#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:59:50 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180938 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/18/2201864.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201864_Fobs loop_ _publ_author_name 'Jones, Matthew D.' 'Almeida Paz, Filipe A.' 'Davies, John E.' 'Johnson, Brian F. G.' _publ_section_title ; (S)-({-})-2,2'-Bis(diphenylphosphino)-1,1'-binaphthyl, a versatile chelating ligand ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o535 _journal_page_last o537 _journal_volume 59 _journal_year 2003 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 103.206 _cell_angle_gamma 90.000 _cell_length_a 9.1206 _cell_length_b 18.7541 _cell_length_c 9.9829 _exptl_crystal_F_000 652.00 _reflns_d_resolution_high 0.8391 _cod_data_source_file cf6247Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' bj0308 in P2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 114.90 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 -22 0 39.29 55.82 19.11 o 1 -22 0 156.26 172.78 23.06 o 1 -21 0 17.32 15.12 10.79 o 2 -21 0 57.94 89.06 14.81 o 3 -21 0 86.70 59.15 14.72 o 0 -20 0 44.01 38.95 17.59 o 1 -20 0 106.45 112.04 14.78 o 2 -20 0 38.11 17.69 18.32 o 3 -20 0 64.91 45.97 12.51 o 4 -20 0 123.33 114.97 21.50 o 1 -19 0 4.92 3.58 12.60 o 2 -19 0 114.78 123.76 13.22 o 3 -19 0 584.39 666.06 39.95 o 4 -19 0 228.71 193.08 28.38 o 5 -19 0 47.00 74.50 23.82 o 0 -18 0 665.56 728.97 48.14 o 1 -18 0 341.01 360.30 21.76 o 2 -18 0 105.03 82.54 13.48 o 3 -18 0 35.33 26.79 16.07 o 4 -18 0 21.04 19.19 13.76 o 5 -18 0 51.35 67.55 23.02 o 6 -18 0 119.05 107.66 19.98 o 1 -17 0 50.27 62.05 9.43 o 2 -17 0 175.87 187.70 15.24 o 3 -17 0 81.40 71.09 16.07 o 4 -17 0 317.43 347.80 31.49 o 5 -17 0 21.64 6.15 13.03 o 6 -17 0 43.60 47.64 16.14 o 0 -16 0 121.30 137.29 13.40 o 1 -16 0 9.02 7.87 6.90 o 2 -16 0 200.91 205.32 10.61 o 3 -16 0 112.17 79.49 15.28 o 4 -16 0 44.07 32.94 11.51 o 5 -16 0 35.98 49.88 14.55 o 6 -16 0 5.56 -4.63 15.35 o 7 -16 0 73.78 73.85 26.93 o 1 -15 0 18.62 11.92 5.66 o 2 -15 0 253.32 255.34 13.94 o 3 -15 0 187.34 143.88 12.81 o 4 -15 0 110.61 104.18 16.07 o 5 -15 0 50.24 50.61 19.19 o 6 -15 0 116.29 111.35 19.19 o 7 -15 0 124.57 155.22 24.62 o 0 -14 0 56.29 72.88 18.82 o 1 -14 0 534.30 531.15 15.09 