#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2202049.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202049_Fobs loop_ _publ_author_name 'Low, John Nicolson' 'Cobo, Justo' 'Nogueras, Manuel' 'S\'anchez, Adolfo' 'Insuasty, Braulio' 'Mosquera, M\'onica' _publ_section_title ; 5-(Benzo[1,3]dioxol-5-yl)-7-(4-chlorophenyl)-3-methyl-1-phenyl-1,6,7,8-tetrahydropyrazolo[3,4-b][1,4]diazepine ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o18 _journal_page_last o20 _journal_volume 59 _journal_year 2003 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.437 _cell_angle_gamma 90.000 _cell_length_a 11.3422 _cell_length_b 15.6889 _cell_length_c 24.1716 _exptl_crystal_F_000 1904.00 _reflns_d_resolution_high 0.7699 _[local]_cod_data_source_file na6190Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 270 - HATOM' _shelx_refln_list_code 4 _shelx_f_calc_maximum 367.74 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1652.93 1467.96 49.22 o 4 0 0 18623.41 19294.99 761.59 o 5 0 0 2474.95 2587.61 117.23 o 6 0 0 361.65 340.69 15.96 o 7 0 0 746.51 720.30 31.86 o 8 0 0 191.31 181.09 19.64 o 9 0 0 215.12 196.29 16.01 o 10 0 0 343.61 359.94 31.97 o 11 0 0 2168.51 2306.68 146.18 o 12 0 0 360.91 362.62 58.82 o 13 0 0 936.67 944.39 139.02 o 14 0 0 0.22 -27.64 83.19 o 3 1 0 7250.02 6810.84 164.06 o 4 1 0 562.21 538.88 18.11 o 5 1 0 2583.92 2810.18 64.07 o 6 1 0 1.68 6.91 13.82 o 7 1 0 486.87 479.52 22.57 o 8 1 0 0.38 -5.59 14.43 o 9 1 0 159.80 167.17 13.09 o 10 1 0 115.50 171.58 26.49 o 11 1 0 1700.30 1630.64 74.49 o 12 1 0 77.32 124.75 27.71 o 13 1 0 16.31 69.39 35.52 o 14 1 0 35.58 66.62 55.55 o 1 2 0 579.74 550.27 12.41 o 2 2 0 15799.10 14557.75 353.82 o 3 2 0 4711.93 4410.05 109.76 o 4 2 0 400.10 438.77 12.36 o 5 2 0 81.66 46.06 15.96 o 6 2 0 342.45 301.08 12.36 o 7 2 0 7.93 33.11 12.36 o 8 2 0 1178.45 1172.36 33.24 o 9 2 0 667.16 588.79 40.28 o 10 2 0 555.55 612.95 25.05 o 11 2 0 568.96 547.42 32.71 o 12 2 0 980.25 916.52 58.18 o 13 2 0 211.09 142.73 40.42 o 14 2 0 116.49 72.01 55.69 o 1 3 0 20720.22 18138.10 466.49 o 2 3 0 444.49 451.59 13.68 o 3 3 0 5971.98 5756.41 123.22 o 4 3 0 53.03 13.82 19.54 o 5 3 0 7119.42 7784.98 192.20 o 6 3 0 1464.17 1516.33 38.90 o 7 3 0 0.92 0.00 12.36 o 8 3 0 