#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/19/2201907.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201907_Fobs loop_ _publ_author_name 'Yan, Ying' 'Wu, Chuan-De' 'Liu, Jiu-Hui' 'Zhang, Quan-Zheng' 'Lu, Can-Zhong' _publ_section_title ; Tetrakis[4-amino-N-(2-hydroxyethyl)pyridinium] hexacosaoxooctamolybdate ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m102 _journal_page_last m104 _journal_volume 59 _journal_year 2003 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 111.146 _cell_angle_gamma 90.000 _cell_length_a 12.6568 _cell_length_b 13.8165 _cell_length_c 14.8916 _exptl_crystal_F_000 1688.00 _reflns_d_resolution_high 0.8371 _[local]_cod_data_source_file cm6029Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' CM6029 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 522.08 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2633.83 2532.54 71.15 o 3 0 0 42711.39 40613.48 1026.57 o 4 0 0 58285.86 49479.51 1251.84 o 5 0 0 42578.32 38755.72 986.85 o 6 0 0 4584.06 5142.72 150.34 o 7 0 0 211.10 154.52 35.33 o 8 0 0 13225.24 13972.91 378.88 o 9 0 0 13158.24 14062.65 384.79 o 10 0 0 337.59 343.09 56.19 o 11 0 0 3888.39 4205.36 149.45 o 12 0 0 165.13 157.92 55.76 o 13 0 0 63.40 142.17 53.21 o 14 0 0 227.52 129.83 56.19 o 1 1 0 1657.09 1626.76 30.99 o 2 1 0 52.75 72.55 12.13 o 3 1 0 223.98 250.89 13.09 o 4 1 0 3714.23 3222.67 67.42 o 5 1 0 245.05 182.65 31.50 o 6 1 0 479.98 527.55 76.41 o 7 1 0 28.77 25.68 18.81 o 8 1 0 1427.67 1505.99 50.40 o 9 1 0 3679.70 3601.89 87.91 o 10 1 0 219.25 192.22 31.79 o 11 1 0 4507.51 4852.30 117.11 o 12 1 0 0.59 -24.72 24.72 o 13 1 0 550.89 540.86 48.38 o 14 1 0 514.02 572.25 51.30 o 0 2 0 60430.65 61175.16 1084.28 o 1 2 0 14576.17 14389.53 209.76 o 2 2 0 718.35 705.85 34.91 o 3 2 0 174.84 296.15 12.97 o 4 2 0 5804.72 5768.93 111.60 o 5 2 0 1557.53 1717.75 43.83 o 6 2 0 52.44 87.99 18.46 o 7 2 0 933.31 720.13 56.62 o 8 2 0 444.15 525.00 55.98 o 9 2 0 784.38 853.92 57.47 o 10 2 0 120.93 88.08 28.78 o 11 2 0 1206.79 1177.19 60.24 o 12 2 0 2309.31 2405.92 77.12 o 13 2 0 14.15 104.29 58.32 o 1 3 0 5635.11 5986.19 91.60 o 2 3 0 4306.55 4570.67 69.70 o 3 3 0 7371.69 7455.52 138.75 o 4 3 0 32397.12 30538.63 549.63 o 5 3 0 9069.37 9381.50 377.58 o 6 3 0 815.91 829.25 31.08 o 7 3 0 819.45 889.71 36.00 o 8 3 0 14099.26 15236.96 473.93 o 9 3 0 2729.94 2518.88 159.66 o 10 3 0 2237.71 2249.53 68.72 o 11 3 0 