o 2 -14 0 336.97 351.96 14.70 o 3 -14 0 263.23 251.19 15.75 o 4 -14 0 81.52 72.71 12.26 o 5 -14 0 34.85 6.88 10.71 o 6 -14 0 72.12 92.89 16.87 o 7 -14 0 15.07 5.36 19.98 o 8 -14 0 24.68 -9.99 24.54 o 1 -13 0 496.06 526.62 21.35 o 2 -13 0 140.73 114.03 7.93 o 3 -13 0 166.27 164.50 17.88 o 4 -13 0 431.45 404.22 26.90 o 6 -13 0 59.55 42.21 16.07 o 7 -13 0 99.24 124.23 18.39 o 8 -13 0 5.65 24.54 16.87 o 0 -12 0 1394.70 1456.79 99.47 o 1 -12 0 323.78 303.30 10.92 o 2 -12 0 116.47 106.33 8.02 o 3 -12 0 42.59 37.74 6.99 o 4 -12 0 8.85 12.02 7.62 o 5 -12 0 409.46 412.86 20.78 o 6 -12 0 259.65 274.24 23.82 o 7 -12 0 121.68 106.50 18.39 o 8 -12 0 50.55 41.34 18.39 o 1 -11 0 245.03 271.55 15.95 o 2 -11 0 221.64 229.46 10.73 o 3 -11 0 133.02 123.19 10.20 o 4 -11 0 34.63 28.01 6.17 o 5 -11 0 33.40 36.23 7.67 o 6 -11 0 133.23 109.54 21.14 o 7 -11 0 42.18 48.94 13.76 o 8 -11 0 38.90 38.23 17.59 o 9 -11 0 20.34 21.43 15.28 o 0 -10 0 2221.70 2347.19 60.38 o 1 -10 0 16.19 10.88 4.53 o 2 -10 0 64.69 85.93 8.87 o 3 -10 0 532.94 551.14 21.64 o 4 -10 0 50.92 49.07 7.02 o 5 -10 0 21.30 14.46 6.45 o 6 -10 0 66.60 66.66 9.79 o 7 -10 0 0.44 -12.96 12.96 o 8 -10 0 40.71 38.23 17.59 o 9 -10 0 202.67 226.10 33.66 o 1 -9 0 155.70 175.00 6.85 o 2 -9 0 591.47 650.04 20.15 o 3 -9 0 25.08 22.54 6.22 o 4 -9 0 155.87 135.76 8.81 o 5 -9 0 231.22 222.86 12.93 o 6 -9 0 463.11 483.20 26.64 o 7 -9 0 724.18 718.62 41.34 o 8 -9 0 2.62 24.40 13.76 o 9 -9 0 67.01 99.91 19.84 o 0 -8 0 75.57 77.49 6.15 o 1 -8 0 248.60 259.18 22.15 o 2 -8 0 15.33 30.35 7.53 o 3 -8 0 998.90 951.92 58.64 o 4 -8 0 3.17 -6.90 7.25 o 5 -8 0 220.75 217.82 12.90 o 6 -8 0 47.13 52.18 8.04 o 7 -8 0 18.09 7.53 9.77 o 8 -8 0 16.13 21.36 14.48 o 9 -8 0 111.33 128.80 20.56 o 1 -7 0 219.39 236.92 18.82 o 2 -7 0 2543.24 2577.51 65.64 o 3 -7 0 1441.26 1521.86 45.66 o 4 -7 0 508.42 499.06 45.79 o 5 -7 0 297.82 291.69 14.47 o 6 -7 0 117.24 135.62 10.97 o 7 -7 0 32.28 32.29 14.26 o 8 -7 0 100.40 107.29 16.00 o 9 -7 0 98.20 76.16 23.60 o 10 -7 0 3.96 -14.48 24.40 o 0 -6 0 674.79 656.67 18.14 o 1 -6 0 2163.86 2150.93 55.21 o 2 -6 0 442.63 513.62 16.63 o 3 -6 0 184.75 188.68 9.70 o 4 -6 0 344.76 405.39 14.48 o 5 -6 0 68.00 64.65 8.00 o 6 -6 0 144.94 168.79 15.28 o 7 -6 0 646.84 689.13 31.27 o 8 -6 0 175.74 207.71 21.28 o 9 -6 0 87.98 120.98 