#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2201930.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201930_Fobs loop_ _publ_author_name 'Jones, Matthew D.' 'Almeida Paz, Filipe A.' 'Davies, John E.' 'Johnson, Brian F. G.' _publ_section_title ; (\h^3^-Allyl)[(S)-(+)-(2-pyrrolidinylmethyl)pyrrolidine]palladium(II) trifluoromethanesulfonate ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m105 _journal_page_last m107 _journal_volume 59 _journal_year 2003 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.1222 _cell_length_b 9.1647 _cell_length_c 20.6053 _exptl_crystal_F_000 912.00 _reflns_d_resolution_high 0.7707 _[local]_cod_data_source_file cv6171Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' bj0239 in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 199.27 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 1085.26 1005.13 42.46 o 6 0 0 2215.37 2302.79 86.30 o 8 0 0 4809.17 4733.65 312.00 o 10 0 0 3496.40 3713.35 295.54 o 2 1 0 22.95 43.89 11.90 o 3 1 0 3.77 13.64 7.23 o 4 1 0 6607.79 6368.48 139.07 o 5 1 0 817.92 829.26 42.09 o 6 1 0 2984.87 3035.51 117.26 o 7 1 0 118.83 140.39 22.62 o 8 1 0 0.99 21.86 46.19 o 9 1 0 2631.29 2718.56 145.89 o 10 1 0 131.89 29.37 83.86 o 11 1 0 836.88 950.52 167.44 o 0 2 0 10669.29 777.22 5193.28 o 1 2 0 912.49 758.19 59.45 o 2 2 0 122.15 135.14 12.69 o 3 2 0 15883.32 16091.52 376.82 o 4 2 0 2603.44 2552.96 61.99 o 5 2 0 16650.53 16719.43 391.48 o 6 2 0 23.63 29.90 16.98 o 7 2 0 2034.42 2006.69 77.78 o 8 2 0 9.86 51.72 23.62 o 9 2 0 84.91 40.23 26.00 o 10 2 0 196.08 190.81 43.86 o 11 2 0 301.81 372.01 97.95 o 1 3 0 5134.17 4523.97 81.99 o 2 3 0 2966.28 3026.40 55.56 o 3 3 0 22.79 19.24 8.48 o 4 3 0 3214.26 3017.55 87.54 o 5 3 0 1362.52 1350.44 35.43 o 6 3 0 1211.61 1278.27 67.85 o 7 3 0 3710.82 3831.76 123.95 o 8 3 0 311.03 259.64 30.80 o 9 3 0 2485.18 2582.73 142.49 o 10 3 0 97.04 156.28 46.46 o 11 3 0 471.63 494.73 209.58 o 0 4 0 15918.73 15990.77 373.65 o 1 4 0 1800.03 1734.43 45.80 o 2 4 0 11696.00 11343.89 210.58 o 3 4 0 254.30 267.90 28.12 o 4 4 0 5350.60 5604.16 121.13 o 5 4 0 3289.87 3467.88 88.56 o 6 4 0 9.43 29.52 12.95 o 7 4 0 126.05 151.16 21.46 o 8 4 0 1369.07 1325.28 95.69 o 9 4 0 26.58 11.24 47.86 o 10 4 0 2099.67 2269.41 151.92 o 11 4 0 119.65 195.27 60.42 o 1 5 0 714.41 