240.35 250.49 13.44 o 9 3 0 25.00 30.78 13.44 o 10 3 0 428.09 446.63 24.77 o 11 3 0 295.14 303.58 27.71 o 12 3 0 2805.05 3069.65 162.48 o 13 3 0 13.18 13.77 29.37 o 14 3 0 43.90 0.00 69.37 o 0 4 0 135236.11 129668.38 9095.96 o 1 4 0 66.04 55.55 19.64 o 2 4 0 723.83 576.99 22.30 o 3 4 0 0.73 0.00 27.91 o 4 4 0 63.31 78.71 11.34 o 5 4 0 612.00 567.49 20.72 o 6 4 0 809.68 867.05 26.32 o 7 4 0 890.60 871.25 37.04 o 8 4 0 416.99 373.45 35.77 o 9 4 0 1450.29 1628.41 51.42 o 10 4 0 0.67 3.93 15.34 o 11 4 0 1161.82 998.42 64.90 o 12 4 0 231.86 214.54 29.84 o 13 4 0 51.00 127.51 46.09 o 1 5 0 11558.73 11245.95 343.69 o 2 5 0 519.16 556.48 33.13 o 3 5 0 2442.77 2482.92 66.63 o 4 5 0 41.81 49.98 12.46 o 5 5 0 13027.98 13781.00 330.08 o 6 5 0 123.40 149.35 11.92 o 7 5 0 8.71 13.82 13.82 o 8 5 0 2614.17 2644.91 86.03 o 9 5 0 130.30 130.76 20.06 o 10 5 0 551.53 521.31 26.25 o 11 5 0 951.98 940.35 56.29 o 12 5 0 27.13 27.64 55.41 o 13 5 0 215.23 269.31 84.16 o 14 5 0 22.74 27.71 39.18 o 0 6 0 17768.39 16687.57 732.04 o 1 6 0 7122.54 6847.11 198.67 o 2 6 0 1739.34 1684.70 43.45 o 3 6 0 286.89 320.05 13.92 o 4 6 0 505.19 462.98 23.94 o 5 6 0 160.90 173.16 11.30 o 6 6 0 1144.10 1269.34 37.20 o 7 6 0 684.09 714.02 25.06 o 8 6 0 213.94 206.92 14.78 o 9 6 0 2729.43 2837.00 93.25 o 10 6 0 104.90 125.72 15.34 o 11 6 0 457.17 412.06 53.62 o 12 6 0 72.46 69.13 39.18 o 13 6 0 730.31 724.51 78.46 o 14 6 0 17.11 -0.05 58.82 o 1 7 0 407.74 459.91 19.74 o 2 7 0 137.76 192.60 13.92 o 3 7 0 2147.57 2128.72 65.09 o 4 7 0 167.64 209.14 15.88 o 5 7 0 52.83 5.53 12.36 o 6 7 0 1576.61 1513.36 39.28 o 7 7 0 247.45 228.23 15.98 o 8 7 0 554.28 525.23 23.71 o 9 7 0 21.20 21.49 13.41 o 10 7 0 168.60 148.54 17.49 o 11 7 0 100.42 101.48 31.91 o 12 7 0 123.83 187.87 45.93 o 13 7 0 89.84 124.61 41.04 o 0 8 0 712.80 701.50 55.83 o 1 8 0 711.78 658.58 27.88 o 2 8 0 8398.74 8586.88 286.73 o 3 8 0 350.84 269.96 12.43 o 4 8 0 1177.96 1108.05 41.73 o 5 8 0 136.35 147.06 16.08 o 6 8 0 4.27 0.00 13.82 o 7 8 0 2046.26 1979.65 58.31 o 8 8 0 4.05 3.06 13.34 o 9 8 0 768.80 744.82 57.99 o 10 8 0 890.02 843.22 43.95 o 11 8 0 498.44 514.62 45.88 o 12 8 0 48.93 -83.19 83.19 o 13 8 0 50.73 110.77 46.09 o 1 9 0 1874.57 2087.92 65.23 o 2 9 0 325.54 335.45 18.53 o 