71 o 8 11 0 259.69 463.18 94.37 o 0 12 0 1986.86 2000.43 234.50 o 2 12 0 29.04 57.86 32.08 o 4 12 0 280.01 363.06 53.87 o 6 12 0 111.74 105.45 50.31 o 2 13 0 154.69 204.82 39.86 o 4 13 0 294.75 411.57 127.74 o 0 14 0 18.52 64.19 66.73 o 2 14 0 14.49 164.41 43.07 o 4 14 0 224.26 282.58 58.34 o 1 1 1 6492.29 6248.69 69.43 o 2 1 1 9180.95 9157.77 115.93 o 3 1 1 5959.28 5568.78 116.80 o 4 1 1 724.58 746.32 22.22 o 5 1 1 81.13 61.25 8.51 o 6 1 1 4157.79 4239.88 53.97 o 7 1 1 226.23 218.06 26.15 o 8 1 1 1721.40 1777.55 59.45 o 9 1 1 2225.03 2183.11 108.35 o 10 1 1 13.58 -91.51 61.01 o 0 2 1 12029.65 11786.58 177.05 o 1 2 1 20701.75 21173.06 216.62 o 2 2 1 41843.43 43071.34 468.18 o 3 2 1 1281.42 1260.43 41.05 o 4 2 1 4321.34 4356.40 64.70 o 5 2 1 1626.40 1778.78 39.28 o 6 2 1 0.05 9.19 15.72 o 7 2 1 804.86 839.77 25.79 o 8 2 1 80.24 77.48 39.40 o 9 2 1 21.03 -15.67 61.01 o 10 2 1 108.36 168.29 63.55 o 1 3 1 14887.67 14963.52 173.55 o 2 3 1 36485.21 37109.82 307.67 o 3 3 1 15059.26 15697.09 139.97 o 4 3 1 30.70 84.41 16.19 o 5 3 1 5621.65 5595.10 122.16 o 6 3 1 4000.51 3914.21 59.40 o 7 3 1 173.73 199.74 23.89 o 8 3 1 3.58 38.59 36.62 o 9 3 1 61.65 69.40 42.26 o 10 3 1 379.45 443.89 56.60 o 11 3 1 37.37 -0.16 45.22 o 0 4 1 18.99 7.93 27.96 o 1 4 1 231.06 185.17 14.43 o 2 4 1 7171.42 6867.66 78.09 o 3 4 1 140.60 106.51 11.54 o 4 4 1 10193.71 10722.15 104.08 o 5 4 1 963.35 854.81 44.69 o 6 4 1 1568.72 1358.42 48.25 o 7 4 1 346.15 360.30 28.23 o 8 4 1 66.57 54.59 24.63 o 9 4 1 369.69 360.69 57.20 o 10 4 1 52.89 -62.10 46.51 o 11 4 1 7.50 1.56 88.65 o 1 5 1 469.16 394.39 18.37 o 2 5 1 408.74 445.35 17.73 o 3 5 1 3.09 -18.13 12.09 o 4 5 1 216.77 244.01 16.53 o 5 5 1 1089.04 1115.34 22.99 o 6 5 1 1567.06 1446.39 45.96 o 7 5 1 1980.55 1818.65 53.06 o 8 5 1 61.27 36.66 25.59 o 9 5 1 32.41 13.66 44.04 o 10 5 1 60.64 36.70 46.50 o 11 5 1 0.09 -16.81 52.35 o 0 6 1 214.27 190.61 22.08 o 1 6 1 2401.90 2556.13 49.62 o 2 6 1 388.93 356.58 18.82 o 3 6 1 3276.06 2954.80 54.05 o 4 6 1 576.31 594.49 22.13 o 5 6 1 115.50 151.56 38.07 o 6 6 1 599.19 573.99 34.82 o 7 6 1 332.04 297.44 30.48 o 8 6 1 43.54 53.09 25.67 o 9 6 1 21.02 36.76 56.24 o 10 6 1 8.03 53.32 47.98 o 1 7 1 10.81 -8.96 12.69 o 2 7 1 831.32 754.40 22.46 o 3 7 1 14.16 -14.18 15.63 o 4 7 1 346.84 314.52 20.81 o 5 7 1 260.85 240.39 43.94 o 6 7 1 603.04 525.20 35.34 o 7 7 1 278.09 202.87 28.88 o 8 7 1 21.96 13.43 28.28 o 9 7 1 25.09 95.55 45.41 o 10 7 1 34.64 66.03 