#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2201957.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201957_Fobs loop_ _publ_author_name 'Cherouana, Aouatef' 'Benali-Cherif, Nourredine' 'Bendjeddou, Lamia' _publ_section_title ; Guaninium sulfate monohydrate ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o180 _journal_page_last o182 _journal_volume 59 _journal_year 2003 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 106.037 _cell_angle_gamma 90.000 _cell_length_a 8.9940 _cell_length_b 10.2020 _cell_length_c 11.0440 _exptl_crystal_F_000 552.00 _reflns_d_resolution_high 0.8003 _[local]_cod_data_source_file dn6052Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' n33-full in P 1 21/c 1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 87.63 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 4586.93 4078.86 113.97 o 5 0 0 46.56 49.33 2.90 o 6 0 0 773.99 754.37 22.13 o 7 0 0 394.87 407.51 13.87 o 8 0 0 17.58 19.59 3.21 o 9 0 0 543.23 531.43 19.43 o 10 0 0 111.88 115.73 7.36 o 1 1 0 272.13 180.72 29.31 o 2 1 0 5630.86 5055.11 147.72 o 3 1 0 0.58 1.51 0.83 o 4 1 0 0.06 1.31 0.94 o 5 1 0 537.19 543.91 10.60 o 6 1 0 2.46 4.04 3.38 o 7 1 0 103.12 113.55 3.68 o 8 1 0 181.31 194.32 5.69 o 9 1 0 639.26 668.18 14.49 o 10 1 0 8.11 3.77 2.77 o 0 2 0 784.28 904.37 31.91 o 1 2 0 1259.77 1169.01 21.44 o 2 2 0 780.31 888.99 18.63 o 3 2 0 48.59 69.37 2.28 o 4 2 0 2.31 -0.60 0.99 o 5 2 0 736.74 795.62 15.75 o 6 2 0 110.36 118.78 3.26 o 7 2 0 389.18 381.98 8.96 o 8 2 0 14.21 15.21 2.63 o 9 2 0 0.82 4.66 3.24 o 10 2 0 98.99 106.25 7.10 o 1 3 0 5564.53 5325.10 144.11 o 2 3 0 247.40 280.24 5.92 o 3 3 0 1153.05 1166.23 22.68 o 4 3 0 525.82 557.64 11.11 o 5 3 0 2.38 4.46 1.24 o 6 3 0 79.43 91.24 3.46 o 7 3 0 152.88 146.44 4.92 o 8 3 0 44.92 47.13 5.97 o 9 3 0 47.16 48.80 4.45 o 10 3 0 0.32 -2.96 4.18 o 0 4 0 1013.06 1085.32 43.48 o 1 4 0 3291.71 3387.61 66.90 o 2 4 0 236.87 230.21 4.86 o 3 4 0 419.78 412.39 12.80 o 4 4 0 144.55 154.88 3.70 o 5 4 0 20.15 28.95 2.76 o 6 4 0 7.55 9.22 1.77 o 7 4 0 134.04 126.84 15.32 o 8 4 0 126.93 140.47 5.29 o 9 4 0 0.10 0.49 3.49 o 10 4 0 98.92 80.01 5.50 o 1 5 0 205.39 220.80 4.60 o 2 5 0 254.63 246.82 5.71 o 3 5 0 747.64 772.24 15.87 o 4 5 0 310.60 306.86 