#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:00:30 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180940 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/20/2202027.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202027_Fobs loop_ _publ_author_name 'Almeida Paz, Filipe A.' 'Shi, Fa-Nian' 'Trindade, Tito' 'Rocha, Jo\~ao' 'Klinowski, Jacek' _publ_section_title ; catena-[1,3-Diammoniopropane di-\m~2~-hydroxo-di-\m~4~-phosphato-trioxotrivanadium dihydrate]: a redetermination at 180(2)K ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m179 _journal_page_last m182 _journal_volume 59 _journal_year 2003 _space_group_IT_number 62 _symmetry_space_group_name_Hall '-P 2ac 2n' _symmetry_space_group_name_H-M 'P n m a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 10.4643 _cell_length_b 17.1418 _cell_length_c 8.4481 _exptl_crystal_F_000 1076.00 _reflns_d_resolution_high 0.7705 _cod_data_source_file lh6045Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' test in Pnma' _shelx_refln_list_code 4 _shelx_f_calc_maximum 312.54 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z' 'x+1/2, -y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z' '-x-1/2, y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 11789.64 7229.19 2158.58 o 4 0 0 31921.61 28232.05 1293.77 o 6 0 0 17612.51 16550.38 1324.78 o 8 0 0 3740.73 3659.79 137.88 o 10 0 0 1838.57 2196.83 99.08 o 12 0 0 5341.83 5249.81 293.53 o 2 1 0 15.92 14.06 2.32 o 4 1 0 19028.07 18908.62 447.60 o 6 1 0 3207.41 2892.93 57.60 o 8 1 0 8516.34 8488.20 233.40 o 10 1 0 538.21 649.01 35.41 o 12 1 0 22.47 42.15 27.57 o 2 2 0 701.08 771.53 23.06 o 4 2 0 10320.33 9279.12 176.80 o 6 2 0 8299.80 8483.35 174.50 o 8 2 0 2729.61 2762.73 71.63 o 10 2 0 3868.50 4064.94 123.88 o 12 2 0 510.75 544.81 39.17 o 2 3 0 3499.24 3199.12 100.78 o 4 3 0 4823.07 5747.23 112.49 o 6 3 0 308.95 313.55 12.04 o 8 3 0 390.97 349.88 15.12 o 10 3 0 831.75 816.54 44.15 o 12 3 0 1115.79 1032.82 62.72 o 0 4 0 425.09 318.38 21.24 o 2 4 0 3603.09 3768.94 83.80 o 4 4 0 3593.85 3321.35 71.28 o 6 4 0 1105.69 1217.41 24.80 o 8 4 0 2179.02 2089.77 54.01 o 10 4 0 233.28 244.42 16.37 o 12 4 0 34.97 8.71 45.82 o 2 5 0 39.14 95.69 6.54 o 4 5 0 9379.59 10236.69 231.35 o 6 5 0 7596.79 7332.50 174.55 o 8 5 0 9663.01 10059.62 200.35 o 10 5 0 7.18 3.13 12.32 o 12 5 0 606.92 548.40 93.97 o 0 6 0 97680.81 102903.45 3217.72 o 2 6 