#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:00:13 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180939 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/19/2201940.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201940_Fobs loop_ _publ_author_name 'Li, Xiao-Fang' 'Feng, Ya-Qing' 'Xiao-Fen, Hu' 'Mian, Xu' _publ_section_title ; 4,11-Bis(4-chlorophenyl)-3,10-bis(2,6-dichlorophenyl)-1,8-dioxa-2,9-diazadispiro[4.1.4.4]pentadeca-2,9-dien-6-one ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o716 _journal_page_last o717 _journal_volume 59 _journal_year 2003 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.152 _cell_angle_gamma 90.000 _cell_length_a 33.5103 _cell_length_b 12.4187 _cell_length_c 32.9461 _exptl_crystal_F_000 5984.00 _reflns_d_resolution_high 0.8400 _cod_data_source_file cv6183Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 030330G in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 785.74 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 209243.89 203913.17 3100.79 o 6 0 0 168052.17 173367.70 3407.16 o 8 0 0 176127.77 183289.20 2436.75 o 10 0 0 138055.08 138075.47 2864.51 o 12 0 0 295421.63 298069.50 4775.82 o 14 0 0 3661.64 3496.80 455.44 o 16 0 0 38427.75 36995.79 1258.62 o 18 0 0 21460.80 20308.93 551.74 o 20 0 0 3851.88 3007.66 304.78 o 22 0 0 8919.07 9230.91 434.63 o 24 0 0 1695.72 1484.92 534.70 o 26 0 0 1931.75 1871.06 579.53 o 28 0 0 5908.98 5957.48 781.70 o 30 0 0 5900.96 6199.80 795.14 o 32 0 0 14380.31 15284.81 1133.70 o 34 0 0 385.58 823.81 619.43 o 36 0 0 138.43 671.48 605.11 o 38 0 0 269.92 716.91 665.54 o 1 1 0 49570.55 45815.95 956.78 o 3 1 0 48661.59 49466.89 770.83 o 5 1 0 1220.92 767.25 226.86 o 7 1 0 36423.88 35570.48 565.93 o 9 1 0 28956.40 30273.68 468.28 o 11 1 0 114807.08 114574.88 1029.50 o 13 1 0 19669.42 20644.01 443.72 o 15 1 0 11735.15 11921.57 373.57 o 17 1 0 17781.95 17449.09 461.37 o 19 1 0 8060.57 7982.20 363.97 o 21 1 0 6212.21 5776.37 346.91 o 23 1 0 15063.32 13823.89 634.31 o 25 1 0 433.64 597.85 369.44 o 27 1 0 219.41 510.14 385.50 o 29 1 0 423.32 619.66 418.74 o 31 1 0 1146.40 1853.37 457.44 o 33 1 0 20.74 349.46 423.43 o 35 1 0 3.20 218.86 441.64 o 37 1 0 138.23 927.69 462.35 o 39 1 0 48.67 783.16 597.33 o 0 2 0 134323.81 125200.48 1402.72 o 2 2 0 461494.88 448175.28 5304.82 o 4 2 0 3608.53 3384.03 179.10 o 6 2 0 112215.62 108102.25 1534.27 o 8 2 0 75.17 -142.03 188.93 o 10 