6.78 o 5 5 0 318.15 306.40 8.20 o 6 5 0 360.26 351.06 10.14 o 7 5 0 137.53 137.89 4.99 o 8 5 0 128.49 128.15 16.78 o 9 5 0 21.35 28.30 13.23 o 0 6 0 75.43 45.78 9.32 o 1 6 0 73.25 68.88 2.65 o 2 6 0 419.31 415.00 11.20 o 3 6 0 104.38 118.86 3.75 o 4 6 0 728.90 722.59 20.51 o 5 6 0 36.03 28.95 15.54 o 6 6 0 0.59 3.13 1.74 o 7 6 0 454.33 462.33 11.03 o 8 6 0 90.23 90.82 6.33 o 9 6 0 0.36 -2.93 2.93 o 1 7 0 436.14 408.63 8.34 o 2 7 0 931.17 915.54 17.98 o 3 7 0 265.22 258.58 6.28 o 4 7 0 52.00 60.73 2.99 o 5 7 0 213.96 213.07 5.26 o 6 7 0 225.46 206.11 6.10 o 7 7 0 1.61 7.66 2.83 o 8 7 0 283.06 289.80 8.41 o 9 7 0 176.97 155.26 18.15 o 0 8 0 4393.25 4325.52 109.45 o 1 8 0 411.67 385.96 9.55 o 2 8 0 378.74 399.89 8.73 o 3 8 0 474.71 493.01 26.43 o 4 8 0 2.54 2.40 3.21 o 5 8 0 89.61 60.96 3.01 o 6 8 0 515.53 552.57 14.61 o 7 8 0 12.41 18.01 3.29 o 8 8 0 112.88 105.57 17.58 o 1 9 0 21.25 11.81 2.34 o 2 9 0 313.44 316.36 9.19 o 3 9 0 701.68 682.66 15.59 o 4 9 0 110.68 106.50 5.40 o 5 9 0 159.90 169.24 6.31 o 6 9 0 4.84 6.60 2.24 o 7 9 0 3.33 -3.81 3.81 o 0 10 0 813.02 859.72 33.75 o 1 10 0 331.48 351.40 9.05 o 2 10 0 278.95 302.04 7.98 o 3 10 0 320.92 351.80 9.90 o 4 10 0 21.72 23.27 4.52 o 5 10 0 0.06 4.45 2.81 o 6 10 0 241.01 226.88 11.28 o 1 11 0 230.47 241.20 7.58 o 2 11 0 3.20 0.93 3.13 o 3 11 0 0.56 1.68 2.32 o 4 11 0 15.89 16.34 3.81 o 5 11 0 52.81 60.44 12.69 o 0 12 0 45.29 39.35 4.77 o 1 12 0 91.06 87.04 10.06 o 2 12 0 132.18 121.26 9.76 o 3 12 0 9.32 10.59 3.89 o -10 1 1 0.27 6.78 2.78 o -9 1 1 0.01 2.64 2.20 o -8 1 1 23.52 22.82 3.50 o -7 1 1 441.47 441.23 9.55 o -6 1 1 154.35 127.52 3.71 o -5 1 1 52.74 58.87 20.61 o -4 1 1 166.51 206.74 4.48 o -3 1 1 679.00 603.70 12.69 o -2 1 1 16.63 26.74 1.04 o -1 1 1 385.80 405.33 53.70 o 0 1 1 61.49 57.00 12.67 o 1 1 1 835.20 781.47 16.13 o 2 1 1 205.21 209.38 4.43 o 3 1 1 27.21 24.25 1.71 o 4 1 1 194.48 172.13 4.71 o 5 1 1 18.26 22.91 2.00 o 6 1 1 13.25 14.77 1.49 o 7 1 1 14.44 14.55 1.70 o 8 1 1 111.73 112.38 4.13 o 9 1 1 53.77 53.70 6.12 o 10 1 1 47.34 45.54 6.16 o -10 2 1 38.18 43.70 5.88 o -9 2 1 190.10 211.58 6.79 o -8 2 1 0.01 0.22 1.54 o -7 2 1 127.24 120.19 4.41 o -6 2 1 235.41 240.33 5.32 o -5 2 1 1013.54 996.23 20.54 o -4 2 1 22.41 36.91 2.44 o -3 2 1 5776.51 5603.96 116.01 o -2 2 1 7.99 14.19 1.00 o -1 2 1 581.52 588.61 11.42 o 0 2 1 5349.56 4912.24 132.80 o 1 2 1 183.11 159.56 3.06 o 2 2 1 483.09 484.80 9.84 o 3 2 1 961.94 892.79 16.85 o 4 2 1 4.00 5.66 1.14 o 5 2 1 591.69 578.78 11.37 o 6 2 1 273.97 269.68 6.01 o 7 2 1 0.43 1.14 1.77 o 8 2 1 64.04 62.14 13.34 o 9 2 1 45.95 52.49 4.46 o 10 2 1 96.06 98.58 6.05 o -10 3 1 92.96 83.47 4.73 o -9 3 1 285.96 299.96 9.06 o -8 3 1 128.11 127.70 4.08 o -7 3 1 67.97 77.70 4.40 o -6 3 1 276.33 269.32 9.59 o -5 3 1 1193.23 1146.46 21.93 o -4 3 1 885.86 894.58 16.59 o -3 3 1 126.18 142.65 3.88 o -2 3 1 640.26 518.50 10.68 o 0 3 1 1448.21 1425.37 27.20 o 1 3 1 2922.35 2688.11 57.11 o 2 3 1 26.50 41.79 1.60 o 3 3 1 0.94 -0.02 0.95 o 4 3 1 1137.87 1155.24 23.88 o 5 3 1 604.71 583.89 11.30 o 6 3 1 208.13 202.45 5.82 o 7 3 1 10.20 12.93 2.70 o 8 3 1 210.80 223.86 8.70 o 9 3 1 69.58 57.17 3.99 o 10 3 1 17.31 21.02 4.23 o -10 4 1 767.68 742.98 34.82 o -9 4 1 52.06 55.19 5.51 o -8 4 1 271.68 267.97 9.58 o -7 4 1 469.36 449.82 9.85 o -6 4 1 44.73 48.51 3.14 o -5 4 1 2165.58 2279.54 41.08 o -4 4 1 577.11 545.79 11.52 o -3 4 1 7679.27 7651.87 271.18 o -2 4 1 4901.59 5082.48 100.72 o -1 4 1 1724.81 1675.27 33.02 o 0 4 1 5.36 2.01 0.88 o 1 4 1 142.59 102.95 2.80 o 2 4 1 5618.58 5600.90 105.81 o 3 4 1 207.72 158.54 5.58 o 4 4 1 683.08 664.30 13.22 o 5 4 1 278.24 303.09 7.09 o 6 4 1 163.03 179.20 5.00 o 7 4 1 2140.80 2168.21 44.01 o 8 4 1 21.10 21.95 69.17 o 9 4 1 51.11 48.48 3.79 o 10 4 1 70.96 63.95 7.44 o -10 5 1 54.75 54.51 5.11 o -9 5 1 0.14 -2.05 2.05 o -8 5 1 3.76 6.74 3.66 o -7 5 1 0.75 -1.66 1.66 o -6 5 1 839.89 827.36 18.58 o -5 5 1 60.50 64.09 2.67 o -4 5 1 4.38 8.00 1.83 o -3 5 1 520.23 562.24 10.59 o -1 5 1 882.71 825.08 15.52 o 0 5 1 17.39 23.76 1.36 o 1 5 1 1566.44 1530.78 29.65 o 2 5 1 643.46 663.72 13.20 o 3 5 1 596.45 614.18 12.66 o 4 5 1 2866.83 3053.90 57.90 o 5 5 1 908.91 948.91 18.30 o 6 5 1 29.12 39.43 2.90 o 7 5 1 119.77 126.20 4.80 o 8 5 1 11.36 23.39 13.57 o 9 5 1 73.35 67.48 4.75 o -9 6 1 418.89 428.27 19.60 o -8 6 1 59.42 53.51 4.05 o -7 6 1 223.79 220.89 7.41 o -6 6 1 35.53 39.54 2.66 o -5 6 1 181.83 167.03 5.26 o -4 6 1 920.65 906.30 18.58 o -3 6 1 1180.17 1301.81 25.05 o -2 6 1 515.89 