0 3208.90 2855.65 75.30 o 4 6 0 5516.41 5600.56 108.67 o 6 6 0 562.73 582.80 18.58 o 8 6 0 12959.17 13218.72 289.34 o 10 6 0 316.58 260.20 21.35 o 12 6 0 5499.98 5762.54 332.22 o 2 7 0 7438.13 6964.10 245.54 o 4 7 0 4.76 6.82 6.31 o 6 7 0 80.25 86.96 7.95 o 8 7 0 53.50 56.43 10.06 o 10 7 0 11015.07 11597.00 349.81 o 12 7 0 5271.22 5649.26 322.56 o 0 8 0 48415.49 56310.49 2477.77 o 2 8 0 23.32 10.16 10.17 o 4 8 0 16716.29 17233.84 347.13 o 6 8 0 23591.26 25481.00 687.27 o 8 8 0 1578.97 1657.65 49.65 o 10 8 0 10128.62 11287.15 435.37 o 12 8 0 127.75 98.88 67.45 o 2 9 0 481.23 621.08 23.75 o 4 9 0 1788.88 1907.07 40.54 o 6 9 0 3840.61 4093.27 103.40 o 8 9 0 9.53 -3.57 11.04 o 10 9 0 30.42 37.80 24.77 o 12 9 0 2.78 -8.51 53.76 o 0 10 0 17738.36 20171.34 746.77 o 2 10 0 7291.78 7855.20 260.32 o 4 10 0 445.52 433.85 29.67 o 6 10 0 1935.35 2068.47 55.36 o 8 10 0 1007.96 1008.62 54.85 o 10 10 0 851.07 895.52 53.84 o 12 10 0 54.33 -2.42 55.68 o 2 11 0 652.69 590.22 26.51 o 4 11 0 0.77 0.57 9.88 o 6 11 0 6418.47 6393.18 302.76 o 8 11 0 7836.99 8384.33 237.16 o 10 11 0 12.77 4.82 55.90 o 0 12 0 22798.16 24694.50 739.88 o 2 12 0 1260.98 1244.71 57.66 o 4 12 0 297.59 292.36 15.67 o 6 12 0 0.87 14.60 15.48 o 8 12 0 3304.38 3375.85 176.49 o 10 12 0 389.69 353.28 48.60 o 2 13 0 11480.53 11969.29 271.81 o 4 13 0 6123.09 6070.51 162.98 o 6 13 0 2717.40 2784.83 165.29 o 8 13 0 68.58 91.33 28.89 o 10 13 0 5583.20 6085.69 401.24 o 0 14 0 10420.93 11224.17 551.47 o 2 14 0 839.76 808.48 58.04 o 4 14 0 2541.33 2774.43 106.82 o 6 14 0 411.85 388.74 34.78 o 8 14 0 4247.30 4003.39 203.73 o 10 14 0 1442.64 1428.98 202.90 o 2 15 0 4001.92 4116.85 168.57 o 4 15 0 1738.15 1675.26 98.12 o 6 15 0 8883.88 10124.24 515.93 o 8 15 0 1764.50 1773.78 128.68 o 10 15 0 1243.97 1343.33 231.39 o 0 16 0 2571.11 2609.25 139.96 o 2 16 0 1877.97 1960.06 97.85 o 4 16 0 553.31 462.93 52.04 o 6 16 0 233.66 258.33 42.46 o 8 16 0 33.82 45.57 33.30 o 2 17 0 76.98 40.96 38.18 o 4 17 0 659.40 631.27 55.08 o 6 17 0 645.42 591.33 53.38 o 8 17 0 1912.89 1829.80 204.88 o 0 18 0 89.93 192.11 69.76 o 2 18 0 1.13 -11.25 56.45 o 4 18 0 2339.13 2541.74 138.01 o 6 18 0 2093.33 1842.79 121.67 o 2 19 0 12012.25 12276.12 642.25 o 4 19 0 4838.30 4899.65 441.33 o 6 19 0 1891.43 1846.91 130.27 o 0 20 0 1684.33 1476.16 146.56 o 2 20 0 980.24 992.40 90.55 o 4 20 0 39.29 44.07 44.44 o 2 21 0 5696.19 5428.33 299.35 o 