50.32 o 0 8 1 455.74 428.96 27.26 o 1 8 1 632.73 631.53 21.59 o 2 8 1 2356.41 2243.18 39.83 o 3 8 1 89.04 40.06 18.31 o 4 8 1 62.80 33.34 18.47 o 5 8 1 0.26 -43.05 28.70 o 6 8 1 55.53 73.12 26.71 o 7 8 1 103.04 73.06 51.92 o 8 8 1 70.77 68.26 28.62 o 9 8 1 68.24 67.93 31.41 o 10 8 1 149.56 229.36 59.03 o 1 9 1 13.11 -10.75 16.90 o 2 9 1 1927.70 1774.67 38.00 o 3 9 1 536.46 586.89 27.81 o 4 9 1 1.25 -20.74 20.23 o 5 9 1 715.43 688.73 41.07 o 6 9 1 656.42 693.57 42.00 o 7 9 1 9.12 59.66 28.91 o 8 9 1 17.39 65.62 31.05 o 9 9 1 131.00 191.12 58.52 o 0 10 1 215.46 231.80 35.32 o 1 10 1 1374.76 1374.51 33.16 o 2 10 1 3304.32 3089.05 58.14 o 3 10 1 59.96 92.13 22.32 o 4 10 1 862.53 809.02 44.20 o 5 10 1 126.98 141.69 30.76 o 6 10 1 105.81 136.50 31.07 o 7 10 1 251.73 294.02 36.55 o 8 10 1 96.40 188.84 39.53 o 1 11 1 226.90 232.34 22.21 o 2 11 1 131.26 160.73 25.86 o 3 11 1 578.13 432.63 28.69 o 4 11 1 26.58 -18.96 28.54 o 5 11 1 136.84 115.95 36.77 o 6 11 1 45.89 95.18 34.76 o 7 11 1 6.31 66.46 34.58 o 8 11 1 7.56 84.17 39.45 o 0 12 1 415.10 533.17 38.01 o 1 12 1 176.94 234.22 25.56 o 2 12 1 288.00 262.70 26.91 o 3 12 1 90.78 84.27 24.12 o 4 12 1 18.71 119.33 32.87 o 5 12 1 33.51 66.97 32.39 o 6 12 1 228.50 251.64 41.82 o 7 12 1 38.75 83.71 37.11 o 1 13 1 9.94 68.42 26.07 o 2 13 1 35.11 100.97 26.56 o 3 13 1 3.18 43.15 32.38 o 4 13 1 44.74 60.71 34.80 o 5 13 1 3.51 27.73 42.47 o 0 14 1 185.74 163.51 48.68 o 1 14 1 157.78 191.77 32.99 o 2 14 1 425.44 530.55 37.35 o 3 14 1 42.66 94.86 36.26 o 4 14 1 11.74 150.45 38.02 o 0 0 2 488.19 93.42 6.99 o 1 0 2 29197.01 30845.00 443.52 o 2 0 2 9439.56 9587.29 143.80 o 3 0 2 2199.51 2107.55 76.58 o 4 0 2 11150.54 11296.20 143.61 o 5 0 2 3050.56 3075.14 47.06 o 6 0 2 2777.40 2889.60 48.34 o 7 0 2 114.83 72.46 82.93 o 8 0 2 255.87 307.84 42.18 o 9 0 2 4.08 25.42 49.57 o 1 1 2 9.81 35.43 4.86 o 2 1 2 1624.19 1650.07 24.01 o 3 1 2 201.35 203.47 10.20 o 4 1 2 5377.33 5106.37 71.24 o 5 1 2 148.73 177.51 11.33 o 6 1 2 1079.35 1085.25 21.73 o 7 1 2 817.10 803.06 48.07 o 8 1 2 2304.85 2443.43 68.95 o 9 1 2 323.40 322.61 56.88 o 10 1 2 648.50 638.05 83.89 o 0 2 2 418.49 397.47 17.64 o 1 2 2 36056.64 36257.28 411.95 o 2 2 2 8591.36 8668.06 96.61 o 3 2 2 1776.72 2082.38 32.43 o 4 2 2 424.98 492.15 16.55 o 5 2 2 308.05 447.93 19.68 o 6 2 2 608.00 661.45 24.14 o 7 2 2 47.09 58.75 18.04 o 8 2 2 846.07 769.61 55.74 o 9 2 2 1564.66 1577.88 76.59 o 10 2 2 118.69 59.11 43.32 o 1 3 2 181.97 