681.02 14.78 o 2 5 0 2280.58 2284.42 45.34 o 3 5 0 1.41 3.66 6.02 o 4 5 0 6375.42 6568.15 150.19 o 5 5 0 505.94 522.49 21.94 o 6 5 0 4166.87 4164.56 130.30 o 7 5 0 1078.84 1128.23 44.97 o 8 5 0 907.47 817.96 57.03 o 9 5 0 236.14 261.32 35.11 o 10 5 0 0.96 -10.70 36.09 o 0 6 0 7669.65 7781.42 205.33 o 1 6 0 112.49 111.02 10.07 o 2 6 0 2659.24 2794.40 65.94 o 3 6 0 5158.25 5093.17 107.78 o 4 6 0 138.15 136.00 24.46 o 5 6 0 4520.82 4622.53 142.66 o 6 6 0 611.78 624.52 43.30 o 7 6 0 1008.19 1034.95 46.12 o 8 6 0 700.30 713.26 87.93 o 9 6 0 6.87 68.37 39.07 o 10 6 0 402.52 461.03 103.54 o 1 7 0 4272.42 4388.72 106.90 o 2 7 0 511.94 485.04 18.36 o 3 7 0 563.77 591.80 20.99 o 4 7 0 22.41 33.93 8.95 o 5 7 0 24.64 15.14 10.44 o 6 7 0 133.13 176.24 24.44 o 7 7 0 937.05 925.64 60.20 o 8 7 0 1.73 26.81 51.63 o 9 7 0 1559.21 1313.60 173.58 o 0 8 0 5176.95 5068.14 197.87 o 1 8 0 218.28 217.34 17.47 o 2 8 0 2116.69 2057.29 63.37 o 3 8 0 137.76 161.22 20.31 o 4 8 0 75.64 78.31 12.02 o 5 8 0 614.18 668.25 82.05 o 6 8 0 155.70 116.64 27.23 o 7 8 0 629.26 644.10 103.82 o 8 8 0 559.77 652.19 109.40 o 1 9 0 401.11 406.90 25.08 o 2 9 0 2905.82 2846.71 186.12 o 3 9 0 239.56 319.86 70.19 o 4 9 0 4743.11 5247.64 246.98 o 5 9 0 3.79 18.59 77.02 o 6 9 0 2575.97 2592.60 227.00 o 7 9 0 243.59 293.89 55.12 o 0 10 0 921.81 952.20 98.51 o 1 10 0 22.42 78.98 42.70 o 2 10 0 1303.83 1272.58 128.37 o 3 10 0 281.47 217.12 59.16 o 4 10 0 341.41 286.47 44.00 o 5 10 0 643.68 620.22 69.46 o 6 10 0 39.69 109.72 106.89 o 1 11 0 1367.03 1421.04 174.70 o 2 11 0 10.70 -23.16 52.74 o 3 11 0 320.06 340.19 69.21 o 4 11 0 21.85 -32.93 52.74 o 2 0 1 39709.78 3335.26 16599.53 o 3 0 1 8369.75 8280.71 193.79 o 4 0 1 11402.71 10305.55 237.43 o 5 0 1 392.98 347.00 27.83 o 6 0 1 8644.60 8571.92 305.81 o 7 0 1 1570.42 1481.85 52.99 o 8 0 1 1982.02 1938.28 102.90 o 9 0 1 327.51 267.23 41.75 o 10 0 1 37.15 23.25 31.31 o 11 0 1 66.46 74.44 49.47 o -11 1 1 271.20 310.36 92.23 o -10 1 1 780.55 762.95 75.10 o -9 1 1 680.87 654.79 56.78 o -8 1 1 1894.61 1890.72 79.03 o -7 1 1 3013.04 3023.61 135.19 o -6 1 1 1802.80 1785.57 53.89 o -5 1 1 658.47 641.33 38.91 o -4 1 1 1890.57 1739.48 43.47 o -3 1 1 5540.89 5444.88 125.06 o -2 1 1 33093.11 26217.34 5020.36 o 2 1 1 34016.60 28593.52 3625.58 o 3 1 1 5778.17 5691.21 137.52 o 4 1 