#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:00:30 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180940 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/20/2202023.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202023_Fobs loop_ _publ_author_name 'Emge, Thomas J.' 'Clements, Matthew J.' 'Myers, David S.' 'Knapp, Spencer' _publ_section_title ; (5-Bromopyrrol-3-yl)cyclohexylmethanone ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o425 _journal_page_last o427 _journal_volume 59 _journal_year 2003 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 110.280 _cell_angle_gamma 90.000 _cell_length_a 12.0951 _cell_length_b 7.3006 _cell_length_c 13.0038 _exptl_crystal_F_000 520.00 _reflns_d_resolution_high 0.7501 _cod_data_source_file lh6040Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' mjc64m in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 291.04 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 12.71 15.98 1.96 o 4 0 0 5966.41 6355.40 133.68 o 6 0 0 1938.10 2246.49 50.40 o 8 0 0 3455.51 3234.22 72.29 o 10 0 0 318.78 337.10 16.03 o 12 0 0 3459.90 3157.46 315.66 o 14 0 0 32.05 10.21 14.63 o 1 1 0 156.64 167.22 4.37 o 2 1 0 48216.68 47183.41 840.63 o 3 1 0 374.71 367.34 6.89 o 4 1 0 20.02 32.74 2.52 o 5 1 0 115.05 108.37 4.18 o 6 1 0 4485.58 4325.83 65.98 o 7 1 0 187.55 199.75 6.20 o 8 1 0 295.23 333.58 8.69 o 9 1 0 2.38 9.03 3.56 o 10 1 0 5619.88 5651.60 95.85 o 11 1 0 71.07 83.34 7.87 o 12 1 0 750.30 725.45 21.18 o 13 1 0 137.85 138.29 16.84 o 14 1 0 804.73 839.44 35.73 o 15 1 0 106.86 90.63 20.96 o 0 2 0 84704.34 77089.41 2220.77 o 1 2 0 265.60 272.66 5.62 o 2 2 0 69.24 80.43 3.91 o 3 2 0 135.24 94.42 3.65 o 4 2 0 3392.14 3412.07 51.91 o 5 2 0 2677.01 2811.78 43.59 o 6 2 0 964.21 1085.20 18.81 o 7 2 0 253.49 270.07 7.72 o 8 2 0 2462.69 2295.85 41.35 o 9 2 0 547.18 514.02 15.76 o 10 2 0 117.87 100.85 8.56 o 11 2 0 364.65 409.57 17.36 o 12 2 0 2261.83 2364.12 59.27 o 13 2 0 232.98 196.80 14.98 o 14 2 0 59.04 57.79 10.77 o 1 3 0 2227.21 2141.34 33.50 o 2 3 0 9792.76 10428.96 154.31 o 3 3 0 1337.64 1309.05 23.70 o 4 3 0 116.84 146.95 5.32 o 5 3 0 1760.52 1707.07 35.30 o 6 3 0 1833.41 1686.87 35.51 o 7 3 0 991.34 979.37 23.59 o 8 3 0 4.22 2.03 4.79 o 9 3 0 32.75 36.79 6.17 o 10 3 0 2068.86 2025.00 44.37 o 11 3 0 392.63 374.32 15.12 o 