172.95 15.43 o 2 3 2 616.40 572.11 16.44 o 3 3 2 138.59 148.72 11.17 o 4 3 2 1413.26 1504.90 31.39 o 5 3 2 154.70 187.41 23.19 o 6 3 2 1180.87 1192.37 32.07 o 7 3 2 198.29 194.17 23.90 o 8 3 2 633.76 653.16 53.63 o 9 3 2 758.45 782.02 58.41 o 10 3 2 565.55 508.53 59.54 o 11 3 2 0.01 -18.57 55.92 o 0 4 2 12.60 -18.80 25.10 o 1 4 2 168.08 160.94 16.18 o 2 4 2 1503.89 1504.59 27.04 o 3 4 2 716.78 800.31 19.38 o 4 4 2 1.74 -20.26 13.50 o 5 4 2 202.93 225.38 22.88 o 6 4 2 97.36 105.82 22.34 o 7 4 2 430.63 423.52 29.78 o 8 4 2 208.22 218.60 28.44 o 9 4 2 92.96 27.96 40.89 o 10 4 2 153.27 102.21 45.78 o 11 4 2 147.24 111.85 51.53 o 1 5 2 16987.29 17403.82 196.35 o 2 5 2 294.63 234.01 15.43 o 3 5 2 1979.62 2089.44 35.01 o 4 5 2 2956.40 2826.65 45.00 o 5 5 2 486.38 447.61 19.80 o 6 5 2 835.69 834.98 37.69 o 7 5 2 688.68 649.15 43.11 o 8 5 2 540.80 535.16 34.54 o 9 5 2 37.38 28.89 38.40 o 10 5 2 47.70 20.27 57.83 o 11 5 2 59.84 57.20 47.63 o 0 6 2 3774.75 3800.94 72.68 o 1 6 2 938.69 949.27 25.44 o 2 6 2 2826.43 2814.67 44.24 o 3 6 2 108.86 143.68 16.25 o 4 6 2 3800.61 3641.22 51.87 o 5 6 2 2635.79 2685.68 49.96 o 6 6 2 985.33 911.20 40.38 o 7 6 2 58.58 34.18 25.56 o 8 6 2 132.57 153.39 29.63 o 9 6 2 354.83 268.40 49.62 o 10 6 2 52.48 -38.46 45.57 o 1 7 2 1439.84 1447.69 29.79 o 2 7 2 953.08 943.82 27.96 o 3 7 2 1999.68 1999.87 39.42 o 4 7 2 682.98 573.99 24.12 o 5 7 2 751.97 696.58 37.99 o 6 7 2 393.52 347.45 32.72 o 7 7 2 342.23 298.94 30.93 o 8 7 2 374.53 412.02 34.21 o 9 7 2 7.29 64.42 43.98 o 10 7 2 130.36 88.66 49.17 o 0 8 2 6026.79 5849.82 91.92 o 1 8 2 4.39 -21.08 14.05 o 2 8 2 42.20 11.35 15.86 o 3 8 2 1999.61 1900.79 45.66 o 4 8 2 212.56 208.96 21.56 o 5 8 2 325.94 320.44 32.54 o 6 8 2 358.54 317.70 41.55 o 7 8 2 91.70 91.13 28.63 o 8 8 2 36.16 46.61 28.96 o 9 8 2 8.25 62.09 32.29 o 10 8 2 56.33 65.10 51.53 o 1 9 2 756.80 786.49 24.86 o 2 9 2 1044.58 993.25 32.76 o 3 9 2 556.49 519.22 27.09 o 4 9 2 1.42 14.32 19.65 o 5 9 2 141.40 100.01 28.81 o 6 9 2 38.17 94.82 28.91 o 7 9 2 151.86 166.53 31.75 o 8 9 2 5.13 51.51 38.62 o 9 9 2 146.54 218.46 36.79 o 0 10 2 255.92 235.09 28.18 o 1 10 2 5.44 12.22 17.38 o 2 10 2 794.31 727.79 32.16 o 3 10 2 1754.16 1680.95 43.51 o 4 10 2 56.57 24.77 27.78 o 5 10 2 475.20 424.59 37.08 o 6 10 2 99.27 119.58 30.71 o 7 10 2 152.46 199.07 34.15 o 8 10 2 56.76 96.92 42.01 o 1 11 2 238.72 219.03 22.49 o 2 11 2 573.67 519.68 29.57 o 3 11 2 43.27 10.70 22.23 o 4 11 2 46.22 -28.32 