#------------------------------------------------------------------------------
#$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $
#$Revision: 26025 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/2202019.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2202019_Fobs
loop_
_publ_author_name
'Lee, Uk'
'Jang, Soon-Jung'
'Joo, Hea-Chung'
'Park, Ki-Min'
_publ_section_title
;
 Anhydrous octaguanidinium hexatungstoplatinate(IV)
;
_journal_issue                   3
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              m116
_journal_page_last               m118
_journal_volume                  59
_journal_year                    2003
_space_group_IT_number           148
_symmetry_space_group_name_Hall  '-R 3'
_symmetry_space_group_name_H-M   'R -3 :H'
_cell_angle_alpha                90.000
_cell_angle_beta                 90.000
_cell_angle_gamma                120.000
_cell_length_a                   12.9280
_cell_length_b                   12.9280
_cell_length_c                   21.9810
_exptl_crystal_F_000             2934.00
_reflns_d_resolution_high        0.7703
_[local]_cod_data_source_file    lh6036Isup2.hkl
_[local]_cod_data_source_block   I
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     ' GuPtW POM'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            1493.06
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-y, x-y, z'
'-x+y, -x, z'
'x+2/3, y+1/3, z+1/3'
'-y+2/3, x-y+1/3, z+1/3'
'-x+y+2/3, -x+1/3, z+1/3'
'x+1/3, y+2/3, z+2/3'
'-y+1/3, x-y+2/3, z+2/3'
'-x+y+1/3, -x+2/3, z+2/3'
'-x, -y, -z'
'y, -x+y, -z'
'x-y, x, -z'
'-x+2/3, -y+1/3, -z+1/3'
'y+2/3, -x+y+1/3, -z+1/3'
'x-y+2/3, x+1/3, -z+1/3'
'-x+1/3, -y+2/3, -z+2/3'
'y+1/3, -x+y+2/3, -z+2/3'
'x-y+1/3, x+2/3, -z+2/3'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
-1 2 0 24845.15 26027.07 2161.80 o
0 3 0 23995.21 18405.13 3365.90 o
-2 4 0 686059.63 638017.88 7594.13 o
-4 5 0 209325.28 213789.95 5185.94 o
-1 5 0 39440.88 40245.69 3681.82 o
-3 6 0 9643.88 5966.81 2630.72 o
0 6 0 17364.54 12738.34 3532.80 o
-5 7 0 10846.12 13064.20 2602.91 o
-2 7 0 113154.94 98203.06 4893.86 o
-7 8 0 22568.75 20839.14 3075.80 o
-4 8 0 55.49 4673.31 2636.68 o
-1 8 0 787176.38 755542.00 13139.71 o
-6 9 0 674868.94 647416.19 11424.97 o
-3 9 0 9178.34 3481.14 3091.70 o
0 9 0 796.40 -3489.09 3489.09 o
-8 10 0 12442.12 11271.97 3004.27 o
-5 10 0 8883.55 10693.77 3197.00 o
-2 10 0 35994.04 41016.63 4587.87 o
-10 11 0 416150.09 388492.63 10167.23 o
-7 11 0 16169.73 15559.81 3369.87 o