1 1846.41 1636.83 46.04 o 5 1 1 701.91 621.54 25.67 o 6 1 1 1809.51 1792.45 75.17 o 7 1 1 3047.08 2947.65 90.81 o 8 1 1 1928.19 1843.26 86.62 o 9 1 1 724.67 902.82 87.91 o 10 1 1 829.44 917.85 90.56 o 11 1 1 258.45 234.59 114.14 o -11 2 1 940.09 991.18 96.34 o -10 2 1 163.32 215.79 52.61 o -9 2 1 1942.96 2012.68 120.86 o -8 2 1 1472.00 1545.49 79.07 o -7 2 1 1655.30 1591.80 67.00 o -6 2 1 1111.51 1099.41 39.15 o -5 2 1 435.75 468.73 21.33 o -4 2 1 81.39 103.52 9.91 o -3 2 1 5078.37 4686.50 105.29 o -2 2 1 3222.32 3128.48 66.48 o -1 2 1 2780.00 2603.93 181.74 o 0 2 1 278.36 233.04 1455.02 o 1 2 1 2298.28 2145.07 42.62 o 2 2 1 2990.52 3029.72 64.50 o 3 2 1 4986.72 4610.53 93.04 o 4 2 1 81.56 80.40 10.84 o 5 2 1 400.48 393.93 25.46 o 6 2 1 1124.46 1040.70 39.09 o 7 2 1 1643.58 1670.12 68.51 o 8 2 1 1463.75 1477.17 92.65 o 9 2 1 1891.22 1906.98 99.57 o 10 2 1 141.13 230.45 102.28 o 11 2 1 951.10 941.54 87.12 o -11 3 1 450.06 530.83 71.93 o -10 3 1 260.23 258.49 72.00 o -9 3 1 163.32 204.33 44.87 o -8 3 1 724.76 691.12 49.21 o -7 3 1 1930.02 1893.79 72.59 o -6 3 1 780.95 766.09 32.83 o -5 3 1 7977.43 8146.20 184.64 o -4 3 1 1021.03 1042.73 42.82 o -3 3 1 12636.10 12400.54 222.44 o -2 3 1 422.07 414.72 13.85 o -1 3 1 3015.40 2920.14 48.18 o 0 3 1 1300.15 1124.78 21.40 o 1 3 1 2935.16 2838.05 53.10 o 2 3 1 477.52 461.88 14.24 o 3 3 1 12694.85 12531.72 239.20 o 4 3 1 1080.01 1160.27 28.24 o 5 3 1 8078.56 8368.85 205.65 o 6 3 1 759.80 800.85 35.71 o 7 3 1 1853.72 1786.60 78.56 o 8 3 1 777.55 832.54 70.53 o 9 3 1 178.83 166.87 30.52 o 10 3 1 289.82 434.66 135.49 o 11 3 1 455.67 574.00 162.70 o -11 4 1 128.17 63.33 68.37 o -10 4 1 24.08 73.61 40.34 o -9 4 1 329.61 322.73 44.39 o -8 4 1 1507.17 1519.71 106.20 o -7 4 1 1156.91 1109.86 66.99 o -6 4 1 6042.54 6260.48 176.79 o -5 4 1 1542.04 1511.69 37.85 o -4 4 1 5442.44 5429.35 107.89 o -3 4 1 3372.39 3440.57 68.13 o -2 4 1 2940.78 2934.02 54.91 o -1 4 1 3014.31 2880.47 45.54 o 0 4 1 3148.20 3337.52 57.39 o 1 4 1 3068.39 2990.94 57.86 o 2 4 1 2926.76 2937.53 54.50 o 3 4 1 3455.90 3539.12 67.89 o 4 4 1 5244.96 5092.78 137.89 o 5 4 1 1540.51 1500.15 55.97 o 6 4 1 6117.23 6269.04 182.02 o 7 4 1 1176.39 1152.17 52.31 o 8 4 1 1525.51 1706.80 122.57 o 9 4 1 341.53 433.63 51.30 o 10 4 1 26.21 93.90 54.98 o 11 4 1 126.44 52.19 