#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/19/2201914.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201914_Fobs loop_ _publ_author_name 'Barnes, John C.' 'Weakley, Timothy J. R.' _publ_section_title ; Tetrahydro-2,6,6-trimethyl-1,4-pyran-2,5-dicarboxylic acid (cineolic acid) ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o728 _journal_page_last o730 _journal_volume 59 _journal_year 2003 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 86.935 _cell_angle_beta 88.987 _cell_angle_gamma 64.078 _cell_length_a 6.4737 _cell_length_b 6.5302 _cell_length_c 13.8836 _exptl_crystal_F_000 232.00 _reflns_d_resolution_high 0.6901 _[local]_cod_data_source_file cm6038IIsup2.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' Cineolic acid jcb54 - Low T version' _shelx_refln_list_code 4 _shelx_f_calc_maximum 74.68 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 75.18 82.95 0.97 o 2 0 0 127.58 156.86 2.23 o 3 0 0 0.77 0.70 0.10 o 4 0 0 52.75 54.29 1.05 o 5 0 0 110.45 110.06 1.63 o 6 0 0 203.89 213.36 3.18 o 7 0 0 3.49 4.30 0.35 o 8 0 0 0.00 0.03 0.18 o -7 1 0 22.41 21.73 0.79 o -6 1 0 26.85 24.27 0.71 o -5 1 0 37.86 36.97 0.55 o -4 1 0 24.13 20.59 0.33 o -3 1 0 17.88 21.01 0.32 o -2 1 0 4.90 3.60 0.10 o -1 1 0 570.85 612.70 12.56 o 0 1 0 126.19 134.99 1.59 o 1 1 0 1751.16 1760.65 24.76 o 2 1 0 2.04 1.28 0.06 o 3 1 0 0.66 1.13 0.09 o 4 1 0 582.23 615.73 7.17 o 5 1 0 117.01 108.31 1.47 o 6 1 0 175.74 173.55 3.93 o 7 1 0 64.54 66.83 1.59 o 8 1 0 7.11 7.81 0.50 o -6 2 0 111.35 115.45 2.68 o -5 2 0 48.09 42.63 0.78 o -4 2 0 25.14 21.69 0.36 o -3 2 0 51.11 47.41 0.63 o -2 2 0 539.19 571.58 6.68 o -1 2 0 290.25 330.34 3.83 o 0 2 0 1085.19 1136.39 16.49 o 1 2 0 341.84 320.19 3.74 o 2 2 0 189.85 200.98 2.32 o 3 2 0 210.72 231.90 3.23 o 4 2 0 359.79 394.03 4.52 o 5 2 0 194.22 198.54 2.92 o 6 2 0 94.71 92.76 2.04 o 7 2 0 87.85 81.94 1.87 o 8 2 0 23.87 24.94 0.60 o 9 2 0 5.60 5.48 0.47 o -5 3 0 0.00 0.02 0.08 o -4 3 0 118.10 108.06 1.68 o -2 3 0 173.33 187.73 2.21 o -1 3 0 3.43 2.70 0.10 o 0 3 0 994.50 1069.36 12.75 o 1 3 0 512.34 589.94 7.81 o 2 3 0 404.96 422.32 4.93 o 3 3 0 41.11 44.22 0.57 