4 21 0 440.19 359.92 70.21 o 0 22 0 539.66 415.03 81.64 o 2 22 0 497.57 399.85 90.44 o 2 0 1 5586.57 5657.94 162.60 o 3 0 1 28284.04 27786.55 776.26 o 4 0 1 2127.53 2129.12 40.79 o 5 0 1 458.93 591.87 16.02 o 6 0 1 16831.79 16314.01 425.77 o 7 0 1 10023.36 10604.30 262.38 o 8 0 1 31570.76 31968.83 660.36 o 9 0 1 445.61 393.45 17.88 o 10 0 1 1.17 4.51 27.16 o 11 0 1 349.36 370.94 33.67 o 12 0 1 4614.25 4869.80 214.57 o 13 0 1 0.23 -21.35 57.00 o 2 1 1 16155.58 15184.49 270.61 o 3 1 1 175.81 198.07 6.28 o 4 1 1 720.33 702.62 14.71 o 5 1 1 1462.80 1585.37 22.44 o 6 1 1 1779.56 1837.22 31.74 o 7 1 1 179.58 195.26 8.59 o 8 1 1 578.07 600.83 18.80 o 9 1 1 43.03 42.91 8.07 o 10 1 1 180.35 164.88 9.32 o 11 1 1 53.10 57.63 14.27 o 12 1 1 695.89 802.93 32.50 o 13 1 1 268.33 258.23 38.51 o 1 2 1 3170.41 2691.66 113.48 o 2 2 1 25020.54 24329.47 408.62 o 3 2 1 425.96 435.51 7.35 o 4 2 1 45.40 13.92 3.02 o 5 2 1 1921.41 1827.96 23.67 o 6 2 1 83.97 78.45 4.26 o 7 2 1 6371.47 6469.40 94.44 o 8 2 1 457.43 433.44 11.07 o 9 2 1 2.16 16.15 6.13 o 10 2 1 3287.98 3366.62 74.32 o 11 2 1 13.42 43.66 15.37 o 12 2 1 2107.59 2026.69 67.80 o 13 2 1 47.13 25.36 54.13 o 0 3 1 7466.27 7874.16 306.94 o 1 3 1 1.00 26.35 3.51 o 2 3 1 1876.17 1978.17 46.36 o 3 3 1 12071.52 11792.81 161.58 o 4 3 1 6541.55 5830.98 74.14 o 5 3 1 6815.64 6929.96 90.80 o 6 3 1 7700.55 7640.31 108.44 o 7 3 1 785.30 767.18 14.96 o 8 3 1 2767.31 2683.33 44.30 o 9 3 1 561.66 607.09 23.93 o 10 3 1 4505.12 4901.92 113.76 o 11 3 1 43.76 49.52 16.09 o 12 3 1 714.32 726.53 36.25 o 13 3 1 168.36 206.41 47.18 o 1 4 1 3633.55 4009.74 69.41 o 2 4 1 243.58 343.05 7.52 o 3 4 1 1152.79 1211.44 20.00 o 4 4 1 4201.38 4292.73 60.13 o 5 4 1 2915.80 2867.09 36.84 o 6 4 1 1691.15 1681.17 23.78 o 7 4 1 4929.10 5017.86 69.00 o 8 4 1 2074.08 2086.51 33.81 o 9 4 1 63.96 61.85 5.50 o 10 4 1 418.86 427.73 19.96 o 11 4 1 19.53 14.74 15.95 o 12 4 1 31.33 22.62 30.14 o 13 4 1 309.68 299.57 57.59 o 0 5 1 58359.36 63031.89 1522.34 o 1 5 1 1374.97 1651.66 27.78 o 2 5 1 960.41 799.89 21.24 o 3 5 1 36.96 39.85 4.38 o 4 5 1 229.12 172.95 5.76 o 5 5 1 81.88 73.44 5.36 o 6 5 1 103.15 80.24 5.79 o 7 5 1 37.89 40.23 3.84 o 8 5 1 1268.34 1234.76 22.48 o 9 5 1 8.03 14.69 6.03 o 10 5 1 323.70 330.66 15.00 o 11 5 1 142.17 154.25 22.36 o 12 5 1 4416.12 4706.69 182.04 o 13 5 1 527.48 405.54 59.49 o 1 6 1 10078.14 10782.42 365.05 o 2 6 1 1481.64 