#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:00:30 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180940 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/20/2202087.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202087_Fobs loop_ _publ_author_name 'Qin, Yong-Hai' 'Wu, Mei-Mei' 'Chen, Zhong-Ning' _publ_section_title ; Tris[\m-bis(diphenylphosphino)methane-\k^2^P:P']di-\m~3~-sulfanido-trisilver(I) hexafluoroantimonate dichloromethane disolvate ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m317 _journal_page_last m318 _journal_volume 59 _journal_year 2003 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.417 _cell_angle_gamma 90.000 _cell_length_a 16.0813 _cell_length_b 18.0049 _cell_length_c 28.1089 _exptl_crystal_F_000 3880.00 _reflns_d_resolution_high 0.8398 _cod_data_source_file na6228Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' q in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 780.16 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 46988.17 67561.78 1703.80 o 4 0 0 204411.23 195100.36 4905.67 o 6 0 0 11262.75 9980.64 295.71 o 8 0 0 166668.08 169978.50 4305.71 o 10 0 0 55998.96 59130.99 1551.77 o 12 0 0 552.01 864.11 150.47 o 14 0 0 3393.86 3262.72 235.55 o 16 0 0 828.46 743.80 186.21 o 18 0 0 93.07 -189.00 189.00 o 1 1 0 43961.05 23408.38 4030.77 o 2 1 0 25689.52 25955.45 523.52 o 3 1 0 5973.70 3323.80 472.22 o 4 1 0 4120.28 4063.91 187.51 o 5 1 0 1021.23 1063.84 36.64 o 6 1 0 7278.19 6244.78 143.50 o 7 1 0 446.60 1096.00 294.99 o 8 1 0 61133.68 62302.33 1142.68 o 9 1 0 173.08 -133.47 133.47 o 10 1 0 4076.57 4239.26 157.62 o 11 1 0 21.22 -86.22 86.22 o 12 1 0 14899.74 13905.03 494.39 o 13 1 0 1117.56 1183.38 202.34 o 14 1 0 93.26 -182.64 182.64 o 15 1 0 267.66 -77.10 100.89 o 16 1 0 950.26 1107.16 202.43 o 17 1 0 333.51 125.10 130.75 o 18 1 0 606.85 312.04 522.11 o 0 2 0 608655.56 563751.63 9974.25 o 1 2 0 46715.47 50638.45 657.87 o 2 2 0 50229.15 53102.96 741.47 o 3 2 0 3516.42 2747.35 66.27 o 4 2 0 17.42 57.56 74.45 o 5 2 0 14961.60 13899.55 231.25 o 6 2 0 34598.66 41824.13 4021.38 o 7 2 0 8068.84 9089.67 159.95 o 8 2 0 54789.20 57037.09 2953.34 o 9 2 0 36784.77 39104.55 1300.13 o 10 2 0 44829.91 45433.44 951.55 o 11 2 0 2017.62 2015.39 115.06 o 12 2 0 3350.71 3274.34 255.78 o 13 2 0 77.21 -18.22 188.74 o 14 2 0 2771.73 2660.14 206.96 o 15 2 0 248.36 -86.04 86.04 o 16 2 0 4275.90 3580.85 349.58 o 17 2 0 719.86 837.84 313.14 o 18 2 0 137.52 -118.38 289.95 o 1 3 0 103197.74 105249.72 1323.73 o 2 3 0 22518.93 27573.23 1231.96 o 3 3 0 37728.14 36060.58 543.49 o 4 3 