1702.97 2010.21 151.34 o 12 3 0 330.84 531.50 83.64 o 13 3 0 944.29 1133.26 81.09 o 0 4 0 272563.50 258178.53 4570.18 o 1 4 0 58346.82 58656.25 850.51 o 2 4 0 18.28 38.94 6.08 o 3 4 0 24400.72 24854.80 868.77 o 4 4 0 133375.59 134839.06 3153.40 o 5 4 0 50267.25 52960.87 2531.92 o 6 4 0 168.29 201.78 25.11 o 7 4 0 581.58 530.27 28.96 o 8 4 0 11033.59 11688.55 416.90 o 9 4 0 1028.48 1073.52 48.53 o 10 4 0 2225.90 2171.95 67.27 o 11 4 0 628.38 589.89 43.87 o 12 4 0 632.35 631.25 73.22 o 13 4 0 448.42 631.68 126.00 o 1 5 0 1883.49 1342.61 37.24 o 2 5 0 2390.93 2772.44 45.25 o 3 5 0 29718.72 31059.35 1325.92 o 4 5 0 16558.76 17543.35 320.31 o 5 5 0 10.28 -3.41 49.38 o 6 5 0 134.20 172.54 21.18 o 7 5 0 11600.33 11642.34 223.90 o 8 5 0 6833.48 7102.16 194.42 o 9 5 0 965.41 942.07 43.84 o 10 5 0 32.02 61.37 27.63 o 11 5 0 3516.60 3598.76 99.03 o 12 5 0 1565.80 1577.52 70.24 o 13 5 0 14.74 -57.72 110.03 o 0 6 0 37340.11 37385.30 668.72 o 1 6 0 10561.85 10713.11 172.84 o 2 6 0 121.58 124.56 8.42 o 3 6 0 2185.13 2188.68 57.96 o 4 6 0 11316.93 12432.34 616.30 o 5 6 0 22109.24 23710.60 530.95 o 6 6 0 212.80 381.56 126.00 o 7 6 0 6998.71 7224.99 206.78 o 8 6 0 264.12 319.94 31.60 o 9 6 0 685.20 685.16 42.03 o 10 6 0 41.14 57.46 31.50 o 11 6 0 4462.56 4658.89 184.79 o 12 6 0 4454.09 4876.41 454.30 o 13 6 0 260.19 193.25 63.42 o 1 7 0 640.30 695.94 16.72 o 2 7 0 97.13 116.30 31.58 o 3 7 0 1507.39 1576.81 27.93 o 4 7 0 7781.17 7748.18 148.59 o 5 7 0 3454.42 3430.34 90.69 o 6 7 0 68.50 86.66 22.03 o 7 7 0 71.91 32.68 35.54 o 8 7 0 3300.96 3634.99 278.66 o 9 7 0 1359.43 1311.94 54.72 o 10 7 0 474.55 582.74 71.09 o 11 7 0 1348.55 1321.58 63.04 o 12 7 0 3.32 -51.08 51.08 o 0 8 0 20010.82 21331.95 387.77 o 1 8 0 4109.57 4076.78 59.07 o 2 8 0 1153.41 1212.51 46.02 o 3 8 0 12191.22 12172.98 271.61 o 4 8 0 26908.80 27069.13 402.64 o 5 8 0 3235.28 3256.75 159.46 o 6 8 0 11.17 83.78 45.97 o 7 8 0 3964.46 4521.41 216.73 o 8 8 0 5978.49 5685.86 184.82 o 9 8 0 884.87 889.78 52.54 o 10 8 0 462.78 448.43 51.08 o 11 8 0 990.07 884.37 178.57 o 12 8 0 4054.61 4324.42 182.22 o 1 9 0 12358.76 13210.53 246.78 o 2 9 0 553.12 539.27 30.91 o 3 9 0 30722.75 31554.39 468.04 o 4 9 0 15223.17 16083.05 246.02 o 5 9 0 87.84 59.14 30.22 o 6 9 0 6.48 14.98 56.61 o 7 9 0 18453.90 18837.34 520.01 o 8 9 0 14239.91 14927.42 294.63 o 9 9 0 510.49 646.84 214.75 o 10 9 0 0.18 63.98 118.76 o 11 9 0 1540.84 1654.80 109.62 