#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:00:13 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180939 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/19/2201909.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201909_Fobs loop_ _publ_author_name 'Jones, Matthew D.' 'Almeida Paz, Filipe A.' 'Davies, John E.' 'Johnson, Brian F. G.' _publ_section_title ; (1R,2R)-(+)-1,2-Diphenylethylenediamine ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o455 _journal_page_last o457 _journal_volume 59 _journal_year 2003 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 5.1447 _cell_length_b 12.3264 _cell_length_c 18.5357 _exptl_crystal_F_000 456.00 _reflns_d_resolution_high 0.8411 _cod_data_source_file cm6032Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' bj0306 in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 85.55 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 273.62 264.18 8.81 o 4 0 0 59.79 54.38 2.53 o 6 0 0 80.51 100.08 7.69 o 1 1 0 1127.40 949.45 64.81 o 2 1 0 48.89 39.57 1.20 o 3 1 0 8.36 9.07 1.17 o 4 1 0 171.30 193.50 10.21 o 5 1 0 9.37 8.87 0.55 o 6 1 0 0.36 -1.06 2.20 o 1 2 0 3721.07 3787.91 142.52 o 2 2 0 27.95 28.83 1.23 o 3 2 0 107.90 95.68 3.97 o 4 2 0 0.98 2.38 0.78 o 5 2 0 19.36 21.49 2.53 o 6 2 0 56.65 80.77 7.53 o 1 3 0 94.01 99.85 3.48 o 2 3 0 165.87 159.85 4.61 o 3 3 0 46.00 52.00 2.99 o 4 3 0 0.05 -0.26 1.28 o 5 3 0 24.73 28.39 5.44 o 0 4 0 383.54 363.76 16.36 o 1 4 0 79.37 87.10 2.90 o 2 4 0 159.18 162.03 4.71 o 3 4 0 270.82 290.37 9.44 o 4 4 0 41.47 48.26 3.58 o 5 4 0 1.19 0.32 1.44 o 1 5 0 968.15 1007.94 38.69 o 2 5 0 2.04 6.10 1.17 o 3 5 0 42.19 41.38 1.22 o 4 5 0 119.69 124.77 4.53 o 5 5 0 0.89 1.82 1.01 o 0 6 0 5.32 5.36 1.09 o 1 6 0 228.55 242.36 7.59 o 2 6 0 1.16 1.13 0.50 o 3 6 0 67.95 67.85 1.82 o 4 6 0 176.14 183.26 6.32 o 5 6 0 0.13 0.13 1.37 o 1 7 0 226.74 204.83 5.84 o 2 7 0 1.17 3.30 0.63 o 3 7 0 537.68 537.49 15.84 o 4 7 0 53.45 52.83 2.63 o 5 7 0 25.89 31.29 4.13 o 0 8 0 100.72 120.86 5.13 o 1 8 0 157.97 164.16 5.76 o 2 8 0 227.15 225.74 6.18 o 3 8 0 118.85 121.37 4.21 o 4 8 0 169.04 170.61 6.45 o 5 8 0 0.22 8.30 3.29 o 1 9 0 419.73 424.13 10.87 o 2 9 0 0.49 2.04 0.90 o 3 9 0 31.34 28.81 1.56 o 4 9 0 63.38 49.81 4.78 o 0 10 0 51.79 60.30 4.08 o 1 10 0 14.82 16.37 1.33 o 2 10 0 22.34 18.70 2.02 o 3 10 0 2.49 1.88 1.60 o 4 10 0 13.52 9.94 2.39 o 1 11 0 0.72 0.19 0.96 o 2 11 0 237.04 231.13 7.57 o 3 11 0 0.86 0.05 0.87 o 0 12 0 22.68 22.51 2.68 o 1 12 0 1.88 2.78 1.82 o 2 12 0 3.25 2.24 1.09 o 3 12 0 4.10 12.48 3.08 o 1 13 0 35.38 38.52 3.58 o 2 13 0 0.03 1.28 1.31 o 0 14 0 45.99 53.86 5.14 o 1 14 0 2.56 4.81 1.41 o 1 0 1 160.76 117.15 22.77 o 2 0 1 457.47 382.25 12.77 o 3 0 1 158.51 160.22 5.14 o 4 0 1 92.89 85.42 1.97 o 5 0 1 49.58 59.47 4.26 o 6 0 1 10.18 11.79 2.97 o 1 1 1 2232.17 2104.12 66.36 o 2 1 1 1206.67 1123.71 23.31 o 3 1 1 561.85 538.98 11.34 