0 2198.40 1537.22 76.03 o 5 3 0 3433.16 3977.23 174.50 o 6 3 0 1400.85 830.69 125.55 o 7 3 0 44494.00 45459.44 1588.27 o 8 3 0 5546.86 5939.02 242.07 o 9 3 0 12082.16 12413.48 327.63 o 10 3 0 1826.38 2390.23 297.28 o 11 3 0 4759.98 4725.69 383.32 o 12 3 0 5572.19 4121.95 222.74 o 13 3 0 7122.29 7667.29 260.66 o 14 3 0 3.65 8.83 263.02 o 15 3 0 1041.38 505.65 207.05 o 16 3 0 20.69 -152.30 386.55 o 17 3 0 4154.03 4240.06 207.74 o 18 3 0 110.11 -655.21 772.05 o 0 4 0 51984.98 48442.88 871.09 o 1 4 0 10095.39 8403.12 221.49 o 2 4 0 19153.81 17582.90 575.47 o 3 4 0 38554.66 47874.35 1631.02 o 4 4 0 4.52 -9.59 24.18 o 5 4 0 65787.14 61179.36 1249.67 o 6 4 0 52449.04 55676.69 2245.81 o 7 4 0 4018.86 3023.08 557.17 o 8 4 0 33570.05 36499.46 729.77 o 9 4 0 64745.14 64199.91 957.80 o 10 4 0 5740.38 5417.72 213.24 o 11 4 0 2269.54 2554.78 127.01 o 12 4 0 123.20 69.55 77.48 o 13 4 0 360.99 61.85 204.78 o 14 4 0 1457.19 1744.94 231.37 o 15 4 0 49.43 -410.10 477.39 o 16 4 0 8022.91 8193.31 520.36 o 17 4 0 3236.59 3394.76 199.48 o 18 4 0 1092.38 361.09 212.02 o 1 5 0 22849.04 20465.69 268.76 o 2 5 0 92177.38 101870.24 1428.25 o 3 5 0 4003.63 4459.23 72.58 o 4 5 0 4917.35 4516.17 77.31 o 5 5 0 544.82 435.73 50.13 o 6 5 0 56.25 288.71 75.54 o 7 5 0 434.72 57.42 73.06 o 8 5 0 22455.74 21444.13 292.58 o 9 5 0 12179.18 12761.84 520.75 o 10 5 0 1201.04 1537.05 184.90 o 11 5 0 996.44 698.56 86.39 o 12 5 0 166.79 430.44 135.82 o 13 5 0 1097.85 904.08 288.38 o 14 5 0 888.63 861.78 115.72 o 15 5 0 69.90 294.55 350.45 o 16 5 0 4.39 263.83 497.00 o 17 5 0 4496.32 4773.34 325.17 o 18 5 0 1405.02 1261.99 226.14 o 0 6 0 38420.43 34976.13 1719.32 o 1 6 0 531.90 959.86 46.88 o 2 6 0 15558.98 18879.57 358.89 o 3 6 0 58383.32 59141.60 756.91 o 4 6 0 19722.12 24553.88 326.07 o 5 6 0 25451.50 25306.42 336.99 o 6 6 0 14400.20 12435.17 317.57 o 7 6 0 4484.71 4272.02 221.65 o 8 6 0 9394.53 10408.77 163.73 o 9 6 0 27714.97 27737.60 428.61 o 10 6 0 6389.19 6075.98 261.36 o 11 6 0 12716.34 13157.91 1038.90 o 12 6 0 4868.36 4749.22 166.48 o 13 6 0 5609.79 5469.51 266.76 o 14 6 0 88.49 318.01 108.94 o 15 6 0 517.96 232.07 169.30 o 16 6 0 5440.27 5638.84 319.59 o 17 6 0 2967.12 3146.77 270.25 o 18 6 0 1265.33 206.61 197.54 o 1 7 0 447.02 631.13 75.22 o 2 7 0 88096.96 85285.70 1084.92 o 3 7 0 1729.91 1488.53 85.54 o 4 7 0 180.69 227.57 31.14 o 5 7 0 556.95 476.39 53.67 o 6 7 0 279.22 78.61 65.71 o 7 7 0 204.83 426.94 132.54 o 8 7 0 40872.44 38897.29 559.87 o 9 7 0 339.50 503.85 43.57 o 10 7 0 338.05 420.26 66.12 o 11 7 0 1060.76 824.27 259.96 o 12 7 0 2293.65 2215.69 125.22 