65.02 o -10 5 1 1384.63 1322.99 117.90 o -9 5 1 177.34 227.67 46.33 o -8 5 1 1671.31 1732.78 71.61 o -7 5 1 703.35 663.40 36.46 o -6 5 1 221.21 241.76 17.11 o -5 5 1 682.98 654.79 28.61 o -4 5 1 1131.37 1172.83 29.72 o -3 5 1 1730.54 1732.87 42.34 o -2 5 1 9709.78 9815.36 161.29 o -1 5 1 2163.81 2120.35 37.80 o 0 5 1 11194.70 11505.72 181.18 o 1 5 1 2238.27 2217.08 44.71 o 2 5 1 9532.63 9898.49 212.62 o 3 5 1 1814.02 1845.76 42.12 o 4 5 1 1088.86 1090.46 29.93 o 5 5 1 688.24 715.05 25.28 o 6 5 1 249.50 257.22 25.30 o 7 5 1 711.13 699.83 42.90 o 8 5 1 1676.48 1700.23 112.71 o 9 5 1 175.43 170.89 63.77 o 10 5 1 1347.34 1319.75 165.21 o -10 6 1 228.10 270.70 63.63 o -9 6 1 1168.60 1248.37 119.15 o -8 6 1 151.72 241.13 36.05 o -7 6 1 1965.90 1966.03 86.82 o -6 6 1 545.18 533.98 32.45 o -5 6 1 421.51 415.71 20.51 o -4 6 1 3923.76 3954.92 99.88 o -3 6 1 1606.85 1641.17 39.15 o -2 6 1 2423.03 2463.49 48.62 o -1 6 1 6095.97 6034.15 121.65 o 0 6 1 75.21 79.25 6.33 o 1 6 1 6164.00 6180.41 116.52 o 2 6 1 2500.44 2543.93 60.72 o 3 6 1 1619.29 1663.38 54.60 o 4 6 1 3861.98 3976.62 92.18 o 5 6 1 386.71 384.37 21.70 o 6 6 1 552.59 562.49 28.06 o 7 6 1 1993.21 1950.97 89.26 o 8 6 1 163.13 126.41 30.12 o 9 6 1 1187.92 1293.75 100.70 o 10 6 1 235.34 313.68 110.23 o -9 7 1 79.30 86.79 66.70 o -8 7 1 37.92 23.36 31.12 o -7 7 1 868.67 958.30 60.31 o -6 7 1 368.52 360.06 33.70 o -5 7 1 2001.33 2110.94 84.61 o -4 7 1 1238.86 1213.74 41.29 o -3 7 1 1961.90 1965.41 57.17 o -2 7 1 1118.89 1124.58 30.51 o -1 7 1 655.14 653.25 19.36 o 0 7 1 6.92 13.95 5.90 o 1 7 1 690.24 704.27 28.47 o 2 7 1 1116.59 1117.19 39.88 o 3 7 1 1934.88 1993.02 58.75 o 4 7 1 1308.92 1348.66 49.68 o 5 7 1 2083.84 2124.56 92.38 o 6 7 1 372.53 328.69 42.77 o 7 7 1 902.49 1008.48 77.18 o 8 7 1 39.80 -3.94 35.99 o 9 7 1 79.78 -16.74 66.70 o -8 8 1 195.44 142.01 47.14 o -7 8 1 689.44 584.56 50.38 o -6 8 1 577.11 566.21 43.66 o -5 8 1 184.90 181.17 30.97 o -4 8 1 1627.83 1618.55 76.00 o -3 8 1 176.67 193.51 18.80 o -2 8 1 1793.52 1626.91 83.11 o -1 8 1 1285.06 1276.48 39.99 o 0 8 1 813.52 827.68 35.36 o 1 8 1 1352.23 1372.45 46.52 o 2 8 1 1771.82 1793.80 68.52 o 3 8 1 200.90 202.21 15.52 o 4 8 1 1522.86 1563.89 66.75 o 5 8 1 196.39 234.60 25.17 o 6 8 1 535.53 543.76 52.39 o 7 8 1 686.44 663.01 71.76 o 8 8 1 184.06 