#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/19/2201981.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201981_Fobs loop_ _publ_author_name 'Kaafarani, Bilal R.' 'Wex, Brigitte' 'Oliver, Allen G.' 'Krause Bauer, Jeanette A.' 'Neckers, Douglas C.' _publ_section_title ; \p--\p-Stacking and nitro--\p-stacking interactions of 1-(4-nitrophenyl)-4-phenyl-2,4-bis(phenylethynyl)butadiene ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o227 _journal_page_last o229 _journal_volume 59 _journal_year 2003 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 100.093 _cell_angle_gamma 90.000 _cell_length_a 13.5829 _cell_length_b 7.6515 _cell_length_c 23.3987 _exptl_crystal_F_000 944.00 _reflns_d_resolution_high 0.9000 _[local]_cod_data_source_file fl60164sup2.hkl _[local]_cod_data_source_block 4 #BEGIN Tags that were not found in dictionaries: _shelx_title ' uc02185s in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 232.04 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1.65 5.61 0.79 o 2 0 0 154.80 126.74 15.72 o 3 0 0 2051.03 1849.27 241.06 o 4 0 0 1360.95 1227.95 160.68 o 5 0 0 15.26 14.40 3.66 o 6 0 0 1498.19 1230.48 160.40 o 7 0 0 73.49 78.89 11.55 o 8 0 0 305.15 325.81 37.53 o 9 0 0 0.05 6.96 8.02 o 10 0 0 1603.63 1105.85 139.65 o 11 0 0 74.14 82.10 14.13 o 12 0 0 977.14 680.63 87.41 o 13 0 0 172.53 135.05 25.55 o 14 0 0 36.11 30.72 17.10 o 1 1 0 210.71 169.68 12.16 o 2 1 0 8222.57 8021.38 619.80 o 3 1 0 1099.23 1131.85 101.73 o 4 1 0 73.39 73.73 7.59 o 5 1 0 913.45 880.07 81.23 o 6 1 0 279.66 237.45 23.41 o 7 1 0 8.45 11.87 3.02 o 8 1 0 0.68 3.73 3.62 o 9 1 0 295.28 261.71 24.99 o 10 1 0 2.80 19.37 8.73 o 11 1 0 1754.00 1431.56 154.23 o 12 1 0 330.85 294.26 36.84 o 13 1 0 5.74 7.07 10.06 o 14 1 0 4.13 25.73 13.00 o 0 2 0 4.15 0.69 1.59 o 1 2 0 3029.68 3137.15 235.36 o 2 2 0 5388.95 5175.16 365.24 o 3 2 0 2577.21 2363.22 197.95 o 4 2 0 888.03 848.56 75.78 o 5 2 0 6971.29 7215.24 642.03 o 6 2 0 1777.93 1890.06 168.47 o 7 2 0 36.77 56.70 6.63 o 8 2 0 6.36 -0.03 4.39 o 9 2 0 452.64 455.61 37.25 o 10 2 0 290.24 284.86 32.52 o 11 2 0 6.56 11.16 7.61 o 12 2 0 0.00 -0.50 9.24 o 13 2 0 293.01 332.72 34.64 o 14 2 0 28.80 53.68 13.94 o 1 3 0 3.53 1.56 2.11 o 2 3 0 15.25 16.26 2.45 o 3 3 0 199.09 208.44 14.90 o 4 3 0 1274.42 1306.40 101.08 o 5 3 0 343.38 384.16 