#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/18/2201873.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201873_Fobs loop_ _publ_author_name 'Rajagopal, K.' 'Krishnakumar, R. V.' 'Mostad, A.' 'Natarajan, S.' _publ_section_title ; DL-Methioninium trichloroacetate at 123K ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o31 _journal_page_last o33 _journal_volume 59 _journal_year 2003 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 70.541 _cell_angle_beta 85.954 _cell_angle_gamma 85.084 _cell_length_a 6.1359 _cell_length_b 8.9746 _cell_length_c 12.7315 _exptl_crystal_F_000 320.00 _reflns_d_resolution_high 0.7687 _[local]_cod_data_source_file ci6188Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' DL-met tcaa in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 116.07 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1149.41 1239.89 10.60 o 2 0 0 2.66 15.54 0.77 o 3 0 0 1102.60 1107.52 5.52 o 4 0 0 2809.37 2739.51 25.71 o 5 0 0 7.96 8.43 2.29 o 6 0 0 42.20 49.63 6.23 o 7 0 0 303.01 303.19 4.06 o -7 1 0 34.65 32.25 2.17 o -6 1 0 77.52 89.09 2.89 o -5 1 0 58.44 64.98 3.24 o -4 1 0 2.61 3.03 1.91 o -3 1 0 2.77 1.76 0.62 o -2 1 0 162.86 168.86 3.48 o -1 1 0 6051.67 5887.82 104.49 o 0 1 0 60.42 56.21 18.49 o 1 1 0 784.12 801.26 3.94 o 2 1 0 916.04 1228.94 89.05 o 3 1 0 587.01 720.46 6.04 o 4 1 0 761.69 776.18 16.78 o 5 1 0 91.41 85.65 2.70 o 6 1 0 571.48 552.26 10.40 o 7 1 0 75.97 67.61 2.33 o -7 2 0 197.01 192.27 3.50 o -6 2 0 57.75 62.39 1.81 o -5 2 0 0.20 -0.17 2.28 o -4 2 0 112.19 111.96 2.13 o -3 2 0 1213.10 1185.22 40.05 o -2 2 0 14.31 10.84 0.69 o -1 2 0 54.57 75.70 2.34 o 0 2 0 2681.07 2679.87 60.39 o 1 2 0 1381.25 1272.24 16.12 o 2 2 0 8676.43 8786.90 34.21 o 3 2 0 0.19 2.38 0.88 o 4 2 0 459.04 497.64 12.03 o 5 2 0 79.47 122.06 3.28 o 6 2 0 634.90 598.26 7.90 o 7 2 0 48.63 50.40 2.20 o -7 3 0 297.68 305.25 4.73 o -6 3 0 0.01 -1.51 1.51 o -5 3 0 84.78 90.86 2.22 o -4 3 0 1558.17 1521.85 17.55 o -3 3 0 2094.70 2113.40 12.52 o -2 3 0 14.27 22.06 1.63 o -1 3 0 308.86 301.09 10.96 o 0 3 0 3241.75 3044.50 14.10 o 1 3 0 7.76 12.11 0.81 o 2 3 0 0.15 5.86 0.78 o 3 3 0 162.20 135.35 1.89 o 4 3 0 143.09 138.98 1.78 o 5 3 0 513.55 472.37 4.27 o 6 3 0 40.64 44.11 1.39 o 7 3 0 62.01 81.42 3.01 o -7 4 0 19.39 20.99 2.09 o -6 4 0 17.24 17.61 1.71 o -5 4 0 