o 4 1 1 41.20 42.53 1.04 o 5 1 1 34.33 36.09 1.75 o 6 1 1 13.83 19.37 3.14 o 1 2 1 1260.29 1170.97 37.56 o 2 2 1 500.88 463.10 12.12 o 3 2 1 52.27 53.16 1.59 o 4 2 1 149.77 156.81 4.20 o 5 2 1 0.13 0.06 1.08 o 6 2 1 41.06 49.15 5.49 o 0 3 1 10.74 13.26 1.18 o 1 3 1 374.43 373.51 8.47 o 2 3 1 298.37 286.13 7.82 o 3 3 1 149.56 147.15 2.81 o 4 3 1 49.67 48.95 1.50 o 5 3 1 124.99 143.25 5.08 o 0 4 1 161.32 166.12 6.40 o 1 4 1 86.42 87.88 1.97 o 2 4 1 40.77 46.81 1.10 o 3 4 1 13.40 18.89 1.05 o 4 4 1 52.51 52.71 1.63 o 5 4 1 25.88 25.03 2.07 o 0 5 1 223.37 231.17 7.28 o 1 5 1 94.51 94.21 2.65 o 2 5 1 147.22 141.06 3.14 o 3 5 1 28.95 34.46 1.20 o 4 5 1 2.84 2.78 0.56 o 5 5 1 33.85 33.27 1.53 o 0 6 1 41.33 54.27 2.43 o 1 6 1 591.73 616.25 14.31 o 2 6 1 117.23 109.66 2.50 o 3 6 1 278.01 269.53 4.92 o 4 6 1 105.71 105.22 3.16 o 5 6 1 13.61 13.24 1.76 o 0 7 1 660.83 735.58 24.40 o 1 7 1 157.13 168.40 4.31 o 2 7 1 132.08 135.66 4.27 o 3 7 1 107.53 110.98 2.30 o 4 7 1 110.72 109.26 3.56 o 5 7 1 6.10 6.71 3.07 o 0 8 1 5.19 4.07 0.65 o 1 8 1 111.03 107.50 3.03 o 2 8 1 60.02 58.37 1.28 o 3 8 1 85.59 91.02 1.85 o 4 8 1 103.24 109.72 2.57 o 5 8 1 1.53 7.45 2.17 o 0 9 1 4.72 4.89 0.84 o 1 9 1 17.10 18.56 0.81 o 2 9 1 186.44 188.99 3.40 o 3 9 1 10.66 9.73 0.76 o 4 9 1 27.70 29.79 3.63 o 0 10 1 8.54 8.62 0.94 o 1 10 1 81.34 81.23 2.12 o 2 10 1 144.96 150.10 3.26 o 3 10 1 25.88 26.30 1.18 o 4 10 1 0.55 2.33 1.86 o 0 11 1 24.42 22.44 1.58 o 1 11 1 101.39 106.22 2.51 o 2 11 1 23.29 21.48 1.70 o 3 11 1 6.77 7.61 1.18 o 4 11 1 10.56 13.09 2.57 o 0 12 1 2.70 5.73 1.45 o 1 12 1 36.65 33.21 1.79 o 2 12 1 18.93 18.93 1.28 o 3 12 1 55.50 52.79 4.62 o 0 13 1 38.90 43.12 7.68 o 1 13 1 0.90 -0.03 1.12 o 2 13 1 12.08 12.50 2.97 o 0 14 1 0.33 1.63 2.04 o 1 14 1 57.21 64.75 3.55 o 1 0 2 56.98 46.66 1.43 o 2 0 2 90.52 86.79 2.75 o 3 0 2 64.57 59.10 1.21 o 4 0 2 48.51 48.49 2.56 o 5 0 2 33.14 38.37 4.39 o 6 0 2 18.25 36.50 5.08 o 1 1 2 4793.21 4676.91 124.66 o 2 1 2 380.83 336.18 5.08 o 3 1 2 6.46 6.21 0.65 o 4 1 2 12.76 13.16 1.00 o 5 1 2 24.01 25.96 2.09 o 6 1 2 56.45 77.44 11.26 o 1 2 2 2882.94 2639.66 96.48 o 2 2 2 95.11 95.15 2.03 o 3 2 2 146.46 153.79 2.79 o 4 2 2 81.54 78.55 1.80 o 5 2 2 133.92 144.86 5.16 o 6 2 2 21.21 31.80 6.64 o 0 3 2 2089.47 2079.40 66.50 o 1 3 2 1387.82 1396.82 30.10 o 2 3 2 327.49 315.29 8.58 o 3 3 2 176.84 181.22 3.30 o 4 3 2 3.41 3.69 0.55 o 5 3 2 88.15 88.14 4.88 o 0 4 2 450.47 421.85 15.52 o 1 4 2 171.70 172.68 3.95 o 2 4 2 51.91 46.19 1.22 o 3 4 2 148.59 138.55 2.64 o 4 4 2 75.27 78.82 2.03 o 5 4 2 34.31 35.49 1.49 o 0 5 2 37.55 46.24 3.54 o 1 5 2 228.88 239.47 5.51 o 2 5 2 207.56 222.22 5.31 o 3 5 2 157.46 151.44 2.43 o 4 5 2 187.06 204.69 6.18 o 5 5 2 3.58 3.20 1.11 o 0 6 2 918.90 974.91 35.13 o 1 6 2 49.69 49.05 1.71 o 2 6 2 75.15 86.02 1.98 o 3 6 2 9.76 10.47 0.82 o 4 6 2 86.48 81.54 3.42 o 5 6 2 4.07 2.42 0.80 o 0 7 2 38.31 