28.23 o 5 11 2 12.20 45.84 29.73 o 6 11 2 390.31 372.60 38.48 o 7 11 2 0.64 72.33 33.96 o 8 11 2 98.08 134.20 37.71 o 0 12 2 3572.04 3502.43 94.37 o 1 12 2 105.55 156.79 25.46 o 2 12 2 3.20 26.40 27.04 o 3 12 2 95.15 144.19 26.22 o 4 12 2 182.07 215.58 34.88 o 5 12 2 187.26 230.18 35.52 o 6 12 2 0.37 51.82 34.67 o 7 12 2 110.26 180.10 50.47 o 1 13 2 165.93 203.74 27.36 o 2 13 2 500.72 562.50 33.84 o 3 13 2 287.95 229.90 36.13 o 4 13 2 144.95 156.09 36.41 o 5 13 2 45.18 148.23 37.06 o 0 14 2 21.51 40.95 46.05 o 1 14 2 37.27 83.51 30.41 o 2 14 2 143.19 242.05 30.58 o 3 14 2 0.92 123.63 38.54 o 4 14 2 102.35 247.16 40.24 o 1 1 3 5672.56 6049.01 80.93 o 2 1 3 7735.09 8242.10 119.94 o 3 1 3 2382.94 2418.16 71.81 o 4 1 3 327.24 383.89 17.53 o 5 1 3 728.03 719.72 15.70 o 6 1 3 594.31 570.86 17.16 o 7 1 3 139.50 150.65 20.30 o 8 1 3 127.73 133.25 32.59 o 9 1 3 1271.11 1336.32 68.92 o 10 1 3 617.55 556.07 81.35 o 0 2 3 26510.32 25549.94 368.02 o 1 2 3 13147.39 13675.28 156.58 o 2 2 3 38209.49 39914.35 400.43 o 3 2 3 10819.99 10900.85 100.48 o 4 2 3 256.81 211.40 13.13 o 5 2 3 488.08 395.90 15.31 o 6 2 3 167.32 185.19 18.28 o 7 2 3 2373.92 2422.31 46.47 o 8 2 3 163.16 168.63 40.99 o 9 2 3 0.23 -13.13 38.37 o 10 2 3 148.65 225.11 47.78 o 11 2 3 26.77 -21.61 62.28 o 1 3 3 37216.59 37512.19 386.82 o 2 3 3 99.94 112.05 13.11 o 3 3 3 11767.56 12446.50 115.27 o 4 3 3 505.98 405.71 17.44 o 5 3 3 64.55 25.96 14.31 o 6 3 3 3092.53 2976.36 51.19 o 7 3 3 1315.09 1273.12 35.03 o 8 3 3 115.20 121.17 41.94 o 9 3 3 35.73 86.38 43.03 o 10 3 3 77.46 6.19 45.81 o 11 3 3 118.77 171.59 76.26 o 0 4 3 4078.74 4152.67 86.43 o 1 4 3 17840.64 17553.88 191.48 o 2 4 3 18.89 18.14 11.92 o 3 4 3 8.76 16.27 10.81 o 4 4 3 0.25 -18.76 12.51 o 5 4 3 2408.43 2174.46 63.89 o 6 4 3 27.79 35.70 20.12 o 7 4 3 196.84 171.41 34.67 o 8 4 3 97.93 52.93 32.91 o 9 4 3 173.28 188.93 44.80 o 10 4 3 170.44 195.79 45.97 o 11 4 3 330.73 297.09 58.82 o 1 5 3 257.96 272.81 17.77 o 2 5 3 4029.36 3823.17 50.36 o 3 5 3 1313.21 1328.48 28.26 o 4 5 3 1702.54 1660.88 31.21 o 5 5 3 793.43 794.49 20.76 o 6 5 3 272.15 225.26 26.52 o 7 5 3 231.50 188.04 28.25 o 8 5 3 41.89 27.88 26.56 o 9 5 3 27.96 52.98 68.63 o 10 5 3 95.57 62.28 44.04 o 11 5 3 55.69 8.45 50.97 o 0 6 3 5.68 -36.33 24.22 o 1 6 3 390.37 391.59 20.54 o 2 6 3 1.24 -10.95 14.14 o 3 6 3 3928.92 3910.69 54.99 o 4 6 3 71.94 62.54 15.47 o 5 6 3 111.98 115.00 19.10 o 6 6 3 1068.62 975.96 41.25 o 7 6 3 307.42 306.43 