3 9 0 276.77 229.64 13.48 o 4 9 0 2315.34 2233.30 79.26 o 5 9 0 972.23 1119.29 39.07 o 6 9 0 105.06 100.10 12.69 o 7 9 0 18.75 9.24 11.32 o 8 9 0 312.41 337.27 22.58 o 9 9 0 355.40 312.58 24.72 o 10 9 0 104.88 100.75 20.77 o 11 9 0 3.60 20.75 41.60 o 12 9 0 666.72 832.18 138.74 o 13 9 0 161.40 111.10 111.10 o 0 10 0 852.16 795.78 41.32 o 1 10 0 6774.58 6641.78 228.15 o 2 10 0 709.19 625.41 24.84 o 3 10 0 338.36 353.25 13.48 o 4 10 0 17.41 22.19 13.36 o 5 10 0 1465.86 1354.88 68.56 o 6 10 0 1008.57 914.11 39.03 o 7 10 0 304.12 291.60 27.71 o 8 10 0 372.14 398.84 28.01 o 9 10 0 173.06 142.87 19.46 o 10 10 0 30.14 36.79 27.50 o 11 10 0 702.55 803.86 80.70 o 12 10 0 0.02 41.49 39.18 o 1 11 0 1143.43 1143.24 48.24 o 2 11 0 184.75 206.74 15.06 o 3 11 0 799.09 783.96 28.15 o 4 11 0 4307.46 4604.80 199.97 o 5 11 0 233.57 223.44 15.13 o 6 11 0 1354.91 1313.12 56.14 o 7 11 0 5.44 -0.06 13.92 o 8 11 0 113.45 151.94 39.08 o 9 11 0 113.61 116.10 20.89 o 10 11 0 1324.30 1625.39 137.91 o 11 11 0 36.30 55.28 55.28 o 12 11 0 898.77 1098.10 86.72 o 0 12 0 124.08 136.84 41.60 o 1 12 0 489.12 446.48 39.28 o 2 12 0 1.08 0.06 16.67 o 3 12 0 151.15 114.14 13.48 o 4 12 0 518.34 434.08 36.38 o 5 12 0 838.84 927.14 53.30 o 6 12 0 93.02 86.89 14.16 o 7 12 0 72.41 88.73 17.14 o 8 12 0 479.21 538.57 48.08 o 9 12 0 396.28 377.80 47.95 o 10 12 0 1514.58 1801.51 136.39 o 11 12 0 8.07 33.31 46.20 o 1 13 0 104.01 138.86 18.52 o 2 13 0 2420.85 2383.72 100.22 o 3 13 0 98.85 86.97 16.70 o 4 13 0 691.81 567.73 28.17 o 5 13 0 32.14 62.65 17.26 o 6 13 0 172.91 204.90 17.19 o 7 13 0 37.09 92.65 32.13 o 8 13 0 0.06 9.27 31.97 o 9 13 0 139.32 158.19 35.38 o 10 13 0 30.94 27.64 55.28 o 11 13 0 98.99 111.20 49.66 o 0 14 0 41.29 0.00 55.55 o 1 14 0 58.11 69.48 22.75 o 2 14 0 471.67 455.84 29.85 o 3 14 0 88.57 80.20 13.45 o 4 14 0 520.21 507.28 56.09 o 5 14 0 20.40 45.14 15.00 o 6 14 0 2.31 11.08 23.58 o 7 14 0 1415.91 1531.46 124.82 o 8 14 0 224.50 224.71 32.07 o 9 14 0 88.29 97.29 39.28 o 10 14 0 0.06 27.87 49.86 o 1 15 0 189.01 207.27 35.66 o 2 15 0 47.30 77.67 34.13 o 3 15 0 66.76 131.67 27.74 o 4 15 0 309.27 360.54 70.06 o 5 15 0 0.72 29.22 33.26 o 6 15 0 663.91 735.45 166.93 o 7 15 0 101.95 120.62 32.18 o 8 15 0 18.20 -22.27 46.41 o 9 15 