511.82 10.17 o -1 6 1 300.97 339.26 7.49 o 0 6 1 2339.67 2412.12 46.64 o 1 6 1 393.71 457.62 9.39 o 2 6 1 158.31 144.52 4.45 o 3 6 1 575.36 560.53 11.60 o 4 6 1 123.49 115.38 3.50 o 5 6 1 16.83 21.84 2.67 o 6 6 1 2.68 2.49 2.52 o 7 6 1 1.98 6.26 3.32 o 8 6 1 27.47 30.27 4.16 o 9 6 1 0.31 -3.61 18.53 o -9 7 1 67.66 57.35 5.69 o -8 7 1 118.68 129.29 6.57 o -7 7 1 183.72 177.59 7.19 o -6 7 1 4.08 11.01 5.11 o -5 7 1 29.69 30.58 2.61 o -4 7 1 248.97 265.88 7.04 o -3 7 1 15.11 18.76 1.86 o -2 7 1 1237.52 1247.53 22.78 o -1 7 1 4.07 0.14 3.48 o 0 7 1 262.05 290.25 6.44 o 1 7 1 308.01 318.01 7.22 o 2 7 1 823.09 843.43 18.85 o 3 7 1 290.70 298.95 9.66 o 4 7 1 4.23 5.40 1.75 o 5 7 1 13.93 14.69 2.39 o 6 7 1 132.62 135.35 14.77 o 7 7 1 4.10 6.96 3.50 o 8 7 1 57.07 60.12 6.49 o -8 8 1 23.17 23.59 58.58 o -7 8 1 0.01 0.93 4.98 o -6 8 1 1.82 8.37 2.94 o -5 8 1 0.84 6.25 2.70 o -4 8 1 109.85 98.10 4.35 o -3 8 1 93.76 79.39 3.36 o -2 8 1 1841.02 1864.25 35.38 o -1 8 1 474.80 490.14 10.43 o 0 8 1 459.20 466.18 9.52 o 1 8 1 6.02 2.87 4.57 o 2 8 1 90.47 93.80 3.56 o 3 8 1 396.29 423.81 9.15 o 4 8 1 650.19 679.45 29.30 o 5 8 1 0.41 2.84 5.33 o 6 8 1 103.52 110.51 4.94 o 7 8 1 1.08 1.17 2.57 o 8 8 1 9.62 11.25 4.66 o -7 9 1 21.77 26.04 3.76 o -6 9 1 134.44 119.74 9.73 o -5 9 1 14.64 12.34 2.66 o -4 9 1 191.15 193.65 7.18 o -3 9 1 76.68 57.99 2.95 o -2 9 1 1022.60 1019.20 20.37 o -1 9 1 1127.95 1098.62 21.13 o 0 9 1 6.24 7.54 2.50 o 1 9 1 80.49 67.58 6.68 o 2 9 1 124.40 113.70 6.71 o 3 9 1 1229.96 1203.60 26.62 o 4 9 1 390.58 388.62 9.37 o 5 9 1 327.59 306.19 9.66 o 6 9 1 242.89 267.18 9.45 o 7 9 1 73.11 63.95 5.77 o -6 10 1 211.54 203.35 10.31 o -5 10 1 9.03 8.64 4.95 o -4 10 1 202.60 190.89 6.27 o -3 10 1 141.67 136.54 7.62 o -2 10 1 171.33 142.25 10.76 o -1 10 1 383.37 355.05 8.85 o 0 10 1 740.13 741.94 19.45 o 1 10 1 0.73 2.04 2.36 o 2 10 1 32.22 31.33 4.87 o 3 10 1 18.46 27.98 3.25 o 4 10 1 1.19 0.62 2.10 o 5 10 1 16.55 15.94 3.08 o 6 10 1 24.54 26.39 5.00 o -5 11 1 204.42 208.39 10.73 o -4 11 1 35.52 35.95 3.51 o -3 11 1 68.76 79.93 7.80 o -2 11 1 389.08 367.13 20.71 o -1 11 1 0.57 4.07 2.32 o 0 11 1 35.52 34.88 3.58 o 1 11 1 145.04 131.50 5.88 o 2 11 1 98.71 103.37 6.68 o 3 11 1 27.50 34.40 3.18 o 4 11 1 24.72 33.34 