36.92 1.41 o 1 7 2 9.65 11.08 0.74 o 2 7 2 39.51 35.90 1.23 o 3 7 2 631.25 658.19 13.47 o 4 7 2 87.05 88.26 3.24 o 5 7 2 71.79 91.92 5.71 o 0 8 2 30.59 29.87 1.64 o 1 8 2 11.93 13.26 0.58 o 2 8 2 46.80 42.70 1.15 o 3 8 2 156.38 159.69 3.80 o 4 8 2 1.01 1.29 0.56 o 5 8 2 6.82 9.04 2.91 o 0 9 2 21.26 20.92 1.00 o 1 9 2 0.51 -0.04 0.97 o 2 9 2 329.48 334.81 7.20 o 3 9 2 25.17 28.25 1.00 o 4 9 2 3.55 2.25 1.40 o 0 10 2 0.27 1.26 1.24 o 1 10 2 240.03 251.70 4.67 o 2 10 2 29.74 29.92 1.05 o 3 10 2 9.68 12.04 1.73 o 4 10 2 17.30 10.84 1.95 o 0 11 2 2.42 2.75 1.28 o 1 11 2 46.60 43.92 1.64 o 2 11 2 53.28 57.34 1.81 o 3 11 2 1.05 1.77 0.92 o 4 11 2 6.42 6.04 1.88 o 0 12 2 19.35 20.99 1.79 o 1 12 2 19.85 20.14 2.12 o 2 12 2 11.31 14.06 2.37 o 3 12 2 11.67 10.44 1.52 o 0 13 2 5.52 7.71 1.87 o 1 13 2 15.16 13.60 1.61 o 2 13 2 5.52 5.28 2.38 o 0 14 2 2.99 1.47 2.11 o 1 14 2 8.61 10.45 1.88 o 1 0 3 7318.85 7402.17 324.22 o 2 0 3 203.30 197.92 5.97 o 3 0 3 62.63 69.36 2.48 o 4 0 3 47.35 46.41 1.21 o 5 0 3 4.91 4.39 0.51 o 6 0 3 17.65 25.13 3.71 o 1 1 3 1675.14 1476.31 21.02 o 2 1 3 41.89 43.50 0.69 o 3 1 3 288.19 283.74 4.37 o 4 1 3 31.44 30.97 0.66 o 5 1 3 44.51 50.41 3.34 o 6 1 3 75.65 92.41 6.04 o 0 2 3 116.97 118.08 4.22 o 1 2 3 1956.91 1837.83 64.66 o 2 2 3 182.91 174.39 5.21 o 3 2 3 23.60 28.10 0.97 o 4 2 3 11.93 10.14 1.13 o 5 2 3 120.33 121.72 3.55 o 6 2 3 5.72 11.06 2.20 o 0 3 3 52.87 56.50 2.05 o 1 3 3 2720.18 2633.14 122.97 o 2 3 3 402.70 383.62 7.83 o 3 3 3 71.50 73.05 1.54 o 4 3 3 6.31 9.09 2.08 o 5 3 3 59.38 61.29 3.87 o 0 4 3 1403.35 1433.17 41.80 o 1 4 3 503.67 492.36 10.94 o 2 4 3 2678.01 2823.67 54.41 o 3 4 3 135.47 140.44 3.15 o 4 4 3 91.72 94.84 2.10 o 5 4 3 72.25 78.81 4.69 o 0 5 3 290.90 311.28 9.43 o 1 5 3 481.40 523.58 11.84 o 2 5 3 548.26 550.76 13.21 o 3 5 3 69.76 66.40 1.39 o 4 5 3 56.25 55.25 2.18 o 5 5 3 30.02 27.30 1.29 o 0 6 3 208.23 217.11 7.19 o 1 6 3 118.12 125.05 2.84 o 2 6 3 43.71 47.08 1.11 o 3 6 3 122.31 119.98 2.39 o 4 6 3 64.49 72.74 3.96 o 5 6 3 8.39 6.75 1.22 o 0 7 3 302.57 331.69 11.78 o 1 7 3 37.75 40.27 1.56 o 2 7 3 126.76 128.86 2.85 o 3 7 3 8.74 8.79 0.55 o 4 7 3 102.61 106.98 3.09 o 5 7 3 23.66 27.43 2.21 o 0 8 3 5.13 4.44 0.74 o 1 8 3 93.79 91.99 1.85 o 2 8 3 32.33 30.33 1.02 o 3 8 3 6.11 5.96 1.08 o 4 8 3 21.14 20.29 0.86 o 5 8 3 4.31 4.27 1.31 o 0 9 3 0.02 -0.82 0.82 o 1 9 3 33.71 38.42 1.44 o 2 9 3 257.12 251.17 5.78 o 3 9 3 156.63 163.30 3.92 o 4 9 3 49.22 53.26 4.63 o 0 10 3 69.73 69.09 4.30 o 1 10 3 191.88 191.17 4.94 o 2 10 3 39.31 39.24 1.40 o 3 10 3 12.60 11.52 1.37 o 4 10 3 0.28 0.00 1.49 o 0 11 3 0.01 0.31 1.17 o 1 11 3 50.37 48.86 1.81 o 2 11 3 10.60 12.16 1.30 o 3 11 3 22.49 20.86 1.27 o 0 12 3 15.86 14.15 1.94 o 1 12 3 0.52 0.92 1.81 o 2 12 3 12.24 12.47 1.18 o 3 12 3 2.93 4.90 1.41 o 0 13 3 1.55 -1.79 2.51 o 1 13 3 8.94 7.77 1.52 o 2 13 3 0.90 0.90 1.33 o 0 14 3 0.35 0.33 1.95 o 1 14 