22.81 o 10 -6 0 6.11 3.84 17.52 o 1 -5 0 793.47 776.09 21.77 o 2 -5 0 1309.69 1265.00 62.99 o 3 -5 0 4829.88 5000.83 126.07 o 4 -5 0 673.48 687.78 23.71 o 5 -5 0 287.51 318.65 29.50 o 6 -5 0 282.58 272.92 14.85 o 7 -5 0 401.87 402.10 23.61 o 8 -5 0 206.33 196.99 22.81 o 9 -5 0 1.19 22.81 15.20 o 10 -5 0 10.01 8.40 17.52 o 0 -4 0 402.20 402.25 13.58 o 1 -4 0 1333.07 1250.47 37.11 o 2 -4 0 3381.10 3391.30 88.79 o 3 -4 0 343.16 314.33 19.48 o 4 -4 0 77.09 76.34 23.20 o 5 -4 0 364.80 371.77 19.69 o 6 -4 0 270.68 277.51 14.39 o 7 -4 0 733.25 778.26 36.34 o 8 -4 0 544.77 501.35 41.92 o 9 -4 0 13.48 17.52 15.20 o 10 -4 0 225.22 213.14 25.92 o 1 -3 0 5477.06 2628.98 118.95 o 2 -3 0 8395.04 7932.86 230.91 o 3 -3 0 2013.46 2072.69 53.80 o 4 -3 0 172.24 179.46 13.32 o 5 -3 0 424.27 404.04 30.15 o 6 -3 0 221.10 199.43 26.28 o 7 -3 0 392.18 378.70 27.33 o 8 -3 0 212.14 220.81 20.56 o 9 -3 0 145.20 144.65 25.12 o 10 -3 0 33.05 37.28 19.76 o 2 -2 0 371.56 372.80 11.84 o 3 -2 0 40.61 36.82 4.30 o 4 -2 0 1281.37 1335.47 79.96 o 5 -2 0 597.00 536.58 28.97 o 6 -2 0 403.77 427.59 17.88 o 7 -2 0 109.48 97.48 10.75 o 8 -2 0 187.94 167.94 34.93 o 9 -2 0 41.13 35.04 16.00 o 10 -2 0 33.68 38.88 22.08 o 2 -1 0 581.21 516.99 42.17 o 3 -1 0 174.14 170.64 8.63 o 4 -1 0 1033.19 1037.84 44.40 o 5 -1 0 18.98 20.03 5.09 o 6 -1 0 111.51 101.93 11.80 o 7 -1 0 172.80 165.06 8.09 o 8 -1 0 27.87 30.58 8.02 o 9 -1 0 101.34 119.02 23.67 o 10 -1 0 19.72 39.67 19.84 o 2 0 0 1191.17 1119.11 38.00 o 3 0 0 1996.97 1963.14 47.17 o 4 0 0 127.72 100.20 11.66 o 5 0 0 1.00 6.88 5.36 o 6 0 0 1272.03 1356.12 61.47 o 7 0 0 361.00 368.34 20.45 o 8 0 0 59.85 78.77 19.69 o 9 0 0 5.36 0.00 12.96 o 10 0 0 39.66 63.35 19.84 o 2 1 0 603.63 568.22 14.55 o 3 1 0 171.17 177.21 5.83 o 4 1 0 1043.07 1053.20 27.53 o 5 1 0 21.65 21.30 2.73 o 6 1 0 114.51 124.68 9.97 o 7 1 0 172.81 170.98 13.77 o 8 1 0 29.31 25.77 14.41 o 9 1 0 102.32 100.20 22.15 o 10 1 0 19.58 6.88 26.79 o 2 2 0 372.96 369.22 9.84 o 3 2 0 37.56 40.68 6.19 o 4 2 0 1279.55 1274.46 26.87 o 5 2 0 600.72 609.09 18.38 o 6 2 0 411.21 437.88 25.27 o 7 2 0 107.49 104.49 7.08 o 8 2 0 184.31 146.53 23.53 o 9 2 0 40.23 38.30 14.55 o 10 2 0 32.17 23.75 16.07 o 1 3 0 5462.01 3366.04 966.87 o 2 3 0 8419.07 7902.23 201.24 o 3 3 0 2017.44 2067.60 55.33 o 4 3 0 170.41 164.79 