4.77 o 5 11 1 125.44 131.73 11.78 o -3 12 1 159.49 164.60 10.65 o -2 12 1 15.86 13.52 3.67 o -1 12 1 255.01 258.53 93.65 o 0 12 1 131.36 117.89 6.43 o 1 12 1 12.78 11.76 3.99 o 2 12 1 59.82 67.56 6.19 o 3 12 1 66.90 52.69 6.94 o -11 0 2 237.30 211.61 13.42 o -10 0 2 129.38 123.81 7.61 o -9 0 2 155.83 156.55 9.49 o -8 0 2 578.68 613.78 18.79 o -7 0 2 51.97 66.71 5.10 o -6 0 2 22.35 17.27 2.84 o -5 0 2 182.97 187.56 7.53 o -4 0 2 842.69 944.89 39.63 o -3 0 2 2723.09 2355.43 63.81 o -2 0 2 282.59 321.26 9.94 o -1 0 2 1927.67 1851.30 56.65 o 3 0 2 1012.76 879.56 22.99 o 4 0 2 5332.82 5049.32 123.24 o 5 0 2 262.04 274.04 9.19 o 6 0 2 500.73 500.81 15.61 o 7 0 2 36.27 47.19 3.89 o 8 0 2 117.03 131.66 7.58 o 9 0 2 88.12 83.84 5.75 o 10 0 2 203.20 207.81 11.35 o -10 1 2 86.02 71.82 4.87 o -9 1 2 265.10 262.21 8.01 o -8 1 2 439.12 452.27 11.08 o -7 1 2 205.14 234.03 6.02 o -6 1 2 253.64 250.10 7.02 o -5 1 2 564.78 581.87 11.89 o -4 1 2 15.56 10.86 1.11 o -3 1 2 2107.47 1808.51 37.02 o 0 1 2 10.90 7.04 0.63 o 2 1 2 2616.11 2430.72 51.01 o 3 1 2 2785.44 2783.11 51.39 o 4 1 2 16.38 8.70 1.14 o 5 1 2 44.64 38.02 2.16 o 6 1 2 28.04 24.03 1.67 o 7 1 2 630.12 623.99 13.73 o 8 1 2 329.12 307.57 10.10 o 9 1 2 4.50 3.43 2.22 o 10 1 2 12.60 8.52 3.55 o -10 2 2 441.47 452.30 15.03 o -9 2 2 82.76 89.45 4.94 o -8 2 2 342.80 370.03 9.66 o -7 2 2 1014.02 1046.35 23.20 o -6 2 2 11.68 6.37 1.70 o -5 2 2 351.63 358.80 8.25 o -2 2 2 954.83 897.34 20.84 o -1 2 2 3747.28 3442.53 68.27 o 0 2 2 3389.46 3086.11 57.00 o 1 2 2 676.12 643.71 12.40 o 2 2 2 3587.39 3269.64 64.20 o 3 2 2 467.02 443.47 9.11 o 4 2 2 1.93 1.22 1.25 o 5 2 2 899.69 928.44 17.75 o 6 2 2 131.11 124.99 3.81 o 7 2 2 252.35 269.04 7.33 o 8 2 2 0.51 -0.16 1.97 o 9 2 2 20.48 19.97 4.43 o 10 2 2 116.04 113.12 6.92 o -10 3 2 151.95 164.74 131.92 o -9 3 2 410.45 418.36 10.28 o -8 3 2 47.33 48.61 3.98 o -7 3 2 29.24 39.27 3.76 o -6 3 2 119.29 114.62 7.04 o -5 3 2 140.64 153.89 3.64 o -4 3 2 82.40 97.93 6.05 o -3 3 2 154.28 174.98 4.03 o -2 3 2 365.78 458.09 9.60 o -1 3 2 0.66 0.16 0.82 o 0 3 2 903.76 878.32 16.46 o 1 3 2 59.39 53.56 1.76 o 2 3 2 413.55 428.06 8.53 o 3 3 2 231.36 237.90 5.58 o 4 3 2 1114.04 1117.50 19.96 o 5 3 2 252.92 253.23 5.28 o 6 3 2 0.17 1.64 1.50 