333.83 334.91 3.27 o -4 4 0 386.68 390.06 7.19 o -3 4 0 2.79 3.33 1.04 o -2 4 0 879.89 944.00 33.59 o -1 4 0 305.33 295.75 6.13 o 0 4 0 1206.98 1269.47 6.42 o 1 4 0 334.90 409.39 9.57 o 2 4 0 57.54 58.40 2.77 o 3 4 0 8.06 7.11 1.07 o 4 4 0 69.61 81.13 1.65 o 5 4 0 7.48 7.29 1.03 o 6 4 0 9.15 9.70 1.59 o 7 4 0 23.33 32.22 2.70 o -6 5 0 3.26 1.93 1.71 o -5 5 0 222.00 216.74 2.82 o -4 5 0 20.47 22.55 1.86 o -3 5 0 985.24 1009.70 15.03 o -2 5 0 405.26 437.41 27.50 o -1 5 0 290.69 290.53 13.00 o 0 5 0 980.17 1061.94 6.03 o 1 5 0 1268.08 1343.64 7.24 o 2 5 0 68.87 60.61 1.62 o 3 5 0 92.53 77.24 1.54 o 4 5 0 506.42 497.92 3.01 o 5 5 0 0.01 0.90 1.08 o 6 5 0 36.30 40.62 1.61 o 7 5 0 144.65 153.78 2.64 o -6 6 0 0.22 -2.03 2.05 o -5 6 0 13.92 6.93 1.95 o -4 6 0 40.94 45.16 3.22 o -3 6 0 816.38 779.50 7.61 o -2 6 0 518.70 507.86 17.46 o -1 6 0 62.22 61.61 1.99 o 0 6 0 46.21 48.82 2.58 o 1 6 0 881.32 834.16 13.75 o 2 6 0 1399.30 1343.80 27.59 o 3 6 0 22.71 18.76 1.10 o 4 6 0 124.32 116.07 1.70 o 5 6 0 48.93 50.13 1.50 o 6 6 0 4.66 3.83 1.46 o -5 7 0 55.43 53.21 2.49 o -4 7 0 2.11 3.98 1.80 o -3 7 0 195.27 190.55 8.24 o -2 7 0 235.70 229.31 6.75 o -1 7 0 69.80 65.78 1.42 o 0 7 0 0.58 1.39 1.04 o 1 7 0 61.08 58.59 1.34 o 2 7 0 164.96 167.40 3.18 o 3 7 0 998.34 1010.49 13.85 o 4 7 0 42.66 41.54 1.35 o 5 7 0 4.01 3.55 1.36 o 6 7 0 206.96 226.71 3.79 o -5 8 0 102.01 95.03 3.12 o -4 8 0 1.82 -0.56 2.99 o -3 8 0 50.80 50.30 2.61 o -2 8 0 14.17 12.47 1.27 o -1 8 0 147.00 145.43 2.04 o 0 8 0 152.43 154.25 1.87 o 1 8 0 2.92 2.56 0.94 o 2 8 0 181.39 172.70 6.23 o 3 8 0 113.38 111.54 2.95 o 4 8 0 265.46 281.84 3.32 o 5 8 0 109.06 110.51 3.04 o -4 9 0 0.01 -0.61 1.95 o -3 9 0 168.83 168.71 3.29 o -2 9 0 176.60 176.50 2.63 o -1 9 0 69.54 66.51 1.59 o 0 9 0 86.00 79.71 2.36 o 1 9 0 205.96 207.07 7.96 o 2 9 0 11.19 15.01 1.87 o 3 9 0 21.00 24.40 1.54 o 4 9 0 25.70 28.47 1.74 o 5 9 0 18.16 15.81 3.24 o -2 10 0 61.53 62.33 2.07 o -1 10 0 170.31 161.15 5.28 o 0 10 0 166.64 154.59 2.96 o 1 10 0 83.82 79.81 2.41 o 2 10 0 207.71 204.23 5.46 o 3 10 0 143.22 155.97 2.77 o -3 -10 1 77.16 85.55 4.11 o -2 -10 1 27.91 27.04 1.75 o -1 -10 1 109.63 102.79 2.72 o 0 -10 1 98.45 85.46 2.54 o 1 -10 1 239.59 227.44 4.07 o 2 -10 1 114.44 108.70 3.03 o -4 -9 1 2.36 2.56 1.56 o -3 -9 1 1.92 1.30 1.34 o -2 -9 1 228.67 216.22 