o 13 7 0 167.36 479.48 159.71 o 14 7 0 4066.52 4063.36 266.24 o 15 7 0 8.24 -116.99 116.99 o 16 7 0 60.69 -140.18 140.18 o 17 7 0 60.37 -165.46 165.46 o 0 8 0 105433.63 115065.38 3067.70 o 1 8 0 51853.15 54335.87 701.24 o 2 8 0 12394.39 12496.94 180.16 o 3 8 0 126436.09 126700.28 1606.78 o 4 8 0 2670.88 1995.71 79.79 o 5 8 0 20653.99 20209.68 357.79 o 6 8 0 340.44 48.31 82.60 o 7 8 0 23439.28 26585.62 2238.76 o 8 8 0 3842.75 3163.53 76.19 o 9 8 0 4482.42 4765.05 139.52 o 10 8 0 828.02 956.42 295.79 o 11 8 0 20880.55 21440.69 667.78 o 12 8 0 1013.75 424.38 149.60 o 13 8 0 11749.05 10580.95 418.80 o 14 8 0 296.92 -125.36 125.36 o 15 8 0 495.83 138.61 169.47 o 16 8 0 2044.68 1946.16 239.04 o 17 8 0 661.58 972.38 224.74 o 1 9 0 32236.29 31438.83 418.45 o 2 9 0 7076.51 6576.40 146.69 o 3 9 0 3470.46 3630.91 151.60 o 4 9 0 1654.51 1554.00 49.99 o 5 9 0 3485.48 3200.31 89.39 o 6 9 0 240.92 198.51 65.71 o 7 9 0 6195.00 6356.25 239.18 o 8 9 0 21291.56 20219.40 416.37 o 9 9 0 5033.27 4386.58 118.87 o 10 9 0 1666.93 1396.67 468.67 o 11 9 0 7493.69 8430.10 368.94 o 12 9 0 762.37 790.18 189.52 o 13 9 0 417.85 -150.29 153.78 o 14 9 0 609.56 101.30 150.47 o 15 9 0 11.80 -129.20 129.20 o 16 9 0 34.52 -144.19 144.19 o 17 9 0 1032.68 885.03 231.37 o 0 10 0 7793.12 8709.64 197.30 o 1 10 0 55109.52 55198.87 718.10 o 2 10 0 1279.49 1672.81 108.04 o 3 10 0 80772.78 82788.90 1287.30 o 4 10 0 251.08 370.54 56.08 o 5 10 0 9572.04 11104.53 171.27 o 6 10 0 6207.51 6368.85 115.58 o 7 10 0 22490.94 23042.78 382.26 o 8 10 0 6.62 125.56 175.53 o 9 10 0 1647.19 1598.51 162.65 o 10 10 0 530.22 613.44 352.20 o 11 10 0 9830.32 9601.59 396.14 o 12 10 0 1025.55 671.44 168.95 o 13 10 0 6915.85 7420.58 358.13 o 14 10 0 562.20 208.36 174.88 o 15 10 0 30.50 182.90 168.78 o 16 10 0 157.08 -162.85 162.85 o 1 11 0 34256.59 37043.05 494.97 o 2 11 0 2140.71 2024.83 123.49 o 3 11 0 431.94 572.83 162.44 o 4 11 0 6046.36 7190.97 154.21 o 5 11 0 339.04 343.31 53.11 o 6 11 0 259.03 578.18 63.00 o 7 11 0 15036.67 13828.69 878.39 o 8 11 0 689.62 585.09 90.51 o 9 11 0 1936.71 1706.26 141.95 o 10 11 0 844.02 1254.58 281.67 o 11 11 0 2092.18 1547.58 191.09 o 12 11 0 8.65 -90.14 90.14 o 13 11 0 95.06 -101.13 101.13 o 14 11 0 86.40 -153.08 153.08 o 15 11 0 1.78 13.25 164.94 o 16 11 0 67.45 -160.06 160.06 o 0 12 0 3196.08 4172.82 129.22 o 1 12 0 19000.48 21550.88 306.26 o 2 12 0 92.82 -35.13 48.59 o 3 12 0 12193.41 14161.50 258.44 o 4 12 0 3.42 50.34 52.89 o 5 12 0 3524.70 3883.48 211.54 o 6 12 0 14234.30 14921.69 273.69 o 7 12 0 6485.48 6175.03 1190.77 o 8 12 0 6035.54 6025.93 179.60 