34.74 o 6 3 0 822.32 861.50 77.24 o 7 3 0 906.20 965.22 85.83 o 8 3 0 285.17 326.31 29.88 o 9 3 0 61.22 71.19 8.59 o 10 3 0 321.83 346.56 34.63 o 11 3 0 111.69 143.14 18.05 o 12 3 0 41.80 56.39 12.09 o 13 3 0 142.61 199.51 22.09 o 0 4 0 2556.11 2651.00 265.73 o 1 4 0 473.14 468.38 33.42 o 2 4 0 493.39 512.01 38.72 o 3 4 0 1526.97 1561.34 117.08 o 4 4 0 10.11 18.48 3.38 o 5 4 0 273.93 253.75 20.01 o 6 4 0 22.50 19.36 6.26 o 7 4 0 767.73 803.87 77.51 o 8 4 0 147.42 155.25 15.82 o 9 4 0 118.90 132.58 14.60 o 10 4 0 0.36 7.25 8.47 o 11 4 0 426.30 447.68 37.65 o 12 4 0 7.16 23.70 14.66 o 13 4 0 104.97 88.98 35.72 o 1 5 0 955.32 937.73 66.58 o 2 5 0 303.52 290.99 21.11 o 3 5 0 48.10 45.62 5.22 o 4 5 0 617.27 582.57 44.04 o 5 5 0 139.68 155.81 13.41 o 6 5 0 0.64 4.79 7.19 o 7 5 0 394.76 409.03 42.14 o 8 5 0 494.15 525.37 52.61 o 9 5 0 8.79 7.48 11.39 o 10 5 0 0.25 2.84 11.85 o 11 5 0 118.70 173.98 21.05 o 12 5 0 24.72 35.08 17.13 o 0 6 0 537.06 485.55 49.10 o 1 6 0 49.64 48.69 5.84 o 2 6 0 28.90 34.73 5.50 o 3 6 0 149.71 177.42 13.91 o 4 6 0 81.15 89.82 9.00 o 5 6 0 6.15 11.53 5.88 o 6 6 0 101.29 106.29 13.16 o 7 6 0 77.95 94.05 13.19 o 8 6 0 154.55 169.48 23.36 o 9 6 0 629.38 618.07 64.15 o 10 6 0 204.98 210.74 27.94 o 1 7 0 23.68 50.59 10.20 o 2 7 0 13.98 19.53 6.77 o 3 7 0 25.92 38.64 7.62 o 4 7 0 147.66 150.47 13.19 o 5 7 0 2.46 16.16 8.25 o 6 7 0 46.92 21.57 17.12 o 7 7 0 32.70 26.38 13.75 o 8 7 0 322.09 277.21 29.21 o 0 8 0 36.28 33.15 13.94 o 1 8 0 1.92 12.18 9.45 o 2 8 0 0.32 4.53 9.79 o 3 8 0 0.69 0.76 10.09 o 4 8 0 2.13 -10.18 11.09 o 5 8 0 30.37 18.08 15.33 o -14 1 1 53.02 73.94 16.57 o -13 1 1 27.93 24.93 10.41 o -12 1 1 3.09 8.47 7.75 o -11 1 1 148.84 142.54 16.49 o -10 1 1 227.91 203.23 23.73 o -9 1 1 10.07 4.87 4.19 o -8 1 1 26.52 22.17 4.69 o -7 1 1 10.33 2.39 2.72 o -6 1 1 97.73 102.64 9.78 o -5 1 1 676.02 647.77 64.68 o -4 1 1 578.47 595.95 59.33 o -3 1 1 1426.04 1412.06 127.50 o -2 1 1 16628.04 15843.82 1340.86 o -1 1 1 151.68 147.35 11.06 o 0 1 1 1128.56 1091.97 81.15 o 1 1 1 64.67 53.25 3.89 o 2 1 1 368.13 360.31 34.64 o 3 1 1 233.75 232.53 20.84 o 4 1 1 117.43 98.95 9.95 o 5 1 1 11.64 12.99 3.31 o 6 1 1 391.64 412.45 37.68 o 7 1 1 86.96 80.71 8.36 o 8 1 1 303.82 265.04 24.86 o 9 1 1 300.79 314.18 42.53 o 10 1 1 790.24 638.74 71.39 o 11 1 1 367.15 357.93 