#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:00:13 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180939 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/19/2201905.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201905_Fobs loop_ _publ_author_name 'Almeida Paz, Filipe A.' 'Khimyak, Yaroslav Z.' 'Klinowski, Jacek' _publ_section_title ; Bis(4,4'-bipyridine)tetraaquacobalt(II) 2,6-naphathalenedicarboxylate dihydrate ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m8 _journal_page_last m10 _journal_volume 59 _journal_year 2003 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 78.585 _cell_angle_beta 84.015 _cell_angle_gamma 73.740 _cell_length_a 6.9856 _cell_length_b 9.2926 _cell_length_c 12.3538 _exptl_crystal_F_000 361.00 _reflns_d_resolution_high 0.8436 _cod_data_source_file cm6026Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' jk0121 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 121.67 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 638.22 651.60 18.42 o 3 0 0 1052.05 998.49 38.88 o 4 0 0 802.66 863.79 59.27 o 5 0 0 76.89 65.98 21.45 o 6 0 0 10.57 16.42 11.65 o 7 0 0 31.76 45.16 10.33 o -7 1 0 137.00 150.58 31.36 o -6 1 0 7.95 23.59 8.28 o -5 1 0 54.07 50.07 16.20 o -4 1 0 191.11 215.88 8.61 o -3 1 0 2302.25 2446.96 81.61 o -2 1 0 335.05 322.13 9.42 o -1 1 0 129.23 126.80 4.96 o 2 1 0 1214.34 1209.81 33.64 o 3 1 0 485.97 522.29 27.04 o 4 1 0 32.14 30.67 15.14 o 5 1 0 108.20 82.67 9.33 o 6 1 0 106.84 74.41 11.02 o 7 1 0 62.48 61.38 14.86 o 8 1 0 56.90 41.48 16.69 o -7 2 0 63.80 67.70 12.83 o -6 2 0 79.42 77.72 25.32 o -5 2 0 3.17 -0.24 2.57 o -4 2 0 534.88 568.66 16.52 o -3 2 0 0.90 1.22 3.68 o -2 2 0 688.31 632.83 19.23 o -1 2 0 164.87 161.58 5.58 o 0 2 0 14802.71 14782.16 570.34 o 1 2 0 3498.18 3209.11 153.40 o 2 2 0 5692.23 5364.76 156.44 o 3 2 0 3.43 21.91 9.08 o 4 2 0 750.36 755.50 17.04 o 5 2 0 133.85 131.96 11.65 o 6 2 0 117.36 104.17 21.71 o 7 2 0 8.82 2.62 8.52 o 8 2 0 208.49 176.98 18.29 o -7 3 0 8.72 2.72 12.05 o -6 3 0 71.89 86.56 16.27 o -5 3 0 56.64 56.71 5.10 o -4 3 0 86.20 84.32 6.96 o -3 3 0 919.76 1014.50 27.88 o -2 3 0 947.27 961.24 27.22 o -1 3 0 179.21 189.50 9.77 o 0 3 0 3032.83 3085.48 116.46 o 1 3 0 750.82 716.76 33.77 o 2 3 0 45.72 40.57 3.76 o 3 3 0 630.91 695.23 31.69 o 4 3 0 3.98 13.56 3.31 o 5 3 0 144.91 