6.50 o -1 -9 1 23.38 25.73 2.04 o 0 -9 1 3.28 2.74 1.25 o 1 -9 1 1.05 1.86 1.32 o 2 -9 1 71.43 70.88 2.47 o 3 -9 1 1.53 1.22 1.82 o -5 -8 1 32.01 37.91 1.90 o -4 -8 1 2.94 1.30 1.46 o -3 -8 1 119.34 123.49 2.22 o -2 -8 1 124.43 127.31 2.49 o -1 -8 1 49.58 45.34 1.40 o 0 -8 1 32.37 31.88 1.47 o 1 -8 1 493.53 468.47 5.50 o 2 -8 1 24.05 24.48 1.44 o 3 -8 1 143.16 135.14 3.55 o 4 -8 1 103.02 103.48 4.50 o -6 -7 1 163.56 169.38 2.85 o -5 -7 1 25.31 30.21 1.68 o -4 -7 1 31.01 35.77 1.61 o -3 -7 1 306.76 321.41 3.10 o -2 -7 1 65.13 67.42 1.61 o -1 -7 1 3.48 5.79 1.69 o 0 -7 1 942.25 905.64 9.79 o 1 -7 1 666.48 648.09 3.56 o 2 -7 1 15.46 14.06 1.18 o 3 -7 1 25.25 28.25 2.32 o 4 -7 1 133.30 128.01 3.94 o 5 -7 1 20.09 17.66 2.19 o -6 -6 1 39.88 43.89 1.85 o -5 -6 1 15.80 13.93 1.49 o -4 -6 1 2.08 1.94 1.18 o -3 -6 1 15.99 17.14 1.27 o -2 -6 1 72.73 73.44 1.94 o -1 -6 1 72.54 71.97 1.80 o 0 -6 1 598.58 606.75 11.22 o 1 -6 1 466.85 466.74 4.37 o 2 -6 1 286.22 273.10 3.77 o 3 -6 1 74.30 68.92 4.12 o 4 -6 1 28.45 31.77 2.11 o 5 -6 1 76.79 72.73 2.62 o 6 -6 1 37.16 33.51 2.58 o -7 -5 1 0.43 -1.54 1.68 o -6 -5 1 98.13 97.68 2.04 o -5 -5 1 76.03 75.53 1.53 o -4 -5 1 950.13 947.64 13.25 o -3 -5 1 13.28 11.70 1.14 o -2 -5 1 41.02 38.52 1.44 o -1 -5 1 12.99 10.17 1.43 o 0 -5 1 398.67 412.45 3.41 o 1 -5 1 37.17 35.07 1.26 o 2 -5 1 134.21 140.35 4.34 o 3 -5 1 124.00 118.65 8.77 o 4 -5 1 86.67 87.60 2.37 o 5 -5 1 151.20 149.68 2.71 o 6 -5 1 10.02 9.43 1.76 o -7 -4 1 282.54 295.17 6.51 o -6 -4 1 73.01 69.89 1.85 o -5 -4 1 120.60 115.48 1.62 o -4 -4 1 396.21 409.08 5.28 o -3 -4 1 1102.17 1057.23 6.29 o -2 -4 1 0.70 4.20 1.42 o -1 -4 1 788.78 766.71 26.28 o 0 -4 1 2.14 5.99 0.91 o 1 -4 1 22.06 21.88 4.83 o 2 -4 1 1704.19 1714.49 46.17 o 3 -4 1 701.34 684.67 8.04 o 4 -4 1 149.74 156.98 2.23 o 5 -4 1 1.24 2.23 1.41 o 6 -4 1 313.71 349.36 4.59 o 7 -4 1 35.17 36.34 2.10 o -7 -3 1 7.22 8.67 2.18 o -6 -3 1 18.10 15.80 1.41 o -5 -3 1 172.41 160.25 1.83 o -4 -3 1 69.48 76.68 1.48 o -3 -3 1 202.76 191.08 2.77 o -2 -3 1 1792.94 1822.61 8.66 o -1 -3 1 1564.84 1638.25 20.16 o 0 -3 1 513.77 513.46 14.58 o 1 -3 1 0.98 2.79 1.05 o 2 -3 1 1013.13 1119.04 46.59 o 3 -3 1 2.33 0.88 1.44 o 4 -3 1 2.59 3.76 1.42 o 5 -3 1 92.83 103.95 2.19 o 6 -3 1 93.66 103.25 2.27 o 7 -3 1 69.26 82.26 2.94 o -7 -2 1 3.11 2.01 1.70 o -6 -2 