0 0.74 61.32 46.36 o 0 16 0 46.41 0.00 55.55 o 1 16 0 81.64 83.66 21.07 o 2 16 0 234.09 270.40 37.85 o 3 16 0 0.17 0.00 19.60 o 4 16 0 11.27 7.94 24.05 o 5 16 0 1071.92 1166.66 96.88 o 6 16 0 388.98 355.42 70.55 o 7 16 0 0.01 27.91 55.83 o 8 16 0 9.28 -39.48 39.48 o 9 16 0 271.98 280.80 84.30 o 1 17 0 138.72 202.93 28.30 o 2 17 0 35.86 52.97 29.93 o 3 17 0 84.00 62.62 27.84 o 4 17 0 26.96 69.37 39.28 o 5 17 0 355.82 473.03 59.02 o 6 17 0 2.68 22.33 46.45 o 7 17 0 0.02 67.19 46.61 o 8 17 0 115.68 102.58 69.37 o 0 18 0 113.38 224.14 84.02 o 1 18 0 0.27 37.33 32.29 o 2 18 0 45.65 76.73 27.91 o 3 18 0 131.71 148.72 32.18 o 4 18 0 4.34 0.00 55.55 o 5 18 0 24.17 14.03 59.31 o 6 18 0 3.41 -27.91 46.61 o 1 19 0 0.35 74.62 32.39 o 2 19 0 136.59 147.85 40.68 o 3 19 0 2.11 33.59 46.55 o 4 19 0 338.31 429.37 87.45 o 5 19 0 1.71 -16.77 46.50 o 0 20 0 28.15 70.34 59.61 o 1 20 0 61.43 112.35 84.02 o 2 20 0 59.97 112.21 59.51 o -14 1 1 339.58 424.61 97.56 o -13 1 1 93.84 63.51 41.22 o -12 1 1 941.29 965.78 55.48 o -11 1 1 9.73 -4.64 22.72 o -10 1 1 1898.58 2061.89 66.02 o -9 1 1 1766.49 1853.23 53.05 o -8 1 1 227.10 229.20 17.75 o -7 1 1 287.90 219.22 19.29 o -6 1 1 27.84 -5.53 14.37 o -5 1 1 26000.72 26785.04 725.21 o -4 1 1 44.30 55.18 15.96 o -3 1 1 1483.50 1535.99 38.25 o -2 1 1 485.04 510.86 12.22 o 2 1 1 97.55 111.38 27.91 o 3 1 1 35408.08 32269.16 740.40 o 4 1 1 4953.11 5110.15 136.89 o 5 1 1 1095.40 1133.56 26.20 o 6 1 1 163.07 161.08 12.36 o 7 1 1 6.69 22.10 12.38 o 8 1 1 1910.04 1926.63 58.08 o 9 1 1 727.59 729.56 36.30 o 10 1 1 22.90 10.04 12.11 o 11 1 1 56.43 38.77 24.77 o 12 1 1 744.56 623.87 47.10 o 13 1 1 27.34 13.82 39.28 o 14 1 1 173.52 138.47 58.82 o -14 2 1 338.34 353.99 83.88 o -13 2 1 105.51 79.86 40.13 o -12 2 1 828.75 825.90 88.12 o -11 2 1 4.47 27.71 27.74 o -10 2 1 3515.19 3889.88 118.88 o -9 2 1 859.22 898.08 30.86 o -8 2 1 1091.29 1077.32 37.15 o -7 2 1 151.60 117.19 12.36 o -6 2 1 65.99 60.80 12.36 o -5 2 1 377.38 415.13 13.82 o -4 2 1 310.59 303.05 13.67 o -3 2 1 4.51 0.00 27.64 o -2 2 1 47747.77 45463.52 1180.05 o 1 2 1 2134.96 1998.15 53.17 o 2 2 1 1633.41 1634.92 36.88 o 3 2 1 8442.10 8206.90 186.79 o 4 2 1 2301.86 2584.08 69.68 o 5 2 1 540.45 651.75 19.53 o 6 2 1 1023.35 1113.27 