2 0 41331.28 39633.67 817.22 o 12 2 0 19610.36 21100.25 374.19 o 14 2 0 6121.67 6332.37 247.93 o 16 2 0 950.67 967.02 259.79 o 18 2 0 14991.96 14678.12 468.04 o 20 2 0 40725.39 40896.32 750.63 o 22 2 0 2224.98 1737.78 396.55 o 24 2 0 1931.70 1722.22 407.20 o 26 2 0 8656.27 9097.66 607.39 o 28 2 0 340.82 477.62 406.95 o 30 2 0 2393.08 2602.24 494.13 o 32 2 0 1357.49 1467.64 447.59 o 34 2 0 28.45 610.51 435.02 o 36 2 0 238.49 91.57 507.69 o 38 2 0 22.03 169.25 621.71 o 1 3 0 74.69 -234.08 234.08 o 3 3 0 97688.41 96518.73 952.40 o 5 3 0 4.31 -157.83 295.36 o 7 3 0 27050.33 27453.42 452.78 o 9 3 0 1675.49 1173.93 232.67 o 11 3 0 75448.13 77341.11 1194.60 o 13 3 0 7144.58 7050.38 280.72 o 15 3 0 21927.62 21501.16 429.80 o 17 3 0 6040.55 6232.83 289.41 o 19 3 0 1590.81 1434.93 232.22 o 21 3 0 15505.30 16142.58 533.89 o 23 3 0 651.02 248.36 293.24 o 25 3 0 92.26 -321.85 349.61 o 27 3 0 1.47 -306.88 390.05 o 29 3 0 1007.23 191.23 405.98 o 31 3 0 4835.79 3938.87 1124.53 o 33 3 0 1624.82 2403.02 659.90 o 35 3 0 844.98 1656.23 1237.43 o 37 3 0 1209.71 1868.36 819.43 o 0 4 0 4475.52 4267.88 402.45 o 2 4 0 38.38 -105.73 223.24 o 4 4 0 4.36 -332.83 350.42 o 6 4 0 102025.34 100147.16 3913.14 o 8 4 0 29869.96 30898.04 508.42 o 10 4 0 24352.07 25000.22 486.43 o 12 4 0 3380.35 3604.01 292.38 o 14 4 0 0.85 -60.99 239.16 o 16 4 0 662.95 589.33 238.80 o 18 4 0 145.62 215.12 230.85 o 20 4 0 0.13 -253.10 296.83 o 22 4 0 4677.58 3925.69 372.16 o 24 4 0 5812.93 5233.08 415.49 o 26 4 0 831.63 711.40 502.66 o 28 4 0 470.95 391.71 493.28 o 30 4 0 802.45 1035.61 579.57 o 32 4 0 21.37 236.70 503.44 o 34 4 0 98.30 690.52 660.96 o 36 4 0 11.88 595.94 1296.17 o 38 4 0 54.53 1312.43 1278.29 o 1 5 0 26172.30 25452.67 516.52 o 3 5 0 2533.76 2372.03 248.48 o 5 5 0 1001.70 1076.04 348.80 o 7 5 0 39270.42 40214.35 920.76 o 9 5 0 15117.52 14909.76 581.85 o 11 5 0 597.40 638.45 249.46 o 13 5 0 19130.56 19752.29 487.48 o 15 5 0 1993.34 2072.61 285.10 o 17 5 0 24964.24 25156.16 593.55 o 19 5 0 3557.54 2754.46 355.79 o 21 5 0 1186.67 1319.67 612.53 o 23 5 0 157.24 -222.90 438.26 o 25 5 0 546.56 404.98 453.95 o 27 5 0 1169.17 1356.28 723.17 o 29 5 0 568.57 764.99 706.16 o 31 5 0 13.45 78.31 841.21 o 33 5 0 90.92 537.16 1292.28 o 35 5 0 838.72 868.63 1143.63 o 37 5 0 286.23 946.91 1558.99 o 0 6 0 781.34 768.15 393.62 o 2 6 0 14681.00 14752.00 698.12 o 4 6 0 5181.47 4857.42 306.18 o 6 6 0 5887.82 6531.92 588.64 o 