1 12.86 11.80 1.44 o -5 -2 1 278.30 281.88 3.65 o -4 -2 1 128.09 122.76 2.37 o -3 -2 1 116.21 110.28 2.98 o -2 -2 1 781.25 884.09 29.56 o -1 -2 1 2799.01 2872.06 19.16 o 0 -2 1 335.40 385.90 6.95 o 1 -2 1 2415.01 2479.06 80.62 o 2 -2 1 67.54 68.20 1.01 o 3 -2 1 895.76 883.02 37.86 o 4 -2 1 294.50 295.88 3.27 o 5 -2 1 279.11 260.97 3.91 o 6 -2 1 0.18 -0.43 1.34 o 7 -2 1 20.88 28.52 2.23 o -7 -1 1 173.47 172.06 3.12 o -6 -1 1 35.05 33.36 1.85 o -5 -1 1 272.53 247.58 6.29 o -4 -1 1 24.15 29.73 1.09 o -3 -1 1 61.93 65.34 2.29 o -2 -1 1 910.97 936.88 30.10 o -1 -1 1 294.56 288.09 2.58 o 0 -1 1 193.38 171.40 2.79 o 1 -1 1 1239.96 1284.93 42.37 o 2 -1 1 4172.01 4077.58 19.80 o 3 -1 1 289.02 321.98 3.19 o 4 -1 1 172.66 182.81 3.63 o 5 -1 1 93.22 91.66 4.09 o 6 -1 1 128.78 125.83 2.65 o 7 -1 1 13.96 12.72 2.08 o -7 0 1 47.93 53.27 2.31 o -6 0 1 41.61 42.99 1.95 o -5 0 1 0.13 0.17 1.48 o -4 0 1 0.11 2.11 0.87 o -3 0 1 63.14 65.40 1.12 o -2 0 1 363.83 411.64 2.45 o -1 0 1 160.28 131.91 4.22 o 0 0 1 244.72 -0.06 0.18 o 1 0 1 115.70 115.12 1.53 o 2 0 1 4179.60 4394.33 90.75 o 3 0 1 2151.06 2218.58 10.16 o 4 0 1 97.16 90.78 2.73 o 5 0 1 33.90 29.87 1.73 o 6 0 1 146.10 140.73 2.73 o 7 0 1 98.60 120.57 11.21 o -7 1 1 484.03 472.26 16.73 o -6 1 1 167.89 198.62 6.49 o -5 1 1 326.56 335.62 8.90 o -4 1 1 201.82 198.38 6.17 o -3 1 1 2466.38 2457.29 14.43 o -2 1 1 514.80 534.93 4.10 o -1 1 1 527.76 517.61 2.74 o 0 1 1 2.84 8.22 0.81 o 1 1 1 123.82 118.18 1.00 o 2 1 1 1806.10 1911.75 50.31 o 3 1 1 1276.17 1288.11 11.50 o 4 1 1 254.60 243.88 4.70 o 5 1 1 0.37 1.40 1.46 o 6 1 1 274.43 274.70 5.95 o 7 1 1 109.54 112.08 3.62 o -7 2 1 1.98 0.81 2.07 o -6 2 1 155.97 152.19 3.18 o -5 2 1 483.18 491.26 14.86 o -4 2 1 52.03 83.47 5.59 o -3 2 1 62.79 364.55 3.33 o -2 2 1 985.27 936.49 5.95 o -1 2 1 46.29 59.26 1.54 o 0 2 1 1571.93 1603.14 21.50 o 1 2 1 23.65 23.51 0.74 o 2 2 1 1339.54 1321.84 6.22 o 3 2 1 121.31 110.56 2.75 o 4 2 1 975.98 1060.48 83.66 o 5 2 1 20.64 25.59 1.37 o 6 2 1 41.13 38.67 1.66 o 7 2 1 0.05 -0.35 1.65 o -7 3 1 24.50 29.41 2.50 o -6 3 1 17.00 21.99 1.73 o -5 3 1 805.66 800.92 4.83 o -4 3 1 672.48 654.28 4.15 o -3 3 1 44.79 43.95 1.11 o -2 3 1 214.33 258.39 21.15 o -1 3 1 9516.84 10272.05 254.03 o 0 3 1 3954.28 4038.55 81.52 o 1 3 1 101.60 98.33 2.98 o 2 3 1 279.32 257.83 4.32 o 3 3 1 