31.94 o 8 6 3 152.53 154.37 29.46 o 9 6 3 12.04 56.31 44.26 o 10 6 3 122.97 108.19 48.88 o 1 7 3 76.40 37.57 24.35 o 2 7 3 884.52 855.85 26.90 o 3 7 3 67.68 53.61 16.87 o 4 7 3 161.05 124.30 23.12 o 5 7 3 65.60 14.14 24.89 o 6 7 3 803.78 690.09 38.39 o 7 7 3 158.59 168.94 28.61 o 8 7 3 130.26 180.68 29.78 o 9 7 3 110.74 96.32 46.39 o 10 7 3 109.56 171.33 79.44 o 0 8 3 322.70 317.87 37.57 o 1 8 3 717.98 712.91 24.24 o 2 8 3 647.01 567.76 25.65 o 3 8 3 425.10 413.08 23.40 o 4 8 3 2273.41 2089.87 43.37 o 5 8 3 7717.27 7041.96 119.88 o 6 8 3 206.79 173.29 29.90 o 7 8 3 521.30 532.86 38.07 o 8 8 3 72.34 100.57 29.54 o 9 8 3 0.08 50.56 34.21 o 10 8 3 20.14 52.14 51.45 o 1 9 3 254.17 301.39 21.56 o 2 9 3 12.45 -15.44 18.39 o 3 9 3 810.89 738.58 30.48 o 4 9 3 42.26 14.11 20.17 o 5 9 3 35.54 32.93 27.21 o 6 9 3 1119.32 1111.15 48.91 o 7 9 3 0.81 11.98 28.01 o 8 9 3 172.18 200.69 34.82 o 9 9 3 70.42 117.57 38.89 o 0 10 3 1251.12 1312.44 46.25 o 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28 279.87 247.31 33.20 o 6 1 28 13.83 36.82 33.63 o 7 1 28 6.07 39.68 39.26 o 0 2 28 740.61 680.88 74.35 o 1 2 28 2.97 -25.05 29.18 o 2 2 28 4.06 9.17 30.19 o 3 2 28 91.28 97.25 28.67 o 4 2 28 461.01 453.99 35.47 o 5 2 28 13.87 27.10 29.27 o 6 2 28 31.10 -15.37 34.24 o 7 2 28 24.75 50.56 90.88 o 1 3 28 1.54 -5.79 28.76 o 2 3 28 0.03 -18.62 25.10 o 3 3 28 66.59 100.13 28.09 o 4 3 28 0.03 12.63 27.75 o 5 3 28 90.62 45.22 33.14 o 6 3 28 69.97 18.96 35.35 o 7 3 28 80.08 91.63 52.10 o 0 4 28 2.63 -73.02 68.95 o 1 4 28 18.90 14.65 26.95 o 2 4 28 278.34 249.14 31.73 o 3 4 28 596.71 630.18 39.65 o 4 4 28 134.24 152.40 31.09 o 5 4 28 6.14 -49.34 33.04 o 6 4 28 1.76 14.41 36.85 o 1 5 28 1.24 27.58 28.46 o 2 5 28 265.76 277.89 33.98 o 3 5 28 4.32 23.00 29.24 o 4 5 28 13.11 -14.22 29.01 o 5 5 28 25.45 3.15 33.56 o 6 5 28 333.52 312.23 49.41 o 0 6 28 13.59 11.19 36.33 o 1 6 28 87.05 39.63 30.78 o 2 6 28 518.04 591.81 60.77 o 3 6 28 9.25 21.69 29.84 o 4 6 28 187.63 149.93 37.98 o 5 6 28 151.30 198.54 40.22 o 1 7 28 1.29 -30.60 29.84 o 2 7 28 329.45 317.77 36.19 o 3 7 28 11.43 55.60 33.82 o 4 7 28 0.01 -9.10 36.75 o 0 8 28 150.39 124.59 53.42 o 1 8 28 22.61 42.97 36.87 o 2 8 28 60.89 96.74 33.49 o 3 8 28 43.47 100.96 38.01 o 1 9 28 175.65 227.11 50.27 o 2 9 28 147.25 176.17 38.13 o 1 1 29 0.98 9.19 30.76 o 2 1 29 99.68 90.94 31.15 o 3 1 29 900.32 856.27 48.33 o 4 1 29 0.22 -50.22 33.48 o 5 1 29 98.13 47.27 29.42 o 6 1 29 217.90 187.40 