8.60 o 5 3 0 430.40 438.80 12.78 o 6 3 0 226.68 211.48 9.30 o 7 3 0 397.12 399.31 15.18 o 8 3 0 217.22 193.99 18.17 o 9 3 0 143.90 144.22 16.87 o 10 3 0 32.74 43.66 20.71 o 1 4 0 1353.50 1339.84 39.41 o 2 4 0 3408.59 3383.45 87.57 o 3 4 0 350.30 329.34 12.33 o 4 4 0 74.61 69.32 16.65 o 5 4 0 358.71 368.08 12.52 o 6 4 0 268.81 274.71 14.74 o 7 4 0 736.17 742.65 26.18 o 8 4 0 538.30 541.24 52.20 o 9 4 0 12.92 32.22 14.62 o 10 4 0 221.83 204.89 26.14 o 1 5 0 807.93 784.95 28.81 o 2 5 0 1338.47 1378.44 36.96 o 3 5 0 4863.33 5071.56 127.79 o 4 5 0 678.74 696.48 18.00 o 5 5 0 292.21 290.92 13.99 o 6 5 0 286.40 284.73 10.45 o 7 5 0 406.60 425.83 18.15 o 8 5 0 201.42 200.04 29.68 o 9 5 0 1.32 18.46 14.62 o 10 5 0 9.97 41.48 16.87 o 1 6 0 2144.91 2138.62 68.34 o 2 6 0 445.88 499.14 17.58 o 3 6 0 187.03 194.92 8.86 o 4 6 0 340.18 366.58 14.82 o 5 6 0 67.78 68.15 13.61 o 6 6 0 139.06 129.33 9.36 o 7 6 0 641.59 664.48 21.90 o 8 6 0 173.36 163.56 12.79 o 9 6 0 88.70 83.11 16.94 o 10 6 0 6.03 -17.67 17.67 o 1 7 0 216.49 236.35 9.66 o 2 7 0 2545.58 2697.14 78.61 o 3 7 0 1467.72 1565.18 47.70 o 4 7 0 497.30 486.22 17.36 o 5 7 0 291.34 281.90 10.84 o 6 7 0 119.70 96.09 14.12 o 7 7 0 33.91 42.87 4.10 o 8 7 0 100.73 99.24 9.96 o 9 7 0 97.19 89.34 18.46 o 10 7 0 3.95 30.77 12.54 o 1 8 0 241.64 263.46 10.51 o 2 8 0 17.12 29.20 5.30 o 3 8 0 1003.22 999.72 37.25 o 4 8 0 4.19 9.80 5.62 o 5 8 0 221.93 213.37 12.65 o 6 8 0 47.71 36.92 8.06 o 7 8 0 17.14 29.12 9.42 o 8 8 0 17.43 21.33 23.53 o 9 8 0 112.33 99.40 26.21 o 1 9 0 153.46 158.55 12.24 o 2 9 0 585.84 679.38 23.52 o 3 9 0 25.63 34.10 13.54 o 4 9 0 158.41 165.80 11.23 o 5 9 0 229.57 223.08 13.74 o 6 9 0 463.58 426.40 38.70 o 7 9 0 736.87 727.96 54.01 o 8 9 0 3.04 10.94 10.07 o 9 9 0 67.08 80.94 20.85 o 1 10 0 17.20 41.92 9.92 o 2 10 0 63.49 65.37 8.03 o 3 10 0 525.83 566.81 25.59 o 4 10 0 51.52 48.40 6.70 o 5 10 0 20.50 24.44 8.04 o 6 10 0 68.47 70.34 7.72 o 7 10 0 0.36 -4.63 11.51 o 8 10 0 41.48 43.95 17.74 o 9 10 0 202.58 229.86 30.91 o 1 11 0 241.44 256.22 18.32 o 2 11 0 222.23 242.01 13.14 o 3 11 0 134.17 142.67 10.61 o 4 11 0 36.55 35.77 8.20 o 5 11 0 30.76 22.84 6.92 o 6 11 0 133.71 111.06 12.00 o 7 11 0 44.68 39.24 12.31 o 8 11 0 38.68 29.32 13.90 o 9 11 0 20.37 6.15 18.53 o 2 12 0 118.08 100.77 8.89 o 3 12 0 41.64 