689.30 671.12 8.84 o 4 3 1 10.43 9.79 1.19 o 5 3 1 229.43 243.72 10.05 o 6 3 1 16.87 15.72 1.34 o 7 3 1 0.37 3.57 1.81 o -7 4 1 184.16 219.74 7.21 o -6 4 1 90.58 102.84 3.09 o -5 4 1 4.94 2.89 1.37 o -4 4 1 11.49 12.30 1.44 o -3 4 1 423.04 439.75 3.39 o -2 4 1 626.05 613.95 6.76 o -1 4 1 1537.21 1549.28 44.48 o 0 4 1 132.00 152.53 10.21 o 2 4 1 3197.09 3135.80 13.61 o 3 4 1 1852.71 1848.22 24.01 o 4 4 1 26.26 24.01 1.03 o 5 4 1 39.33 39.49 1.26 o 6 4 1 437.89 454.00 6.86 o 7 4 1 24.96 27.43 1.69 o -6 5 1 0.95 2.52 2.11 o -5 5 1 129.49 132.49 2.38 o -4 5 1 60.16 66.82 2.15 o -3 5 1 376.16 372.28 5.37 o -2 5 1 1.28 2.19 1.09 o -1 5 1 0.10 1.69 0.88 o 0 5 1 160.05 174.03 2.58 o 1 5 1 857.98 923.14 6.25 o 2 5 1 5.03 6.96 1.12 o 3 5 1 4.84 8.84 1.05 o 4 5 1 63.78 57.36 1.55 o 5 5 1 24.10 22.65 1.20 o 6 5 1 0.13 0.35 1.27 o 7 5 1 9.09 10.15 1.57 o -6 6 1 52.44 48.79 3.54 o -5 6 1 242.93 268.46 4.89 o -4 6 1 392.76 395.63 4.32 o -3 6 1 74.48 79.62 6.27 o -2 6 1 31.06 33.44 1.58 o -1 6 1 240.73 235.88 2.64 o 0 6 1 28.83 27.56 1.72 o 1 6 1 174.91 165.83 2.96 o 2 6 1 35.81 35.09 1.24 o 3 6 1 58.29 68.71 2.58 o 4 6 1 286.38 277.34 6.22 o 5 6 1 676.27 699.90 7.44 o 6 6 1 3.06 3.96 1.38 o 7 6 1 3.02 6.84 2.81 o -5 7 1 447.17 452.93 8.86 o -4 7 1 67.45 60.87 2.31 o -3 7 1 63.81 58.86 2.11 o -2 7 1 9.68 8.38 1.84 o -1 7 1 956.33 889.54 11.71 o 0 7 1 7.67 7.38 1.85 o 1 7 1 2.64 2.69 1.44 o 2 7 1 233.31 241.01 2.94 o 3 7 1 87.52 91.64 1.57 o 4 7 1 262.17 268.81 3.12 o 5 7 1 38.78 39.51 1.47 o 6 7 1 50.00 66.38 2.34 o -5 8 1 4.33 2.15 2.86 o -4 8 1 61.02 59.75 2.41 o -3 8 1 13.42 15.12 1.91 o -2 8 1 2.12 1.92 1.21 o -1 8 1 0.06 1.11 1.05 o 0 8 1 231.36 217.50 3.84 o 1 8 1 71.01 69.05 1.43 o 2 8 1 1.81 3.29 1.02 o 3 8 1 4.42 6.17 1.10 o 4 8 1 0.30 0.27 1.13 o 5 8 1 0.34 0.83 1.21 o -4 9 1 25.27 25.34 2.42 o -3 9 1 334.86 332.01 4.31 o -2 9 1 154.49 146.22 3.46 o -1 9 1 5.58 4.10 1.15 o 0 9 1 8.85 12.03 1.18 o 1 9 1 569.60 544.19 6.40 o 2 9 1 47.54 43.09 1.41 o 3 9 1 1.72 4.24 1.38 o 4 9 1 27.24 29.86 1.69 o 5 9 1 61.60 68.56 2.67 o -3 10 1 6.81 5.73 1.71 o -2 10 1 3.05 4.53 1.58 o -1 10 1 0.29 1.99 1.19 o 0 10 1 142.09 153.07 3.53 o 1 10 1 78.70 79.39 2.46 o 2 10 1 56.78 49.64 2.03 o 3 10 1 105.22 105.44 2.92 o 4 10 1 164.51 180.07 3.54 o -1 11 1 33.22 29.57 1.83 o 0 11 1 26.99 22.06 2.61 o 1 11 