148.57 6.99 o 6 3 0 73.64 60.12 7.98 o 7 3 0 83.30 91.83 23.40 o 8 3 0 105.82 124.28 16.95 o -6 4 0 354.97 333.93 39.19 o -5 4 0 49.53 48.48 7.05 o -4 4 0 104.75 105.29 9.82 o -3 4 0 125.06 110.88 6.81 o -2 4 0 168.67 177.71 13.21 o -1 4 0 2006.17 1986.70 64.58 o 0 4 0 3687.94 3763.41 108.69 o 1 4 0 468.16 457.32 35.00 o 2 4 0 1188.37 1151.86 37.14 o 3 4 0 25.45 25.36 3.67 o 4 4 0 1121.80 1134.61 33.73 o 5 4 0 46.14 49.61 4.40 o 6 4 0 251.18 275.64 12.35 o 7 4 0 164.63 167.32 18.04 o 8 4 0 134.16 142.26 16.12 o -5 5 0 210.97 197.56 18.95 o -4 5 0 0.94 -0.18 5.31 o -3 5 0 475.35 479.22 22.55 o -2 5 0 581.14 628.31 24.74 o -1 5 0 15.14 19.80 3.91 o 0 5 0 803.91 839.27 40.27 o 1 5 0 997.50 975.94 55.08 o 2 5 0 815.55 827.27 46.87 o 3 5 0 345.30 336.29 35.54 o 4 5 0 125.16 135.45 14.15 o 5 5 0 130.36 130.14 8.60 o 6 5 0 21.69 18.47 4.85 o 7 5 0 70.90 77.32 13.52 o 8 5 0 0.29 4.72 17.36 o -5 6 0 150.03 155.07 24.99 o -4 6 0 5.48 18.75 5.72 o -3 6 0 17.41 30.51 5.18 o -2 6 0 19.52 21.20 5.03 o -1 6 0 12.53 18.66 4.10 o 0 6 0 2630.43 2649.24 135.20 o 1 6 0 111.02 102.38 11.12 o 2 6 0 74.97 82.48 7.89 o 3 6 0 116.64 131.03 7.06 o 4 6 0 56.12 61.22 6.54 o 5 6 0 77.36 83.96 8.71 o 6 6 0 63.97 61.35 9.74 o 7 6 0 2.03 11.22 14.97 o -4 7 0 1.07 -15.41 15.94 o -3 7 0 107.00 90.32 10.24 o -2 7 0 3.62 -2.26 6.00 o -1 7 0 574.77 503.43 24.41 o 0 7 0 54.79 49.71 7.63 o 1 7 0 803.84 832.14 61.79 o 2 7 0 316.80 337.49 28.84 o 3 7 0 60.38 63.69 7.26 o 4 7 0 27.11 30.37 7.11 o 5 7 0 356.34 385.94 27.09 o 6 7 0 2.44 6.06 7.98 o 7 7 0 1.56 4.81 15.02 o -3 8 0 14.22 16.47 17.52 o -2 8 0 41.06 46.36 16.51 o -1 8 0 52.57 43.24 16.47 o 0 8 0 1111.37 1188.18 58.89 o 1 8 0 1434.96 1378.74 150.76 o 2 8 0 44.73 44.93 21.21 o 3 8 0 36.63 44.62 10.52 o 4 8 0 241.62 256.31 32.04 o 5 8 0 84.20 73.03 10.87 o 6 8 0 163.45 170.59 21.65 o -2 9 0 107.35 133.07 20.27 o -1 9 0 53.36 27.73 16.56 o 0 9 0 0.47 -15.50 28.89 o 1 9 0 1224.35 1298.06 124.36 o 2 9 0 159.27 195.61 24.75 o 3 9 0 43.49 40.83 19.35 o 4 9 0 42.98 33.70 15.50 o 5 9 0 78.20 74.27 10.78 o 6 9 0 15.42 7.64 8.18 o 0 10 0 382.40 343.70 41.74 o 1 10 0 169.81 125.13 33.70 o 2 10 0 62.31 116.65 17.67 o 3 10 0 11.56 0.53 25.13 o 4 10 0 27.82 36.20 15.98 o -4 -10 1 4.28 20.61 20.08 o -3 -10 1 0.94 21.23 13.82 o -2 -10 1 75.08 94.60 17.57 o -1 -10 1 1.21 20.75 16.99 o 0 -10 1 42.81 38.80 18.63 o -5 -9 1 80.01 171.26 443.58 o -4 -9 1 1.01 4.42 13.55 o -3 -9 1 49.50 43.05 7.63 o -2 -9 1 129.84 164.85 22.44 o -1 -9 1 61.28 97.06 19.74 o 0 -9 1 277.86 339.90 33.70 o 1 -9 1 682.32 627.99 60.37 o 2 -9 1 106.65 93.11 21.81 o -6 -8 1 117.51 120.70 28.00 o -5 -8 1 28.90 16.58 6.66 o -4 -8 1 187.28 164.23 12.58 o -3 -8 1 104.44 104.87 18.68 o -2 -8 1 157.08 154.49 57.00 o -1 -8 1 10.46 8.57 10.69 o 0 -8 1 75.72 92.83 7.83 o 1 -8 1 387.41 395.70 36.93 o 2 -8 1 63.51 68.17 19.16 o 3 -8 1 20.50 46.84 13.87 o -7 -7 1 173.96 89.11 23.64 o -6 -7 1 24.17 20.92 5.83 o -5 -7 1 4.50 6.13 5.83 o -4 -7 1 2.43 9.10 6.96 o -3 -7 1 97.70 106.33 13.67 o -2 -7 1 359.93 364.80 40.30 o -1 -7 1 40.63 32.53 6.42 o 0 -7 1 12.02 10.16 4.91 o 1 -7 1 2932.90 3034.34 135.99 o 2 -7 1 109.50 95.24 14.61 o 3 -7 1 261.51 53.15 33.94 o 4 -7 1 3.54 11.75 14.92 o -7 -6 1 15.75 9.10 8.57 o -6 -6 1 50.11 51.32 5.90 o -5 -6 1 53.86 43.49 8.17 o -4 -6 1 2.85 8.10 3.36 o -3 -6 1 312.81 337.89 17.88 o -2 -6 1 145.31 135.96 10.69 o -1 -6 1 0.64 7.10 8.06 o 0 -6 1 46.85 50.78 7.76 o 1 -6 1 245.57 232.01 10.77 o 2 -6 1 540.49 536.80 22.60 o 3 -6 1 103.38 84.28 10.45 o 4 -6 1 63.92 61.06 11.08 o 5 -6 1 118.06 124.89 19.26 o -7 -5 1 69.84 92.47 20.03 o -6 -5 1 82.37 96.07 12.25 o -5 -5 1 48.80 37.35 4.95 o -4 -5 1 10.59 12.02 4.02 o -3 -5 1 525.01 555.41 19.33 o -2 -5 1 527.02 470.89 26.91 o -1 -5 1 1367.35 1314.03 45.13 o 0 -5 1 129.81 120.82 9.14 o 1 -5 1 2512.22 2593.33 75.03 o 2 -5 1 1535.76 1542.63 68.22 o 3 -5 1 367.04 377.05 20.86 o 4 -5 1 34.97 25.39 6.07 o 5 -5 1 366.03 361.02 30.45 o -8 -4 1 48.70 43.59 18.73 o -7 -4 1 179.48 189.25 16.54 o -6 -4 1 31.90 40.24 7.45 o -5 -4 1 268.21 281.03 12.37 o -4 -4 1 864.81 857.02 25.27 o -3 -4 1 60.39 66.71 4.64 o -2 -4 1 1191.65 1129.16 37.44 o -1 -4 1 1152.75 1108.30 35.74 o 0 -4 1 318.41 304.84 16.67 o 1 -4 1 0.74 82.57 12.70 o 2 -4 1 693.25 703.74 24.99 o 3 -4 1 164.65 161.63 7.64 o 4 -4 1 101.75 101.21 9.71 o 5 -4 1 126.60 126.11 16.18 o 6 -4 1 68.65 72.22 12.57 o -8 -3 1 178.42 217.39 41.91 o -7 -3 1 145.42 169.36 15.68 o -6 -3 1 95.03 80.00 12.50 o -5 -3 1 622.29 659.35 28.49 o -4 -3 1 173.35 182.46 7.94 o -3 -3 1 104.70 108.84 6.85 o -2 -3 1 617.31 570.75 17.22 o -1 -3 1 953.20 873.42 44.14 o 0 -3 1 1673.31 1530.66 67.06 o 1 -3 1 402.11 416.03 16.39 o 