o 4 3 0 4.81 3.61 0.11 o 5 3 0 0.27 0.68 0.10 o 6 3 0 115.35 110.01 1.73 o 7 3 0 8.85 7.76 0.29 o 8 3 0 75.62 77.11 4.21 o 9 3 0 0.07 -0.05 0.26 o -5 4 0 0.77 0.96 0.19 o -4 4 0 23.70 21.66 0.70 o -3 4 0 17.15 13.84 0.35 o -2 4 0 315.15 310.52 4.39 o -1 4 0 289.89 309.45 3.59 o 0 4 0 91.17 95.88 1.17 o 1 4 0 170.73 215.14 2.50 o 2 4 0 6.94 7.63 0.16 o 3 4 0 70.36 73.22 0.91 o 4 4 0 266.41 280.06 3.25 o 5 4 0 1.31 1.06 0.42 o 6 4 0 206.70 211.67 3.14 o 7 4 0 0.91 0.49 0.13 o 8 4 0 3.60 3.66 0.24 o 9 4 0 6.02 6.87 0.40 o -4 5 0 9.89 9.80 0.48 o -3 5 0 16.07 15.35 0.40 o -2 5 0 95.56 93.24 1.47 o -1 5 0 7.54 6.45 0.28 o 0 5 0 23.57 21.96 0.46 o 1 5 0 14.35 16.15 0.37 o 2 5 0 20.95 23.46 0.36 o 3 5 0 39.03 31.27 0.46 o 4 5 0 45.27 43.46 0.68 o 5 5 0 6.68 5.86 0.23 o 6 5 0 0.10 0.11 0.11 o 7 5 0 47.40 44.85 0.86 o 8 5 0 8.10 8.33 0.34 o 9 5 0 0.21 0.06 0.14 o -3 6 0 7.96 8.19 0.46 o -2 6 0 67.42 61.90 1.09 o -1 6 0 6.35 6.50 0.31 o 0 6 0 34.61 36.40 0.70 o 1 6 0 22.57 23.93 0.51 o 2 6 0 47.77 46.62 0.82 o 4 6 0 654.41 659.27 13.01 o 5 6 0 103.12 102.14 1.62 o 6 6 0 103.23 103.64 1.66 o 7 6 0 36.95 37.67 0.76 o 8 6 0 27.63 27.89 0.72 o 9 6 0 1.17 1.19 0.22 o -2 7 0 21.90 21.02 0.80 o -1 7 0 0.65 0.31 0.14 o 0 7 0 45.44 44.99 1.15 o 1 7 0 0.00 0.11 0.17 o 2 7 0 3.86 4.22 0.22 o 3 7 0 0.89 0.71 0.12 o 4 7 0 54.95 57.17 1.23 o 5 7 0 57.30 54.30 1.41 o 6 7 0 22.68 22.46 0.77 o 7 7 0 0.03 0.31 0.19 o 8 7 0 0.44 0.73 0.24 o -1 8 0 98.75 105.33 2.53 o 0 8 0 5.64 7.00 0.43 o 1 8 0 45.33 45.90 1.90 o 2 8 0 4.43 4.48 0.24 o 3 8 0 3.98 4.16 0.23 o 4 8 0 21.38 21.73 0.52 o 5 8 0 0.03 -0.09 0.16 o 6 8 0 14.97 14.96 0.63 o 7 8 0 20.60 21.70 0.83 o 2 9 0 12.29 14.35 0.45 o 3 9 0 2.54 2.05 0.21 o 4 9 0 82.35 90.58 1.54 o 5 9 0 110.31 121.67 2.85 o 6 9 0 0.18 0.18 0.19 o -6 -9 1 34.78 37.00 1.17 o -5 -9 1 6.07 6.69 0.46 o -4 -9 1 12.38 13.28 0.62 o -3 -9 1 1.09 1.04 0.16 o -2 -9 1 3.52 3.88 0.44 o -7 -8 1 0.07 0.02 0.20 o -6 -8 1 22.60 23.13 0.82 o -5 -8 1 54.94 58.58 1.54 o -4 -8 1 0.20 0.21 0.14 o -3 -8 1 7.73 8.18 0.31 o -2 -8 1 14.70 13.85 0.41 o -1 -8 1 9.73 9.82 0.53 o 0 -8 1 238.77 267.32 4.63 o -8 -7 1 1.64 2.34 0.24 