223.43 57.35 o -7 9 1 130.57 107.46 38.15 o -6 9 1 461.52 478.97 84.70 o -5 9 1 270.37 255.29 40.49 o -4 9 1 121.02 117.04 48.56 o -3 9 1 421.70 371.07 38.49 o -2 9 1 3167.35 3060.84 196.78 o -1 9 1 276.76 268.92 37.73 o 0 9 1 6170.71 6704.49 250.74 o 1 9 1 271.87 341.46 26.61 o 2 9 1 3243.63 3267.10 221.31 o 3 9 1 419.56 338.04 39.79 o 4 9 1 115.54 119.87 47.16 o 5 9 1 264.33 253.72 43.73 o 6 9 1 474.29 469.19 60.45 o 7 9 1 122.48 158.79 51.95 o -6 10 1 1165.89 1098.94 92.67 o -5 10 1 240.29 193.96 41.58 o -4 10 1 1683.79 1676.59 144.03 o -3 10 1 448.75 506.65 48.94 o -2 10 1 845.12 862.06 95.72 o -1 10 1 520.36 545.74 57.92 o 0 10 1 682.88 713.03 85.12 o 1 10 1 492.68 383.17 72.00 o 2 10 1 810.75 704.38 95.16 o 3 10 1 436.58 586.61 88.47 o 4 10 1 1669.83 1520.95 157.40 o 5 10 1 251.91 314.79 95.16 o 6 10 1 1187.85 1169.65 96.59 o -4 11 1 145.19 106.05 76.19 o -3 11 1 1157.38 1160.95 152.65 o -2 11 1 75.27 16.47 49.68 o 0 11 1 1.88 6.42 55.81 o 1 11 1 349.25 282.42 78.70 o 2 11 1 81.30 111.63 75.63 o 3 11 1 1176.96 1111.55 131.72 o 4 11 1 132.78 6.70 88.75 o 2 0 2 23922.08 1309.61 5576.66 o 3 0 2 1353.39 1345.65 38.71 o 4 0 2 594.02 522.10 26.32 o 5 0 2 29.86 35.53 11.68 o 6 0 2 1043.75 1013.52 35.53 o 7 0 2 44.98 60.69 23.00 o 8 0 2 3364.52 3330.80 210.14 o 9 0 2 2897.42 3113.93 146.71 o 10 0 2 1103.79 1105.91 85.45 o 11 0 2 1025.89 1123.40 92.06 o -11 1 2 342.57 288.32 55.47 o -10 1 2 525.18 557.79 59.15 o -9 1 2 1096.97 1067.44 72.37 o -8 1 2 1615.05 1519.87 70.82 o -7 1 2 1881.50 1752.11 76.01 o -6 1 2 2707.46 2784.07 111.01 o -5 1 2 6801.20 6536.56 242.49 o -4 1 2 3928.59 3691.50 84.25 o -3 1 2 4482.66 4364.93 100.29 o -2 1 2 8516.44 7936.13 201.33 o -1 1 2 15849.63 595.98 2524.25 o 1 1 2 16089.85 1175.11 4651.22 o 2 1 2 8662.24 8279.03 191.17 o 3 1 2 4370.15 4318.02 92.97 o 4 1 2 3847.77 3696.61 86.76 o 5 1 2 6927.34 6613.44 155.57 o 6 1 2 2767.42 2781.62 76.53 o 7 1 2 1895.06 1881.81 63.13 o 8 1 2 1616.82 1537.83 76.17 o 9 1 2 1116.39 1256.67 107.72 o 10 1 2 493.80 426.00 80.37 o 11 1 2 354.53 401.76 99.63 o -11 2 2 233.44 254.83 58.87 o -10 2 2 207.14 192.38 42.89 o -9 2 2 106.88 102.07 30.71 o -8 2 2 221.07 251.85 41.02 o -7 2 2 1060.73 1012.99 48.32 o -6 2 2 2112.38 2105.33 72.54 o -5 2 2 3070.50 3091.91 75.49 o -4 2 2 2439.87 2222.87 55.07 o -3 2 2 