o 0 10 0 11625.38 11811.09 412.46 o 1 10 0 8326.09 8787.77 139.86 o 2 10 0 2373.47 2532.02 51.15 o 3 10 0 477.65 498.91 41.43 o 4 10 0 855.84 923.06 64.56 o 5 10 0 2912.18 2989.24 77.50 o 6 10 0 263.56 266.36 32.73 o 7 10 0 1309.90 1208.05 57.04 o 8 10 0 209.08 144.77 92.16 o 9 10 0 151.77 105.48 38.68 o 10 10 0 1.54 -8.80 108.12 o 11 10 0 1637.81 1672.12 133.46 o 1 11 0 458.03 452.20 61.30 o 2 11 0 262.36 270.62 50.23 o 3 11 0 2490.85 2552.73 54.73 o 4 11 0 818.37 815.68 32.68 o 5 11 0 782.36 773.71 50.44 o 6 11 0 66.57 214.11 36.18 o 7 11 0 1199.72 1131.13 109.19 o 8 11 0 782.40 724.44 156.65 o 9 11 0 44.79 48.54 54.27 o 10 11 0 249.78 253.00 56.84 o 0 12 0 189.47 262.63 42.14 o 1 12 0 173.45 104.07 34.69 o 2 12 0 311.66 382.08 40.65 o 3 12 0 1737.24 1884.40 60.76 o 4 12 0 1635.82 1437.18 84.29 o 5 12 0 4.48 27.67 46.40 o 6 12 0 142.54 99.60 51.51 o 7 12 0 4368.73 4612.89 180.74 o 8 12 0 5817.88 5618.92 324.04 o 9 12 0 945.71 883.67 68.97 o 1 13 0 5238.05 5630.63 126.93 o 2 13 0 854.51 885.66 59.38 o 3 13 0 12858.94 13213.54 259.37 o 4 13 0 7559.02 7908.40 246.58 o 5 13 0 0.35 98.33 52.36 o 6 13 0 28.28 80.88 57.89 o 7 13 0 8089.41 7972.20 254.67 o 8 13 0 7199.75 7592.66 254.65 o 0 14 0 119.17 123.44 53.63 o 1 14 0 558.83 736.99 106.84 o 2 14 0 1536.26 1569.13 122.60 o 3 14 0 114.69 -38.74 38.74 o 4 14 0 52.63 -8.09 50.23 o 5 14 0 504.27 432.48 68.11 o 6 14 0 1192.51 1159.15 100.04 o 7 14 0 87.75 29.80 72.79 o 1 15 0 1162.42 1198.74 60.05 o 2 15 0 0.39 17.28 66.83 o 3 15 0 3223.45 3133.45 135.81 o 4 15 0 2388.16 2495.56 126.44 o 5 15 0 9.31 23.84 66.83 o 0 16 0 736.67 826.66 84.28 o 1 16 0 304.50 213.37 47.37 o 2 16 0 168.69 -48.10 51.08 o 3 16 0 334.43 194.53 63.00 o -14 1 1 2.34 -33.04 51.72 o -13 1 1 11.70 -29.78 34.72 o -12 1 1 4726.42 5292.79 129.31 o -11 1 1 9649.59 10338.06 212.49 o -10 1 1 1288.09 1368.26 54.03 o -9 1 1 1296.57 1456.29 70.03 o -8 1 1 1318.50 1275.90 46.08 o -7 1 1 17286.20 17969.93 335.36 o -6 1 1 680.90 835.43 31.13 o -5 1 1 20859.16 19497.21 826.26 o -4 1 1 28425.98 29013.56 880.71 o -3 1 1 14057.20 14433.42 896.37 o -2 1 1 3710.80 4038.03 97.82 o -1 1 1 91610.52 96930.18 1715.46 o 0 1 1 123933.89 120258.11 1737.66 o 1 1 1 10815.17 10015.96 274.90 o 2 1 1 50.54 722.26 599.55 o 3 1 1 203072.31 178328.38 4183.93 o 4 1 1 54089.02 44850.38 803.59 o 5 1 1 416.66 596.26 26.30 o 6 1 1 118.30 149.32 26.60 o 7 1 1 3569.56 3451.95 80.22 o 8 