o -7 -7 1 4.46 4.67 0.39 o -6 -7 1 20.35 20.41 0.73 o -5 -7 1 15.18 14.48 0.58 o -4 -7 1 113.46 115.64 2.03 o -3 -7 1 24.43 27.70 1.09 o -2 -7 1 23.56 22.12 0.50 o -1 -7 1 9.37 6.84 0.33 o 0 -7 1 35.47 36.46 0.73 o 1 -7 1 129.93 131.94 2.07 o 2 -7 1 0.00 -0.08 0.17 o -9 -6 1 0.02 -0.13 0.13 o -8 -6 1 0.35 0.25 0.14 o -7 -6 1 41.77 41.78 0.83 o -6 -6 1 1.28 1.23 0.16 o -4 -6 1 30.91 31.58 0.49 o -3 -6 1 70.98 61.21 1.01 o -2 -6 1 8.73 9.76 0.29 o -1 -6 1 16.91 12.77 0.58 o 0 -6 1 21.00 17.58 0.42 o 1 -6 1 13.51 13.39 0.37 o 2 -6 1 41.43 39.12 1.12 o 3 -6 1 12.84 12.46 0.57 o -9 -5 1 3.87 4.09 0.28 o -8 -5 1 24.45 25.70 0.91 o -7 -5 1 1.67 1.90 0.19 o -6 -5 1 0.44 0.51 0.12 o -5 -5 1 19.04 17.27 0.41 o -4 -5 1 32.49 30.23 0.45 o -3 -5 1 341.10 348.37 4.03 o -2 -5 1 146.43 137.18 1.65 o -1 -5 1 0.00 -0.01 0.07 o 0 -5 1 60.26 48.99 0.83 o 2 -5 1 31.64 28.85 0.86 o 3 -5 1 0.55 1.08 0.18 o 4 -5 1 3.41 3.68 0.31 o -9 -4 1 7.58 7.74 0.35 o -8 -4 1 19.97 20.21 0.53 o -7 -4 1 118.43 116.01 1.86 o -6 -4 1 49.92 47.60 0.86 o -5 -4 1 14.67 13.77 0.50 o -4 -4 1 136.75 152.63 1.82 o -3 -4 1 65.39 74.53 0.93 o -2 -4 1 16.91 15.62 0.33 o -1 -4 1 14.36 14.79 0.25 o 0 -4 1 17.28 15.09 0.47 o 1 -4 1 318.56 322.66 3.74 o 2 -4 1 24.43 22.45 0.37 o 4 -4 1 0.85 0.80 0.16 o 5 -4 1 22.44 21.97 0.75 o -9 -3 1 0.03 0.03 0.12 o -8 -3 1 1.44 1.36 0.18 o -7 -3 1 33.44 33.86 0.70 o -6 -3 1 9.45 8.66 0.29 o -5 -3 1 326.89 347.71 5.00 o -4 -3 1 339.33 372.28 4.33 o -3 -3 1 126.35 136.01 1.60 o -2 -3 1 459.66 502.60 6.03 o -1 -3 1 3.44 4.81 0.16 o 0 -3 1 22.78 25.15 0.39 o 1 -3 1 340.79 380.17 4.36 o 2 -3 1 233.31 244.99 2.86 o 3 -3 1 47.53 40.52 1.01 o 4 -3 1 6.29 5.31 0.32 o 5 -3 1 1.07 1.64 0.16 o -9 -2 1 31.28 33.20 1.16 o -8 -2 1 0.73 0.77 0.20 o -7 -2 1 22.23 21.93 0.75 o -6 -2 1 278.26 274.19 4.02 o -5 -2 1 28.66 29.84 0.59 o -4 -2 1 157.95 177.42 2.08 o -3 -2 1 54.30 63.24 0.77 o -2 -2 1 189.77 212.23 2.44 o 0 -2 1 925.45 974.62 14.75 o 1 -2 1 466.17 479.75 5.60 o 2 -2 1 11.82 10.74 0.26 o 3 -2 1 33.64 41.03 0.56 o 4 -2 1 143.01 134.41 1.64 o 5 -2 1 256.80 267.71 3.92 o 6 -2 1 74.98 80.99 2.00 o 7 -2 1 20.10 20.99 0.80 o -8 -1 1 