12 3 0 335.24 324.12 14.88 o 13 3 0 719.33 733.60 27.05 o 14 3 0 449.01 410.09 39.67 o 0 4 0 5418.05 5835.61 124.59 o 1 4 0 993.27 964.69 17.15 o 2 4 0 156.87 148.16 5.42 o 3 4 0 959.86 824.23 15.09 o 4 4 0 1309.83 1312.76 25.08 o 5 4 0 3046.30 3116.01 61.29 o 6 4 0 23.67 34.06 5.75 o 7 4 0 855.91 823.69 36.29 o 8 4 0 765.31 716.44 22.39 o 9 4 0 856.54 838.27 23.01 o 10 4 0 2.72 -2.48 5.93 o 11 4 0 622.38 631.17 20.51 o 12 4 0 498.04 468.69 24.04 o 13 4 0 396.65 389.06 17.75 o 1 5 0 2579.10 2502.73 40.40 o 2 5 0 693.31 742.01 14.65 o 3 5 0 1075.15 1090.38 22.16 o 4 5 0 183.77 205.42 9.64 o 5 5 0 2144.27 2097.20 44.21 o 6 5 0 310.85 309.01 13.73 o 7 5 0 787.24 820.40 22.38 o 8 5 0 229.72 215.36 13.92 o 9 5 0 27.82 31.83 6.88 o 10 5 0 63.09 49.21 8.03 o 11 5 0 305.16 309.35 14.93 o 12 5 0 63.93 70.58 11.79 o 0 6 0 61.79 55.97 8.28 o 1 6 0 1067.93 1088.35 33.94 o 2 6 0 107.43 103.17 6.71 o 3 6 0 864.23 769.71 27.27 o 4 6 0 83.30 98.77 8.11 o 5 6 0 1069.06 1089.32 27.19 o 6 6 0 27.29 28.85 6.42 o 7 6 0 533.53 547.33 23.13 o 8 6 0 10.20 6.95 7.76 o 9 6 0 420.83 435.90 17.24 o 10 6 0 38.87 32.29 8.10 o 11 6 0 286.36 291.07 15.59 o 1 7 0 1007.40 1009.49 23.72 o 2 7 0 45.42 50.70 6.88 o 3 7 0 404.07 431.42 17.48 o 4 7 0 190.38 187.65 11.36 o 5 7 0 878.06 848.45 23.87 o 6 7 0 6.73 2.85 5.97 o 7 7 0 259.27 282.99 13.96 o 8 7 0 114.65 98.07 10.34 o 9 7 0 11.65 12.48 7.90 o 10 7 0 212.02 212.56 14.87 o 0 8 0 538.43 550.39 25.03 o 1 8 0 455.57 494.01 19.48 o 2 8 0 21.22 33.44 7.03 o 3 8 0 200.19 180.34 13.09 o 4 8 0 25.32 19.87 7.01 o 5 8 0 110.24 114.98 10.73 o 6 8 0 14.31 23.55 8.63 o 7 8 0 93.15 88.93 10.65 o 8 8 0 110.94 119.51 14.13 o 1 9 0 131.59 155.82 19.65 o 2 9 0 109.36 118.47 12.36 o 3 9 0 63.73 54.54 10.37 o 4 9 0 35.94 19.05 8.09 o 5 9 0 41.39 43.19 9.21 o -15 0 1 602.85 620.62 43.47 o -13 0 1 21.08 -0.65 12.91 o -11 0 1 1907.74 1851.60 56.50 o -9 0 1 1058.22 1131.12 29.63 o -7 0 1 9864.59 10391.29 218.83 o -5 0 1 3071.78 2944.54 63.98 o -3 0 1 14794.53 15487.98 321.19 o -1 0 1 1393.50 1376.07 51.73 o 1 0 1 1117.85 1147.56 24.67 o 3 0 1 5039.20 5022.52 105.77 o 5 0 1 4089.47 3819.47 82.32 o 7 0 1 1573.62 1647.89 39.00 o 9 0 1 5212.69 5221.45 114.21 o 11 0 1 506.45 512.15 30.60 o 13 0 1 1280.51 1208.64 63.25 o -15 1 1 612.31 640.44 33.79 o -14 1 1 22.19 17.29 10.50 o -13 1 1 