-4 11 0 161679.72 145822.33 7137.13 o
-1 11 0 28645.74 33927.19 4750.80 o
-9 12 0 3223.55 7007.98 3004.27 o
-6 12 0 310.21 -1891.58 3191.04 o
-3 12 0 70917.02 73958.28 6286.71 o
0 12 0 2351.18 -2084.31 3697.72 o
-11 13 0 17863.07 19956.94 3719.57 o
-8 13 0 206596.77 202835.91 8484.28 o
-5 13 0 84169.71 95238.52 6956.31 o
-2 13 0 410.28 2759.87 3457.29 o
-13 14 0 26245.81 22104.83 4126.90 o
-10 14 0 28356.77 29665.18 4490.51 o
-7 14 0 8508.61 13847.06 3848.72 o
-4 14 0 19432.73 7808.72 4591.84 o
-1 14 0 15387.31 5927.07 4325.59 o
-12 15 0 38955.99 38644.21 4752.79 o
-9 15 0 27505.93 33416.54 4558.06 o
-6 15 0 5835.12 9843.36 4095.11 o
-3 15 0 202010.41 196606.81 9789.71 o
-11 16 0 6258.05 -2575.09 4007.68 o
-8 16 0 5022.41 10809.01 3912.31 o
-5 16 0 249.80 -878.23 4059.34 o
-1 1 1 478911.41 455019.72 3346.03 o
-3 2 1 135601.97 125624.97 3340.06 o
0 2 1 114086.51 108869.02 3137.40 o
-5 3 1 65820.20 62686.31 3195.02 o
-2 3 1 2342.56 4987.25 2273.07 o
1 3 1 897149.25 847142.44 10248.69 o
-7 4 1 41407.43 45445.54 3034.07 o
-4 4 1 1471.63 4508.39 2296.92 o
-1 4 1 2356.98 -405.34 2547.27 o
2 4 1 10585.56 17813.02 4023.58 o
-9 5 1 19140.27 15643.27 2881.08 o
-6 5 1 48267.32 47531.84 3193.03 o
-3 5 1 1195196.50 1116817.38 10683.83 o
0 5 1 11960.17 3969.93 2912.87 o
3 5 1 269173.16 261921.84 8541.90 o
-11 6 1 1901.68 3504.98 2618.80 o
-8 6 1 511465.28 496425.78 9054.54 o
-5 6 1 25171.01 25874.08 2751.93 o
-2 6 1 39824.27 30867.28 3224.82 o
1 6 1 33619.41 35250.50 3999.73 o
4 6 1 249157.27 259773.97 8716.75 o
-13 7 1 411.14 675.56 2829.42 o
-10 7 1 16842.54 18560.11 3121.50 o
-7 7 1 161827.94 158052.02 5332.98 o
-4 7 1 52139.38 51519.65 3499.02 o
-1 7 1 959357.75 920363.63 12937.04 o
2 7 1 36485.48 41835.25 4818.36 o
5 7 1 3029.14 -558.33 3348.01 o
-15 8 1 248.63 -2871.14 2871.14 o
-12 8 1 515030.88 502998.63 11369.33 o
-9 8 1 5720.50 5497.89 2676.42 o
-6 8 1 43670.14 42943.97 3671.89 o
-3 8 1 3384.45 1531.94 2807.56 o
0 8 1 342.84 -3441.40 3441.40 o
3 8 1 60292.57 61635.22 5766.13 o
6 8 1 135204.41 125702.45 7270.25 o
-14 9 1 18493.02 17648.10 3729.51 o
-11 9 1 8739.25 669.60 2811.54 o
-8 9 1 44073.83 47456.34 4107.03 o
-5 9 1 342972.56 326446.09 8309.43 o
-2 9 1 46054.77 48618.70 4411.03 o
1 9 1 42542.44 42077.66 4931.61 o
4 9 1 132913.09 140835.08 7351.72 o
7 9 1 10774.48 3230.78 4005.69 o
-16 10 1 90715.78 104847.42 6618.53 o
-13 10 1 6750.33 5654.86 3361.92 o
-10 10 1 281504.94 273591.22 8178.29 o
-7 10 1 55956.74 58332.90 4440.84 o
-4 10 1 37004.93 30479.83 4013.64 o
