#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2201995.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201995_Fobs loop_ _publ_author_name 'Vincendeau, Sandrine' 'Colli\`ere, Vincent' 'Faulmann, Christophe' _publ_section_title ; Cp~2~Ti(dddse): a well known precursor for Se-containing donors ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m268 _journal_page_last m270 _journal_volume 59 _journal_year 2003 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 94.648 _cell_angle_gamma 90.000 _cell_length_a 12.7474 _cell_length_b 10.9055 _cell_length_c 21.5888 _exptl_crystal_F_000 1760.00 _reflns_d_resolution_high 0.8078 _[local]_cod_data_source_file fl60302sup2.hkl _[local]_cod_data_source_block 2 #BEGIN Tags that were not found in dictionaries: _shelx_title ' cp2ti(dddse) in P 21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 417.23 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4342.67 4041.20 326.37 o 3 0 0 751.61 708.61 252.68 o 4 0 0 43942.00 42340.95 2152.87 o 5 0 0 50030.38 48482.23 2384.14 o 6 0 0 198.88 120.87 138.67 o 7 0 0 19023.60 17092.36 1248.95 o 8 0 0 235.14 360.74 137.70 o 9 0 0 71.78 57.08 124.44 o 10 0 0 153.47 233.49 150.92 o 11 0 0 29952.10 29708.37 1696.19 o 12 0 0 20490.51 21671.61 1274.01 o 13 0 0 1571.70 1467.63 118.15 o 14 0 0 5319.09 5331.51 270.56 o 15 0 0 1119.75 1018.08 106.51 o 1 1 0 787.44 687.54 119.35 o 2 1 0 85870.23 78834.66 2021.64 o 3 1 0 24710.38 24832.37 651.22 o 4 1 0 128389.80 126906.82 4722.22 o 5 1 0 125.91 43.70 109.52 o 6 1 0 7692.08 6555.93 131.93 o 7 1 0 2805.37 2529.07 142.79 o 8 1 0 64486.23 59610.95 1578.05 o 9 1 0 6626.92 6774.98 192.20 o 10 1 0 261.42 246.02 80.12 o 11 1 0 293.66 374.14 81.64 o 12 1 0 82.88 172.08 103.93 o 13 1 0 14519.69 14712.29 637.11 o 14 1 0 631.85 709.09 90.57 o 15 1 0 9346.05 8548.72 369.99 o 1 2 0 242.36 242.10 132.14 o 2 2 0 1988.51 2049.12 132.63 o 3 2 0 13347.52 13435.29 193.45 o 4 2 0 54086.64 51442.17 1268.01 o 5 2 0 3154.90 2965.67 102.13 o 6 2 0 2837.96 2949.94 98.97 o 7 2 0 27193.98 27024.24 536.28 o 8 2 0 1356.34 1376.80 92.76 o 9 2 0 828.80 855.37 82.01 o 10 2 0 294.00 260.69 71.57 o 11 2 0 29202.24 30484.20 730.23 o 12 2 0 8698.36 9896.35 229.94 o 13 2 0 138.55 230.44 105.24 o 14 2 0 1270.03 1288.03 144.35 o 15 2 0 5.18 27.25 76.39 o 1 3 0 12076.99 12447.13 179.50 o 2 3 0 2560.30 2885.49 120.90 o 3 3 0 41821.67 41890.10 431.68 o 4 3 0 32739.20 31104.10 437.52 