1798.11 37.64 o 3 6 1 272.93 421.95 9.72 o 4 6 1 308.07 325.38 7.74 o 5 6 1 963.97 990.13 18.02 o 6 6 1 2767.66 2725.55 37.64 o 7 6 1 4786.34 4907.14 82.01 o 8 6 1 9346.03 9552.45 149.01 o 9 6 1 1765.91 1793.72 42.13 o 10 6 1 80.83 91.59 12.74 o 11 6 1 3075.87 3432.15 107.20 o 12 6 1 332.03 300.47 30.79 o 13 6 1 90.27 166.54 52.26 o 0 7 1 4491.03 5014.91 112.93 o 1 7 1 1797.08 2282.95 35.94 o 2 7 1 365.45 331.04 9.08 o 3 7 1 61.33 74.04 6.12 o 4 7 1 9522.27 9853.94 201.77 o 5 7 1 1033.96 1049.53 24.25 o 6 7 1 849.99 849.60 15.55 o 7 7 1 7160.09 7465.18 102.89 o 8 7 1 1.17 5.63 7.66 o 9 7 1 466.31 474.19 14.70 o 10 7 1 589.18 612.05 25.88 o 11 7 1 139.68 173.68 33.58 o 12 7 1 311.65 209.96 56.47 o 1 8 1 1662.19 1857.60 37.35 o 2 8 1 41119.14 43625.99 679.12 o 3 8 1 4696.50 5124.88 99.38 o 4 8 1 4443.61 4354.80 91.65 o 5 8 1 284.93 295.04 11.27 o 6 8 1 4285.25 4376.65 65.77 o 7 8 1 3945.62 4239.51 61.33 o 8 8 1 455.52 472.38 14.57 o 9 8 1 249.66 270.33 14.57 o 10 8 1 1648.83 1839.40 58.82 o 11 8 1 96.17 89.79 27.66 o 12 8 1 3729.62 3951.04 160.71 o 0 9 1 486.73 491.41 18.43 o 1 9 1 654.85 606.43 24.60 o 2 9 1 221.08 209.48 12.89 o 3 9 1 4950.66 5174.96 109.20 o 4 9 1 6573.02 6703.38 126.55 o 5 9 1 5570.53 5704.29 89.89 o 6 9 1 2448.52 2477.86 42.59 o 7 9 1 2388.34 2512.17 53.39 o 8 9 1 1717.41 1716.28 33.71 o 9 9 1 994.73 1029.46 38.61 o 10 9 1 1230.60 1336.90 56.77 o 11 9 1 26.19 19.24 29.69 o 12 9 1 463.08 429.22 51.07 o 1 10 1 688.26 770.34 18.14 o 2 10 1 6208.18 6325.81 169.22 o 3 10 1 3952.84 4142.33 76.75 o 4 10 1 365.74 427.10 13.08 o 5 10 1 3696.17 3828.61 63.97 o 6 10 1 8433.64 8786.41 139.49 o 7 10 1 2643.43 2716.40 68.55 o 8 10 1 7685.96 8056.04 149.18 o 9 10 1 42.28 40.45 14.06 o 10 10 1 2.14 7.09 19.49 o 11 10 1 102.43 65.77 41.81 o 12 10 1 1158.59 977.79 101.16 o 0 11 1 25569.64 26648.28 902.46 o 1 11 1 1002.49 1125.38 25.08 o 2 11 1 3913.63 4152.47 100.80 o 3 11 1 597.81 618.22 20.63 o 4 11 1 4964.66 5016.95 156.50 o 5 11 1 19.03 8.48 8.06 o 6 11 1 711.22 781.14 22.82 o 7 11 1 0.55 -2.01 7.83 o 8 11 1 1935.26 1948.05 57.36 o 9 11 1 79.52 37.60 26.85 o 10 11 1 465.95 512.04 34.23 o 11 11 1 57.85 37.08 29.13 o 1 12 1 4270.75 4554.45 80.87 o 2 12 1 1854.75 1953.51 53.98 o 3 12 1 186.45 231.67 12.97 o 4 12 1 72.94 73.50 7.48 o 5 12 1 148.09 153.65 15.37 o 6 12 1 450.24 439.54 27.28 o 7 12 1 1598.16 1566.27 44.46 o 8 12 1 445.77 478.76 22.36 