8 6 0 124.05 15.65 357.58 o 10 6 0 7.14 -161.52 385.18 o 12 6 0 275.90 257.84 369.48 o 14 6 0 1.16 -137.38 249.13 o 16 6 0 9337.55 9070.17 832.48 o 18 6 0 11700.21 11179.70 658.84 o 20 6 0 1520.65 1566.18 498.53 o 22 6 0 3646.59 3788.29 561.88 o 24 6 0 8905.46 8802.32 704.08 o 26 6 0 2373.50 2315.26 583.94 o 28 6 0 127.21 388.10 1517.84 o 30 6 0 319.28 523.64 670.81 o 32 6 0 488.27 1326.90 1490.87 o 34 6 0 222.11 1713.94 736.07 o 36 6 0 27.98 914.27 1296.14 o 1 7 0 2485.48 2407.39 319.05 o 3 7 0 32.28 -82.14 253.98 o 5 7 0 22795.71 22772.06 513.10 o 7 7 0 30.51 -26.25 402.35 o 9 7 0 12.51 239.61 847.31 o 11 7 0 536.91 963.62 425.65 o 13 7 0 25916.81 26165.00 938.61 o 15 7 0 56.60 101.37 387.74 o 17 7 0 251.10 144.95 505.46 o 19 7 0 1727.23 1393.73 483.84 o 21 7 0 3089.79 3549.12 580.94 o 23 7 0 6021.71 5563.37 629.99 o 25 7 0 826.84 936.49 676.10 o 27 7 0 861.09 1483.27 743.16 o 29 7 0 5662.41 6397.74 941.95 o 31 7 0 55.87 976.83 716.86 o 33 7 0 332.39 1021.61 684.32 o 0 8 0 149.09 222.94 388.52 o 2 8 0 2145.16 2527.83 318.31 o 4 8 0 21780.30 21657.99 566.22 o 6 8 0 253.73 28.57 426.17 o 8 8 0 1616.73 1296.21 430.00 o 10 8 0 675.11 1021.67 548.66 o 12 8 0 8233.91 7634.61 582.44 o 14 8 0 1010.92 1181.78 464.06 o 16 8 0 195.08 -376.62 396.43 o 18 8 0 7745.22 6839.72 597.16 o 20 8 0 3477.01 2555.90 677.49 o 22 8 0 4005.33 4481.46 640.98 o 24 8 0 6116.31 6380.15 687.88 o 26 8 0 176.11 1001.75 1486.16 o 28 8 0 85.49 1833.10 776.38 o 30 8 0 325.34 925.70 1786.21 o 32 8 0 120.00 1256.54 1614.17 o 1 9 0 141.42 300.57 390.66 o 3 9 0 3050.26 3578.29 484.28 o 5 9 0 32.92 284.95 442.65 o 7 9 0 7391.00 6472.50 597.40 o 9 9 0 292.53 423.20 463.14 o 11 9 0 16.99 -138.98 450.67 o 13 9 0 1092.45 1061.12 486.16 o 15 9 0 238.18 571.72 470.32 o 17 9 0 945.76 1172.21 618.50 o 19 9 0 6498.23 6417.85 1008.65 o 21 9 0 619.14 827.72 629.51 o 23 9 0 307.74 668.91 779.17 o 25 9 0 64.08 535.05 1813.80 o 27 9 0 257.55 1298.31 1301.33 o 29 9 0 58.15 993.91 1731.04 o 31 9 0 694.00 1870.06 773.46 o 0 10 0 28892.83 27307.95 1733.12 o 2 10 0 4932.02 5935.64 841.87 o 4 10 0 1860.66 2030.08 474.26 o 6 10 0 25058.08 24884.61 952.46 o 8 10 0 325.40 417.77 517.18 o 10 10 0 1039.47 1052.84 529.93 o 12 10 0 622.72 1527.38 506.26 o 14 10 0 7546.86 8092.95 678.63 o 16 10 0 8819.82 8854.91 678.94 o 18 10 0 6267.37 6599.72 606.32 o 20 10 0 267.42 1968.53 665.92 o 22 10 0 151.92 703.40 1293.54 o 24 10 0 1451.16 