o 7 3 2 65.34 63.74 3.30 o 8 3 2 115.50 108.61 7.08 o 9 3 2 152.32 145.56 5.43 o -10 4 2 45.54 39.17 5.38 o -9 4 2 0.30 2.74 2.38 o -8 4 2 69.83 74.01 3.83 o -7 4 2 26.23 23.75 2.31 o -6 4 2 100.28 117.33 4.23 o -5 4 2 313.05 334.78 7.71 o -4 4 2 177.23 197.62 5.12 o -3 4 2 5.99 9.86 3.24 o -2 4 2 1.53 4.04 0.92 o -1 4 2 697.84 722.18 14.30 o 0 4 2 110.59 122.88 3.64 o 1 4 2 4201.46 4328.95 84.34 o 2 4 2 8.34 12.65 1.31 o 3 4 2 272.48 290.56 10.01 o 4 4 2 1.91 3.21 1.21 o 5 4 2 19.01 17.20 1.91 o 6 4 2 0.04 5.79 1.74 o 7 4 2 68.34 64.30 4.27 o 8 4 2 1.65 -0.20 2.57 o 9 4 2 93.36 95.42 31.85 o -10 5 2 76.16 74.55 8.53 o -9 5 2 13.04 13.69 3.35 o -8 5 2 52.06 44.65 5.92 o -7 5 2 61.36 61.88 2.65 o -6 5 2 3.81 4.34 2.74 o -5 5 2 23.26 26.46 2.00 o -4 5 2 1454.96 1394.50 26.44 o -3 5 2 1.04 3.27 1.88 o -2 5 2 106.93 95.35 2.77 o -1 5 2 1230.32 1278.55 24.36 o 0 5 2 14.10 16.38 1.24 o 1 5 2 306.54 345.52 9.93 o 2 5 2 333.09 343.96 7.48 o 3 5 2 17.06 15.59 1.69 o 4 5 2 53.52 62.10 2.29 o 5 5 2 825.75 812.37 15.32 o 6 5 2 268.54 265.15 6.56 o 7 5 2 5.62 7.78 2.79 o 8 5 2 20.90 20.96 3.07 o 9 5 2 55.42 52.17 13.18 o -9 6 2 73.02 80.64 4.85 o -8 6 2 1.61 4.02 2.53 o -7 6 2 419.89 416.39 9.80 o -6 6 2 595.14 639.76 14.23 o -5 6 2 393.34 397.64 8.49 o -4 6 2 1708.91 1725.01 32.50 o -3 6 2 712.92 753.08 14.88 o -2 6 2 332.54 351.87 7.17 o -1 6 2 1479.22 1411.03 26.75 o 0 6 2 0.46 0.07 1.12 o 1 6 2 185.42 191.51 8.07 o 2 6 2 247.02 274.49 5.72 o 3 6 2 7.62 6.72 1.51 o 4 6 2 454.62 416.79 11.21 o 5 6 2 0.14 -0.49 1.83 o 6 6 2 63.78 62.49 3.85 o 7 6 2 422.23 398.21 10.61 o 8 6 2 34.43 43.84 5.62 o -9 7 2 9.25 13.28 5.29 o -8 7 2 25.17 43.47 5.32 o -7 7 2 171.27 178.26 5.41 o -6 7 2 0.04 2.19 1.84 o -5 7 2 913.63 921.75 19.15 o -4 7 2 517.00 529.38 11.06 o -3 7 2 422.41 399.36 8.72 o -2 7 2 2125.60 2146.49 40.12 o -1 7 2 608.55 636.06 11.75 o 0 7 2 271.06 284.54 7.70 o 1 7 2 817.34 861.64 16.81 o 2 7 2 149.92 144.34 5.44 o 3 7 2 35.04 25.67 1.90 o 4 7 2 0.05 7.56 6.49 o 5 7 2 177.39 179.72 4.87 o 6 7 2 147.33 140.51 5.92 o 7 7 2 102.87 116.16 5.54 o 8 7 2 127.75 138.17 15.78 o -8 8 2 165.30 132.58 8.86 o -7 8 2 71.67 70.01 4.15 o -6 8 2 16.13 12.57 3.08 o -5 8 2 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