o 9 12 1 656.80 592.96 31.10 o 10 12 1 1042.11 992.51 48.76 o 11 12 1 921.75 832.33 61.43 o 0 13 1 1058.45 1098.27 39.10 o 1 13 1 2927.06 2876.65 57.05 o 2 13 1 1626.53 1644.32 49.20 o 3 13 1 643.78 646.61 23.24 o 4 13 1 4736.44 4951.79 85.11 o 5 13 1 2163.05 2207.75 72.61 o 6 13 1 298.62 334.31 16.92 o 7 13 1 303.93 312.89 20.08 o 8 13 1 847.13 875.08 30.96 o 9 13 1 701.14 704.00 42.68 o 10 13 1 1176.32 1225.02 56.14 o 1 14 1 452.12 494.86 26.16 o 2 14 1 5471.51 5367.01 119.95 o 3 14 1 1515.23 1430.81 41.85 o 4 14 1 490.98 510.93 21.12 o 5 14 1 1314.21 1265.42 50.27 o 6 14 1 6.26 29.91 14.63 o 7 14 1 670.62 685.11 36.06 o 8 14 1 1093.85 1123.92 38.87 o 9 14 1 0.49 2.13 21.99 o 10 14 1 1640.71 1529.62 70.60 o 0 15 1 3257.43 3727.88 125.63 o 1 15 1 424.92 386.54 29.84 o 2 15 1 3045.45 3048.84 84.89 o 3 15 1 2318.23 2352.11 64.95 o 4 15 1 1.97 1.28 8.09 o 5 15 1 2780.73 2959.33 85.40 o 6 15 1 130.91 96.52 20.16 o 7 15 1 3130.45 3434.08 120.30 o 8 15 1 1.89 -16.69 16.69 o 9 15 1 970.29 900.19 54.51 o 1 16 1 538.08 516.58 29.74 o 2 16 1 2971.05 3139.01 87.37 o 3 16 1 45.26 66.29 18.48 o 4 16 1 523.45 467.91 22.18 o 5 16 1 973.28 924.30 54.26 o 6 16 1 7285.29 7909.28 226.44 o 7 16 1 1839.23 1897.47 71.25 o 8 16 1 3155.17 3214.83 124.77 o 9 16 1 32.29 56.23 34.18 o 0 17 1 2079.25 2316.84 107.89 o 1 17 1 57.83 40.59 22.78 o 2 17 1 791.44 855.34 41.81 o 3 17 1 263.58 219.13 26.62 o 4 17 1 248.36 217.78 23.51 o 5 17 1 165.41 159.09 26.27 o 6 17 1 38.12 53.04 25.79 o 7 17 1 570.12 533.68 49.30 o 8 17 1 397.78 344.84 40.51 o 1 18 1 773.85 786.63 44.48 o 2 18 1 5209.60 5116.52 163.51 o 3 18 1 13.24 -19.74 26.97 o 4 18 1 2486.16 2514.92 132.67 o 5 18 1 265.19 272.12 30.71 o 6 18 1 752.75 801.53 55.62 o 7 18 1 324.83 241.25 30.54 o 0 19 1 129.91 94.78 41.51 o 1 19 1 1266.24 1172.83 55.04 o 2 19 1 0.86 -16.18 26.34 o 3 19 1 436.93 390.69 35.76 o 4 19 1 6055.14 6182.54 216.14 o 5 19 1 762.04 709.76 46.62 o 6 19 1 1517.69 1426.80 77.19 o 1 20 1 0.62 1.74 32.94 o 2 20 1 543.18 462.81 39.73 o 3 20 1 25.11 13.25 28.30 o 4 20 1 473.10 415.60 40.97 o 5 20 1 114.79 107.94 31.46 o 0 21 1 1783.74 1894.25 135.60 o 1 21 1 638.38 558.82 46.99 o 2 21 1 819.65 694.47 50.41 o 3 21 1 1558.66 1493.55 77.80 o 4 21 1 95.37 82.54 41.57 o 1 22 1 466.17 404.20 38.25 o 0 0 2 23985.43 20983.80 1201.56 o 1 0 2 438.23 432.33 9.93 o 2 0 2 216.54 258.07 16.07 o 3 0 2 6175.06 5873.06 