-1 10 1 5222.09 7202.70 3669.90 o
2 10 1 4846.63 4029.54 3689.77 o
5 10 1 11171.46 4210.35 3705.66 o
-15 11 1 1310.19 5076.66 3165.21 o
-12 11 1 1505.22 5573.40 3049.97 o
-9 11 1 9415.58 6503.29 2972.48 o
-6 11 1 21098.17 19335.02 3677.85 o
-3 11 1 61284.76 58772.02 5454.18 o
0 11 1 294064.00 303472.97 10449.38 o
3 11 1 9501.46 6175.44 3711.62 o
-14 12 1 148371.36 152516.38 7441.13 o
-11 12 1 43537.99 35814.79 4224.26 o
-8 12 1 3320.09 6602.64 2819.48 o
-5 12 1 150514.34 148574.25 7180.84 o
-2 12 1 32212.68 31815.06 4949.49 o
1 12 1 12013.73 5356.82 3991.78 o
4 12 1 1028.42 5497.89 3604.33 o
-13 13 1 16083.86 17691.81 3644.07 o
-10 13 1 1327.98 790.81 3159.25 o
-7 13 1 6285.53 9267.14 3580.49 o
-4 13 1 41745.82 42149.19 5309.13 o
-1 13 1 1394.98 -3693.74 3693.74 o
2 13 1 220259.98 199936.94 9485.71 o
-15 14 1 39.79 3959.99 3463.26 o
-12 14 1 11363.68 7091.43 3274.50 o
-9 14 1 303258.75 278276.47 10075.83 o
-6 14 1 9023.24 8637.28 3715.60 o
-3 14 1 17109.97 15754.53 4420.97 o
0 14 1 510.49 975.59 3381.79 o
-14 15 1 50967.16 56177.07 5509.81 o
-11 15 1 5294.31 10626.21 3542.73 o
-8 15 1 3281.33 3530.81 3566.58 o
-5 15 1 5457.77 12017.08 4160.68 o
-2 15 1 185835.64 187510.55 9336.68 o
-10 16 1 2096.69 -3306.29 3379.80 o
-7 16 1 163995.50 166872.09 9199.58 o
-4 16 1 3234.94 5583.33 4333.54 o
0 1 2 422234.38 418016.75 3713.61 o
-2 2 2 86908.46 89466.43 2674.44 o
1 2 2 163109.08 153786.03 4118.95 o
-4 3 2 18182.20 16702.31 2416.13 o
-1 3 2 7857.93 10727.55 2424.08 o
2 3 2 372861.69 368907.22 8090.86 o
-6 4 2 13683.73 15067.05 2445.94 o
-3 4 2 1273718.13 1231667.13 10121.53 o
0 4 2 6467.91 4605.75 2680.40 o
3 4 2 27337.60 25492.58 4240.15 o
-8 5 2 3620.51 1039.18 2360.50 o
-5 5 2 20131.79 26815.89 2670.46 o
-2 5 2 92644.03 98882.60 3954.03 o
1 5 2 53506.15 59837.03 4057.35 o
4 5 2 393883.53 392919.53 10226.84 o
-10 6 2 58545.75 69263.13 4460.71 o
-7 6 2 1002461.56 966103.25 11810.44 o
-4 6 2 59733.36 62420.06 3485.11 o
-1 6 2 28908.70 29277.72 3210.91 o
2 6 2 51145.17 52153.49 5237.60 o
5 6 2 15199.85 16722.18 3822.89 o
-12 7 2 149534.80 161916.63 6711.92 o
-9 7 2 46247.24 48594.86 3890.45 o
-6 7 2 43132.30 44877.27 3502.99 o
-3 7 2 134401.25 137506.94 4943.53 o
0 7 2 125718.03 129090.23 5682.68 o
3 7 2 114792.00 112769.40 6606.61 o
6 7 2 6759.96 1649.17 3739.44 o
-14 8 2 22405.04 24471.29 3793.09 o
-11 8 2 135598.28 133894.66 5992.64 o
-8 8 2 1855.00 4834.25 2503.56 o
-5 8 2 240704.30 222908.08 6477.46 o
-2 8 2 639803.81 620280.38 10908.36 o
1 8 2 76403.51 92882.01 5990.66 o