1 1 8623.38 9026.92 225.77 o 9 1 1 3292.30 3406.18 86.91 o 10 1 1 66.82 54.06 24.08 o 11 1 1 268.49 181.36 34.04 o 12 1 1 276.78 338.85 38.35 o 13 1 1 168.66 219.76 39.39 o -14 2 1 2.79 -15.12 106.41 o -13 2 1 62.12 -8.71 51.93 o -12 2 1 2648.77 2568.44 80.71 o -11 2 1 9076.60 9655.70 198.89 o -10 2 1 578.11 626.20 41.68 o -9 2 1 2553.71 2593.45 70.28 o -8 2 1 14.18 -1.31 37.25 o -7 2 1 6996.30 6708.09 145.04 o -6 2 1 523.24 546.21 26.33 o -5 2 1 1730.05 1704.15 93.24 o -4 2 1 2442.30 2323.92 103.05 o -3 2 1 408.76 312.78 12.63 o -2 2 1 4213.89 4055.75 173.88 o -1 2 1 98.46 147.52 7.52 o 0 2 1 19178.73 19650.62 732.99 o 1 2 1 4824.98 4698.98 315.57 o 2 2 1 3296.99 3380.02 64.23 o 3 2 1 44218.81 43770.50 782.39 o 4 2 1 11528.61 9627.23 456.06 o 5 2 1 2143.99 1859.61 58.76 o 6 2 1 0.09 0.13 15.83 o 7 2 1 9760.92 9147.79 272.68 o 8 2 1 36029.50 37344.14 681.41 o 9 2 1 11254.72 11293.91 223.79 o 10 2 1 162.62 83.91 55.97 o 11 2 1 319.95 329.13 62.79 o 12 2 1 6058.53 6793.47 155.63 o 13 2 1 2550.05 2788.72 88.20 o -14 3 1 246.65 178.16 43.75 o -13 3 1 0.08 -74.32 94.92 o -12 3 1 60.20 69.53 88.32 o -11 3 1 4391.57 4317.33 106.80 o -10 3 1 454.64 444.34 81.73 o -9 3 1 2828.45 2790.80 75.52 o -8 3 1 0.44 -40.43 49.80 o -7 3 1 5998.37 5922.06 121.62 o -6 3 1 2184.98 2130.71 52.80 o -5 3 1 12828.59 11679.48 541.53 o -4 3 1 6553.96 6576.66 124.67 o -3 3 1 6425.83 6505.17 120.91 o -2 3 1 32.17 144.60 46.61 o -1 3 1 54581.45 55258.40 1264.69 o 0 3 1 55782.78 54748.69 1248.86 o 1 3 1 460.99 572.68 31.09 o 2 3 1 278.57 328.39 22.79 o 3 3 1 27992.31 25427.03 457.98 o 4 3 1 25097.57 24016.98 575.02 o 5 3 1 176.56 196.36 17.48 o 6 3 1 2405.42 2714.55 98.14 o 7 3 1 8292.05 8251.68 255.60 o 8 3 1 6455.11 6763.07 165.03 o 9 3 1 83.23 107.17 24.52 o 10 3 1 258.10 257.91 48.74 o 11 3 1 2084.88 2241.33 73.14 o 12 3 1 671.14 720.75 52.04 o 13 3 1 0.59 29.57 39.80 o -13 4 1 68.76 -33.09 33.09 o -12 4 1 219.69 141.11 38.10 o -11 4 1 194.48 154.36 33.27 o -10 4 1 1578.44 1639.33 58.18 o -9 4 1 1922.79 1758.84 55.77 o -8 4 1 11726.15 11795.72 228.67 o -7 4 1 19.04 -4.88 17.03 o -6 4 1 2425.29 2578.63 74.08 o -5 4 1 7727.66 8729.14 165.48 o -4 4 1 16403.98 14503.19 301.01 o -3 4 1 3503.78 2986.80 58.94 o -2 4 1 1201.18 1169.27 21.27 o -1 4 1 2824.14 2846.82 44.96 o 0 4 1 11198.67 10773.78 159.59 o 1 4 1 7792.87 7886.20 102.74 o 2 4 1 3.30 21.20 6.14 o 3 4 1 22518.41 23842.79 701.15 o 4 4 