1052.25 1057.50 32.06 o -12 1 1 172.67 172.68 15.71 o -11 1 1 396.54 371.15 13.67 o -10 1 1 5.42 0.82 4.18 o -9 1 1 3586.86 3632.60 57.37 o -8 1 1 545.45 542.59 11.74 o -7 1 1 2664.77 2744.26 43.38 o -6 1 1 268.71 262.62 6.65 o -5 1 1 7869.01 8179.17 121.55 o -4 1 1 4050.31 4309.18 70.98 o -3 1 1 2146.78 2170.02 36.52 o -2 1 1 103.07 112.52 3.97 o -1 1 1 3921.84 4148.03 67.36 o 0 1 1 264.38 264.81 4.76 o 1 1 1 132.31 132.38 3.46 o 2 1 1 769.93 771.10 13.88 o 3 1 1 14597.60 15163.45 243.14 o 4 1 1 161.93 152.10 4.68 o 5 1 1 1689.27 1636.61 26.37 o 6 1 1 130.53 155.76 6.93 o 7 1 1 3116.45 2990.65 47.16 o 8 1 1 698.46 703.64 14.34 o 9 1 1 91.17 95.21 8.79 o 10 1 1 32.99 32.42 5.29 o 11 1 1 1904.65 2010.01 50.64 o 12 1 1 34.79 47.66 8.84 o 13 1 1 475.04 491.87 20.79 o 14 1 1 25.93 17.83 13.03 o -15 2 1 471.58 488.34 42.04 o -14 2 1 404.25 370.29 21.60 o -13 2 1 7.60 5.39 7.52 o -12 2 1 1.46 -3.66 5.65 o -11 2 1 1206.62 1167.78 35.63 o -10 2 1 478.65 451.05 15.06 o -9 2 1 791.17 843.05 41.00 o -8 2 1 42.92 41.36 3.85 o -7 2 1 6045.86 6286.99 95.09 o -6 2 1 2179.28 2195.10 34.95 o -5 2 1 999.21 906.98 19.70 o -4 2 1 73.96 66.27 3.62 o -3 2 1 14499.19 14974.18 241.46 o -2 2 1 18325.20 18884.96 337.94 o -1 2 1 626.01 700.39 11.83 o 0 2 1 129.82 151.03 3.95 o 1 2 1 1904.97 1822.05 28.16 o 2 2 1 132.68 124.71 4.17 o 3 2 1 1583.24 1493.78 26.20 o 4 2 1 2804.64 3101.29 52.26 o 5 2 1 2747.86 2643.99 45.51 o 6 2 1 1698.50 1647.73 30.19 o 7 2 1 717.96 748.90 16.41 o 8 2 1 184.26 184.60 7.74 o 9 2 1 3138.59 3058.83 61.50 o 10 2 1 539.09 539.06 21.42 o 11 2 1 347.10 326.92 17.29 o 12 2 1 6.96 4.94 6.61 o 13 2 1 677.76 693.77 31.40 o 14 2 1 22.56 21.31 9.49 o -14 3 1 90.47 88.44 10.24 o -13 3 1 481.17 473.95 19.80 o -12 3 1 830.83 817.74 29.33 o -11 3 1 41.15 25.31 6.66 o -10 3 1 33.61 28.92 6.19 o -9 3 1 1131.33 1097.02 26.74 o -8 3 1 1860.19 1729.59 37.56 o -7 3 1 1005.47 998.27 23.76 o -6 3 1 775.88 809.45 20.48 o -5 3 1 5236.01 5526.13 92.04 o -4 3 1 12364.13 12978.59 210.70 o -3 3 1 269.37 249.81 7.86 o -2 3 1 287.93 281.25 6.46 o -1 3 1 5275.20 5250.23 86.50 o 0 3 1 1998.28 1921.96 30.35 o 1 3 1 8.60 8.78 2.36 o 2 3 1 1267.13 1358.48 22.21 o 3 3 1 2706.24 2555.46 39.69 o 4 3 1 1483.14 1356.98 24.99 o 5 3 1 355.09 361.62 9.28 o 6 3 1 256.49 270.42 8.29 o 7 3 1 1103.60 1105.26 26.06 o 8 3 1 