3 6.05 6.72 2.31 o 0 0 4 6833.24 7900.14 320.42 o 1 0 4 3.62 4.31 0.63 o 2 0 4 202.59 195.83 6.44 o 3 0 4 78.05 82.02 2.63 o 4 0 4 9.15 9.52 0.47 o 5 0 4 131.28 136.92 5.29 o 6 0 4 40.46 52.13 4.85 o 0 1 4 18.95 18.78 0.64 o 1 1 4 2490.22 2377.56 57.55 o 2 1 4 53.89 44.50 0.65 o 3 1 4 7.83 6.02 0.33 o 4 1 4 12.67 14.03 0.83 o 5 1 4 60.30 61.60 2.24 o 6 1 4 1.08 4.17 1.76 o 0 2 4 0.00 0.90 0.51 o 1 2 4 259.91 243.43 6.99 o 2 2 4 683.30 625.60 10.19 o 3 2 4 211.22 217.68 3.46 o 4 2 4 177.94 183.13 3.10 o 5 2 4 19.55 20.87 2.44 o 0 3 4 605.22 554.72 16.56 o 1 3 4 606.55 568.19 21.31 o 2 3 4 83.84 82.41 2.22 o 3 3 4 98.18 89.76 1.73 o 4 3 4 137.13 136.02 2.27 o 5 3 4 9.37 8.36 1.25 o 0 4 4 59.37 53.58 2.27 o 1 4 4 415.23 409.25 8.91 o 2 4 4 73.47 79.91 1.86 o 3 4 4 62.66 68.81 1.81 o 4 4 4 122.07 127.98 2.80 o 5 4 4 17.57 16.19 1.72 o 0 5 4 51.71 53.57 4.37 o 1 5 4 64.87 82.28 2.84 o 2 5 4 54.73 52.54 1.56 o 3 5 4 233.48 239.05 3.98 o 4 5 4 15.26 17.41 1.19 o 5 5 4 86.02 88.38 4.14 o 0 6 4 0.32 1.13 0.92 o 1 6 4 88.36 95.13 2.41 o 2 6 4 168.65 173.41 3.53 o 3 6 4 274.06 272.11 4.70 o 4 6 4 75.31 76.75 1.84 o 5 6 4 2.44 1.53 0.70 o 0 7 4 297.77 332.60 12.62 o 1 7 4 186.59 195.25 4.53 o 2 7 4 294.26 292.05 6.37 o 3 7 4 9.17 7.66 0.72 o 4 7 4 3.18 1.79 0.71 o 5 7 4 21.52 26.84 3.66 o 0 8 4 13.86 14.17 1.41 o 1 8 4 167.03 168.65 4.01 o 2 8 4 23.75 25.24 1.37 o 3 8 4 6.88 7.38 0.77 o 4 8 4 1.15 3.28 0.87 o 5 8 4 4.60 6.79 1.67 o 0 9 4 0.05 1.65 0.94 o 1 9 4 18.28 17.39 0.83 o 2 9 4 105.63 112.48 2.89 o 3 9 4 33.89 34.92 1.87 o 4 9 4 8.39 13.61 2.83 o 0 10 4 116.40 129.80 4.50 o 1 10 4 24.10 25.95 1.03 o 2 10 4 20.51 23.44 2.06 o 3 10 4 135.61 140.31 4.19 o 4 10 4 9.57 6.79 2.29 o 0 11 4 24.80 26.38 1.47 o 1 11 4 93.21 98.51 3.36 o 2 11 4 52.15 48.80 1.92 o 3 11 4 37.45 36.11 1.80 o 0 12 4 57.18 72.47 5.42 o 1 12 4 58.15 49.25 2.55 o 2 12 4 21.40 20.54 2.14 o 3 12 4 6.18 8.85 1.72 o 0 13 4 56.83 50.68 4.55 o 1 13 4 18.13 18.00 2.17 o 2 13 4 5.93 7.06 2.34 o 0 14 4 21.66 16.63 3.09 o 1 14 4 4.01 4.19 1.72 o 1 0 5 197.37 182.52 3.58 o 2 0 5 750.35 719.28 11.79 o 3 0 5 0.43 -0.21 0.82 o 4 0 5 0.88 1.61 0.33 o 5 0 5 35.04 41.15 4.06 o 0 1 5 533.70 559.31 11.82 o 1 1 5 5720.88 6179.54 203.59 o 2 1 5 484.29 438.74 6.06 o 3 1 5 45.63 48.12 1.12 o 4 1 5 123.00 124.14 3.20 o 5 1 5 40.29 41.70 2.10 o 0 2 5 7.59 7.35 0.74 o 1 2 5 1295.22 1194.07 42.65 o 2 2 5 1644.84 1649.16 35.50 o 3 2 5 12.71 12.43 0.42 o 4 2 5 31.43 30.32 0.86 o 5 2 5 29.43 25.53 1.56 o 0 3 5 7.95 9.53 1.00 o 1 3 5 917.77 907.69 36.73 o 2 3 5 905.08 833.41 16.68 o 3 3 5 23.49 22.14 0.67 o 4 3 5 81.08 86.18 1.65 o 5 3 5 219.82 249.79 12.73 o 0 4 5 267.14 275.95 12.33 o 1 4 5 986.24 1042.71 20.77 o 2 4 5 716.17 721.59 15.52 o 3 4 5 39.50 40.23 0.83 o 4 4 5 88.11 88.95 2.08 o 5 4 5 132.58 141.19 9.27 o 0 5 5 1.19 0.88 1.36 o 1 5 5 322.00 338.38 7.47 o 2 5 5 78.07 83.21 1.62 o 3 5 5 45.16 