46.72 o 12 1 1 38.52 13.87 9.22 o 13 1 1 132.82 147.31 19.48 o 14 1 1 150.51 158.31 19.68 o -14 2 1 97.53 97.60 16.56 o -13 2 1 540.94 558.38 49.37 o -12 2 1 241.54 280.17 26.05 o -11 2 1 0.12 0.41 7.47 o -10 2 1 137.28 148.50 13.68 o -9 2 1 83.61 100.72 9.63 o -8 2 1 127.67 136.43 11.80 o -7 2 1 267.00 301.60 24.11 o -6 2 1 12.67 7.99 3.47 o -5 2 1 13.15 8.47 4.00 o -4 2 1 96.78 97.65 9.21 o -3 2 1 3293.89 3200.94 263.49 o -2 2 1 177.75 135.10 11.12 o -1 2 1 5585.04 5510.67 393.49 o 0 2 1 1853.37 1818.12 138.33 o 1 2 1 53843.31 52838.48 3761.40 o 2 2 1 6697.24 6939.52 493.38 o 3 2 1 2811.27 2672.49 197.81 o 4 2 1 643.98 635.18 56.97 o 5 2 1 242.90 320.55 28.74 o 6 2 1 2.51 5.32 3.65 o 7 2 1 382.82 407.27 36.72 o 8 2 1 153.88 151.41 14.37 o 9 2 1 141.45 156.90 15.04 o 10 2 1 357.82 372.94 33.89 o 11 2 1 246.20 232.73 23.35 o 12 2 1 431.20 443.82 49.19 o 13 2 1 1.79 -5.05 11.78 o 14 2 1 0.13 -14.31 14.31 o -13 3 1 84.02 76.20 14.60 o -12 3 1 1.38 -7.50 10.24 o -11 3 1 379.83 379.02 31.30 o -10 3 1 675.00 695.30 55.30 o -9 3 1 30.78 34.35 6.55 o -8 3 1 152.69 195.08 16.41 o -7 3 1 513.52 545.09 48.72 o -6 3 1 43.74 64.33 7.11 o -5 3 1 0.17 -0.19 3.43 o -4 3 1 57.90 49.32 4.76 o -3 3 1 788.06 726.75 54.62 o -2 3 1 3.11 4.45 1.96 o -1 3 1 4.40 10.06 2.20 o 0 3 1 235.14 195.27 15.17 o 1 3 1 310.25 342.05 27.92 o 2 3 1 820.51 732.29 52.12 o 3 3 1 30.09 41.81 3.70 o 4 3 1 2683.60 2793.32 216.34 o 5 3 1 919.92 839.10 75.36 o 6 3 1 22.42 18.03 4.65 o 7 3 1 2.85 2.11 4.92 o 8 3 1 188.46 224.76 21.35 o 9 3 1 464.39 475.61 38.25 o 10 3 1 649.19 699.25 56.46 o 11 3 1 17.92 30.14 9.72 o 12 3 1 90.88 108.80 14.79 o 13 3 1 121.24 112.63 17.30 o -13 4 1 79.29 175.27 26.83 o -12 4 1 1.32 8.77 17.34 o -11 4 1 59.55 86.40 16.74 o -10 4 1 881.87 882.21 71.36 o -9 4 1 77.62 88.10 10.37 o -8 4 1 181.05 216.97 20.68 o -7 4 1 500.55 553.64 50.22 o -6 4 1 0.13 -5.61 5.61 o -5 4 1 643.52 604.17 48.84 o -4 4 1 33.22 40.57 4.35 o -3 4 1 64.09 84.08 6.91 o -2 4 1 139.87 132.22 9.75 o -1 4 1 1096.31 1073.78 76.23 o 0 4 1 127.06 144.19 10.75 o 1 4 1 2397.64 2414.62 181.79 o 2 4 1 129.70 148.45 11.72 o 3 4 1 115.33 131.72 10.46 o 4 4 1 58.88 54.16 5.10 o 5 4 1 628.03 594.27 48.32 o 6 4 1 236.56 260.57 24.42 o 7 4 1 651.91 617.95 55.62 o 8 4 1 30.34 23.28 7.38 o 9 4 1 64.50 72.63 10.62 o 10 4 1 672.13 663.84 