2 -3 1 103.71 108.57 4.46 o 3 -3 1 51.99 43.14 5.72 o 4 -3 1 253.81 264.45 18.56 o 5 -3 1 206.64 230.83 14.71 o 6 -3 1 17.41 24.22 8.95 o -8 -2 1 3.47 17.17 15.18 o -7 -2 1 89.76 92.83 12.82 o -6 -2 1 68.30 79.99 21.42 o -5 -2 1 2.26 3.59 1.56 o -4 -2 1 1182.74 1203.14 41.64 o -3 -2 1 301.45 330.19 9.87 o -2 -2 1 1166.50 1122.86 27.89 o -1 -2 1 1342.34 1249.94 44.54 o 0 -2 1 60.93 64.85 5.49 o 1 -2 1 3021.40 3022.85 96.67 o 2 -2 1 206.24 187.28 8.24 o 3 -2 1 964.20 983.90 28.12 o 4 -2 1 567.07 606.25 24.23 o 5 -2 1 43.12 44.81 4.04 o 6 -2 1 60.97 61.64 10.01 o 7 -2 1 34.23 26.25 13.29 o -8 -1 1 30.00 22.08 14.61 o -7 -1 1 147.59 162.54 25.40 o -6 -1 1 120.17 156.08 16.14 o -5 -1 1 17.00 28.59 7.45 o -4 -1 1 384.30 389.34 13.02 o -3 -1 1 38.15 36.12 2.56 o -2 -1 1 2.79 7.08 1.92 o -1 -1 1 902.28 300.29 232.68 o 1 -1 1 7200.65 6880.16 211.99 o 2 -1 1 147.98 180.19 8.55 o 3 -1 1 379.50 349.08 12.35 o 4 -1 1 304.86 292.06 14.95 o 5 -1 1 93.27 93.98 16.47 o 6 -1 1 209.68 231.49 16.97 o 7 -1 1 75.97 78.66 15.41 o -7 0 1 111.07 101.95 10.43 o -6 0 1 273.68 296.22 20.43 o -5 0 1 74.10 66.81 8.99 o -4 0 1 143.89 140.98 7.27 o -3 0 1 636.04 614.27 16.35 o -2 0 1 36.50 39.85 2.09 o -1 0 1 1277.02 50.88 72.15 o 2 0 1 7514.62 7461.36 201.35 o 3 0 1 4000.78 3908.96 110.56 o 4 0 1 856.93 923.83 38.41 o 5 0 1 112.78 88.74 11.58 o 6 0 1 191.01 190.70 18.10 o 7 0 1 37.98 34.61 15.60 o -7 1 1 129.26 141.90 16.29 o -6 1 1 686.57 758.50 61.74 o -5 1 1 0.96 1.42 3.64 o -4 1 1 0.65 3.59 2.45 o -3 1 1 1726.33 1814.23 76.42 o -2 1 1 161.11 158.23 6.25 o -1 1 1 1136.77 1073.38 33.19 o 2 1 1 14198.75 13315.95 608.40 o 3 1 1 155.91 199.34 43.55 o 4 1 1 62.11 88.20 6.90 o 5 1 1 191.94 201.99 13.77 o 6 1 1 5.66 -7.94 8.64 o 7 1 1 61.15 46.90 26.46 o 8 1 1 36.99 24.10 14.93 o -7 2 1 154.22 161.14 20.44 o -6 2 1 108.86 90.49 12.40 o -5 2 1 35.40 32.90 4.46 o -4 2 1 6.29 7.10 3.51 o -3 2 1 43.00 39.70 3.77 o -2 2 1 306.84 293.72 8.95 o -1 2 1 60.99 64.47 4.29 o 0 2 1 640.33 631.82 29.84 o 1 2 1 93.22 334.33 38.07 o 2 2 1 7823.04 7728.92 211.36 o 3 2 1 1856.26 1969.87 59.34 o 4 2 1 63.23 59.44 4.36 o 5 2 1 2.72 9.94 5.31 o 6 2 1 68.78 78.22 10.28 o 7 2 1 44.48 32.42 9.38 o 8 2 1 2.98 19.23 27.42 o -7 3 1 31.74 29.52 13.87 o -6 3 1 112.93 119.87 10.96 o -5 3 1 16.02 11.41 11.57 o -4 3 1 85.83 87.27 7.22 o -3 3 1 386.55 367.95 