3760.32 3732.67 73.51 o 9 3 1 8.14 5.37 5.35 o 10 3 1 276.95 256.73 12.31 o 11 3 1 721.84 685.84 24.44 o 12 3 1 228.53 223.94 13.29 o 13 3 1 289.93 274.87 14.85 o 14 3 1 188.58 168.66 19.09 o -14 4 1 727.14 760.39 29.07 o -13 4 1 12.87 9.06 9.01 o -12 4 1 1.89 6.43 6.84 o -11 4 1 234.37 207.90 12.36 o -10 4 1 814.46 772.20 22.42 o -9 4 1 284.05 311.55 12.97 o -8 4 1 31.23 30.53 5.85 o -7 4 1 899.92 908.61 22.96 o -6 4 1 2186.11 2221.65 45.88 o -5 4 1 42.13 50.41 5.45 o -4 4 1 60.29 66.41 6.22 o -3 4 1 5305.03 5481.74 83.08 o -2 4 1 16090.44 16697.17 246.41 o -1 4 1 8.25 18.18 2.80 o 0 4 1 105.40 114.06 4.82 o 1 4 1 232.61 185.27 5.74 o 2 4 1 1738.81 1636.14 26.93 o 3 4 1 6.66 11.65 2.58 o 4 4 1 2579.76 2716.05 47.29 o 5 4 1 379.21 353.71 12.82 o 6 4 1 3220.08 3165.64 62.93 o 7 4 1 9.47 9.15 4.81 o 8 4 1 502.50 477.38 15.92 o 9 4 1 670.86 673.43 20.13 o 10 4 1 1220.45 1163.67 34.26 o 11 4 1 95.74 100.85 9.87 o 12 4 1 85.75 93.11 10.36 o 13 4 1 41.89 40.95 9.25 o -13 5 1 78.68 66.35 12.16 o -12 5 1 780.26 765.42 36.17 o -11 5 1 25.68 35.16 8.93 o -10 5 1 2.03 3.22 6.32 o -9 5 1 17.31 14.87 6.28 o -8 5 1 1411.34 1379.78 32.91 o -7 5 1 37.68 45.77 6.57 o -6 5 1 319.80 310.06 12.35 o -5 5 1 1371.65 1441.61 32.46 o -4 5 1 7476.06 7700.98 128.11 o -3 5 1 10.15 16.76 3.85 o -2 5 1 192.66 197.78 6.70 o -1 5 1 804.15 805.69 16.95 o 0 5 1 2615.10 2549.88 41.12 o 1 5 1 85.83 110.20 5.33 o 2 5 1 606.07 642.88 13.23 o 3 5 1 35.80 59.84 4.20 o 4 5 1 2057.70 1960.59 41.41 o 5 5 1 9.84 12.64 5.15 o 6 5 1 167.57 174.77 10.01 o 7 5 1 123.10 125.84 11.04 o 8 5 1 3714.13 3661.15 74.21 o 9 5 1 18.70 12.47 6.27 o 10 5 1 690.82 662.03 21.54 o 11 5 1 60.75 69.52 9.54 o 12 5 1 369.95 401.97 18.02 o -12 6 1 41.99 59.59 10.25 o -11 6 1 0.10 3.37 7.42 o -10 6 1 534.07 515.40 19.09 o -9 6 1 0.06 9.57 6.75 o -8 6 1 1.61 0.70 5.70 o -7 6 1 8.54 12.35 5.72 o -6 6 1 960.73 965.45 28.07 o -5 6 1 110.74 110.91 8.56 o -4 6 1 16.21 22.35 5.70 o -3 6 1 787.02 794.96 32.92 o -2 6 1 6557.53 6515.00 173.05 o -1 6 1 3.55 -0.13 3.59 o 0 6 1 66.74 78.82 5.39 o 1 6 1 78.46 91.45 6.78 o 2 6 1 1867.48 1808.69 34.43 o 3 6 1 256.72 254.57 18.21 o 4 6 1 620.69 666.93 29.37 o 5 6 1 13.16 17.28 5.61 o 6 6 1 2059.39 2148.74 46.93 o 7 6 1 102.72 90.75 9.00 o 8 6 1 530.78 505.29 18.27 o 9 6 1 23.79 29.15 8.25 o 10 6 1 986.46 963.85 