1 26302.49 24968.50 591.60 o 5 4 1 15.78 69.73 41.71 o 6 4 1 2605.08 2777.11 156.47 o 7 4 1 11801.99 11978.09 612.34 o 8 4 1 4461.72 4818.70 108.01 o 9 4 1 0.75 17.80 22.34 o 10 4 1 301.27 246.68 32.81 o 11 4 1 1257.34 1165.16 56.52 o 12 4 1 1602.68 1849.74 82.59 o 13 4 1 279.27 312.22 78.96 o -13 5 1 880.02 930.93 57.45 o -12 5 1 7101.68 8024.17 337.70 o -11 5 1 10862.12 11775.24 240.02 o -10 5 1 736.85 783.41 119.19 o -9 5 1 664.11 653.67 47.46 o -8 5 1 1341.06 1314.18 45.26 o -7 5 1 26973.38 26601.73 487.00 o -6 5 1 1104.48 1339.35 59.81 o -5 5 1 52252.71 53612.50 958.65 o -4 5 1 21302.27 21491.35 388.59 o -3 5 1 3171.57 3241.82 91.35 o -2 5 1 204.39 572.65 421.82 o -1 5 1 52078.73 50182.54 729.01 o 0 5 1 23358.28 22122.15 338.54 o 1 5 1 1179.85 791.19 25.95 o 2 5 1 3343.14 3843.06 53.96 o 3 5 1 67215.44 67871.82 854.88 o 4 5 1 105561.71 102712.16 1492.89 o 5 5 1 18950.36 19121.62 352.12 o 6 5 1 578.25 479.24 80.24 o 7 5 1 1496.88 1493.97 92.59 o 8 5 1 7517.70 7964.65 164.17 o 9 5 1 2518.69 2741.96 95.15 o 10 5 1 79.09 34.89 27.82 o 11 5 1 816.86 835.91 66.41 o 12 5 1 33.03 -32.83 32.83 o 13 5 1 121.52 203.98 77.47 o -13 6 1 427.23 400.55 87.26 o -12 6 1 3899.01 4380.22 168.18 o -11 6 1 4256.04 4733.65 141.14 o -10 6 1 140.31 134.46 29.54 o -9 6 1 606.86 615.47 67.04 o -8 6 1 4865.01 5031.67 110.73 o -7 6 1 5347.19 5877.28 241.89 o -6 6 1 27.80 33.06 39.16 o -5 6 1 2079.45 2052.51 49.20 o -4 6 1 20701.20 22466.13 406.31 o -3 6 1 3581.12 3341.14 70.18 o -2 6 1 513.15 530.15 21.81 o -1 6 1 0.60 -8.68 8.68 o 0 6 1 2420.43 2242.37 79.71 o 1 6 1 1703.84 1344.71 47.26 o 2 6 1 7.32 16.63 7.07 o 3 6 1 1580.00 1834.98 31.22 o 4 6 1 11863.38 11406.96 336.08 o 5 6 1 15910.88 16607.75 252.94 o 6 6 1 106.26 88.15 19.45 o 7 6 1 0.32 38.33 45.44 o 8 6 1 8415.74 9367.00 168.02 o 9 6 1 3981.16 4176.02 82.86 o 10 6 1 234.62 279.17 48.88 o 11 6 1 514.44 530.34 64.06 o 12 6 1 1440.29 1702.17 253.07 o -12 7 1 1943.63 2401.84 128.99 o -11 7 1 8.55 -53.21 53.21 o -10 7 1 589.04 470.37 65.55 o -9 7 1 78.37 214.11 56.61 o -8 7 1 3240.38 3068.90 99.42 o -7 7 1 148.86 104.57 22.69 o -6 7 1 302.60 328.43 25.54 o -5 7 1 288.62 238.76 44.48 o -4 7 1 148.48 220.63 63.85 o -3 7 1 4.67 16.84 16.31 o -2 7 1 95.87 123.07 13.13 o -1 7 1 3860.74 4424.65 140.95 o 0 7 1 4115.26 4893.05 94.29 o 1 7 1 333.70 267.84 14.87 o 2 7 1 1001.67 968.60 42.71 o 3 7 1 2997.97 2306.74 443.49 o 4 7 1 38.51 84.17 