2054.85 1415.96 o 26 10 0 1014.96 1349.60 1796.73 o 28 10 0 622.31 1742.01 1316.91 o 1 11 0 814.32 637.42 680.28 o 3 11 0 89.77 -325.94 682.52 o 5 11 0 6.79 -438.59 624.72 o 7 11 0 348.29 185.01 627.23 o 9 11 0 141.80 996.99 599.94 o 11 11 0 1643.86 1557.75 510.92 o 13 11 0 505.90 856.14 486.07 o 15 11 0 967.22 2621.19 563.14 o 17 11 0 4.50 1065.74 782.08 o 19 11 0 3155.68 6213.64 2085.42 o 21 11 0 123.25 1614.75 1543.74 o 23 11 0 82.83 925.54 1367.64 o 25 11 0 0.05 1064.33 1337.71 o 0 12 0 842.43 599.06 982.68 o 2 12 0 1269.78 578.21 858.70 o 4 12 0 490.60 202.47 656.17 o 6 12 0 347.57 359.05 592.21 o 8 12 0 624.19 -47.93 667.77 o 10 12 0 195.48 62.45 607.84 o 12 12 0 2953.45 3246.55 718.21 o 14 12 0 3390.63 3669.56 759.14 o 16 12 0 550.03 1795.92 1829.35 o 18 12 0 306.37 2731.76 1165.99 o 20 12 0 14.97 3344.74 1374.35 o 22 12 0 774.34 2713.34 2273.95 o 1 13 0 1841.49 2634.68 778.80 o 3 13 0 1046.37 978.73 687.36 o 5 13 0 409.28 1142.00 696.66 o 7 13 0 97.14 -412.91 653.19 o 9 13 0 2101.82 1329.42 688.31 o 11 13 0 0.12 429.63 973.56 o 13 13 0 1013.94 2183.99 701.74 o 15 13 0 1006.10 614.01 636.80 o 17 13 0 22.38 -649.76 985.34 o 0 14 0 493.03 742.51 1026.11 o 2 14 0 230.48 82.64 680.53 o 4 14 0 1138.73 1930.70 913.23 o 6 14 0 948.99 2280.94 776.77 o 8 14 0 89.60 437.46 692.10 o 10 14 0 298.07 306.39 1172.22 o 12 14 0 260.02 646.32 667.60 o -39 1 1 136.87 88.98 764.62 o -37 1 1 78.60 764.38 498.80 o -35 1 1 805.58 1075.13 462.73 o -33 1 1 3736.82 3940.24 531.70 o -31 1 1 0.06 982.58 434.70 o -29 1 1 421.89 550.95 401.25 o -27 1 1 2340.90 1812.27 443.51 o -25 1 1 2032.75 1576.76 418.39 o -23 1 1 21440.88 22399.05 788.74 o -21 1 1 6924.01 7068.54 359.22 o -19 1 1 43369.09 40622.91 688.66 o -17 1 1 663.77 362.86 228.54 o -15 1 1 4119.84 4492.38 280.54 o -13 1 1 19549.16 20438.33 435.20 o -11 1 1 9785.38 9725.20 324.08 o -9 1 1 4754.29 4263.47 351.11 o -7 1 1 428686.53 422430.34 2985.67 o -5 1 1 15480.43 16408.21 331.63 o -3 1 1 186063.16 188540.89 3779.10 o -1 1 1 4404.35 4873.69 291.45 o 1 1 1 18341.38 16348.88 637.10 o 3 1 1 5914.03 6360.33 237.34 o 5 1 1 272.44 376.88 213.92 o 7 1 1 178408.16 183308.75 1411.06 o 9 1 1 75544.65 74186.75 752.90 o 11 1 1 23533.19 24355.17 459.69 o 13 1 1 20822.26 21058.68 455.15 o 15 1 1 1328.23 1348.50 242.82 o 17 1 1 3012.40 2456.96 269.58 o 19 1 1 3799.75 4212.60 322.08 o 21 1 1 52.02 -6.54 241.70 o 23 1 1 315.82 206.02 262.55 o 25 1 1 