42.73 0.91 o 4 5 5 109.90 108.97 3.04 o 5 5 5 10.81 10.32 1.38 o 0 6 5 120.38 130.87 4.19 o 1 6 5 19.91 26.50 1.20 o 2 6 5 158.27 163.73 3.33 o 3 6 5 204.57 200.98 3.49 o 4 6 5 58.81 57.35 1.45 o 5 6 5 3.01 2.88 1.55 o 0 7 5 9.98 11.15 0.91 o 1 7 5 61.63 66.17 2.33 o 2 7 5 72.61 73.16 2.20 o 3 7 5 247.41 241.80 5.51 o 4 7 5 23.12 23.56 0.65 o 5 7 5 11.04 11.76 2.26 o 0 8 5 109.70 107.57 3.78 o 1 8 5 6.88 4.82 0.54 o 2 8 5 138.45 133.12 2.87 o 3 8 5 128.01 135.84 2.60 o 4 8 5 10.67 8.84 1.68 o 0 9 5 263.07 267.09 8.59 o 1 9 5 105.44 103.19 2.43 o 2 9 5 43.93 39.25 1.26 o 3 9 5 46.66 45.41 1.91 o 4 9 5 14.53 19.64 3.09 o 0 10 5 61.77 59.14 3.89 o 1 10 5 20.91 21.51 1.12 o 2 10 5 110.29 118.53 3.66 o 3 10 5 5.50 5.61 1.17 o 4 10 5 3.16 4.29 2.14 o 0 11 5 59.76 56.72 5.89 o 1 11 5 42.41 40.51 1.74 o 2 11 5 81.62 76.69 3.01 o 3 11 5 6.82 9.27 1.91 o 0 12 5 0.98 -0.56 1.85 o 1 12 5 54.90 53.76 3.19 o 2 12 5 27.68 30.00 1.97 o 3 12 5 50.86 47.08 3.12 o 0 13 5 49.65 47.54 4.93 o 1 13 5 5.42 2.10 1.28 o 2 13 5 11.40 11.64 1.92 o 0 14 5 25.76 23.64 3.65 o 1 14 5 4.62 8.13 1.94 o 0 0 6 855.33 860.07 22.63 o 1 0 6 2647.72 2799.90 59.51 o 2 0 6 107.17 108.42 3.99 o 3 0 6 304.70 291.71 4.67 o 4 0 6 77.74 79.79 1.95 o 5 0 6 14.68 14.15 1.81 o 0 1 6 4.88 6.41 0.61 o 1 1 6 1584.44 1519.04 28.78 o 2 1 6 368.52 370.09 5.88 o 3 1 6 142.56 143.13 2.53 o 4 1 6 134.65 136.90 1.97 o 5 1 6 23.47 21.96 6.14 o 0 2 6 584.70 591.79 15.38 o 1 2 6 486.83 501.81 14.78 o 2 2 6 724.72 708.87 12.28 o 3 2 6 37.65 33.69 1.06 o 4 2 6 25.77 22.63 0.87 o 5 2 6 50.45 48.60 2.40 o 0 3 6 36.81 38.97 1.40 o 1 3 6 645.94 632.45 22.37 o 2 3 6 415.50 406.88 10.88 o 3 3 6 125.21 116.96 2.42 o 4 3 6 41.29 39.69 1.21 o 5 3 6 80.23 82.54 4.56 o 0 4 6 151.60 151.80 6.84 o 1 4 6 96.10 100.13 2.17 o 2 4 6 37.25 31.16 0.79 o 3 4 6 116.53 115.78 1.84 o 4 4 6 43.59 39.72 1.56 o 5 4 6 39.52 41.03 2.55 o 0 5 6 8.36 11.22 1.77 o 1 5 6 155.54 148.71 4.80 o 2 5 6 478.48 505.90 10.34 o 3 5 6 120.45 109.24 2.01 o 4 5 6 159.75 168.46 4.05 o 5 5 6 41.69 45.59 3.09 o 0 6 6 413.26 445.42 15.71 o 1 6 6 296.01 316.76 8.14 o 2 6 6 117.65 125.11 2.33 o 3 6 6 29.65 24.26 0.78 o 4 6 6 1.97 1.94 0.37 o 5 6 6 23.04 23.20 3.59 o 0 7 6 506.27 513.85 19.42 o 1 7 6 65.84 63.99 1.61 o 2 7 6 38.90 39.66 1.66 o 3 7 6 6.67 10.28 0.70 o 4 7 6 2.89 2.60 0.60 o 5 7 6 23.68 30.46 2.36 o 0 8 6 112.04 113.86 4.73 o 1 8 6 142.27 137.95 3.37 o 2 8 6 16.35 13.87 0.76 o 3 8 6 37.25 36.27 1.10 o 4 8 6 64.49 64.44 2.87 o 0 9 6 264.01 260.61 8.37 o 1 9 6 27.41 30.18 1.12 o 2 9 6 94.62 99.29 2.86 o 3 9 6 52.22 51.32 1.40 o 4 9 6 10.40 6.53 2.87 o 0 10 6 119.63 124.59 4.04 o 1 10 6 185.34 187.83 4.10 o 2 10 6 10.29 11.18 1.04 o 3 10 6 7.04 6.99 1.41 o 4 10 6 9.68 5.99 2.71 o 0 11 6 33.37 30.72 3.43 o 1 11 6 69.85 68.11 2.27 o 2 11 6 73.59 76.48 2.85 o 3 11 6 4.97 3.51 1.02 o 0 12 6 5.55 5.84 1.84 o 1 12 6 20.76 17.05 1.80 o 2 