19.71 21.87 0.56 o -7 -1 1 45.45 45.31 0.87 o -6 -1 1 9.99 7.50 0.46 o -5 -1 1 124.95 128.46 2.24 o -4 -1 1 6.41 6.89 0.15 o -3 -1 1 74.50 61.41 0.75 o -2 -1 1 71.87 72.89 1.08 o -1 -1 1 21.36 24.45 0.30 o 0 -1 1 5576.83 5535.44 111.50 o 1 -1 1 360.26 367.24 4.48 o 2 -1 1 298.17 344.69 3.99 o 3 -1 1 20.38 24.88 0.36 o 4 -1 1 26.80 26.44 0.50 o 5 -1 1 201.44 192.45 2.30 o 6 -1 1 0.55 0.45 0.17 o 7 -1 1 0.05 0.08 0.16 o -8 0 1 2.46 2.04 0.33 o -7 0 1 23.98 26.66 0.60 o -6 0 1 8.99 8.98 0.64 o -5 0 1 26.34 22.53 0.43 o -4 0 1 28.05 30.12 0.43 o -3 0 1 634.88 678.33 8.15 o -2 0 1 183.21 209.20 2.41 o 2 0 1 134.85 149.03 1.73 o 3 0 1 248.89 276.89 4.59 o 4 0 1 280.17 293.67 3.40 o 5 0 1 1.36 1.36 0.11 o 6 0 1 6.63 8.14 0.28 o 7 0 1 29.27 28.98 0.94 o -7 1 1 2.40 2.05 0.30 o -6 1 1 32.09 29.04 1.40 o -5 1 1 11.75 6.23 0.31 o -4 1 1 115.29 115.25 2.86 o -3 1 1 200.85 211.16 2.46 o -2 1 1 399.30 450.84 5.34 o -1 1 1 2132.39 2128.86 42.42 o 0 1 1 304.23 310.65 7.00 o 1 1 1 1685.72 1699.57 34.26 o 2 1 1 7.17 5.72 0.11 o 3 1 1 67.64 76.37 0.93 o 4 1 1 164.28 180.46 2.12 o 5 1 1 378.11 393.62 5.47 o 6 1 1 0.97 0.79 0.15 o 7 1 1 28.15 29.45 0.63 o -6 2 1 26.81 27.33 0.59 o -5 2 1 4.69 4.45 0.20 o -4 2 1 50.56 40.41 0.58 o -3 2 1 2.08 1.85 0.14 o -2 2 1 42.54 41.92 0.55 o -1 2 1 81.47 83.09 0.99 o 0 2 1 3206.73 2595.03 51.67 o 1 2 1 957.16 962.41 20.09 o 2 2 1 60.11 71.62 0.86 o 3 2 1 624.00 651.36 7.88 o 4 2 1 7.13 8.66 0.17 o 5 2 1 270.90 264.82 3.09 o 7 2 1 5.77 4.18 0.36 o 8 2 1 16.37 16.70 0.72 o 9 2 1 6.18 6.79 0.50 o -5 3 1 6.32 5.49 0.23 o -3 3 1 78.08 71.92 3.56 o -2 3 1 28.85 30.78 0.44 o -1 3 1 1210.25 1310.33 15.68 o 0 3 1 0.55 0.94 0.11 o 1 3 1 1813.26 1781.17 36.03 o 2 3 1 93.46 98.52 1.17 o 3 3 1 38.32 39.13 0.51 o 4 3 1 266.49 263.53 3.05 o 5 3 1 5.69 8.27 0.21 o 6 3 1 20.60 17.85 0.42 o 7 3 1 5.26 3.96 0.22 o 8 3 1 23.41 24.78 0.59 o 9 3 1 5.38 6.40 0.54 o -5 4 1 2.17 2.23 0.25 o -4 4 1 2.57 2.22 0.17 o -3 4 1 20.19 18.34 0.42 o -2 4 1 66.96 66.05 1.41 o -1 4 1 1.41 1.73 0.14 o 0 4 1 175.80 203.56 2.38 o 1 4 1 92.81 98.41 1.46 o 3 4 1 214.03 220.31 2.57 o 4 4 1 55.62 58.05 0.76 o 5 4 1 20.18 20.42 