11742.83 12067.04 640.39 o 27 1 1 3288.61 3040.53 461.40 o 29 1 1 9482.80 9044.46 643.09 o 31 1 1 0.06 198.89 416.03 o 33 1 1 572.38 610.12 419.16 o 35 1 1 922.39 564.64 460.42 o 37 1 1 145.49 456.54 473.48 o 39 1 1 15.80 -136.61 556.41 o -38 2 1 252.53 792.16 780.75 o -36 2 1 64.41 779.54 528.50 o -34 2 1 519.75 879.78 436.03 o -32 2 1 1065.56 841.96 417.72 o -30 2 1 4612.13 4564.00 537.85 o -28 2 1 158.86 568.12 414.90 o -26 2 1 2549.01 2779.44 448.69 o -24 2 1 1158.27 528.77 367.49 o -22 2 1 540.75 73.24 258.46 o -20 2 1 93.75 -87.10 257.51 o -18 2 1 11775.44 11667.44 425.19 o -16 2 1 20763.48 20140.27 501.04 o -14 2 1 38.67 -135.98 224.27 o -12 2 1 134506.31 136438.73 2454.68 o -10 2 1 2501.74 2929.96 258.08 o -8 2 1 3630.76 3259.82 430.08 o -6 2 1 350103.94 355558.19 2798.58 o -4 2 1 133318.16 128887.38 2697.37 o -2 2 1 165452.72 166608.70 4622.94 o 0 2 1 268390.25 254152.95 2040.04 o 2 2 1 12843.16 12761.32 262.08 o 4 2 1 2300.62 1899.43 183.93 o 6 2 1 15843.33 15981.00 351.73 o 8 2 1 903.56 867.71 195.26 o 10 2 1 8359.79 8173.72 277.18 o 12 2 1 67411.02 67845.46 725.14 o 14 2 1 90.45 38.98 177.38 o 16 2 1 790.36 352.39 245.64 o 18 2 1 23414.54 24416.14 574.44 o 20 2 1 7470.23 7576.40 388.38 o 22 2 1 580.09 134.14 259.80 o 24 2 1 241.73 -236.61 349.20 o 26 2 1 7242.13 7125.46 563.75 o 28 2 1 107.87 75.11 405.77 o 30 2 1 3679.15 3479.84 504.34 o 32 2 1 790.20 897.20 634.59 o 34 2 1 4.13 -100.88 429.81 o 36 2 1 13.05 502.56 551.39 o 38 2 1 7.35 1033.10 1012.19 o -37 3 1 1079.01 1809.10 706.82 o -35 3 1 16.81 455.78 843.42 o -33 3 1 77.35 11.81 479.16 o -31 3 1 50.32 231.41 480.65 o -29 3 1 464.79 605.99 437.68 o -27 3 1 1.35 79.18 379.33 o -25 3 1 5286.71 5169.99 503.70 o -23 3 1 112.10 -166.51 409.08 o -21 3 1 472.37 475.06 283.70 o -19 3 1 359.35 170.51 192.66 o -17 3 1 5180.83 5107.73 266.29 o -15 3 1 7722.40 7679.15 292.84 o -13 3 1 36212.69 37356.88 522.13 o -11 3 1 38325.08 37586.55 571.97 o -9 3 1 22109.91 23128.45 438.53 o -7 3 1 21778.81 22151.40 399.59 o -5 3 1 149128.31 150958.00 1445.64 o -3 3 1 13065.52 12937.85 451.85 o -1 3 1 311945.97 316167.53 6811.73 o 1 3 1 1192.59 500.12 252.55 o 3 3 1 4052.93 3512.68 283.09 o 5 3 1 41678.51 42934.19 576.60 o 7 3 1 7876.12 8021.35 302.61 o 9 3 1 23.61 -202.95 210.51 o 11 3 1 13813.19 13921.30 389.03 o 13 3 1 15617.87 15749.02 391.21 o 15 3 1 4865.62 5401.02 276.58 o 17 3 1 97.05 254.65 211.34 o 19 3 1 1013.94 