12 6 3.45 5.46 1.28 o 3 12 6 8.19 7.52 1.50 o 0 13 6 297.64 317.94 20.60 o 1 13 6 9.08 9.36 1.47 o 2 13 6 3.59 1.22 1.29 o 0 14 6 3.05 0.97 2.02 o 1 0 7 208.22 199.18 3.50 o 2 0 7 1872.15 1919.93 45.37 o 3 0 7 369.02 359.76 6.04 o 4 0 7 132.31 120.03 2.93 o 5 0 7 6.33 6.75 0.88 o 0 1 7 241.86 236.95 4.67 o 1 1 7 909.99 949.82 12.27 o 2 1 7 81.66 78.63 1.17 o 3 1 7 32.46 32.09 0.67 o 4 1 7 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29.05 27.44 1.10 o 2 8 7 219.41 209.07 5.14 o 3 8 7 27.45 27.05 1.01 o 4 8 7 2.82 1.19 1.67 o 0 9 7 58.77 56.85 2.54 o 1 9 7 217.28 213.25 4.95 o 2 9 7 90.85 86.71 2.62 o 3 9 7 13.78 12.96 0.89 o 4 9 7 25.37 27.51 2.80 o 0 10 7 28.45 31.32 1.98 o 1 10 7 12.45 9.90 1.12 o 2 10 7 15.79 18.28 1.34 o 3 10 7 12.26 13.13 2.05 o 4 10 7 23.90 24.62 2.65 o 0 11 7 629.34 672.38 40.19 o 1 11 7 24.63 26.18 1.91 o 2 11 7 46.25 46.71 3.08 o 3 11 7 19.15 21.32 1.68 o 0 12 7 0.17 -1.91 2.31 o 1 12 7 12.86 15.28 5.95 o 2 12 7 14.72 16.68 2.16 o 0 13 7 35.26 36.68 3.78 o 1 13 7 23.15 26.53 5.59 o 2 13 7 12.70 14.91 2.11 o 0 0 8 635.60 672.64 17.99 o 1 0 8 83.42 88.24 2.92 o 2 0 8 568.74 526.67 12.24 o 3 0 8 233.96 221.18 5.07 o 4 0 8 4.43 4.62 0.87 o 5 0 8 8.90 10.55 2.46 o 0 1 8 379.09 383.09 7.45 o 1 1 8 143.06 151.91 2.95 o 2 1 8 845.35 827.39 15.67 o 3 1 8 367.22 352.55 8.28 o 4 1 8 98.91 100.21 1.65 o 5 1 8 3.65 4.15 0.66 o 0 2 8 328.82 351.74 8.51 o 1 2 8 338.01 371.67 5.88 o 2 2 8 143.07 137.29 2.50 o 3 2 8 28.42 31.48 0.75 o 4 2 8 351.86 355.04 6.29 o 5 2 8 6.93 6.14 0.95 o 0 3 8 103.31 94.87 2.68 o 1 3 8 828.86 911.53 14.45 o 2 3 8 69.82 65.55 1.73 o 3 3 8 108.24 105.94 1.78 o 4 3 8 201.63 201.56 3.56 o 5 3 8 24.14 24.88 1.56 o 0 4 8 29.79 27.50 1.23 o 1 4 8 406.36 462.15 9.79 o 2 4 8 146.09 151.79 4.27 o 3 4 8 37.73 37.27 1.21 o 4 4 8 9.06 8.64 0.71 o 5 4 8 45.51 41.54 3.66 o 0 5 8 29.24 29.39 3.43 o 1 5 8 409.21 432.98 11.14 o 2 5 8 77.41 82.87 1.62 o 3 5 8 471.87 461.80 8.40 o 4 5 8 12.32 9.09 0.68 o 5 5 8 25.91 25.16 2.25 o 0 6 8 89.48 75.71 5.90 o 1 6 8 73.24 73.21 1.98 o 2 6 8 54.04 51.02 1.36 o 3 6 8 190.95 189.50 3.22 o 4 6 8 18.82 15.14 0.73 o 5 6 8 26.02 23.17 1.69 o 0 7 8 406.88 420.54 16.49 o 1 7 8 106.27 110.08 4.11 o 2 7 8 47.98 41.37 1.18 o 3 7 8 11.44 10.13 0.96 o 4 7 8 1.79 1.25 0.56 o 0 8 8 8.69 8.09 1.31 o 1 8 8 151.28 150.81 3.61 o 2 8 8 73.19 72.25 1.80 o 3 8 8 53.60 43.85 1.28 o 4 8 8 6.85 8.10 2.90 o 0 9 8 208.67 205.11 6.94 o 1 9 8 27.26 27.55 1.65 o 2 9 8 9.71 9.21 0.88 o 3 9 8 14.79 13.70 0.83 o 4 9 8 3.34 6.89 2.45 o 0 10 8 23.44 26.41 1.82 o 1 10 8 57.50 61.22 3.33 o 2 10 8 66.90 61.08 2.43 o 3 10 8 15.52 14.43 1.67 o 0 11 8 48.82 47.40 3.65 o 1 11 8 11.28 13.55 2.58 o 2 11 8 24.09 21.46 1.64 o 3 11 8 6.13 4.58 1.64 o 0 12 8 44.14 51.00 4.54 o 1 12 8 78.34 79.69 4.42 o 2 12 8 20.29 28.38 2.13 o 0 13 8 39.57 49.12 4.64 o 1 13 8 4.32 5.26 3.41 o 1 0 9 7.58 8.36 1.32 o 2 0 9 309.53 