#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/20/2202010.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202010_Fobs loop_ _publ_author_name 'Chen, Hsiao Wei' 'Tiekink, Edward R. T.' _publ_section_title ; Chloro[tris(perfluorophenyl)phosphine]gold(I) ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m50 _journal_page_last m52 _journal_volume 59 _journal_year 2003 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.632 _cell_angle_gamma 90.000 _cell_length_a 15.4344 _cell_length_b 11.8116 _cell_length_c 22.4469 _exptl_crystal_F_000 2832.00 _reflns_d_resolution_high 0.7102 _[local]_cod_data_source_file lh6026Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Template texray.inf' _shelx_refln_list_code 4 _shelx_f_calc_maximum 654.70 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l 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19.84 146.56 o 20 1 0 20.33 93.90 152.96 o 21 1 0 14189.76 14466.25 565.62 o 0 2 0 310993.66 289847.31 6573.20 o 1 2 0 39.76 86.67 14.57 o 2 2 0 681.63 721.75 33.12 o 3 2 0 223.34 254.90 27.48 o 4 2 0 16555.72 17059.96 374.09 o 5 2 0 7597.08 7909.02 158.82 o 6 2 0 35366.33 37243.98 624.01 o 7 2 0 288.34 241.87 41.84 o 8 2 0 96372.55 95251.14 1545.78 o 9 2 0 1705.75 1622.88 75.85 o 10 2 0 4934.40 4794.40 137.34 o 11 2 0 63.65 -40.66 51.61 o 12 2 0 50570.86 50002.32 994.40 o 13 2 0 32.53 18.08 64.42 o 14 2 0 36450.53 36580.80 773.34 o 15 2 0 651.34 578.53 140.59 o 16 2 0 1088.45 1190.45 207.56 o 17 2 0 96.10 198.62 171.83 o 18 2 0 9966.39 9571.57 452.94 o 19 2 0 103.99 293.24 156.43 o 20 2 0 5258.79 5764.76 338.93 o 21 2 0 59.18 262.05 177.23 o 1 3 0 126862.95 131262.73 2453.96 o 2 3 0 9636.86 10287.81 167.30 o 3 3 0 5512.86 5449.16 141.67 o 4 3 0 23.97 23.18 23.26 o 5 3 0 66652.87 70202.05 1513.98 o 6 3 0 6526.33 6194.32 169.80 o 7 3 0 50269.49 51437.20 855.70 o 8 3 0 1574.29 1491.88 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8337.51 375.12 o 19 4 0 785.16 686.74 339.08 o 20 4 0 5119.78 5098.91 318.44 o 1 5 0 105382.66 109825.77 1555.16 o 2 5 0 16457.47 16021.55 289.67 o 3 5 0 12683.07 11902.49 299.02 o 4 5 0 801.01 930.92 57.25 o 5 5 0 75044.28 75076.53 1832.48 o 6 5 0 11928.56 12222.83 265.24 o 7 5 0 22138.31 20676.87 627.26 o 8 5 0 579.19 625.86 62.08 o 9 5 0 12169.47 11355.04 246.47 o 10 5 0 60.09 156.70 58.68 o 11 5 0 52.27 86.67 62.17 o 12 5 0 1549.15 1400.29 127.51 o 13 5 0 56735.15 53959.89 942.92 o 14 5 0 1890.43 1856.66 118.67 o 15 5 0 630.64 574.55 92.30 o 16 5 0 589.63 654.21 114.05 o 17 5 0 1723.99 1625.95 155.03 o 18 5 0 23.31 96.37 118.66 o 19 5 0 860.51 912.25 332.02 o 20 5 0 604.79 737.85 186.83 o 0 6 0 186098.69 187806.09 4279.80 o 1 6 0 1147.81 1066.80 81.95 o 2 6 0 425.55 787.24 281.66 o 3 6 0 4606.35 4875.95 120.92 o 4 6 0 7745.93 7468.51 149.00 o 5 6 0 718.56 755.68 48.47 o 6 6 0 2786.62 2605.02 82.39 o 7 6 0 1185.28 1064.15 61.04 o 8 6 0 36898.03 35381.84 1231.42 o 9 6 0 2397.25 2119.47 100.10 o 10 6 0 2011.23 1906.89 120.14 o 11 6 0 1448.90 1392.32 107.42 o 12 6 0 51523.57 49738.98 873.38 o 13 6 0 231.96 192.74 115.34 o 14 6 0 16682.26 15749.31 393.16 o 15 6 0 1370.24 1413.75 114.67 o 16 6 0 26.49 10.43 88.32 o 17 6 0 57.45 170.16 108.25 o 18 6 0 6801.54 7839.92 320.34 o 19 6 0 2179.65 2350.91 194.62 o 20 6 0 4823.17 5197.75 263.95 o 1 7 0 55997.64 57333.98 957.61 o 2 7 0 3639.63 3541.74 107.50 o 3 7 0 815.20 807.21 75.34 o 4 7 0 7600.72 7465.70 155.73 o 5 7 0 31735.20 30944.88 1120.08 o 6 7 0 13553.38 13744.57 313.52 o 7 7 0 14343.17 13782.87 285.02 o 8 7 0 27.62 8.12 55.63 o 9 7 0 7648.32 7306.59 228.52 o 10 7 0 342.84 376.73 72.35 o 11 7 0 566.37 564.00 81.91 o 12 7 0 5726.37 5237.43 179.46 o 13 7 0 41332.97 38591.80 1132.04 o 14 7 0 430.87 445.33 89.82 o 15 7 0 60.04 77.57 85.69 o 16 7 0 32.90 63.77 88.28 o 17 7 0 1318.12 1519.71 156.99 o 18 7 0 345.13 522.48 135.38 o 19 7 0 717.63 766.22 186.48 o 0 8 0 55991.73 54550.27 1040.02 o 1 8 0 5143.34 5095.36 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o 17 9 0 625.46 672.54 135.39 o 18 9 0 1027.47 1465.09 200.67 o 0 10 0 47007.18 46868.32 1706.64 o 1 10 0 12785.69 11593.47 396.69 o 2 10 0 32.82 121.37 206.94 o 3 10 0 167.44 212.97 114.07 o 4 10 0 7717.57 7472.38 337.04 o 5 10 0 1077.74 1182.83 112.29 o 6 10 0 5126.58 4583.75 248.47 o 7 10 0 729.01 877.35 152.09 o 8 10 0 20034.12 19689.41 610.59 o 9 10 0 1084.43 1143.74 271.35 o 10 10 0 324.36 330.38 140.05 o 11 10 0 2014.79 2166.61 204.41 o 12 10 0 12528.25 11884.55 1009.35 o 13 10 0 1143.51 1226.66 190.72 o 14 10 0 4304.79 4319.02 285.28 o 15 10 0 2000.32 2339.76 236.46 o 16 10 0 42.35 102.88 154.75 o 17 10 0 1.35 214.70 174.63 o 1 11 0 19871.40 19125.45 585.53 o 2 11 0 5387.92 5239.08 419.91 o 3 11 0 1.40 44.55 110.62 o 4 11 0 589.95 441.68 102.67 o 5 11 0 9920.75 9992.48 395.93 o 6 11 0 4810.98 5031.33 278.73 o 7 11 0 5269.29 5300.14 284.72 o 8 11 0 177.31 68.95 177.23 o 9 11 0 4587.26 4822.84 284.86 o 10 11 0 19.35 43.10 128.23 o 11 11 0 1791.37 1657.22 204.45 o 12 11 0 1905.99 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