1341.06 226.58 o 21 3 1 886.95 876.77 276.99 o 23 3 1 308.93 -21.24 314.90 o 25 3 1 696.19 190.93 374.55 o 27 3 1 8464.46 8325.79 601.30 o 29 3 1 1.65 -224.34 419.75 o 31 3 1 2523.02 2140.83 555.45 o 33 3 1 140.38 316.79 487.99 o 35 3 1 640.51 772.05 690.10 o 37 3 1 0.94 34.91 1347.48 o -38 4 1 277.51 381.86 1265.05 o -36 4 1 463.04 1613.06 1211.46 o -34 4 1 216.39 189.54 1155.21 o -32 4 1 26.18 398.04 489.25 o -30 4 1 2261.34 2112.23 554.25 o -28 4 1 12.80 -475.05 475.05 o -26 4 1 324.48 427.19 500.69 o -24 4 1 3426.70 2430.06 357.83 o -22 4 1 18920.11 19263.70 605.39 o -20 4 1 1306.79 552.42 347.85 o -18 4 1 16212.95 15865.66 444.08 o -16 4 1 17334.72 17665.37 450.87 o -14 4 1 3715.17 3629.14 317.72 o -12 4 1 5324.32 5595.77 313.31 o -10 4 1 212.22 105.39 200.99 o -8 4 1 4409.87 4580.52 381.43 o -6 4 1 1907.09 1576.11 392.26 o -4 4 1 23311.83 22088.16 591.44 o -2 4 1 73.19 -208.41 208.41 o 0 4 1 2845.54 2595.73 271.93 o 2 4 1 23847.05 23137.81 469.29 o 4 4 1 20637.08 20794.75 445.70 o 6 4 1 75.58 129.98 264.97 o 8 4 1 32944.23 34570.90 871.43 o 10 4 1 537.90 454.74 238.07 o 12 4 1 122344.47 126973.78 1732.54 o 14 4 1 8547.29 8422.97 377.26 o 16 4 1 15366.36 15807.71 477.05 o 18 4 1 16471.98 16619.90 463.61 o 20 4 1 472.38 64.44 231.66 o 22 4 1 244.35 -167.06 293.52 o 24 4 1 1484.25 1591.43 336.52 o 26 4 1 6103.22 6088.33 666.75 o 28 4 1 1349.47 1627.10 501.20 o 30 4 1 2033.12 2087.03 548.89 o 32 4 1 375.13 637.85 664.61 o 34 4 1 2253.83 1567.11 1429.50 o 36 4 1 141.52 737.71 1229.28 o 38 4 1 4.89 793.98 734.43 o -37 5 1 4.90 741.47 1423.40 o -35 5 1 1580.75 2253.67 792.15 o -33 5 1 647.06 1192.93 1093.29 o -31 5 1 520.69 589.87 633.02 o -29 5 1 3220.18 3524.49 797.36 o -27 5 1 4315.84 4292.18 807.71 o -25 5 1 3351.45 2720.22 524.75 o -23 5 1 4511.51 4721.01 559.34 o -21 5 1 6195.17 5438.97 581.65 o -19 5 1 7093.08 6933.92 432.71 o -17 5 1 4124.76 3844.58 301.13 o -15 5 1 175.23 76.90 241.96 o -13 5 1 11872.86 11588.03 394.86 o -11 5 1 61432.40 61694.03 1071.24 o -9 5 1 196.64 61.44 345.44 o -7 5 1 1260.51 1067.55 333.90 o -5 5 1 19612.19 19711.63 615.41 o -3 5 1 5830.21 5945.31 283.66 o -1 5 1 12743.61 12706.68 395.34 o 1 5 1 1201.43 1061.47 257.24 o 3 5 1 5963.08 5940.63 320.82 o 5 5 1 4091.02 3611.50 316.67 o 7 5 1 5743.54 5785.82 308.70 o 9 5 1 3319.08 3247.04 286.14 o 11 5 1 15.40 -244.51 244.51 o 13 5 1 10764.03 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