52.78 o 11 4 1 213.04 272.32 27.32 o 12 4 1 256.13 288.37 51.24 o -12 5 1 34.30 54.41 19.98 o -11 5 1 1.87 36.51 16.54 o -10 5 1 6.04 -2.02 11.90 o -9 5 1 358.62 432.93 44.39 o -8 5 1 323.42 387.23 40.29 o -7 5 1 40.36 60.05 10.23 o -6 5 1 239.43 261.94 27.43 o -5 5 1 661.10 694.95 51.54 o -4 5 1 180.00 195.93 14.48 o -3 5 1 102.87 129.47 10.60 o -2 5 1 43.96 51.85 5.17 o -1 5 1 144.09 157.81 11.32 o 0 5 1 39.57 50.83 5.07 o 1 5 1 107.62 126.27 9.71 o 2 5 1 94.33 97.18 7.86 o 3 5 1 24.26 29.52 5.03 o 4 5 1 196.97 217.51 17.01 o 5 5 1 42.10 61.19 6.79 o 6 5 1 144.59 157.61 15.84 o 7 5 1 226.96 274.92 32.47 o 8 5 1 82.91 84.60 11.96 o 9 5 1 106.92 127.55 15.98 o 10 5 1 19.81 33.39 12.67 o 11 5 1 34.39 28.55 14.84 o -10 6 1 282.82 276.69 29.11 o -9 6 1 8.74 7.45 11.68 o -8 6 1 1.42 7.20 10.12 o -7 6 1 134.91 142.71 15.95 o -6 6 1 1114.82 974.06 76.55 o -5 6 1 306.66 326.56 23.51 o -4 6 1 2.61 7.90 5.60 o -3 6 1 9.89 12.41 5.30 o -2 6 1 476.29 470.75 33.92 o -1 6 1 46.62 56.72 6.28 o 0 6 1 139.63 172.43 13.34 o 1 6 1 527.98 474.56 34.09 o 2 6 1 144.30 152.40 12.18 o 3 6 1 107.18 107.69 9.46 o 4 6 1 100.35 94.07 9.29 o 5 6 1 9.50 13.24 6.15 o 6 6 1 0.63 10.40 8.91 o 7 6 1 104.31 121.85 17.44 o 8 6 1 230.69 266.64 30.10 o 9 6 1 37.55 70.02 17.13 o 10 6 1 107.64 169.33 27.63 o -8 7 1 12.77 -12.51 18.07 o -7 7 1 124.59 76.61 14.71 o -6 7 1 460.42 406.96 39.44 o -5 7 1 434.11 381.66 29.72 o -4 7 1 118.11 126.69 12.00 o -3 7 1 17.58 29.77 7.37 o -2 7 1 247.86 277.41 20.99 o -1 7 1 36.17 41.37 7.21 o 0 7 1 243.70 242.40 18.61 o 1 7 1 0.00 2.60 6.36 o 2 7 1 62.11 51.92 7.92 o 3 7 1 47.97 34.63 7.56 o 4 7 1 114.07 115.35 12.13 o 5 7 1 4.65 6.80 8.38 o 6 7 1 13.64 10.58 12.06 o 7 7 1 24.81 23.26 13.74 o 8 7 1 37.38 -0.67 26.74 o -5 8 1 470.86 384.76 38.54 o -4 8 1 41.46 24.89 15.47 o -3 8 1 34.63 43.53 12.71 o -2 8 1 0.45 22.27 9.97 o -1 8 1 201.07 186.23 16.86 o 0 8 1 0.54 -5.33 9.33 o 1 8 1 41.86 50.50 10.32 o 2 8 1 81.86 88.19 11.91 o 3 8 1 119.10 112.14 14.71 o 4 8 1 92.56 74.54 12.97 o -15 0 2 21.04 -2.92 16.00 o -14 0 2 63.17 77.77 31.26 o -13 0 2 1034.53 865.70 130.92 o -12 0 2 2117.24 1368.84 315.30 o -11 0 2 229.24 196.67 69.83 o -10 0 2 3.86 15.10 7.57 o -9 0 2 388.85 364.45 48.64 o -8 0 2 18.86 10.80 5.07 o -7 0 2 350.00 348.26 45.75 o -6 0 2 6191.24 6629.84 1038.67 o -5 0 