329.18 8.53 o 3 0 9 59.67 61.40 2.26 o 4 0 9 0.33 1.07 0.48 o 5 0 9 32.77 34.87 1.68 o 0 1 9 6.64 6.72 1.21 o 1 1 9 8.42 8.92 0.53 o 2 1 9 286.57 276.63 6.67 o 3 1 9 239.59 238.93 4.63 o 4 1 9 66.41 66.66 1.25 o 5 1 9 4.54 4.44 1.37 o 0 2 9 139.99 161.08 5.75 o 1 2 9 28.02 23.01 0.78 o 2 2 9 279.64 261.85 5.60 o 3 2 9 169.86 168.04 3.47 o 4 2 9 20.01 18.26 0.67 o 5 2 9 31.65 29.47 3.13 o 0 3 9 31.47 32.70 1.38 o 1 3 9 86.99 93.35 1.65 o 2 3 9 30.41 29.25 1.32 o 3 3 9 433.38 431.46 7.50 o 4 3 9 77.79 82.05 2.26 o 5 3 9 4.83 5.05 1.90 o 0 4 9 8.65 7.54 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1.31 0.51 o 3 5 10 2.20 1.10 0.47 o 4 5 10 45.22 39.08 1.02 o 5 5 10 12.93 14.95 1.24 o 0 6 10 278.64 282.74 10.00 o 1 6 10 82.92 81.82 2.28 o 2 6 10 18.26 15.47 1.20 o 3 6 10 26.23 23.45 1.03 o 4 6 10 3.83 1.50 0.54 o 0 7 10 139.40 138.01 5.28 o 1 7 10 36.49 34.47 1.45 o 2 7 10 78.99 64.46 1.64 o 3 7 10 8.90 7.97 0.64 o 4 7 10 45.90 39.51 1.56 o 0 8 10 34.78 30.90 1.55 o 1 8 10 247.27 247.44 5.38 o 2 8 10 56.18 54.57 1.70 o 3 8 10 27.73 22.04 1.07 o 4 8 10 40.34 30.64 2.81 o 0 9 10 133.55 123.70 4.27 o 1 9 10 55.88 50.64 2.06 o 2 9 10 11.99 9.45 0.90 o 3 9 10 13.99 8.94 0.81 o 0 10 10 54.18 52.30 3.78 o 1 10 10 198.87 198.50 8.19 o 2 10 10 42.86 39.03 1.68 o 3 10 10 8.93 11.83 1.77 o 0 11 10 49.87 52.25 3.95 o 1 11 10 48.79 39.81 2.76 o 2 11 10 7.65 5.21 1.41 o 0 12 10 3.47 6.61 2.05 o 1 12 10 32.06 31.98 8.18 o 2 12 10 5.22 8.42 4.86 o 0 13 10 9.37 11.78 2.37 o 1 0 11 260.09 270.15 8.27 o 2 0 11 87.80 79.73 3.22 o 3 0 11 751.69 762.96 16.48 o 4 0 11 116.60 118.84 6.38 o 5 0 11 0.25 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7 11 96.13 108.45 4.08 o 0 8 11 3.11 3.05 1.35 o 1 8 11 54.04 52.88 1.43 o 2 8 11 13.32 10.90 0.77 o 3 8 11 24.73 19.21 0.91 o 4 8 11 38.16 34.85 2.26 o 0 9 11 74.96 78.91 5.34 o 1 9 11 193.93 199.63 5.25 o 2 9 11 59.36 57.93 1.96 o 3 9 11 3.29 4.17 1.02 o 0 10 11 3.96 5.16 2.03 o 1 10 11 48.35 41.45 2.35 o 2 10 11 5.86 2.93 1.30 o 3 10 11 3.70 5.05 1.12 o 0 11 11 13.68 13.00 2.43 o 1 11 11 47.28 50.27 3.01 o 2 11 11 23.15 26.34 2.46 o 0 12 11 20.95 28.49 3.23 o 1 12 11 2.37 2.80 1.47 o 0 0 12 1531.05 1653.35 39.07 o 1 0 12 9.26 9.89 0.47 o 2 0 12 148.09 144.81 4.16 o 3 0 12 14.68 11.13 0.87 o 4 0 12 122.13 125.10 3.62 o 5 0 12 12.87 8.28 3.34 o 0 1 12 5.82 7.42 1.13 o 1 1 12 77.87 84.47 1.87 o 2 1 12 140.99 135.02 3.24 o 3 1 12 180.27 178.94 4.01 o 4 1 12 148.42 137.69 3.84 o 5 1 12 15.83 19.34 3.41 o 0 2 12 249.96 232.76 10.92 o 1 2 12 90.36 93.19 2.86 o 2 2 12 43.30 41.85 1.02 o 3 2 12 59.50 61.90 1.16 o 4 2 12 12.87 12.38 1.61 o 5 2 12 21.38 22.70 1.56 o 0 3 12 25.19 27.66 2.75 o 1 3 12 110.37 112.65 2.68 o 2 3 12 77.13 73.73 1.58 o 3 3 12 40.01 36.47 1.57 o 4 3 12 16.20 17.52 0.74 o 0 4 12 71.63 64.62 3.46 o 1 4 12 122.02 120.27 2.47 o 2 4 12 100.03 96.26 2.28 o 3 4 12 42.39 37.26 1.15 o 4 4 12 