o 5 3 0 4983.55 4732.57 116.75 o 6 3 0 2622.70 2678.07 122.05 o 7 3 0 244.71 175.03 88.13 o 8 3 0 18581.63 17773.01 201.05 o 9 3 0 13.86 -20.90 80.69 o 10 3 0 3847.54 3799.32 89.78 o 11 3 0 5893.10 6594.31 109.35 o 12 3 0 7548.18 8198.54 133.34 o 13 3 0 3138.68 3090.72 90.55 o 14 3 0 1024.97 950.86 80.91 o 15 3 0 2027.55 1680.96 115.79 o 0 4 0 34336.63 35993.73 258.34 o 1 4 0 5080.14 5122.02 114.42 o 2 4 0 331.41 348.95 97.06 o 3 4 0 9864.36 9493.05 201.99 o 4 4 0 29754.52 27965.24 426.97 o 5 4 0 861.98 657.28 83.31 o 6 4 0 2480.82 2281.37 80.48 o 7 4 0 5603.62 5215.22 167.63 o 8 4 0 985.21 1064.52 75.18 o 9 4 0 1607.46 1825.73 85.76 o 10 4 0 1360.54 1509.78 74.13 o 11 4 0 3388.40 3650.45 104.58 o 12 4 0 278.99 198.57 86.73 o 13 4 0 1822.24 2001.81 101.14 o 14 4 0 25.90 55.74 72.57 o 1 5 0 24244.16 24786.40 392.37 o 2 5 0 9150.45 8733.39 105.95 o 3 5 0 3680.26 3530.89 82.11 o 4 5 0 3593.62 3324.38 82.52 o 5 5 0 4525.98 4263.01 97.53 o 6 5 0 60.95 3.69 73.71 o 7 5 0 257.21 206.28 77.76 o 8 5 0 2273.73 2274.96 96.85 o 9 5 0 88.48 122.33 67.28 o 10 5 0 2382.76 2626.09 94.60 o 11 5 0 3672.72 4225.88 130.92 o 12 5 0 5481.89 5754.97 156.78 o 13 5 0 749.08 718.48 87.75 o 14 5 0 21.74 -26.29 71.98 o 0 6 0 4018.07 3908.28 161.54 o 1 6 0 2042.19 2037.84 85.31 o 2 6 0 19267.42 20080.63 189.57 o 3 6 0 72.60 72.22 65.09 o 4 6 0 462.86 480.96 65.19 o 5 6 0 13638.30 13405.50 203.74 o 6 6 0 316.28 308.49 69.33 o 7 6 0 5732.67 5759.41 265.63 o 8 6 0 17.41 142.34 71.04 o 9 6 0 5466.54 5611.37 189.10 o 10 6 0 199.46 272.25 97.34 o 11 6 0 7.58 144.92 118.01 o 12 6 0 48.45 76.50 111.09 o 13 6 0 1043.06 983.44 97.66 o 14 6 0 20.08 473.20 85.94 o 1 7 0 30337.66 31083.43 218.68 o 2 7 0 1079.71 1062.34 78.85 o 3 7 0 819.17 1038.73 72.42 o 4 7 0 8315.31 8643.19 155.66 o 5 7 0 1261.89 1238.48 65.08 o 6 7 0 2610.32 2713.61 103.58 o 7 7 0 1842.98 2022.78 145.47 o 8 7 0 306.04 330.76 98.47 o 9 7 0 23.82 45.74 76.94 o 10 7 0 1873.18 2075.23 137.18 o 11 7 0 1771.93 1792.70 108.72 o 12 7 0 2316.19 2342.25 102.02 o 13 7 0 10571.02 9903.98 244.57 o 0 8 0 25033.26 25972.29 663.16 o 1 8 0 344.10 293.13 78.46 o 2 8 0 7914.98 8361.01 89.26 o 3 8 0 647.17 694.67 73.71 o 4 8 0 3616.84 3497.05 72.85 o 5 8 0 27925.32 28931.32 514.01 o 6 8 0 15.47 -76.67 89.08 o 7 8 0 9488.74 10275.77 225.92 o 8 8 0 3466.86 3756.99 131.29 o 9 8 0 18169.13 19988.33 621.67 o 10 8 0 207.28 227.52 75.26 o 11 8 0 2979.43 2745.29 90.23 