7331.13 7085.18 163.96 o -2 2 2 1176.10 1129.45 24.53 o -1 2 2 12867.97 12852.43 242.57 o 0 2 2 665.37 651.26 66.13 o 1 2 2 13233.03 13387.42 287.72 o 2 2 2 1149.82 1090.85 31.12 o 3 2 2 7390.33 7205.32 152.86 o 4 2 2 2611.82 2504.20 75.47 o 5 2 2 2920.54 2907.09 65.99 o 6 2 2 2128.14 2183.61 71.37 o 7 2 2 958.33 968.57 40.26 o 8 2 2 276.83 311.10 31.68 o 9 2 2 90.53 108.04 41.06 o 10 2 2 222.06 224.87 37.74 o 11 2 2 230.47 235.43 54.16 o -11 3 2 416.69 403.26 94.33 o -10 3 2 1468.27 1525.33 154.75 o -9 3 2 1278.80 1305.63 91.30 o -8 3 2 656.57 624.26 48.71 o -7 3 2 1858.08 1933.91 93.84 o -6 3 2 283.97 271.21 19.97 o -5 3 2 652.01 656.90 24.29 o -4 3 2 3440.85 3454.70 71.85 o -3 3 2 7927.71 7962.99 159.85 o -2 3 2 3723.60 3564.28 74.30 o -1 3 2 5440.71 5188.19 91.61 o 0 3 2 8733.21 8546.96 151.08 o 1 3 2 5432.70 5144.12 103.39 o 2 3 2 3584.24 3382.15 74.63 o 3 3 2 7966.52 8071.22 160.63 o 4 3 2 3501.64 3564.50 74.35 o 5 3 2 645.67 665.66 26.59 o 6 3 2 307.51 299.88 17.99 o 7 3 2 1810.08 1752.06 69.24 o 8 3 2 624.40 576.65 41.65 o 9 3 2 1212.10 1239.30 67.63 o 10 3 2 1475.27 1688.88 110.61 o 11 3 2 411.01 391.42 72.28 o -11 4 2 267.20 168.38 57.73 o -10 4 2 579.67 595.56 68.53 o -9 4 2 1109.68 1217.50 92.46 o -8 4 2 1750.88 1891.40 86.73 o -7 4 2 2429.89 2541.34 89.60 o -6 4 2 647.59 685.68 34.01 o -5 4 2 958.98 988.69 41.30 o -4 4 2 1589.94 1739.41 44.79 o -3 4 2 3700.92 3781.50 74.93 o -2 4 2 3034.25 3037.95 49.92 o -1 4 2 9549.27 9308.64 162.17 o 0 4 2 9494.99 9245.11 178.83 o 1 4 2 9592.76 9436.78 186.90 o 2 4 2 3154.77 3151.40 70.11 o 3 4 2 3751.42 3825.44 78.66 o 4 4 2 1561.90 1703.39 38.65 o 5 4 2 1044.38 1106.91 33.87 o 6 4 2 655.60 614.98 40.78 o 7 4 2 2420.19 2581.71 100.69 o 8 4 2 1750.45 1838.45 74.79 o 9 4 2 1116.00 1254.92 93.07 o 10 4 2 587.45 531.27 96.56 o 11 4 2 281.20 326.84 63.84 o -10 5 2 122.41 54.54 52.05 o -9 5 2 179.08 111.96 45.48 o -8 5 2 487.54 548.62 39.68 o -7 5 2 773.13 816.86 37.01 o -6 5 2 2938.12 2912.51 91.70 o -5 5 2 6661.69 6670.12 176.81 o -4 5 2 6213.04 6097.60 136.64 o -3 5 2 5260.32 5089.63 100.86 o -2 5 2 3455.81 3532.26 58.29 o -1 5 2 1421.62 1335.05 28.36 o 0 5 2 121.09 136.52 11.20 o 1 5 2 1433.67 1413.47 32.51 o 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33.03 o -5 7 2 361.42 373.56 21.36 o -4 7 2 147.90 