0.36 o 6 4 1 47.44 47.48 0.85 o 7 4 1 72.84 67.16 1.16 o 8 4 1 20.83 21.43 0.65 o 9 4 1 13.19 13.51 0.46 o -4 5 1 2.67 2.59 0.27 o -3 5 1 0.98 0.83 0.13 o -2 5 1 11.05 10.89 0.32 o -1 5 1 8.88 8.76 0.39 o 0 5 1 63.98 59.96 1.40 o 1 5 1 327.42 375.07 10.86 o 2 5 1 1.51 0.89 0.11 o 3 5 1 43.73 42.00 0.58 o 4 5 1 4.83 4.00 0.22 o 5 5 1 0.09 0.07 0.06 o 6 5 1 261.17 251.98 3.71 o 7 5 1 8.01 7.61 0.29 o 8 5 1 40.12 39.51 1.10 o 9 5 1 7.27 7.89 0.53 o -3 6 1 0.17 0.15 0.16 o -2 6 1 5.01 4.86 0.25 o -1 6 1 0.83 1.34 0.16 o 0 6 1 1.05 0.94 0.32 o 1 6 1 15.99 10.67 0.31 o 2 6 1 0.25 0.13 0.16 o 3 6 1 23.60 18.53 0.44 o 4 6 1 71.20 66.52 1.18 o 5 6 1 119.53 118.53 1.84 o 6 6 1 36.43 36.91 0.72 o 7 6 1 28.82 28.08 1.15 o 8 6 1 16.76 16.54 0.47 o 9 6 1 1.30 0.68 0.17 o -2 7 1 19.45 19.47 0.52 o -1 7 1 76.44 78.35 2.52 o 0 7 1 11.35 10.46 0.34 o 1 7 1 49.91 48.52 0.89 o 2 7 1 28.25 26.40 0.57 o 3 7 1 39.35 32.96 0.65 o 4 7 1 4.62 3.14 0.19 o 5 7 1 2.02 2.62 0.29 o 6 7 1 8.17 7.51 0.42 o 7 7 1 42.42 44.23 1.25 o 8 7 1 9.39 9.51 0.53 o -1 8 1 4.58 3.94 0.27 o 0 8 1 1.15 1.43 0.18 o 1 8 1 2.31 2.76 0.21 o 2 8 1 0.11 0.28 0.11 o 3 8 1 1.07 1.18 0.15 o 4 8 1 36.18 39.24 0.92 o 5 8 1 107.14 110.75 2.56 o 6 8 1 5.75 6.12 0.44 o 7 8 1 32.28 34.64 1.09 o 2 9 1 2.97 3.71 0.25 o 3 9 1 33.64 35.28 0.76 o 4 9 1 94.10 100.38 1.67 o 5 9 1 114.10 125.25 2.91 o 6 9 1 20.84 20.06 0.80 o -6 -9 2 0.31 0.32 0.20 o -5 -9 2 28.47 27.78 0.95 o -4 -9 2 18.63 21.97 0.82 o -3 -9 2 53.70 58.58 1.10 o -2 -9 2 2.12 2.39 0.22 o -7 -8 2 3.90 3.72 0.36 o -6 -8 2 17.12 16.90 0.68 o -5 -8 2 0.00 0.07 0.16 o -4 -8 2 0.08 0.17 0.17 o -3 -8 2 25.06 25.34 0.58 o -2 -8 2 21.84 23.27 0.55 o -1 -8 2 9.82 9.75 0.54 o 0 -8 2 5.40 3.78 0.36 o -8 -7 2 0.26 0.29 0.16 o -7 -7 2 10.75 9.88 0.38 o -6 -7 2 20.82 19.90 0.72 o -5 -7 2 78.12 75.19 1.81 o -4 -7 2 0.84 0.46 0.11 o -3 -7 2 49.58 50.99 1.25 o -2 -7 2 37.52 37.44 0.72 o -1 -7 2 34.50 38.43 0.79 o 0 -7 2 127.43 132.01 2.35 o 1 -7 2 5.39 4.45 0.35 o 2 -7 2 5.49 5.29 0.43 o -9 -6 2 0.00 0.01 0.15 o -8 -6 2 105.75 106.46 1.79 o -7 -6 2 2.62 2.99 0.23 o -6 -6 2 56.85 56.76 1.03 o -5 -6 2 24.17 21.98 1.03 o -4 -6 2 