o 12 8 0 2356.74 1913.68 123.86 o 1 9 0 26714.85 28082.69 455.02 o 2 9 0 2766.45 3003.14 117.06 o 3 9 0 138.43 114.55 69.77 o 4 9 0 16143.60 17876.09 167.48 o 5 9 0 1069.76 1139.47 79.25 o 6 9 0 2398.40 2639.66 103.75 o 7 9 0 1014.77 1093.53 74.54 o 8 9 0 679.28 768.04 124.68 o 9 9 0 1993.43 2196.58 82.89 o 10 9 0 1514.71 1374.26 86.91 o 11 9 0 454.12 399.98 90.55 o 0 10 0 14672.97 15496.64 157.44 o 1 10 0 201.93 140.13 79.59 o 2 10 0 10475.91 12069.05 164.59 o 3 10 0 2898.97 3185.06 91.58 o 4 10 0 35.46 13.79 83.06 o 5 10 0 7820.33 8267.38 141.59 o 6 10 0 72.98 54.33 69.06 o 7 10 0 21.09 -42.33 77.88 o 8 10 0 980.70 1081.45 141.43 o 9 10 0 6599.76 6433.93 374.52 o 10 10 0 1355.38 1110.39 122.30 o 1 11 0 36.04 56.75 81.44 o 2 11 0 5184.88 5664.65 208.25 o 3 11 0 730.94 653.05 73.43 o 4 11 0 1039.11 1030.88 71.09 o 5 11 0 3018.67 3127.02 75.53 o 6 11 0 8284.73 8494.00 215.30 o 7 11 0 3.14 -44.91 78.05 o 8 11 0 1827.26 1811.55 89.43 o 9 11 0 1586.56 2212.14 133.23 o 0 12 0 844.06 830.46 241.10 o 1 12 0 336.15 323.86 77.55 o 2 12 0 8613.87 9134.67 124.28 o 3 12 0 541.95 579.02 97.31 o 4 12 0 35.32 27.81 81.87 o 5 12 0 468.69 522.44 73.27 o 6 12 0 558.85 389.05 103.00 o 7 12 0 343.11 217.24 119.65 o 1 13 0 19.76 -77.45 77.45 o 2 13 0 1140.67 870.40 124.16 o 3 13 0 73.85 -61.30 61.30 o -15 1 1 10.03 -18.67 72.93 o -14 1 1 1233.86 1115.36 92.47 o -13 1 1 72.08 14.61 87.90 o -12 1 1 1812.12 2052.13 127.00 o -11 1 1 12400.40 12263.86 262.09 o -10 1 1 462.37 300.39 87.83 o -9 1 1 247.77 151.08 83.10 o -8 1 1 1671.72 1629.39 106.52 o -7 1 1 1319.17 1295.30 99.22 o -6 1 1 12078.47 10435.07 226.54 o -5 1 1 295.39 290.57 96.57 o -4 1 1 2849.14 2804.59 149.31 o -3 1 1 35.76 43.06 154.84 o -2 1 1 20038.87 19225.84 370.86 o -1 1 1 3937.55 4060.60 172.47 o 0 1 1 234.73 212.66 225.30 o 1 1 1 206.82 166.88 126.22 o 2 1 1 16803.87 16391.89 359.33 o 3 1 1 12913.66 12363.30 319.38 o 4 1 1 11432.27 11231.43 305.04 o 5 1 1 523.03 350.17 110.47 o 6 1 1 28769.23 27317.41 712.78 o 7 1 1 240.36 319.46 109.43 o 8 1 1 80.27 122.86 91.56 o 9 1 1 5866.38 5783.40 169.84 o 10 1 1 506.92 481.36 95.04 o 11 1 1 336.59 420.04 91.79 o 12 1 1 414.02 349.66 88.44 o 13 1 1 46.44 57.80 99.44 o 14 1 1 36.10 -79.37 79.37 o 15 1 1 11.32 9.01 78.46 o -15 2 1 1685.29 1493.16 163.59 o -14 2 1 2066.85 2012.36 90.18 o -13 2 1 205.06 178.03 82.78 o -12 2 1 699.85 864.40 85.01 o -11 2 1 808.19 947.92 106.75 o -10 2 1 