2 2041.49 1799.52 291.41 o -4 0 2 673.25 661.08 74.79 o -3 0 2 23.66 18.78 3.08 o -2 0 2 2584.04 2242.76 252.35 o -1 0 2 1905.94 1807.55 289.75 o 0 0 2 15419.17 12210.38 1820.50 o 1 0 2 17.22 24.99 4.09 o 2 0 2 30879.63 24902.37 4032.58 o 3 0 2 3.26 7.84 3.87 o 4 0 2 1234.13 1079.23 138.04 o 5 0 2 474.74 469.77 75.86 o 6 0 2 252.24 216.48 28.14 o 7 0 2 0.09 7.32 7.00 o 8 0 2 6.90 -1.47 5.71 o 9 0 2 45.25 39.38 8.64 o 10 0 2 7022.72 5719.49 746.22 o 11 0 2 387.17 312.36 42.58 o 12 0 2 343.38 285.84 37.87 o 13 0 2 91.09 68.42 18.70 o 14 0 2 87.95 92.87 37.04 o -14 1 2 208.68 245.08 55.00 o -13 1 2 145.89 155.36 24.85 o -12 1 2 0.18 5.61 6.78 o -11 1 2 602.91 496.44 45.70 o -10 1 2 11.12 12.47 4.74 o -9 1 2 22.23 23.08 4.89 o -8 1 2 701.82 655.63 58.09 o -7 1 2 111.74 121.03 11.40 o -6 1 2 100.03 111.06 9.19 o -5 1 2 200.92 207.22 18.51 o -4 1 2 205.19 220.06 20.11 o -3 1 2 1138.24 1053.95 106.68 o -2 1 2 4690.41 4296.24 364.77 o -1 1 2 883.30 789.44 57.90 o 0 1 2 955.98 862.38 67.58 o 1 1 2 49.76 57.68 4.71 o 2 1 2 122.14 104.53 9.44 o 3 1 2 4096.80 3799.77 373.22 o 4 1 2 524.21 574.19 51.28 o 5 1 2 9.12 12.69 2.78 o 6 1 2 268.75 301.81 33.00 o 7 1 2 193.62 225.48 21.90 o 8 1 2 69.78 84.65 10.32 o 9 1 2 1.04 -5.33 5.33 o 10 1 2 4.17 4.79 6.33 o 11 1 2 4492.76 3690.40 403.57 o 12 1 2 106.35 90.84 12.75 o 13 1 2 194.30 192.63 36.40 o 14 1 2 162.91 196.41 25.70 o -14 2 2 47.97 43.29 17.62 o -13 2 2 6.77 1.27 11.04 o -12 2 2 105.56 128.89 17.40 o -11 2 2 184.65 236.77 25.64 o -10 2 2 527.22 519.35 41.19 o -9 2 2 48.32 53.24 7.27 o -8 2 2 242.64 269.14 21.93 o -7 2 2 737.80 851.49 68.34 o -6 2 2 1980.64 2118.45 203.06 o -5 2 2 8.69 14.65 3.58 o -4 2 2 2.91 12.55 2.63 o -3 2 2 141.75 178.74 15.63 o -2 2 2 555.31 619.04 43.89 o -1 2 2 10473.09 9622.51 723.31 o 0 2 2 33801.12 32033.85 2380.17 o 1 2 2 9227.00 9156.65 644.27 o 2 2 2 311.64 301.03 22.28 o 3 2 2 79.74 79.18 6.53 o 4 2 2 3649.14 3466.70 308.12 o 5 2 2 2192.38 2443.44 258.35 o 6 2 2 819.29 823.78 79.88 o 7 2 2 97.21 145.01 13.77 o 8 2 2 975.54 946.19 93.37 o 9 2 2 120.58 110.19 11.65 o 10 2 2 7.37 2.96 6.95 o 11 2 2 1555.94 1412.53 136.73 o 12 2 2 3.33 2.03 9.61 o 13 2 2 21.57 10.20 11.91 o 14 2 2 13.85 11.59 15.31 o -14 3 2 0.40 40.28 43.05 o -13 3 2 88.95 151.45 27.22 o -12 3 2 343.57 381.23 46.90 o -11 3 2 215.91 245.13 