30.79 o 7 2 1 100.47 98.68 13.85 o 8 2 1 278.64 241.23 13.44 o 9 2 1 5548.43 5878.95 178.00 o 10 2 1 198.13 214.37 22.60 o 11 2 1 643.43 736.47 34.52 o 12 2 1 1.84 5.53 21.04 o 13 2 1 850.54 777.16 72.76 o 14 2 1 126.39 221.93 83.19 o -14 3 1 525.69 549.58 78.56 o -13 3 1 121.16 65.84 35.45 o -12 3 1 116.97 101.80 32.07 o -11 3 1 135.33 117.87 27.67 o -10 3 1 438.39 421.92 23.73 o -9 3 1 402.43 486.38 24.77 o -8 3 1 0.85 16.58 12.36 o -7 3 1 15.88 20.73 13.82 o -6 3 1 15.22 22.11 12.36 o -5 3 1 1015.31 865.20 22.62 o -4 3 1 20.58 36.88 16.01 o -3 3 1 1651.22 1895.70 46.87 o -2 3 1 999.06 953.10 84.02 o -1 3 1 4531.96 4051.48 106.32 o 0 3 1 5814.77 4823.88 132.31 o 1 3 1 1085.02 771.98 21.10 o 2 3 1 12523.02 11280.02 256.20 o 3 3 1 14.95 55.55 27.64 o 4 3 1 41.49 27.78 19.64 o 5 3 1 5247.16 5884.11 160.66 o 6 3 1 532.51 604.74 19.23 o 7 3 1 466.66 362.18 24.83 o 8 3 1 1501.31 1369.60 47.02 o 9 3 1 1224.40 1263.39 47.02 o 10 3 1 510.85 538.65 26.29 o 11 3 1 386.43 360.80 27.59 o 12 3 1 112.08 146.19 29.84 o 13 3 1 8.07 17.41 35.47 o 14 3 1 28.39 5.57 46.04 o -14 4 1 331.64 394.29 66.51 o -13 4 1 513.53 572.24 66.51 o -12 4 1 2.99 35.27 29.84 o -11 4 1 519.69 419.94 32.57 o -10 4 1 1009.39 862.44 40.90 o -9 4 1 5.03 22.11 18.43 o -8 4 1 489.68 549.50 43.41 o -7 4 1 8.10 11.11 12.36 o -6 4 1 232.00 269.45 11.28 o -5 4 1 677.81 684.53 30.33 o -4 4 1 2149.22 1928.38 49.75 o -3 4 1 22.78 -13.96 19.74 o -2 4 1 13521.29 12892.19 295.93 o -1 4 1 6410.14 5694.11 174.21 o 1 4 1 703.48 643.91 40.03 o 2 4 1 32303.08 28134.31 860.61 o 3 4 1 2485.10 2122.32 50.84 o 4 4 1 3266.17 3139.38 85.96 o 5 4 1 263.34 231.72 11.78 o 6 4 1 11.61 22.15 12.38 o 7 4 1 2333.43 2149.64 60.49 o 8 4 1 877.89 889.23 54.52 o 9 4 1 2644.79 2863.09 87.07 o 10 4 1 11.53 51.98 14.83 o 11 4 1 722.39 715.01 41.53 o 12 4 1 198.94 224.09 32.82 o 13 4 1 128.81 222.49 83.47 o 14 4 1 0.40 55.41 58.82 o -14 5 1 18.42 -46.16 49.51 o -13 5 1 43.82 0.00 46.09 o -12 5 1 393.64 370.87 42.55 o -11 5 1 159.56 136.43 41.18 o -10 5 1 71.66 31.23 24.57 o -9 5 1 1534.09 1459.35 59.38 o -8 5 1 511.12 418.68 19.54 o -7 5 1 296.54 316.05 14.46 o -6 5 1 822.69 760.22 26.21 o -5 5 1 16725.92 18567.76 445.03 o -4 5 1 46.16 48.61 13.89 o -3 5 1 872.78 714.71 19.82 