149.14 11.27 o -3 7 2 1465.61 1514.95 48.41 o -2 7 2 2212.62 2243.71 62.64 o -1 7 2 2319.38 2300.05 64.17 o 0 7 2 4778.84 4953.21 115.30 o 1 7 2 2271.95 2201.63 55.77 o 2 7 2 2137.00 2043.13 69.87 o 3 7 2 1551.70 1672.32 69.21 o 4 7 2 129.28 124.83 13.74 o 5 7 2 353.31 330.56 19.66 o 6 7 2 532.29 613.60 47.08 o 7 7 2 718.37 726.16 53.07 o 8 7 2 1323.79 1261.10 86.57 o 9 7 2 643.31 588.57 102.98 o -8 8 2 162.95 249.76 57.01 o -7 8 2 428.21 406.20 43.60 o -6 8 2 419.96 481.07 48.51 o -5 8 2 444.75 472.51 34.74 o -4 8 2 1941.99 2019.81 83.15 o -3 8 2 388.77 398.56 27.91 o -2 8 2 1840.82 1884.55 70.84 o -1 8 2 613.52 614.62 33.95 o 0 8 2 375.83 393.47 17.64 o 1 8 2 597.91 630.76 27.76 o 2 8 2 1778.23 1881.49 61.71 o 3 8 2 413.44 439.81 27.71 o 4 8 2 1965.21 2058.36 97.46 o 5 8 2 415.06 434.30 62.93 o 6 8 2 405.09 428.10 65.02 o 7 8 2 400.47 285.49 61.68 o 8 8 2 152.03 141.60 46.99 o -7 9 2 562.21 596.98 102.54 o -6 9 2 1119.09 1034.76 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154.78 63.64 o 2 4 24 735.13 599.73 101.58 o 3 4 24 153.17 186.70 85.12 o -1 5 24 114.39 75.71 67.54 o 0 5 24 84.28 39.35 78.70 o 1 5 24 123.38 127.82 111.63 o 1 0 25 319.75 215.34 63.07 o 2 0 25 403.18 446.21 83.86 o 3 0 25 1292.12 1082.09 108.55 o 4 0 25 705.07 590.14 74.09 o -4 1 25 74.52 30.99 53.64 o -3 1 25 117.38 111.75 57.17 o -2 1 25 143.37 147.45 51.85 o -1 1 25 273.71 277.84 66.24 o 0 1 25 305.24 300.65 152.93 o 1 1 25 280.34 351.05 74.93 o 2 1 25 127.41 90.68 89.02 o 3 1 25 131.24 123.45 56.12 o 4 1 25 79.71 64.95 68.09 o -3 2 25 123.59 186.63 67.66 o -2 2 25 363.27 307.58 69.98 o -1 2 25 574.75 552.34 78.20 o 0 2 25 696.73 806.77 91.85 o 1 2 25 586.54 602.00 83.03 o 2 2 25 354.51 372.08 66.17 o 3 2 25 124.98 215.72 77.30 o -2 3 25 589.78 469.46 65.37 o -1 3 25 281.68 199.64 81.35 o 0 3 25 203.51 223.02 69.35 o 1 3 25 277.15 245.04 51.52 o 2 3 25 565.03 432.28 72.98 o -1 4 25 303.03 320.12 88.88 o 0 4 25 5.84 11.45 44.09 o 1 4 25 289.67 328.19 98.51 o 0 0 26 663.72 487.26 123.35 o 1 0 26 963.90 867.38 106.75 o 2 0 26 206.63 113.72 45.98 o -2 1 26 232.56 281.65 123.35 o -1 1 26 98.01 120.24 61.13 o 0 1 26 221.08 180.51 55.43 o 1 1 26 98.88 153.62 62.81 o 2 1 26 246.36 207.60 65.62 o -1 2 26 85.86 49.92 54.93 o 0 2 26 354.24 285.37 53.56 o 1 2 26 82.20 83.91 46.51 o