37.45 o 7 1 29 40.67 61.04 40.83 o 0 2 29 145.30 178.27 47.33 o 1 2 29 0.20 37.19 30.90 o 2 2 29 63.26 47.31 30.67 o 3 2 29 240.52 152.21 30.31 o 4 2 29 149.77 112.65 30.67 o 5 2 29 279.86 396.70 37.03 o 6 2 29 64.89 -18.62 35.02 o 1 3 29 303.96 306.55 38.34 o 2 3 29 104.38 98.79 28.71 o 3 3 29 5.75 9.90 27.59 o 4 3 29 144.76 156.95 47.60 o 5 3 29 623.08 684.64 47.79 o 6 3 29 231.05 301.92 45.96 o 0 4 29 610.41 665.41 114.71 o 1 4 29 313.19 362.48 40.73 o 2 4 29 240.86 206.92 32.57 o 3 4 29 117.81 129.77 31.52 o 4 4 29 27.36 -19.91 31.84 o 5 4 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0.10 13.16 31.70 o 4 2 30 5.15 -45.86 30.58 o 5 2 30 216.96 216.85 44.94 o 6 2 30 89.43 23.04 36.25 o 1 3 30 198.50 174.93 55.31 o 2 3 30 65.69 124.92 57.80 o 3 3 30 29.74 34.98 28.72 o 4 3 30 0.05 -9.74 39.76 o 5 3 30 0.75 21.15 35.79 o 6 3 30 3.82 -32.96 61.85 o 0 4 30 26.80 8.33 48.18 o 1 4 30 227.06 188.44 36.04 o 2 4 30 291.23 324.57 46.18 o 3 4 30 178.40 190.63 33.96 o 4 4 30 4.83 -29.57 31.68 o 5 4 30 159.36 149.47 38.72 o 1 5 30 30.17 50.68 41.83 o 2 5 30 265.50 205.35 33.48 o 3 5 30 5.72 -46.62 31.08 o 4 5 30 4.60 7.15 31.79 o 5 5 30 86.34 81.53 38.48 o 0 6 30 0.13 -27.95 49.13 o 1 6 30 114.27 70.41 32.26 o 2 6 30 78.10 91.54 33.60 o 3 6 30 583.60 696.58 51.61 o 4 6 30 122.13 86.63 58.61 o 1 7 30 327.77 374.67 39.24 o 2 7 30 0.78 29.38 33.97 o 3 7 30 112.16 133.66 36.42 o 0 8 30 491.30 392.74 64.03 o 1 8 30 67.53 53.01 40.41 o 1 1 31 8.75 -53.39 35.59 o 2 1 31 212.26 171.40 35.23 o 3 1 31 28.21 -26.57 32.86 o 4 1 31 65.72 60.02 35.96 o 5 1 31 15.84 -53.09 35.39 o 0 2 31 212.72 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129.35 56.33 o 1 4 33 84.95 29.31 37.13 o 2 4 33 2.10 -55.36 36.91 o 3 4 33 234.59 271.86 43.25 o 1 5 33 4.91 -47.36 38.64 o 2 5 33 0.09 -56.36 37.58 o 0 0 34 110.77 76.90 71.81 o 1 0 34 185.11 150.54 54.53 o 2 0 34 9.52 -10.72 51.89 o 3 0 34 259.31 215.74 60.03 o 1 1 34 1.81 -42.38 34.90 o 2 1 34 1.61 -53.44 35.63 o 3 1 34 32.22 -18.02 37.05 o 0 2 34 2.37 -24.77 52.43 o 1 2 34 289.29 312.08 42.84 o 2 2 34 12.88 -19.81 39.53 o 3 2 34 71.69 5.35 39.43 o 1 3 34 41.12 -10.71 37.71 o 2 3 34 15.46 -41.79 37.22 o 3 3 34 7.77 -30.82 39.13 o 0 4 34 15.13 -44.09 52.82 o 1 4 34 93.71 86.45 40.03 o 2 4 34 27.94 -40.18 38.76 o 1 1 35 163.84 197.26 43.17 o 2 1 35 225.99 162.87 40.86 o 0 2 35 4.34 1.43 54.65 o 1 2 35 9.79 -57.16 38.11 o 2 2 35 100.51 32.52 64.12 o 1 3 35 2.25 -8.07 39.14 o