77.25 66.74 0.89 o -3 -6 2 134.75 132.30 3.52 o -2 -6 2 90.59 88.19 1.38 o -1 -6 2 6.57 8.39 0.27 o 0 -6 2 90.12 79.12 1.73 o 1 -6 2 10.54 10.19 0.32 o 2 -6 2 0.13 0.11 0.14 o 3 -6 2 4.04 4.25 0.36 o -9 -5 2 13.38 14.36 0.48 o -8 -5 2 0.19 0.54 0.15 o -7 -5 2 7.95 7.26 0.29 o -6 -5 2 60.67 56.94 1.01 o -5 -5 2 92.75 86.81 1.39 o -4 -5 2 92.51 108.80 2.07 o -3 -5 2 56.89 55.58 0.74 o -2 -5 2 0.70 0.93 0.09 o -1 -5 2 56.84 49.68 0.67 o 0 -5 2 39.11 40.63 0.72 o 1 -5 2 654.98 651.37 9.04 o 2 -5 2 3.07 2.02 0.24 o 3 -5 2 10.99 10.30 0.48 o 4 -5 2 0.17 0.21 0.16 o -9 -4 2 0.06 -0.02 0.14 o -8 -4 2 5.58 6.28 0.30 o -7 -4 2 2.75 2.42 0.24 o -6 -4 2 1.10 0.60 0.12 o -5 -4 2 17.79 20.42 1.25 o -4 -4 2 42.29 50.45 0.70 o -3 -4 2 18.20 20.20 0.32 o -2 -4 2 46.45 52.84 0.68 o -1 -4 2 57.96 65.63 0.83 o 0 -4 2 62.29 54.41 0.71 o 1 -4 2 3.31 4.65 0.22 o 2 -4 2 3.12 4.21 0.25 o 3 -4 2 2.69 2.97 0.73 o 4 -4 2 22.46 22.31 0.73 o -9 -3 2 2.97 2.67 0.23 o -8 -3 2 48.91 47.47 1.17 o -7 -3 2 2.50 2.47 0.20 o -6 -3 2 98.70 98.40 1.58 o -5 -3 2 4.01 3.77 0.20 o -4 -3 2 60.01 57.56 0.77 o -3 -3 2 58.35 59.03 0.74 o -2 -3 2 10.24 11.17 0.19 o -1 -3 2 230.94 251.97 2.90 o 0 -3 2 962.49 1071.87 12.90 o 1 -3 2 226.33 233.04 2.71 o 2 -3 2 29.58 33.23 0.63 o 3 -3 2 34.04 34.84 0.58 o 4 -3 2 1.19 1.21 0.17 o 5 -3 2 51.34 53.00 0.97 o 6 -3 2 129.85 136.62 7.57 o -9 -2 2 22.77 24.33 0.64 o -8 -2 2 11.74 12.70 0.41 o -7 -2 2 7.00 5.98 0.27 o -6 -2 2 109.88 108.10 1.89 o -5 -2 2 33.29 36.61 0.67 o -4 -2 2 146.26 183.86 2.69 o -3 -2 2 0.18 0.10 0.05 o -2 -2 2 36.56 34.82 0.44 o -1 -2 2 327.13 349.38 5.35 o 0 -2 2 17.15 22.09 0.30 o 1 -2 2 6.46 5.69 0.12 o 2 -2 2 21.86 23.90 0.35 o 3 -2 2 0.17 0.13 0.05 o 4 -2 2 2.30 2.05 0.28 o 5 -2 2 14.19 13.05 0.36 o 6 -2 2 19.98 21.28 0.52 o 7 -2 2 37.19 37.92 1.18 o -8 -1 2 1.74 1.53 0.19 o -7 -1 2 37.13 38.55 0.78 o -6 -1 2 57.01 54.06 0.96 o -5 -1 2 99.10 88.90 6.52 o -4 -1 2 7.12 7.99 0.16 o -3 -1 2 65.30 61.98 1.03 o -2 -1 2 1.51 0.10 0.04 o -1 -1 2 1501.13 1512.13 29.85 o 0 -1 2 1.51 0.97 0.14 o 1 -1 2 292.05 315.03 3.75 o 2 -1 2 31.61 31.28 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