37.86 10.57 o 4 12 0 9.43 10.62 6.45 o 5 12 0 403.17 402.14 30.48 o 6 12 0 257.17 225.95 23.09 o 7 12 0 121.43 105.48 23.09 o 8 12 0 51.09 91.00 19.26 o 2 13 0 139.71 126.91 17.59 o 3 13 0 161.99 159.73 12.43 o 4 13 0 431.89 428.01 24.14 o 5 13 0 1.96 10.42 8.20 o 6 13 0 57.78 37.65 16.94 o 7 13 0 99.38 99.33 16.94 o 8 13 0 5.68 2.32 18.53 o 2 14 0 335.06 272.29 20.71 o 3 14 0 262.56 263.25 16.09 o 4 14 0 84.15 88.98 11.23 o 5 14 0 32.95 12.31 11.51 o 6 14 0 70.38 59.95 15.35 o 7 14 0 14.51 19.26 15.42 o 8 14 0 25.22 27.80 26.21 o 2 15 0 255.44 257.01 22.23 o 3 15 0 188.38 206.39 14.26 o 4 15 0 112.48 114.32 16.87 o 5 15 0 47.56 53.79 13.83 o 6 15 0 111.53 105.34 19.26 o 7 15 0 126.92 157.90 25.41 o 3 16 0 113.52 90.42 13.83 o 4 16 0 46.91 20.71 11.51 o 5 16 0 34.63 40.69 16.14 o 6 16 0 5.27 29.97 22.30 o 7 16 0 74.26 64.72 20.05 o 3 17 0 85.12 45.25 13.03 o 4 17 0 319.07 339.18 31.49 o 5 17 0 20.83 31.49 16.94 o 6 17 0 43.22 52.34 18.46 o 3 18 0 35.21 32.22 13.83 o 4 18 0 21.80 19.19 19.19 o 5 18 0 51.43 102.23 26.93 o 6 18 0 118.10 126.19 25.41 o 4 19 0 229.94 232.61 29.18 o 5 19 0 46.42 28.45 19.98 o 4 20 0 123.96 99.04 26.14 o -1 -22 1 27.10 25.71 18.71 o 0 -22 1 3.51 -8.16 11.61 o 1 -22 1 40.80 54.50 29.68 o -3 -21 1 110.78 78.94 15.72 o -2 -21 1 86.34 97.49 25.16 o -1 -21 1 63.16 59.42 12.62 o 0 -21 1 58.27 78.82 15.22 o 1 -21 1 67.01 62.55 20.05 o 2 -21 1 45.43 55.05 14.05 o 3 -21 1 59.20 31.77 19.84 o -4 -20 1 87.32 111.35 23.02 o -3 -20 1 424.74 411.22 29.80 o -2 -20 1 20.00 22.50 11.33 o -1 -20 1 60.70 58.71 12.13 o 0 -20 1 56.87 58.91 13.10 o 1 -20 1 134.84 142.53 14.79 o 2 -20 1 88.58 118.76 17.96 o 3 -20 1 0.38 19.51 18.79 o 4 -20 1 14.06 11.44 19.91 o -5 -19 1 75.56 145.37 32.29 o -4 -19 1 55.33 39.96 18.46 o -3 -19 1 241.64 200.52 45.28 o -2 -19 1 10.61 11.61 24.11 o -1 -19 1 83.00 95.57 18.57 o 0 -19 1 17.85 2.28 10.98 o 1 -19 1 136.52 169.03 20.89 o 2 -19 1 103.46 83.65 20.89 o 3 -19 1 56.02 53.40 13.61 o 4 -19 1 27.09 -2.32 12.24 o 5 -19 1 27.86 45.18 21.43 o -6 -18 1 39.01 63.13 25.41 o -5 -18 1 134.85 114.61 19.98 o -4 -18 1 154.65 183.53 26.86 o -3 -18 1 126.24 123.44 18.39 o -2 -18 1 51.58 50.51 12.08 o -1 -18 1 38.79 25.89 8.90 o 0 -18 1 32.37 9.69 8.36 o 1 -18 1 98.00 112.26 17.52 o 2 -18 1 192.51 204.42 16.31 o 3 -18 1 0.14 22.08 17.52 