16.87 o -2 3 1 897.54 931.84 32.60 o -1 3 1 233.00 253.09 10.00 o 0 3 1 4410.64 4171.88 168.91 o 1 3 1 2684.16 2661.25 143.54 o 2 3 1 1258.18 1281.37 36.28 o 3 3 1 228.66 196.59 5.76 o 4 3 1 906.84 972.23 27.59 o 5 3 1 251.81 263.98 21.10 o 6 3 1 121.30 127.94 13.67 o 7 3 1 6.70 -11.38 17.89 o 8 3 1 27.82 55.54 18.99 o -5 4 1 43.75 33.29 5.46 o -4 4 1 73.06 79.02 6.18 o -3 4 1 237.76 235.77 16.94 o -2 4 1 183.97 183.42 17.24 o -1 4 1 960.69 976.49 28.98 o 0 4 1 134.15 131.53 11.17 o 1 4 1 257.73 233.19 12.11 o 2 4 1 1632.56 1639.36 43.28 o 3 4 1 1651.81 1730.37 48.57 o 4 4 1 106.74 99.76 7.90 o 5 4 1 233.08 221.02 9.53 o 6 4 1 107.90 101.28 6.11 o 7 4 1 56.73 60.93 10.24 o 8 4 1 145.82 133.49 17.71 o -5 5 1 42.67 28.71 6.87 o -4 5 1 319.14 329.87 18.44 o -3 5 1 278.00 287.67 11.91 o -2 5 1 652.72 630.92 33.68 o -1 5 1 140.36 129.15 7.19 o 0 5 1 1125.44 1124.56 39.79 o 1 5 1 3230.37 3196.46 118.06 o 2 5 1 9.02 10.42 7.30 o 3 5 1 131.47 148.66 7.86 o 4 5 1 244.35 226.64 12.22 o 5 5 1 74.76 75.05 8.31 o 6 5 1 105.40 97.02 7.01 o 7 5 1 3.14 -3.96 8.46 o 8 5 1 16.55 42.63 21.35 o -5 6 1 179.67 152.91 25.42 o -4 6 1 49.21 47.73 6.59 o -3 6 1 148.69 141.66 16.39 o -2 6 1 44.04 40.31 4.95 o -1 6 1 100.23 100.12 6.27 o 0 6 1 71.92 76.71 6.64 o 1 6 1 3.85 59.23 14.64 o 2 6 1 201.02 185.13 10.10 o 3 6 1 388.43 388.40 16.91 o 4 6 1 78.88 76.76 6.06 o 5 6 1 125.45 129.62 16.37 o 6 6 1 57.92 56.10 6.40 o 7 6 1 0.54 -20.85 20.85 o -4 7 1 15.35 10.06 15.36 o -3 7 1 101.77 89.14 8.72 o -2 7 1 0.49 3.79 6.80 o -1 7 1 18.19 15.45 6.71 o 0 7 1 179.54 152.83 10.95 o 1 7 1 27.50 40.01 7.91 o 2 7 1 230.78 212.02 15.82 o 3 7 1 62.72 66.26 7.88 o 4 7 1 77.97 92.83 15.24 o 5 7 1 241.20 258.08 25.59 o 6 7 1 28.69 30.34 13.19 o 7 7 1 10.72 21.38 12.81 o -3 8 1 0.32 -11.17 11.17 o -2 8 1 22.51 19.61 11.82 o -1 8 1 138.97 150.73 15.60 o 0 8 1 154.82 134.80 20.51 o 1 8 1 58.41 92.01 20.12 o 2 8 1 948.73 875.16 78.28 o 3 8 1 1104.19 1147.41 90.05 o 4 8 1 105.05 84.93 11.98 o 5 8 1 135.49 133.47 30.55 o 6 8 1 150.27 138.55 15.02 o 7 8 1 112.94 119.78 25.13 o -2 9 1 98.95 120.94 25.61 o -1 9 1 35.03 28.89 18.73 o 0 9 1 442.18 472.15 50.60 o 1 9 1 0.80 35.05 15.12 o 2 9 1 185.38 173.03 21.66 o 3 9 1 642.09 715.76 57.00 o 4 9 1 10.58 17.28 18.34 o 5 9 1 12.78 0.00 15.50 o 6 9 1 113.19 143.91 16.01 o -1 10 1 87.60 109.43 