4 8 2 1285.09 5362.78 3693.74 o
7 8 2 693.40 4746.83 3163.23 o
-16 9 2 164645.75 182461.70 8341.22 o
-13 9 2 38443.19 41046.43 4260.02 o
-10 9 2 10713.28 7574.26 2904.92 o
-7 9 2 52299.08 46917.88 4037.48 o
-4 9 2 2501.10 -188.76 2718.15 o
-1 9 2 233.98 1140.51 3351.99 o
2 9 2 1348.04 1162.37 3483.13 o
5 9 2 364476.34 369547.03 11585.91 o
-15 10 2 2981.90 -2825.44 2825.44 o
-12 10 2 17661.75 22623.42 3753.35 o
-9 10 2 52528.24 45836.97 4200.41 o
-6 10 2 162638.97 156263.77 6455.60 o
-3 10 2 3138.59 -455.01 3290.39 o
0 10 2 348965.09 373689.84 11289.86 o
3 10 2 1921.93 -3554.66 3554.66 o
6 10 2 1652.78 7323.90 3330.13 o
-14 11 2 21827.37 23372.50 3850.71 o
-11 11 2 302476.88 303077.56 9249.26 o
-8 11 2 30607.98 33726.51 3783.15 o
-5 11 2 1765.94 2885.05 3004.27 o
-2 11 2 4948.88 4440.84 3775.21 o
1 11 2 34627.77 34046.41 4915.72 o
4 11 2 6315.92 5688.64 3872.57 o
-16 12 2 3871.25 4820.34 3340.06 o
-13 12 2 576.41 -2879.09 2879.09 o
-10 12 2 1603.81 8355.13 3087.72 o
-7 12 2 4167.83 4840.21 2982.41 o
-4 12 2 525748.25 504927.94 12517.79 o
-1 12 2 143.52 9815.54 4150.74 o
2 12 2 14010.93 15635.32 4013.64 o
-15 13 2 173866.73 189356.42 8738.61 o
-12 13 2 6542.21 12505.87 3133.42 o
-9 13 2 148006.42 146247.53 7061.62 o
-6 13 2 430.67 4047.42 3397.69 o
-3 13 2 7599.81 14979.62 3946.08 o
0 13 2 19506.40 19786.06 4399.11 o
-14 14 2 781.35 -101.33 2932.74 o
-11 14 2 18483.00 17103.67 3771.23 o
-8 14 2 114053.63 105697.84 6570.85 o
-5 14 2 728.73 2602.91 3594.39 o
-2 14 2 141110.16 168479.53 8516.07 o
-13 15 2 230768.19 246385.89 9841.37 o
-10 15 2 10885.65 10695.76 3622.21 o
-7 15 2 81.65 -3361.92 3361.92 o
-4 15 2 122.84 -3801.04 3801.04 o
-12 16 2 10.69 -294.07 3242.70 o
-9 16 2 12803.68 8776.36 4111.00 o
-6 16 2 103341.47 101652.41 8074.97 o
0 0 3 2229224.75 1986752.25 8812.13 o
1 1 3 25048.36 24989.88 2201.54 o
-1 2 3 16389.82 16608.92 2014.77 o
2 2 3 764430.31 730397.19 8690.92 o
-3 3 3 1116.38 -898.10 2066.43 o
0 3 3 11135.36 12799.94 2515.48 o
3 3 3 5561.28 1150.44 3981.85 o
-5 4 3 137655.50 138418.94 4214.32 o
-2 4 3 757633.94 733457.13 7931.91 o
1 4 3 226790.23 217175.72 5555.51 o
4 4 3 5267.58 9924.82 3650.03 o
-7 5 3 145063.53 142796.20 4887.90 o
-4 5 3 260578.55 257455.19 5607.18 o
-1 5 3 86496.25 83990.40 3850.71 o
2 5 3 22889.14 26241.66 3685.79 o
5 5 3 3993.97 4442.82 3630.16 o
-9 6 3 1168.05 -2330.69 2330.69 o
-6 6 3 6853.12 8084.90 2284.99 o
-3 6 3 6173.95 8025.29 2346.59 o
0 6 3 31900.73 37217.58 3602.34 o
3 6 3 717933.88 690638.31 13441.72 o