1108.02 1181.11 76.14 o -9 2 1 1954.30 1759.97 94.76 o -8 2 1 344.52 313.30 82.81 o -7 2 1 10662.94 10182.60 116.33 o -6 2 1 12917.74 11716.70 184.09 o -5 2 1 3136.05 2873.25 99.50 o -4 2 1 5.53 82.54 103.50 o -3 2 1 19456.97 19437.37 407.36 o -2 2 1 20809.88 21803.38 430.30 o -1 2 1 2785.16 2851.41 185.28 o 0 2 1 46817.01 51003.93 298.26 o 1 2 1 1205.49 1031.02 140.91 o 2 2 1 64076.05 65616.00 1263.06 o 3 2 1 11591.61 11735.40 270.46 o 4 2 1 12591.82 11338.90 199.72 o 5 2 1 2508.32 2184.45 99.20 o 6 2 1 5308.38 5326.72 149.16 o 7 2 1 5416.53 5368.58 139.40 o 8 2 1 918.23 910.21 97.83 o 9 2 1 1154.10 1122.93 81.79 o 10 2 1 2993.06 3139.23 109.75 o 11 2 1 1569.57 1602.39 92.60 o 12 2 1 2260.44 2610.79 90.72 o 13 2 1 322.95 292.97 82.99 o 14 2 1 1877.67 1877.48 93.29 o 15 2 1 1567.24 1192.47 88.42 o -15 3 1 615.47 454.49 91.60 o -14 3 1 838.43 727.80 154.48 o -13 3 1 186.57 78.10 80.99 o -12 3 1 7328.81 8163.75 165.11 o -11 3 1 23744.06 25444.76 474.17 o -10 3 1 11.77 87.53 76.00 o -9 3 1 447.04 421.68 80.43 o -8 3 1 217.00 248.58 92.75 o -7 3 1 15419.12 15475.99 148.85 o -6 3 1 46135.30 44052.53 976.75 o -5 3 1 242.56 137.07 82.29 o -4 3 1 32921.52 30967.45 690.06 o -3 3 1 490.97 536.60 85.89 o -2 3 1 46464.04 50666.38 762.16 o -1 3 1 20699.51 22625.50 278.36 o 0 3 1 58018.31 63678.19 819.23 o 1 3 1 23.63 69.50 126.95 o 2 3 1 13955.80 14376.10 260.98 o 3 3 1 20806.36 19952.95 383.47 o 4 3 1 22495.16 21221.02 438.24 o 5 3 1 328.79 239.60 75.73 o 6 3 1 36392.85 33821.12 915.81 o 7 3 1 3794.86 3354.09 93.93 o 8 3 1 556.16 429.26 75.07 o 9 3 1 1784.22 1700.22 90.46 o 10 3 1 848.99 792.08 79.09 o 11 3 1 8137.86 9096.68 130.00 o 12 3 1 68.24 50.80 80.02 o 13 3 1 14.26 1.07 81.96 o 14 3 1 139.91 231.21 83.29 o 15 3 1 820.69 526.78 79.28 o -15 4 1 2145.96 2253.30 139.04 o -14 4 1 391.86 337.92 81.92 o -13 4 1 156.25 105.93 87.79 o -12 4 1 139.03 281.42 93.98 o -11 4 1 1805.01 2007.56 108.88 o -10 4 1 1793.73 1934.47 75.72 o -9 4 1 407.23 450.65 66.51 o -8 4 1 2071.59 1995.14 82.78 o -7 4 1 20451.44 20044.56 530.70 o -6 4 1 13525.79 13642.14 475.84 o -5 4 1 61.60 99.68 76.18 o -4 4 1 1523.44 1388.13 79.22 o -3 4 1 42.15 62.86 77.23 o -2 4 1 28052.75 27101.42 253.57 o -1 4 1 14317.71 14870.94 146.34 o 0 4 1 59.56 78.30 98.59 o 1 4 1 22043.88 23012.53 218.76 o 2 4 1 34707.54 34013.00 363.43 o 3 4 1 1890.42 1937.93 96.49 o 4 4 1 10011.56 9543.38 183.68 o 5 4 1 4666.18 4508.63 91.45 o 