1 14.36 16.08 1.93 o -2 -10 2 87.18 86.04 2.30 o -1 -10 2 4.75 5.51 1.73 o 0 -10 2 26.59 28.11 2.02 o 1 -10 2 5.11 7.25 1.55 o -4 -9 2 3.10 3.84 1.60 o -3 -9 2 0.76 1.49 1.39 o -2 -9 2 72.37 77.96 3.07 o -1 -9 2 88.07 85.09 2.64 o 0 -9 2 0.07 0.36 1.24 o 1 -9 2 195.10 180.83 2.61 o 2 -9 2 69.33 73.77 2.56 o 3 -9 2 21.08 18.78 2.08 o -5 -8 2 72.87 75.84 2.23 o -4 -8 2 282.57 290.80 9.61 o -3 -8 2 0.24 0.42 1.34 o -2 -8 2 4.58 7.12 1.30 o -1 -8 2 657.14 668.64 4.90 o 0 -8 2 63.30 67.33 1.79 o 1 -8 2 82.42 81.44 1.85 o 2 -8 2 6.08 5.24 1.71 o 3 -8 2 110.34 111.35 2.83 o 4 -8 2 1.02 -0.47 1.88 o -6 -7 2 134.45 143.86 3.38 o -5 -7 2 8.26 8.23 1.55 o -4 -7 2 0.00 0.20 1.34 o -3 -7 2 174.26 177.15 2.66 o -2 -7 2 67.76 67.74 1.79 o -1 -7 2 0.20 0.53 1.01 o 0 -7 2 200.92 206.70 2.22 o 1 -7 2 511.74 494.71 6.92 o 2 -7 2 503.95 500.95 14.58 o 3 -7 2 477.54 479.33 4.92 o 4 -7 2 182.03 189.23 3.45 o 5 -7 2 16.09 16.51 2.21 o -6 -6 2 77.27 82.73 2.21 o -5 -6 2 37.22 36.98 1.67 o -4 -6 2 265.26 268.71 2.90 o -3 -6 2 127.29 127.43 2.00 o -2 -6 2 1567.03 1571.85 31.90 o -1 -6 2 65.12 68.84 1.55 o 0 -6 2 315.59 312.85 7.67 o 1 -6 2 254.15 240.71 2.39 o 2 -6 2 73.61 68.14 3.18 o 3 -6 2 834.49 823.29 6.21 o 4 -6 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194.88 203.84 2.43 o -2 -3 2 89.18 91.97 2.48 o -1 -3 2 2494.72 2461.66 11.01 o 0 -3 2 3590.21 3497.13 15.03 o 1 -3 2 571.40 579.17 12.55 o 2 -3 2 62.25 73.07 3.63 o 3 -3 2 2188.69 2269.80 15.74 o 4 -3 2 84.76 75.56 2.16 o 5 -3 2 46.83 52.10 1.77 o 6 -3 2 102.57 100.11 2.31 o 7 -3 2 88.15 82.21 2.96 o -7 -2 2 39.30 42.75 2.48 o -6 -2 2 7.57 5.71 1.36 o -5 -2 2 13.40 16.43 1.07 o -4 -2 2 19.37 17.92 1.28 o -3 -2 2 20.35 22.09 1.11 o -2 -2 2 542.10 545.16 3.58 o -1 -2 2 28.60 41.10 2.24 o 0 -2 2 923.55 872.80 15.73 o 1 -2 2 286.19 332.29 7.87 o 2 -2 2 1179.03 1299.30 67.93 o 3 -2 2 313.67 301.02 4.21 o 4 -2 2 454.82 439.00 3.92 o 5 -2 2 35.17 27.51 1.45 o 6 -2 2 21.83 21.12 1.62 o 7 -2 2 111.66 108.37 4.30 o -7 -1 2 185.54 176.22 4.67 o -6 -1 2 0.00 0.55 1.64 o -5 -1 2 37.58 34.82 1.04 o -4 -1 2 2444.76 2360.33 13.28 o -3 -1 2 1141.57 1084.51 14.60 o -2 -1 2 2300.86 2244.02 33.71 o -1 -1 2 3116.74 3164.22 29.80 o 0 -1 2 1494.65 1494.63 7.36 o 1 -1 2 137.51 168.39 1.39 o 2 -1 2 3315.52 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