28.10 o 11 6 1 1.43 0.39 7.56 o -10 7 1 8.78 0.70 8.22 o -9 7 1 95.88 99.89 10.61 o -8 7 1 508.04 511.05 18.79 o -7 7 1 140.32 109.18 9.92 o -6 7 1 8.69 16.39 6.56 o -5 7 1 111.23 108.26 10.64 o -4 7 1 2062.32 2004.36 47.30 o -3 7 1 107.36 85.05 8.34 o -2 7 1 64.52 64.37 6.27 o -1 7 1 8.99 9.19 4.81 o 0 7 1 1468.60 1470.53 27.09 o 1 7 1 155.93 175.25 14.02 o 2 7 1 126.85 141.36 10.78 o 3 7 1 578.93 566.17 17.92 o 4 7 1 1178.97 1212.52 30.22 o 5 7 1 55.36 56.91 8.11 o 6 7 1 12.56 11.90 9.59 o 7 7 1 9.53 12.86 7.15 o 8 7 1 1248.93 1257.91 44.17 o 9 7 1 28.86 20.76 8.39 o 10 7 1 630.56 603.98 22.74 o -8 8 1 16.14 0.98 7.63 o -7 8 1 151.73 153.28 12.20 o -6 8 1 233.13 233.11 13.56 o -5 8 1 151.70 136.32 11.14 o -4 8 1 4.49 14.54 6.67 o -3 8 1 5.10 -2.67 6.09 o -2 8 1 1430.07 1439.47 34.90 o -1 8 1 1.49 3.97 5.71 o 0 8 1 52.24 48.60 8.35 o 1 8 1 301.13 289.46 21.35 o 2 8 1 660.38 673.73 20.67 o 3 8 1 202.78 239.93 14.81 o 4 8 1 13.87 20.80 7.13 o 5 8 1 43.29 35.19 8.33 o 6 8 1 472.85 515.73 19.38 o 7 8 1 72.06 72.52 9.98 o 8 8 1 216.56 231.66 23.95 o -6 9 1 23.92 10.47 16.75 o -5 9 1 7.17 17.03 8.56 o -4 9 1 259.10 260.81 14.61 o -3 9 1 69.24 54.73 10.12 o -2 9 1 29.63 35.23 8.98 o -1 9 1 173.34 172.62 17.28 o 0 9 1 281.48 252.02 19.34 o 1 9 1 145.79 128.47 12.63 o 2 9 1 38.16 17.48 8.78 o 3 9 1 392.52 348.91 25.45 o 4 9 1 259.61 249.02 14.64 o 5 9 1 22.38 22.88 10.37 o -14 0 2 202.59 170.62 24.02 o -12 0 2 2034.11 2229.33 54.62 o -10 0 2 1601.27 1466.91 87.99 o -8 0 2 2019.84 1995.92 46.59 o -6 0 2 2871.08 2822.30 62.10 o -4 0 2 10173.41 10291.88 214.63 o -2 0 2 1118.81 1111.30 25.95 o 0 0 2 2587.17 2676.38 56.32 o 2 0 2 7822.40 8079.19 168.47 o 4 0 2 10653.49 11095.79 231.90 o 6 0 2 4960.48 5036.50 108.42 o 8 0 2 2158.55 2134.53 50.08 o 10 0 2 1235.30 1265.55 81.39 o 12 0 2 493.71 375.89 31.13 o 14 0 2 428.72 501.24 40.45 o -15 1 2 58.20 43.89 12.80 o -14 1 2 524.69 543.47 26.81 o -13 1 2 14.66 14.97 6.64 o -12 1 2 83.05 92.95 8.30 o -11 1 2 220.57 199.23 10.22 o -10 1 2 2704.92 2615.62 63.82 o -9 1 2 173.51 176.54 6.92 o -8 1 2 2845.84 2928.14 46.55 o -7 1 2 10.77 12.63 2.74 o -6 1 2 9390.43 9647.07 143.42 o -5 1 2 5.11 4.89 1.95 o -4 1 2 1953.27 1931.87 30.12 o -3 1 2 561.94 578.05 10.02 o -2 1 2 428.57 391.58 7.03 o -1 1 2 324.65 335.42 6.78 o 0 1 2 13521.20 13378.10 214.91 o 