6 6 3 13942.17 8178.29 4232.21 o
-11 7 3 105617.16 112312.40 5573.40 o
-8 7 3 551886.44 559851.25 9869.18 o
-5 7 3 56836.02 50085.07 3417.56 o
-2 7 3 188412.52 187858.27 5799.91 o
1 7 3 11219.75 18591.90 3471.20 o
4 7 3 956.32 3107.59 3729.51 o
7 7 3 10916.59 2831.40 3671.89 o
-13 8 3 75495.16 80666.23 5633.01 o
-10 8 3 27657.43 32750.91 3497.03 o
-7 8 3 32784.88 32929.74 3375.83 o
-4 8 3 714.69 1768.39 2700.27 o
-1 8 3 545786.63 550582.13 10725.56 o
2 8 3 9864.18 9312.84 4017.61 o
5 8 3 230771.70 221080.09 9141.96 o
8 8 3 9656.08 9549.29 3671.89 o
-15 9 3 10445.62 2640.66 3431.46 o
-12 9 3 50990.82 48497.50 4653.44 o
-9 9 3 2226.76 7407.35 2741.99 o
-6 9 3 768896.63 694105.56 11536.24 o
-3 9 3 13022.88 19420.46 3161.24 o
0 9 3 1516.36 2708.21 3373.84 o
3 9 3 4958.27 2829.42 3711.62 o
6 9 3 22885.79 17594.45 4188.49 o
-14 10 3 16158.42 18881.99 3642.08 o
-11 10 3 34807.24 32532.35 3803.02 o
-8 10 3 5627.94 2076.36 2885.05 o
-5 10 3 2214.76 7071.56 3016.19 o
-2 10 3 38132.94 42208.80 4387.19 o
1 10 3 324888.13 323920.69 10379.83 o
4 10 3 22979.01 21153.08 4424.94 o
-16 11 3 151.51 -2894.99 2894.99 o
-13 11 3 6079.98 9175.74 3433.45 o
-10 11 3 384663.59 344346.56 9815.54 o
-7 11 3 10877.03 13622.54 3157.26 o
-4 11 3 157290.06 160565.50 6932.47 o
-1 11 3 30970.00 35333.95 4593.83 o
2 11 3 23257.97 20264.91 4518.33 o
5 11 3 10292.28 6590.72 4055.37 o
-15 12 3 178332.69 163545.92 8225.98 o
-12 12 3 868.82 3896.41 2964.53 o
-9 12 3 2561.87 8573.69 2986.39 o
-6 12 3 20389.73 13996.08 3705.66 o
-3 12 3 77055.29 76356.55 6113.85 o
0 12 3 4918.09 2177.70 3417.56 o
3 12 3 42646.59 42018.05 5205.81 o
-14 13 3 16575.54 15482.32 3807.00 o
-11 13 3 20541.26 22595.61 3868.59 o
-8 13 3 261211.50 265762.66 9183.69 o
-5 13 3 85002.87 86507.88 6548.99 o
-2 13 3 750.02 2157.83 3689.77 o
1 13 3 19241.41 19605.24 4534.22 o
-13 14 3 19127.78 9670.49 3743.42 o
-10 14 3 32218.31 31743.53 4283.87 o
-7 14 3 5140.89 12555.54 3659.96 o
-4 14 3 16153.78 7631.88 4309.70 o
-1 14 3 20128.45 21778.97 4520.31 o
-12 15 3 33917.39 29339.32 4510.38 o
-9 15 3 29066.17 21512.72 4377.25 o
-6 15 3 5161.55 3435.44 4128.88 o
-3 15 3 189908.61 190975.80 9587.04 o
-11 16 3 8812.62 2787.69 3997.75 o
-8 16 3 2533.78 -3652.02 3652.02 o
-5 16 3 324.41 2441.96 4420.97 o
-1 1 4 424155.41 424301.44 4629.60 o
-3 2 4 18249.89 19283.36 2314.80 o
0 2 4 245678.30 244696.98 4246.11 o
-5 3 4 152978.55 158560.67 4331.55 o
-2 3 4 38161.08 45376.00 2757.89 o
1 3 4 748622.75 769999.13 8649.20 o
-7 4 4 50974.08 51163.99 3270.52 o