6 4 1 22025.38 22278.49 472.21 o 7 4 1 10579.89 10152.51 214.89 o 8 4 1 6.15 12.60 79.15 o 9 4 1 3878.10 4077.96 129.72 o 10 4 1 5100.18 5288.14 94.91 o 11 4 1 2167.85 2179.87 102.03 o 12 4 1 1614.12 1658.19 101.02 o 13 4 1 463.78 361.16 80.29 o 14 4 1 1504.93 1569.52 87.23 o -14 5 1 412.44 280.33 83.24 o -13 5 1 98.70 29.82 74.81 o -12 5 1 237.62 284.20 81.82 o -11 5 1 15146.13 16592.95 172.60 o -10 5 1 72.75 226.04 93.49 o -9 5 1 7394.50 7684.32 202.90 o -8 5 1 3375.41 3146.70 83.40 o -7 5 1 15126.71 15165.83 441.53 o -6 5 1 23892.87 24088.95 575.60 o -5 5 1 7318.36 7315.88 175.16 o -4 5 1 13291.63 12778.38 313.77 o -3 5 1 623.98 549.40 88.36 o -2 5 1 30091.19 29850.32 300.36 o -1 5 1 39976.56 40992.05 165.55 o 0 5 1 6750.64 6613.26 102.10 o 1 5 1 45.27 35.57 87.72 o 2 5 1 309.80 323.25 76.14 o 3 5 1 745.20 607.89 69.53 o 4 5 1 8141.75 8103.24 148.27 o 5 5 1 6712.33 6977.49 200.77 o 6 5 1 15037.87 15317.27 217.42 o 7 5 1 14108.34 14151.42 378.81 o 8 5 1 463.94 536.72 66.66 o 9 5 1 283.58 235.76 79.71 o 10 5 1 7795.74 8489.60 148.80 o 11 5 1 5125.86 5420.07 107.56 o 12 5 1 1051.88 1012.46 78.90 o 13 5 1 54.54 69.49 74.70 o 14 5 1 57.81 -26.33 83.38 o -14 6 1 473.09 132.83 119.05 o -13 6 1 4.33 1.34 93.32 o -12 6 1 57.83 30.46 86.74 o -11 6 1 690.35 701.21 91.25 o -10 6 1 10612.05 11717.24 169.20 o -9 6 1 282.35 123.55 97.06 o -8 6 1 2747.49 2726.12 73.07 o -7 6 1 20107.58 20385.94 450.99 o -6 6 1 1121.52 1146.72 75.99 o -5 6 1 8.96 -16.85 73.05 o -4 6 1 404.94 374.11 91.48 o -3 6 1 5124.44 5381.34 94.17 o -2 6 1 5012.86 5136.19 108.21 o -1 6 1 2047.14 2075.20 81.64 o 0 6 1 4300.27 4409.18 87.16 o 1 6 1 9920.58 9953.40 119.08 o 2 6 1 40009.82 41560.36 288.32 o 3 6 1 15.37 16.71 68.03 o 4 6 1 2297.97 2213.68 70.68 o 5 6 1 32.51 57.58 70.58 o 6 6 1 7266.67 7354.88 240.89 o 7 6 1 20790.10 21007.22 536.28 o 8 6 1 2340.20 2215.69 71.60 o 9 6 1 5015.28 5266.67 169.22 o 10 6 1 5018.17 5336.18 139.74 o 11 6 1 1655.23 1635.09 145.78 o 12 6 1 707.10 861.98 88.61 o 13 6 1 2365.21 2239.47 90.46 o 14 6 1 141.71 458.62 124.01 o -13 7 1 229.69 442.97 114.49 o -12 7 1 194.65 118.54 96.28 o -11 7 1 4763.29 4991.78 101.62 o -10 7 1 34.70 74.12 82.71 o -9 7 1 171.37 145.90 99.59 o -8 7 1 4146.82 4493.94 100.77 o -7 7 1 4550.40 4902.72 136.49 o -6 7 1 12321.71 12362.07 263.18 o -5 7 1 0.24 -2.99 60.99 o -4 7 1 3796.72 3956.58 79.38 o -3 7 1 1067.47 1130.59 90.47 o -2 7 1 14489.65 14911.80 