0.74 1.00 0.56 o 0 5 12 143.14 136.09 5.40 o 1 5 12 75.25 74.76 1.83 o 2 5 12 114.96 121.85 2.68 o 3 5 12 21.23 18.96 0.79 o 4 5 12 3.40 5.77 0.94 o 0 6 12 52.18 51.90 2.25 o 1 6 12 83.24 84.59 1.87 o 2 6 12 34.10 33.85 0.90 o 3 6 12 18.23 14.96 0.70 o 4 6 12 15.34 15.20 1.71 o 0 7 12 528.22 561.64 17.40 o 1 7 12 298.06 302.23 7.24 o 2 7 12 11.53 9.52 0.74 o 3 7 12 15.62 15.66 0.88 o 4 7 12 33.56 30.35 2.49 o 0 8 12 16.53 16.70 1.24 o 1 8 12 12.62 12.51 1.40 o 2 8 12 34.07 28.60 1.33 o 3 8 12 33.12 29.36 1.71 o 0 9 12 2.79 2.77 1.57 o 1 9 12 33.38 26.13 1.62 o 2 9 12 31.31 24.41 1.49 o 3 9 12 9.95 7.21 1.32 o 0 10 12 0.40 2.34 1.88 o 1 10 12 2.47 1.79 2.58 o 2 10 12 31.69 29.12 2.06 o 0 11 12 1.92 0.31 1.79 o 1 11 12 0.07 -0.55 1.07 o 2 11 12 12.20 8.95 1.93 o 0 12 12 6.20 8.22 2.66 o 1 12 12 9.49 7.92 1.35 o 1 0 13 80.02 84.69 2.18 o 2 0 13 48.35 47.85 1.40 o 3 0 13 2.81 4.78 1.32 o 4 0 13 21.85 26.08 1.35 o 0 1 13 256.08 268.59 6.11 o 1 1 13 59.64 62.13 1.29 o 2 1 13 197.33 198.61 5.35 o 3 1 13 122.49 120.42 3.86 o 4 1 13 32.58 27.59 1.07 o 0 2 13 391.68 438.74 9.69 o 1 2 13 24.87 23.34 0.95 o 2 2 13 477.31 480.81 11.27 o 3 2 13 160.90 156.96 3.86 o 4 2 13 17.65 15.50 0.86 o 0 3 13 140.66 149.00 4.11 o 1 3 13 29.53 29.22 1.44 o 2 3 13 207.12 203.42 3.81 o 3 3 13 22.89 27.30 1.11 o 4 3 13 10.34 9.89 0.95 o 0 4 13 33.87 32.66 2.38 o 1 4 13 139.89 134.99 3.15 o 2 4 13 225.93 229.16 4.33 o 3 4 13 16.28 9.93 0.78 o 4 4 13 11.23 10.21 0.99 o 0 5 13 163.23 176.70 5.60 o 1 5 13 325.74 332.36 6.63 o 2 5 13 24.21 21.29 0.85 o 3 5 13 22.69 23.01 1.53 o 4 5 13 16.77 13.22 1.09 o 0 6 13 96.96 88.90 4.46 o 1 6 13 418.19 426.92 8.72 o 2 6 13 41.16 37.06 1.33 o 3 6 13 33.11 31.34 1.24 o 4 6 13 14.74 15.39 1.33 o 0 7 13 276.32 282.95 9.34 o 1 7 13 105.45 107.70 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241.87 255.85 4.07 o 2 1 16 92.69 92.41 1.97 o 3 1 16 26.04 26.12 1.31 o 4 1 16 59.15 49.17 3.37 o 0 2 16 32.17 34.23 2.90 o 1 2 16 196.03 204.89 4.09 o 2 2 16 16.39 15.60 0.64 o 3 2 16 76.15 71.60 2.33 o 4 2 16 4.22 4.17 0.92 o 0 3 16 6.02 3.66 1.10 o 1 3 16 230.91 227.75 5.59 o 2 3 16 160.64 158.57 7.39 o 3 3 16 13.51 14.28 0.88 o 4 3 16 38.96 30.92 1.70 o 0 4 16 65.68 63.85 3.28 o 1 4 16 51.50 52.07 2.01 o 2 4 16 0.41 1.47 0.70 o 3 4 16 47.76 49.33 2.75 o 0 5 16 140.60 147.68 5.72 o 1 5 16 7.87 10.55 2.54 o 2 5 16 108.18 103.85 2.82 o 3 5 16 30.30 28.75 1.79 o 0 6 16 1.91 3.35 2.16 o 1 6 16 27.60 24.15 1.81 o 2 6 16 20.92 24.57 1.75 o 3 6 16 5.39 6.37 0.96 o 0 7 16 153.41 158.21 11.35 o 1 7 16 44.64 45.59 1.96 o 2 7 16 17.92 15.73 1.56 o 3 7 16 1.02 -0.75 1.35 o 0 8 16 62.84 79.39 12.32 o 1 8 16 13.43 11.14 2.08 o 2 8 16 1.83 2.41 1.05 o 0 9 16 47.78 51.07 3.38 o 1 9 16 1.09 -1.24 1.39 o 0 10 16 16.01 22.42 2.51 o 1 0 17 74.78 79.54 3.57 o 2 0 17 2.00 0.76 1.26 o 3 0 17 0.61 -0.89 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