25.76 o -10 3 2 80.49 106.02 16.61 o -9 3 2 243.20 280.55 23.70 o -8 3 2 11.49 10.21 4.75 o -7 3 2 172.61 202.53 19.10 o -6 3 2 1694.54 1849.83 164.93 o -5 3 2 172.20 175.09 16.55 o -4 3 2 27.21 29.81 3.44 o -3 3 2 188.40 187.12 14.22 o -2 3 2 55.17 85.84 6.46 o -1 3 2 93.32 117.41 9.08 o 0 3 2 202.76 203.02 15.70 o 1 3 2 88.92 114.55 8.57 o 2 3 2 4729.81 4548.05 322.93 o 3 3 2 210.25 243.83 18.37 o 4 3 2 747.94 821.28 64.52 o 5 3 2 199.38 203.53 17.54 o 6 3 2 286.43 357.98 35.08 o 7 3 2 13.97 5.18 5.29 o 8 3 2 401.90 413.47 37.50 o 9 3 2 1.35 10.67 7.11 o 10 3 2 583.59 545.10 47.94 o 11 3 2 2.08 7.02 9.69 o 12 3 2 53.55 33.49 12.50 o 13 3 2 79.11 91.28 17.76 o -13 4 2 142.87 169.42 25.54 o -12 4 2 228.09 293.48 36.93 o -11 4 2 0.00 -11.34 11.34 o -10 4 2 104.92 121.76 16.08 o -9 4 2 0.10 -3.11 7.20 o -8 4 2 18.76 19.63 7.58 o -7 4 2 22.50 21.56 6.59 o -6 4 2 704.14 753.01 75.52 o -5 4 2 13.63 15.13 4.51 o -4 4 2 461.31 449.07 32.02 o -3 4 2 396.61 399.95 28.40 o -2 4 2 5.78 -1.34 2.77 o -1 4 2 1.36 -0.33 2.50 o 0 4 2 561.49 551.94 41.33 o 1 4 2 2.49 4.75 2.80 o 2 4 2 1651.60 1578.61 126.08 o 3 4 2 1716.97 1623.26 114.82 o 4 4 2 1256.70 1137.24 83.78 o 5 4 2 217.72 224.21 19.45 o 6 4 2 451.84 445.32 43.62 o 7 4 2 80.16 88.10 10.66 o 8 4 2 3.42 -6.44 7.21 o 9 4 2 700.61 712.83 62.99 o 10 4 2 315.79 337.76 31.54 o 11 4 2 88.50 106.35 18.78 o 12 4 2 14.72 -8.67 19.84 o -12 5 2 46.71 78.26 21.07 o -11 5 2 38.58 44.63 17.08 o -10 5 2 77.54 105.05 16.96 o -9 5 2 24.21 14.30 12.68 o -8 5 2 131.83 169.50 19.56 o -7 5 2 258.84 259.64 24.89 o -6 5 2 78.07 94.56 9.79 o -5 5 2 79.13 80.21 7.00 o -4 5 2 236.18 236.09 17.36 o -3 5 2 121.82 142.39 12.15 o -2 5 2 7.33 6.99 3.38 o -1 5 2 10.38 12.34 3.40 o 0 5 2 41.22 36.55 5.40 o 1 5 2 19.79 31.04 4.08 o 2 5 2 4.83 11.39 3.87 o 3 5 2 40.53 40.23 5.23 o 4 5 2 129.27 141.89 13.14 o 5 5 2 847.62 790.58 66.75 o 6 5 2 92.01 103.08 10.68 o 7 5 2 462.20 450.08 41.47 o 8 5 2 292.94 324.29 30.85 o 9 5 2 15.10 16.98 10.79 o 10 5 2 25.94 51.35 13.60 o 11 5 2 261.72 362.83 38.27 o -10 6 2 20.38 93.02 21.34 o -9 6 2 145.55 175.45 23.01 o -8 6 2 74.37 93.03 13.54 o -7 6 2 136.76 129.38 15.07 o -6 6 2 8.83 2.72 7.22 o -5 6 2 89.79 101.47 9.17 o -4 6 2 81.44 104.57 9.25 o -3 6 2 60.89 68.43 7.05 o 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