15.71 o 5 7 1 7281.04 7044.32 157.32 o 6 7 1 391.66 378.46 24.65 o 7 7 1 14446.66 15248.85 522.79 o 8 7 1 1227.13 1376.46 44.01 o 9 7 1 1374.31 1438.42 70.44 o 10 7 1 781.92 873.95 51.28 o 11 7 1 7337.18 8122.23 259.77 o 12 7 1 3039.87 3603.40 160.08 o -12 8 1 103.53 165.16 69.81 o -11 8 1 780.02 828.37 94.07 o -10 8 1 654.47 660.65 73.64 o -9 8 1 3444.41 3359.67 129.43 o -8 8 1 7819.62 7954.19 240.64 o -7 8 1 818.07 720.68 54.49 o -6 8 1 1693.28 1973.20 82.59 o -5 8 1 3071.49 3190.51 189.04 o -4 8 1 34516.77 35547.26 978.19 o -3 8 1 9009.66 8725.98 222.29 o -2 8 1 412.28 422.96 17.10 o -1 8 1 1188.85 1198.30 23.84 o 0 8 1 2864.92 2702.38 68.13 o 1 8 1 8435.63 8766.21 117.52 o 2 8 1 979.25 1107.77 33.98 o 3 8 1 20809.62 21235.45 274.69 o 4 8 1 4800.94 4894.15 104.92 o 5 8 1 175.06 227.28 24.18 o 6 8 1 1542.34 1538.53 47.57 o 7 8 1 10821.15 11164.97 456.40 o 8 8 1 10313.05 11184.22 336.97 o 9 8 1 1838.78 1879.37 119.41 o 10 8 1 134.26 123.46 43.63 o 11 8 1 1199.84 1323.04 99.19 o -12 9 1 2240.60 2315.22 91.28 o -11 9 1 3529.15 3744.03 166.47 o -10 9 1 142.34 180.05 62.57 o -9 9 1 763.54 556.79 65.55 o -8 9 1 366.72 324.78 59.17 o -7 9 1 7113.15 7031.35 212.09 o -6 9 1 570.24 533.80 48.53 o -5 9 1 2016.43 1846.39 71.52 o -4 9 1 2273.73 2139.36 76.63 o -3 9 1 263.23 223.67 32.46 o -2 9 1 46.54 54.65 23.11 o -1 9 1 21545.84 22384.15 378.02 o 0 9 1 13989.09 15413.38 201.46 o 1 9 1 4108.72 4398.54 64.81 o 2 9 1 3517.68 3418.06 100.18 o 3 9 1 10987.75 11339.09 247.98 o 4 9 1 14466.54 15321.27 357.40 o 5 9 1 4836.85 5022.34 146.90 o 6 9 1 1264.90 1226.31 51.02 o 7 9 1 1627.31 1546.25 109.83 o 8 9 1 5153.20 5363.05 538.65 o 9 9 1 2975.13 2839.48 244.16 o 10 9 1 600.79 649.05 59.88 o 11 9 1 145.15 198.20 54.47 o -11 10 1 1324.66 1263.65 74.95 o -10 10 1 0.79 -31.50 37.47 o -9 10 1 6640.33 6532.32 433.08 o -8 10 1 14686.37 15562.59 306.39 o -7 10 1 2745.79 2548.81 238.41 o -6 10 1 77.13 66.99 27.09 o -5 10 1 41.56 72.21 66.62 o -4 10 1 15884.12 15896.93 321.57 o -3 10 1 20483.93 21747.51 328.53 o -2 10 1 0.41 -1.19 23.40 o -1 10 1 33.58 30.56 15.40 o 0 10 1 27595.48 29219.71 549.49 o 1 10 1 13802.72 14854.06 227.25 o 2 10 1 443.40 475.96 25.47 o 3 10 1 2239.62 2304.02 50.14 o 4 10 1 2365.12 2251.64 104.18 o 5 10 1 8359.32 8535.03 418.90 o 6 10 1 235.50 266.15 46.82 o 7 10 1 2212.05 1963.38 203.28 o 8 10 1 138.92 112.58 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