185.43 o 4 0 2 13952.20 13878.57 375.21 o 5 0 2 5260.22 5132.48 80.23 o 6 0 2 3.54 38.87 8.82 o 7 0 2 31.56 21.05 10.12 o 8 0 2 20.78 35.97 10.09 o 9 0 2 1813.87 1688.23 49.97 o 10 0 2 1386.93 1399.75 58.58 o 11 0 2 1195.81 1169.70 51.47 o 12 0 2 204.94 175.29 42.35 o 13 0 2 1154.19 1112.40 130.50 o 1 1 2 4367.58 3985.73 93.88 o 2 1 2 35570.43 32841.06 782.84 o 3 1 2 889.37 819.61 18.18 o 4 1 2 2941.82 3081.11 63.22 o 5 1 2 2842.08 2771.02 49.27 o 6 1 2 6745.52 6538.34 92.26 o 7 1 2 335.08 357.52 12.59 o 8 1 2 3160.75 3050.98 53.69 o 9 1 2 1122.86 1091.18 34.31 o 10 1 2 11.22 24.17 8.53 o 11 1 2 869.04 898.64 33.25 o 12 1 2 332.28 386.67 27.60 o 13 1 2 1.90 16.55 36.84 o 0 2 2 1590.86 1564.04 41.60 o 1 2 2 4878.70 4483.35 92.06 o 2 2 2 76.05 139.51 6.06 o 3 2 2 3644.37 3575.84 65.28 o 4 2 2 4308.00 4039.09 67.20 o 5 2 2 2521.49 2599.96 46.60 o 6 2 2 3123.51 3043.84 45.70 o 7 2 2 173.79 183.16 7.00 o 8 2 2 35.57 32.84 7.51 o 9 2 2 118.33 103.18 8.48 o 10 2 2 1984.74 2028.66 54.61 o 11 2 2 148.47 119.85 16.46 o 12 2 2 250.36 253.79 34.77 o 13 2 2 227.12 204.46 34.09 o 1 3 2 1066.26 1074.13 18.63 o 2 3 2 61340.13 57112.79 1077.08 o 3 3 2 202.70 173.18 4.80 o 4 3 2 4707.68 4749.84 66.02 o 5 3 2 3595.38 3471.89 46.82 o 6 3 2 11524.07 11385.47 157.35 o 7 3 2 6004.97 5852.13 93.11 o 8 3 2 89.54 74.28 8.71 o 9 3 2 31.33 36.11 8.19 o 10 3 2 7855.32 8161.83 188.51 o 11 3 2 69.32 68.71 25.85 o 12 3 2 5195.29 5523.60 188.71 o 13 3 2 103.33 111.91 45.23 o 0 4 2 24784.73 25176.85 587.70 o 1 4 2 3640.46 3432.77 68.06 o 2 4 2 2893.84 2790.41 41.56 o 3 4 2 2376.98 2315.62 34.58 o 4 4 2 104.68 102.81 4.12 o 5 4 2 4830.33 4903.57 65.06 o 6 4 2 71.98 97.91 5.14 o 7 4 2 522.57 514.63 11.49 o 8 4 2 628.06 605.28 13.96 o 9 4 2 212.11 233.80 13.14 o 10 4 2 255.48 253.73 24.78 o 11 4 2 663.71 739.67 36.26 o 12 4 2 1431.81 1416.23 58.72 o 13 4 2 247.84 258.72 45.70 o 1 5 2 349.15 473.25 9.73 o 2 5 2 3147.20 2750.02 63.54 o 3 5 2 7123.57 7175.10 92.30 o 4 5 2 646.95 755.92 13.11 o 5 5 2 1478.94 1533.25 20.95 o 6 5 2 14018.78 13439.53 177.75 o 7 5 2 162.12 166.12 8.35 o 8 5 2 2213.49 2225.87 35.87 o 9 5 2 3246.50 3372.90 64.36 o 10 5 2 1976.09 2010.53 58.04 o 11 5 2 604.07 556.60 32.54 o 12 5 2 2488.71 2555.99 109.02 o 13 5 2 124.87 77.27 44.17 o 0 6 2 421.23 437.18 14.97 o 1 6 2 296.27 267.57 7.44 o 2 6 2 2069.78 2312.09 60.77 o 3 6 2 2120.86 2055.09 37.60 o 4 6 2 2021.51 