o -2 5 1 148.72 143.26 12.46 o -1 5 1 49531.36 44994.93 1168.93 o 0 5 1 12170.26 11702.02 414.85 o 1 5 1 4865.80 4641.68 130.80 o 2 5 1 425.23 401.66 12.48 o 3 5 1 791.64 751.07 24.82 o 4 5 1 2030.29 2053.67 49.29 o 5 5 1 142.61 130.90 11.30 o 6 5 1 1.11 0.00 11.30 o 7 5 1 232.24 248.26 13.44 o 8 5 1 123.20 106.55 13.44 o 9 5 1 121.67 106.55 13.44 o 10 5 1 450.91 382.42 76.19 o 11 5 1 896.38 909.24 84.09 o 12 5 1 161.24 181.08 39.18 o 13 5 1 70.25 124.78 58.82 o 14 5 1 24.55 38.76 46.09 o -14 6 1 55.28 110.91 66.51 o -13 6 1 114.77 124.61 39.18 o -12 6 1 397.75 295.55 45.93 o -11 6 1 125.80 155.00 36.53 o -10 6 1 467.94 417.66 35.46 o -9 6 1 1715.08 1697.92 55.37 o -8 6 1 1447.14 1606.67 53.48 o -7 6 1 110.40 111.38 12.06 o -6 6 1 1714.99 1661.14 55.57 o -5 6 1 3865.83 4186.69 103.79 o -4 6 1 442.92 372.45 20.97 o -3 6 1 17.33 18.55 16.06 o -2 6 1 3339.50 3195.41 75.31 o -1 6 1 2686.70 2737.11 77.88 o 0 6 1 151.17 111.59 13.96 o 1 6 1 33.97 62.81 13.96 o 2 6 1 312.99 350.45 15.92 o 3 6 1 1345.47 1128.68 36.40 o 4 6 1 2329.34 2176.25 57.84 o 5 6 1 0.32 22.17 12.36 o 6 6 1 104.75 109.46 12.46 o 7 6 1 1201.26 1251.82 36.73 o 8 6 1 342.79 278.66 19.27 o 9 6 1 3.47 3.07 16.89 o 10 6 1 225.83 259.84 27.64 o 11 6 1 4468.37 4598.92 184.93 o 12 6 1 45.60 0.00 83.47 o 13 6 1 5.33 55.55 83.47 o 14 6 1 46.89 -41.55 58.82 o -13 7 1 263.03 310.71 46.09 o -12 7 1 652.82 722.12 79.87 o -11 7 1 48.16 0.00 45.67 o -10 7 1 891.12 848.48 50.74 o -9 7 1 211.95 206.55 27.64 o -8 7 1 0.13 -3.07 13.41 o -7 7 1 381.47 418.20 22.62 o -6 7 1 1581.45 1709.63 57.60 o -5 7 1 389.90 373.15 15.58 o -4 7 1 17.73 11.91 20.07 o -3 7 1 4003.43 4214.48 129.28 o -2 7 1 7496.50 7535.82 201.09 o -1 7 1 9910.23 8905.10 254.75 o 0 7 1 2825.43 2735.64 93.97 o 1 7 1 311.96 280.16 13.96 o 2 7 1 829.96 859.14 27.85 o 3 7 1 2190.28 1957.36 55.26 o 4 7 1 0.22 0.00 19.64 o 5 7 1 642.07 709.20 28.68 o 6 7 1 389.45 310.03 14.78 o 7 7 1 15.79 27.59 11.28 o 8 7 1 296.82 290.65 35.87 o 9 7 1 317.06 317.24 17.11 o 10 7 1 278.25 265.04 27.64 o 11 7 1 420.37 445.54 58.82 o 12 7 1 1253.20 1288.54 97.91 o 13 7 1 1.33 66.51 46.09 o -13 8 1 111.31 171.50 46.09 o -12 8 1 55.77 0.00 138.19 o -11 8 1 299.86 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