-4 4 4 1439.33 3757.32 2199.55 o
-1 4 4 37331.35 47200.02 3016.19 o
2 4 4 4722.06 6765.57 2686.36 o
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-6 5 4 11889.39 14914.05 2465.81 o
-3 5 4 1777182.75 1648197.75 13135.73 o
0 5 4 46309.73 49337.98 3367.88 o
3 5 4 125388.33 134431.14 6191.34 o
-11 6 4 2147.86 4866.04 2581.05 o
-8 6 4 425664.41 412940.06 8504.15 o
-5 6 4 35627.35 40444.39 3393.71 o
-2 6 4 8918.84 7232.50 2732.06 o
1 6 4 50441.95 51344.80 4208.36 o
4 6 4 339056.75 323229.22 9960.58 o
-13 7 4 279.85 -2668.48 2668.48 o
-10 7 4 10820.76 5919.13 2900.95 o
-7 7 4 189759.64 188064.91 5940.98 o
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-1 7 4 858663.88 820396.13 11876.00 o
2 7 4 40598.13 39619.80 4448.78 o
5 7 4 2803.22 2074.38 3616.25 o
-15 8 4 46.83 5940.98 3016.19 o
-12 8 4 425248.78 438148.50 10713.64 o
-9 8 4 1652.54 -190.75 2519.45 o
-6 8 4 42681.16 39397.26 3761.30 o
-3 8 4 8.12 6058.21 2606.88 o
0 8 4 133.25 -1452.46 3300.33 o
3 8 4 32560.88 35163.07 4500.44 o
6 8 4 110139.33 99051.49 6690.06 o
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-11 9 4 3895.17 14147.09 3083.75 o
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-2 9 4 4957.11 7403.38 2920.82 o
1 9 4 52955.40 57921.61 5523.72 o
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7 9 4 13255.35 15836.00 4208.36 o
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-13 10 4 13891.71 10373.87 3622.21 o
-10 10 4 304786.66 297953.25 8875.71 o
-7 10 4 36794.80 30998.42 3777.19 o
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-1 10 4 4759.92 2284.99 3401.66 o
2 10 4 6243.61 4138.82 3799.05 o
5 10 4 3235.96 7421.26 3502.99 o
-15 11 4 3224.39 -3121.50 3121.50 o
-12 11 4 472.42 -2960.56 2960.56 o
-9 11 4 1536.20 2364.47 2624.76 o
-6 11 4 30233.84 27809.37 3747.39 o
-3 11 4 78815.45 67778.87 5674.73 o
0 11 4 216099.23 211888.45 9040.63 o
3 11 4 2645.75 7904.09 3745.40 o
-14 12 4 139858.56 124724.88 7284.16 o
-11 12 4 63911.29 64587.83 5418.42 o
-8 12 4 2315.27 939.83 2819.48 o
-5 12 4 128651.27 127743.05 6696.02 o
-2 12 4 13683.07 22591.63 4057.35 o
1 12 4 16744.01 15373.04 4333.54 o
-13 13 4 11559.54 10906.37 3803.02 o
-10 13 4 5423.74 8094.84 3232.77 o
-7 13 4 7698.43 5009.10 3226.81 o
-4 13 4 68500.59 73556.93 6223.13 o
-1 13 4 2329.17 2082.32 3564.59 o
2 13 4 220137.41 184192.36 9285.02 o
-12 14 4 6790.09 9445.96 3590.42 o
-9 14 4 293141.91 273684.63 9863.22 o
-6 14 4 10696.56 8017.35 3896.41 o
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