2122.08 30.75 o 5 6 2 1567.39 1590.60 22.59 o 6 6 2 269.22 279.78 10.47 o 7 6 2 67.92 60.65 5.94 o 8 6 2 1085.75 1066.05 21.08 o 9 6 2 143.40 126.63 12.16 o 10 6 2 6.52 1.44 14.03 o 11 6 2 632.90 586.65 40.66 o 12 6 2 644.76 625.07 54.15 o 1 7 2 1111.32 1272.81 28.17 o 2 7 2 1267.93 1282.96 25.01 o 3 7 2 53.33 50.62 6.41 o 4 7 2 2513.06 2646.29 38.44 o 5 7 2 534.02 466.72 11.00 o 6 7 2 725.67 786.07 16.89 o 7 7 2 172.70 171.38 7.91 o 8 7 2 3312.83 3178.20 66.88 o 9 7 2 237.17 245.42 19.56 o 10 7 2 27.75 31.37 11.84 o 11 7 2 434.76 395.74 43.27 o 12 7 2 426.64 365.03 46.44 o 0 8 2 615.61 558.78 21.66 o 1 8 2 4796.69 4920.32 79.43 o 2 8 2 0.39 2.27 4.96 o 3 8 2 382.38 412.32 11.13 o 4 8 2 5866.50 5760.14 98.10 o 5 8 2 215.48 203.29 9.52 o 6 8 2 5047.84 5211.99 71.86 o 7 8 2 93.29 91.79 7.16 o 8 8 2 866.96 846.81 19.12 o 9 8 2 876.55 854.89 29.04 o 10 8 2 5913.67 6235.48 170.06 o 11 8 2 1.88 -27.97 27.97 o 12 8 2 11.58 -53.79 53.79 o 1 9 2 5141.87 5691.43 89.33 o 2 9 2 21624.64 22953.29 295.53 o 3 9 2 1299.02 1295.81 22.63 o 4 9 2 6049.14 6103.50 106.02 o 5 9 2 2176.72 2178.88 35.57 o 6 9 2 1949.60 1998.04 33.56 o 7 9 2 4686.94 4891.55 76.08 o 8 9 2 143.62 140.74 13.64 o 9 9 2 946.30 946.01 42.31 o 10 9 2 2851.58 2985.35 93.19 o 11 9 2 34.73 -7.72 30.86 o 12 9 2 1429.59 1374.60 132.42 o 0 10 2 36078.17 37457.98 756.80 o 1 10 2 488.19 496.00 14.43 o 2 10 2 2701.88 2712.22 41.30 o 3 10 2 2791.48 2795.07 45.49 o 4 10 2 3251.90 3276.28 82.90 o 5 10 2 7831.91 8328.19 127.29 o 6 10 2 1613.61 1610.93 28.17 o 7 10 2 489.48 465.85 17.12 o 8 10 2 3659.76 3676.73 82.79 o 9 10 2 1290.64 1278.67 46.22 o 10 10 2 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12 6 4 1977.58 1635.36 139.38 o 1 7 4 1971.26 1950.68 35.72 o 2 7 4 3340.24 3397.72 53.04 o 3 7 4 30.75 40.81 6.39 o 4 7 4 4852.70 4914.17 84.11 o 5 7 4 1137.92 1151.63 24.90 o 6 7 4 5434.57 5384.61 80.54 o 7 7 4 4947.00 4983.50 104.54 o 8 7 4 980.33 966.64 30.26 o 9 7 4 209.93 217.78 16.35 o 10 7 4 217.17 198.43 19.79 o 11 7 4 9.17 -15.46 24.56 o 0 8 4 7865.59 7595.75 170.75 o 1 8 4 7014.40 7036.02 125.91 o 2 8 4 3174.43 3053.37 49.79 o 3 8 4 19.44 31.20 5.30 o 4 8 4 3639.93 3416.52 58.87 o 5 8 4 1857.32 1932.47 41.29 o 6 8 4 2602.54 2585.52 73.38 o 7 8 4 17.30 15.17 10.24 o 8 8 4 2014.27 2082.02 74.15 o 9 8 4 2581.60 2764.00 80.69 o 10 8 4 1421.34 1489.92 76.20 o 11 8 4 5.64 2.54 28.51 o 1 9 4 450.99 