139.18 o -1 7 1 6030.60 5921.73 92.07 o 0 7 1 17158.78 16944.15 187.59 o 1 7 1 38.05 -52.07 81.05 o 2 7 1 1684.31 1643.34 79.19 o 3 7 1 2014.54 2066.11 85.17 o 4 7 1 80.28 68.90 61.59 o 5 7 1 6286.64 6146.30 124.83 o 6 7 1 8389.33 8608.14 126.68 o 7 7 1 9.31 -68.16 68.16 o 8 7 1 580.80 466.83 83.70 o 9 7 1 132.21 279.62 109.68 o 10 7 1 2145.16 2361.84 108.27 o 11 7 1 1160.09 1046.32 88.66 o 12 7 1 58.00 0.31 88.93 o 13 7 1 512.30 481.31 92.40 o -12 8 1 1525.61 1400.14 238.90 o -11 8 1 204.42 346.02 85.21 o -10 8 1 1939.38 1845.86 99.67 o -9 8 1 73.70 191.43 81.08 o -8 8 1 1066.11 1024.78 92.47 o -7 8 1 66.13 103.34 93.84 o -6 8 1 10.46 35.64 69.06 o -5 8 1 889.61 982.54 79.57 o -4 8 1 190.97 305.54 70.25 o -3 8 1 375.23 380.98 85.11 o -2 8 1 2844.70 2767.02 79.79 o -1 8 1 855.63 908.92 78.53 o 0 8 1 5474.41 5651.41 88.01 o 1 8 1 94.20 138.97 72.51 o 2 8 1 11685.59 12017.54 96.77 o 3 8 1 185.55 175.93 77.35 o 4 8 1 7529.57 7306.10 220.46 o 5 8 1 2374.14 2546.40 87.08 o 6 8 1 716.21 828.74 83.53 o 7 8 1 1601.25 1727.90 87.86 o 8 8 1 1775.80 1905.50 101.47 o 9 8 1 1859.32 1738.40 100.09 o 10 8 1 151.73 71.08 79.81 o 11 8 1 1562.53 1539.89 84.46 o 12 8 1 12.17 35.97 81.86 o -11 9 1 1106.88 823.22 84.50 o -10 9 1 470.37 460.62 78.11 o -9 9 1 63.04 60.77 76.97 o -8 9 1 1273.44 1243.11 81.70 o -7 9 1 1736.86 1805.08 81.21 o -6 9 1 356.19 529.37 85.86 o -5 9 1 4097.80 4548.17 154.59 o -4 9 1 5982.49 6363.09 90.45 o -3 9 1 309.97 393.03 69.24 o -2 9 1 13.58 -0.15 70.19 o -1 9 1 3827.74 4023.05 110.92 o 0 9 1 946.78 978.53 73.01 o 1 9 1 2810.45 3116.15 74.49 o 2 9 1 58.43 150.76 76.41 o 3 9 1 2299.80 2460.46 82.14 o 4 9 1 1453.77 1683.75 102.87 o 5 9 1 194.86 323.13 77.09 o 6 9 1 778.62 785.67 87.20 o 7 9 1 855.60 1050.67 89.83 o 8 9 1 277.85 276.71 72.40 o 9 9 1 4.05 -71.70 71.70 o 10 9 1 780.36 613.15 92.25 o 11 9 1 140.06 93.20 80.92 o -10 10 1 490.91 376.56 72.35 o -9 10 1 512.68 378.14 70.47 o -8 10 1 942.34 984.01 84.34 o -7 10 1 4421.40 4620.10 204.84 o -6 10 1 16.33 -33.77 78.69 o -5 10 1 662.27 579.22 100.72 o -4 10 1 267.83 249.59 77.75 o -3 10 1 1361.25 1329.02 94.93 o -2 10 1 413.83 499.97 86.01 o -1 10 1 35.39 132.76 135.40 o 0 10 1 6731.43 7480.67 95.58 o 1 10 1 259.62 244.74 79.69 o 2 10 1 102.21 180.36 78.59 o 3 10 1 6.46 -73.58 74.50 o 4 10 1 1165.21 1402.94 76.96 o 5 10 1 14825.47 16128.49 407.37 o 6 10 1 57.70 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