24.02 o 0 10 1 11.83 26.24 28.36 o 1 10 1 54.01 40.83 24.70 o 2 10 1 366.94 348.18 43.14 o 3 10 1 1249.07 1365.41 113.91 o 4 10 1 0.39 10.21 20.41 o 5 10 1 1.87 1.06 22.92 o -4 -10 2 18.77 19.93 19.93 o -3 -10 2 36.56 113.67 28.98 o -2 -10 2 2.77 -17.96 20.56 o -1 -10 2 17.60 21.66 14.78 o -5 -9 2 170.32 213.71 23.64 o -4 -9 2 9.91 -1.06 17.38 o -3 -9 2 181.88 188.58 30.67 o -2 -9 2 76.66 59.84 14.30 o -1 -9 2 0.40 8.47 18.01 o 0 -9 2 183.25 170.77 29.75 o 1 -9 2 111.81 67.93 14.88 o 2 -9 2 52.10 59.55 22.87 o -6 -8 2 4.45 10.09 9.00 o -5 -8 2 22.37 31.31 9.64 o -4 -8 2 87.48 63.16 14.61 o -3 -8 2 190.79 198.24 33.53 o -2 -8 2 7.08 9.46 5.80 o -1 -8 2 32.66 55.85 19.69 o 0 -8 2 142.04 118.05 23.40 o 1 -8 2 144.47 146.26 17.09 o 2 -8 2 88.93 70.82 17.04 o 3 -8 2 2.52 15.45 18.15 o -7 -7 2 35.39 29.03 12.90 o -6 -7 2 245.10 219.45 29.20 o -5 -7 2 370.97 346.78 19.47 o -4 -7 2 13.68 19.60 5.48 o -3 -7 2 9.01 -1.58 11.25 o -2 -7 2 438.14 466.06 21.73 o -1 -7 2 43.48 36.22 3.41 o 0 -7 2 27.98 27.11 19.64 o 1 -7 2 195.63 197.34 13.77 o 2 -7 2 70.82 73.81 12.97 o 3 -7 2 280.61 219.01 35.34 o 4 -7 2 111.63 92.05 16.08 o -7 -6 2 55.71 45.06 16.08 o -6 -6 2 29.20 9.48 7.07 o -5 -6 2 140.61 147.06 11.78 o -4 -6 2 2.52 -3.06 3.76 o -3 -6 2 51.98 56.65 4.93 o -2 -6 2 24.86 25.14 7.15 o -1 -6 2 123.87 135.89 5.83 o 0 -6 2 85.15 82.78 13.97 o 1 -6 2 95.53 96.04 16.22 o 2 -6 2 80.72 77.37 11.89 o 3 -6 2 627.81 652.43 41.94 o 4 -6 2 3.44 5.27 7.59 o 5 -6 2 0.63 -9.10 14.49 o -7 -5 2 21.69 26.77 16.61 o -6 -5 2 555.75 614.10 212.72 o -5 -5 2 248.32 245.85 11.62 o -4 -5 2 112.55 111.78 6.09 o -3 -5 2 104.81 107.47 6.84 o -2 -5 2 495.55 470.34 20.43 o -1 -5 2 811.05 867.41 26.25 o 0 -5 2 151.39 157.01 10.45 o 1 -5 2 402.76 397.07 19.34 o 2 -5 2 893.16 887.73 41.10 o 3 -5 2 954.17 1004.98 65.58 o 4 -5 2 562.55 572.94 34.98 o 5 -5 2 22.69 18.70 9.41 o -7 -4 2 286.23 267.89 21.98 o -6 -4 2 6.20 16.78 7.24 o -5 -4 2 517.41 567.66 25.11 o -4 -4 2 441.47 466.07 16.82 o -3 -4 2 58.82 61.96 5.34 o -2 -4 2 308.94 279.52 10.41 o -1 -4 2 4397.29 4471.06 128.65 o 0 -4 2 114.55 119.20 14.40 o 1 -4 2 827.47 827.32 25.97 o 2 -4 2 226.49 232.39 21.69 o 3 -4 2 631.21 617.91 29.47 o 4 -4 2 172.38 172.62 10.47 o 5 -4 2 174.85 177.78 10.70 o 6 -4 2 3.37 -8.38 10.50 o -8 -3 2 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