479.96 16.27 o 2 9 4 1502.02 1502.92 28.14 o 3 9 4 447.93 449.01 20.75 o 4 9 4 2531.18 2392.08 56.92 o 5 9 4 1513.04 1469.29 35.55 o 6 9 4 4.80 9.08 10.44 o 7 9 4 75.91 81.27 10.11 o 8 9 4 988.80 1006.90 33.28 o 9 9 4 1780.95 1809.90 58.18 o 10 9 4 753.54 673.27 43.44 o 11 9 4 153.65 107.36 42.01 o 0 10 4 4534.86 4374.66 115.79 o 1 10 4 696.88 675.13 16.46 o 2 10 4 256.18 241.18 11.73 o 3 10 4 1536.20 1379.53 37.64 o 4 10 4 884.80 897.77 33.34 o 5 10 4 1281.44 1247.32 54.41 o 6 10 4 110.85 110.87 12.11 o 7 10 4 25.74 40.96 13.26 o 8 10 4 206.29 187.56 18.75 o 9 10 4 1209.60 1169.93 47.66 o 10 10 4 498.28 533.72 50.72 o 11 10 4 853.28 847.74 106.95 o 1 11 4 429.11 410.15 16.76 o 2 11 4 1830.89 1848.39 55.02 o 3 11 4 2694.03 2855.88 57.95 o 4 11 4 664.21 731.67 55.16 o 5 11 4 708.01 769.31 35.16 o 6 11 4 237.63 274.75 18.80 o 7 11 4 1.18 -3.07 14.57 o 8 11 4 685.76 674.80 32.91 o 9 11 4 110.51 139.97 22.13 o 10 11 4 612.70 509.71 49.08 o 0 12 4 15072.18 14925.91 848.19 o 1 12 4 13.95 21.73 11.90 o 2 12 4 123.99 106.11 9.18 o 3 12 4 2560.59 2417.01 71.75 o 4 12 4 2908.30 2935.96 88.68 o 5 12 4 1324.64 1359.19 48.49 o 6 12 4 1606.06 1493.72 69.65 o 7 12 4 49.24 36.91 15.31 o 8 12 4 52.78 59.76 17.36 o 9 12 4 68.52 62.48 25.10 o 10 12 4 153.36 119.29 47.25 o 1 13 4 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484.98 22.76 o 3 2 7 806.05 796.21 23.19 o 4 2 7 20.51 19.08 11.22 o 5 2 7 11.03 8.95 10.64 o 6 2 7 2291.16 2225.88 76.04 o 7 2 7 394.23 418.29 36.00 o 8 2 7 406.15 376.49 26.95 o 9 2 7 9.64 59.65 32.00 o 10 2 7 47.71 94.96 33.81 o 0 3 7 1204.49 1195.85 47.99 o 1 3 7 3393.12 3361.51 102.02 o 2 3 7 649.18 746.43 33.11 o 3 3 7 2952.07 3084.50 81.39 o 4 3 7 890.04 920.02 42.71 o 5 3 7 6395.18 6631.69 180.74 o 6 3 7 558.04 537.92 24.82 o 7 3 7 264.15 217.36 18.29 o 8 3 7 579.60 575.59 30.62 o 9 3 7 5750.90 6279.40 254.56 o 10 3 7 4.34 39.27 23.81 o 1 4 7 43.53 54.00 10.52 o 2 4 7 84.67 94.54 12.58 o 3 4 7 8.20 9.50 10.92 o 4 4 7 176.53 181.72 12.97 o 5 4 7 685.74 635.19 22.13 o 6 4 7 2481.49 2428.15 104.97 o 7 4 7 314.04 308.76 21.37 o 8 4 7 628.24 599.52 40.51 o 9 4 7 179.23 191.34 29.20 o 10 4 7 8.68 1.10 31.05 o 0 5 7 6251.82 5982.63 160.15 o 1 5 7 7345.08 7305.87 139.84 o 2 5 7 1328.15 1254.73 39.39 o 3 5 7 1774.54 1713.87 50.84 o 4 5 7 351.02 403.08 19.44 o 5 5 7 2947.35 2898.63 66.72 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