1 1 2 3457.30 3669.63 59.95 o 2 1 2 4491.75 4422.64 66.02 o 3 1 2 254.19 253.08 5.86 o 4 1 2 1426.71 1434.83 23.24 o 5 1 2 487.81 470.38 9.60 o 6 1 2 6499.42 6677.49 100.59 o 7 1 2 100.89 109.24 5.06 o 8 1 2 1762.75 1783.55 33.55 o 9 1 2 230.95 252.39 9.61 o 10 1 2 1555.07 1514.98 30.45 o 11 1 2 0.20 3.35 7.15 o 12 1 2 1341.02 1377.30 39.12 o 13 1 2 59.04 63.30 11.08 o 14 1 2 503.25 495.48 28.62 o -15 2 2 202.53 190.15 20.31 o -14 2 2 133.75 137.56 11.74 o -13 2 2 357.11 335.66 15.12 o -12 2 2 1105.69 1083.36 32.45 o -11 2 2 467.02 467.10 16.01 o -10 2 2 854.09 914.18 23.42 o -9 2 2 611.18 641.33 15.52 o -8 2 2 1205.60 1163.39 20.87 o -7 2 2 644.10 624.39 12.50 o -6 2 2 1153.63 1114.27 19.33 o -5 2 2 1067.64 970.49 18.78 o -4 2 2 6233.42 6214.15 102.09 o -3 2 2 898.98 962.23 17.84 o -2 2 2 150.15 133.81 4.25 o -1 2 2 5988.53 6187.56 91.89 o 0 2 2 2914.60 2924.12 44.35 o 1 2 2 1763.68 1785.64 27.80 o 2 2 2 5297.87 5450.89 89.09 o 3 2 2 971.17 929.22 17.60 o 4 2 2 5845.14 5816.27 95.76 o 5 2 2 0.47 6.51 2.71 o 6 2 2 3684.95 3667.74 62.64 o 7 2 2 1225.99 1195.23 23.80 o 8 2 2 1625.81 1548.23 30.07 o 9 2 2 3.90 5.52 5.00 o 10 2 2 781.67 793.24 30.02 o 11 2 2 708.84 724.85 46.75 o 12 2 2 254.73 240.63 13.05 o 13 2 2 6.94 3.77 10.08 o 14 2 2 334.41 347.98 19.37 o -14 3 2 50.71 67.50 9.98 o -13 3 2 90.61 91.85 10.16 o -12 3 2 51.80 43.73 7.99 o -11 3 2 1337.09 1328.35 37.36 o -10 3 2 738.42 675.31 33.35 o -9 3 2 664.75 633.11 18.21 o -8 3 2 889.38 907.32 27.40 o -7 3 2 569.54 596.83 19.33 o -6 3 2 3058.35 3075.56 53.47 o -5 3 2 2.35 3.49 2.77 o -4 3 2 111.95 97.90 6.45 o -3 3 2 2519.12 2412.33 37.70 o -2 3 2 585.36 510.22 9.89 o -1 3 2 710.24 699.11 12.63 o 0 3 2 2373.73 2289.86 35.78 o 1 3 2 8372.87 8607.49 139.48 o 2 3 2 2114.01 2088.80 32.96 o 3 3 2 666.66 723.41 14.84 o 4 3 2 1125.11 1093.08 21.04 o 5 3 2 2321.49 2287.09 40.60 o 6 3 2 2049.94 2016.66 36.71 o 7 3 2 339.69 332.06 12.32 o 8 3 2 994.84 977.02 25.46 o 9 3 2 1185.09 1169.86 33.30 o 10 3 2 550.25 524.30 17.62 o 11 3 2 5.44 6.79 6.48 o 12 3 2 479.69 469.76 24.96 o 13 3 2 303.17 261.90 15.07 o -14 4 2 45.67 42.63 9.96 o -13 4 2 673.12 712.69 23.24 o -12 4 2 84.85 81.91 13.13 o -11 4 2 652.81 603.91 21.10 o -10 4 2 107.90 111.73 9.43 o -9 4 2 1601.49 1652.04 37.38 o -8 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