o 4 -18 1 9.84 -14.55 14.55 o 5 -18 1 18.40 33.66 19.19 o -7 -17 1 12.34 11.58 25.41 o -6 -17 1 66.08 63.93 23.09 o -5 -17 1 16.90 24.62 22.30 o -4 -17 1 110.42 92.89 16.87 o -3 -17 1 10.34 7.67 10.71 o -2 -17 1 320.87 331.04 19.12 o -1 -17 1 52.99 38.44 11.80 o 0 -17 1 41.16 51.09 13.83 o 1 -17 1 20.15 35.48 8.33 o 2 -17 1 152.54 173.17 13.72 o 3 -17 1 131.63 118.95 19.04 o 4 -17 1 32.51 47.35 15.28 o 5 -17 1 42.83 32.14 19.91 o 6 -17 1 4.32 16.07 21.50 o -7 -16 1 9.22 2.32 16.94 o -6 -16 1 25.35 27.73 14.62 o -5 -16 1 65.34 79.20 14.62 o -4 -16 1 15.74 12.31 11.51 o -3 -16 1 161.25 193.08 20.71 o -2 -16 1 446.18 442.28 16.18 o -1 -16 1 787.56 822.31 26.28 o 0 -16 1 421.91 433.43 15.46 o 1 -16 1 708.01 766.71 24.60 o 2 -16 1 216.57 223.02 10.37 o 3 -16 1 158.25 119.67 19.04 o 4 -16 1 19.68 27.51 12.24 o 5 -16 1 160.22 147.04 26.06 o 6 -16 1 140.58 145.66 23.02 o 7 -16 1 182.69 223.35 29.97 o -7 -15 1 47.51 59.22 21.57 o -6 -15 1 50.82 28.45 18.46 o -5 -15 1 98.19 85.36 16.94 o -4 -15 1 71.40 52.20 16.87 o -3 -15 1 163.41 152.22 14.85 o -2 -15 1 601.66 620.75 23.00 o -1 -15 1 147.40 143.04 8.15 o 0 -15 1 23.71 27.11 7.54 o 1 -15 1 107.08 106.17 7.56 o 2 -15 1 339.56 342.67 17.95 o 3 -15 1 305.37 329.78 19.40 o 4 -15 1 254.87 291.18 29.10 o 5 -15 1 155.12 176.07 21.50 o 6 -15 1 53.80 53.65 19.91 o 7 -15 1 17.77 30.70 23.02 o -8 -14 1 88.94 119.96 22.30 o -7 -14 1 53.51 26.14 14.62 o -6 -14 1 51.39 30.77 20.78 o -5 -14 1 9.89 39.96 16.14 o -4 -14 1 368.16 309.46 19.13 o -3 -14 1 87.03 79.61 9.10 o -2 -14 1 243.72 228.27 11.53 o -1 -14 1 106.09 105.89 7.25 o 0 -14 1 240.33 228.97 10.01 o 1 -14 1 216.70 212.08 10.19 o 2 -14 1 631.82 612.15 23.23 o 3 -14 1 139.38 131.45 18.10 o 4 -14 1 6.45 5.18 8.02 o 5 -14 1 60.43 32.14 13.03 o 6 -14 1 155.87 160.14 21.50 o 7 -14 1 6.55 16.07 17.59 o -8 -13 1 33.53 24.54 24.54 o -7 -13 1 120.36 147.47 23.09 o -6 -13 1 197.55 201.99 23.82 o -5 -13 1 132.84 143.84 12.39 o -4 -13 1 9.31 12.09 6.96 o -3 -13 1 2.93 -6.05 6.05 o -2 -13 1 177.44 179.11 9.78 o -1 -13 1 264.74 251.33 9.30 o 0 -13 1 592.00 586.28 17.31 o 1 -13 1 247.98 232.66 11.25 o 2 -13 1 171.71 172.88 8.67 o 3 -13 1 32.89 34.63 7.76 o 4 -13 1 39.81 45.73 9.12 o 5 -13 1 19.00 36.65 22.23 o 6 -13 1 156.48 150.01 19.19 o 7 -13 1 4.72 12.24 14.55 o 8 -13 1 82.55 81.16 23.75 o -9 -12 1 183.82 210.10 36.05 o -8 -12 1 64.79 96.65 19.98 o -7 -12 1 90.19 157.97 31.49 o -6 -12 1 67.12 57.56 13.03 o -5 -12 1 115.52 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429.39 15.97 o -3 -8 2 1287.58 1235.01 39.09 o -2 -8 2 356.24 373.55 15.21 o -1 -8 2 511.53 542.52 28.27 o 0 -8 2 147.72 142.99 5.22 o 1 -8 2 533.34 563.33 29.10 o 2 -8 2 272.87 277.12 12.39 o 3 -8 2 193.18 211.86 17.09 o 4 -8 2 325.79 350.79 15.28 o 5 -8 2 264.03 265.13 13.49 o 6 -8 2 27.98 33.40 8.51 o 7 -8 2 48.97 39.53 11.44 o 8 -8 2 152.75 177.95 22.81 o 9 -8 2 1.79 16.72 14.48 o -10 -7 2 25.07 22.08 26.71 o -8 -7 2 87.16 122.64 15.28 o -7 -7 2 208.53 230.73 16.34 o -6 -7 2 46.89 36.52 10.13 o -5 -7 2 323.67 318.67 19.73 o -4 -7 2 259.40 269.98 15.96 o -3 -7 2 1318.51 1404.27 37.61 o -2 -7 2 0.36 4.22 3.76 o -1 -7 2 3.68 1.52 4.30 o 0 -7 2 0.48 -2.38 2.38 o 1 -7 2 174.24 187.26 14.66 o 2 -7 2 500.07 533.27 28.02 o 3 -7 2 312.76 352.66 12.93 o 4 -7 2 819.35 813.76 27.44 o 5 -7 2 562.71 549.18 22.68 o 6 -7 2 202.68 210.96 14.37 o 7 -7 2 9.96 24.55 8.22 o 8 -7 2 11.71 14.41 11.37 o 9 -7 2 78.26 73.70 16.72 o -10 -6 2 2.07 11.44 18.32 o -8 -6 2 238.91 217.70 19.04 o -7 -6 2 846.34 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643.83 61.32 o -9 1 2 323.09 261.21 26.06 o -8 1 2 218.43 222.77 16.33 o -7 1 2 7.79 8.66 7.15 o -6 1 2 140.02 145.85 10.14 o -5 1 2 447.38 418.99 16.18 o -4 1 2 46.05 46.09 5.51 o -3 1 2 569.09 588.88 83.80 o -2 1 2 2017.38 2018.91 55.82 o -1 1 2 2349.80 2166.75 43.17 o 0 1 2 5948.72 5075.77 375.89 o 1 1 2 1574.53 1504.69 30.73 o 2 1 2 674.90 633.05 12.77 o 3 1 2 102.90 96.83 4.88 o 4 1 2 418.92 418.77 10.59 o 5 1 2 42.96 59.74 5.41 o 6 1 2 56.58 56.02 6.74 o 7 1 2 173.50 195.37 24.14 o 8 1 2 28.44 20.98 7.55 o 9 1 2 22.18 51.11 21.36 o -10 2 2 58.21 59.00 17.67 o -9 2 2 120.72 99.76 16.87 o -8 2 2 35.67 41.68 9.16 o -7 2 2 186.07 164.89 7.37 o -6 2 2 49.24 65.93 7.52 o -5 2 2 438.69 435.00 52.13 o -4 2 2 422.92 419.21 24.04 o -3 2 2 41.78 41.13 3.55 o -2 2 2 2007.89 1995.68 36.06 o -1 2 2 12300.63 11325.64 239.68 o 0 2 2 3998.21 3824.05 129.95 o 1 2 2 2706.45 2634.40 49.31 o 2 2 2 293.73 287.90 8.45 o 3 2 2 405.75 417.30 9.94 o 4 2 2 332.04 367.32 14.01 o 5 2 2 542.93 582.28 15.56 o 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