o 9 12 0 1195.52 1240.80 203.65 o 10 12 0 319.52 636.05 108.38 o 11 12 0 2434.35 2384.49 216.38 o 12 12 0 2990.28 2399.13 220.73 o 13 12 0 3930.64 4715.97 316.63 o 14 12 0 1033.08 710.85 199.29 o 15 12 0 2.80 -142.45 142.45 o 1 13 0 191.05 348.66 79.45 o 2 13 0 26125.54 29260.67 655.62 o 3 13 0 177.76 192.93 87.31 o 4 13 0 168.72 37.25 92.29 o 5 13 0 5358.52 5310.92 154.20 o 6 13 0 44.02 210.17 70.71 o 7 13 0 1222.76 1122.23 358.91 o 8 13 0 5685.76 4553.51 142.44 o 9 13 0 5.55 229.92 116.82 o 10 13 0 559.23 648.63 298.93 o 11 13 0 106.49 223.70 146.28 o 12 13 0 77.03 -129.89 129.89 o 13 13 0 25.65 -30.16 152.74 o 14 13 0 51.50 68.70 156.57 o 15 13 0 0.17 -26.15 168.08 o 0 14 0 3761.37 4862.43 234.86 o 1 14 0 22.07 -20.47 68.11 o 2 14 0 467.12 545.23 229.56 o 3 14 0 1951.03 3190.55 178.81 o 4 14 0 881.38 1086.58 169.48 o 5 14 0 1554.51 1461.19 181.01 o 6 14 0 6499.17 5443.12 153.21 o 7 14 0 211.13 333.16 274.27 o 8 14 0 4938.54 5435.27 410.37 o 9 14 0 191.79 270.56 181.88 o 10 14 0 1586.03 1657.60 213.24 o 11 14 0 102.63 208.53 156.75 o 12 14 0 1836.53 1328.07 231.20 o 13 14 0 1314.94 1299.65 236.43 o 14 14 0 204.30 419.85 183.25 o 1 15 0 15116.47 16977.03 386.51 o 2 15 0 134.58 -98.04 126.76 o 3 15 0 1268.87 1294.58 187.00 o 4 15 0 346.45 414.96 87.97 o 5 15 0 897.53 749.20 239.83 o 6 15 0 639.64 862.37 218.26 o 7 15 0 222.28 322.35 94.93 o 8 15 0 1111.12 1913.38 478.93 o 9 15 0 2165.39 2431.38 129.93 o 10 15 0 0.38 105.31 181.33 o 11 15 0 981.49 638.14 210.80 o 12 15 0 442.54 140.88 195.45 o 13 15 0 150.48 -156.22 156.22 o 0 16 0 822.28 791.57 145.41 o 1 16 0 1055.66 1555.58 127.72 o 2 16 0 2915.49 3290.84 352.46 o 3 16 0 1659.43 1633.32 130.26 o 4 16 0 0.93 -78.76 78.76 o 5 16 0 1127.70 1560.54 356.30 o 6 16 0 851.44 1349.22 228.63 o 7 16 0 156.56 681.44 179.85 o 8 16 0 2094.84 2639.96 416.02 o 9 16 0 1774.79 2158.10 283.95 o 10 16 0 114.78 663.95 209.92 o 11 16 0 218.03 27.37 172.96 o 12 16 0 701.04 1225.55 232.59 o 1 17 0 2460.77 2409.64 152.94 o 2 17 0 0.37 -136.01 190.66 o 3 17 0 671.52 536.12 126.67 o 4 17 0 310.40 441.19 213.06 o 5 17 0 6.59 87.13 112.32 o 6 17 0 0.65 329.29 145.33 o 7 17 0 564.41 991.53 148.22 o 8 17 0 2.03 380.56 358.21 o 9 17 0 3847.39 4158.87 293.83 o 10 17 0 335.34 663.77 229.28 o 11 17 0 3050.11 3928.93 362.31 o 0 18 0 6036.40 6703.10 343.83 o 1 18 0 1195.95 1426.83 193.71 o 2 18 0 127.50 171.11 285.77 o 3 18 0 1629.84 2776.88 177.64 o 4 18 0 689.48 1466.19 345.66 o 5 18 0 9.91 766.92 156.84 o 6 18 0 110.94 608.92 479.91 o 7 18 0 24.36 390.19 176.10 o 8 18 0 1818.50 2107.91 210.80 o 9 18 0 207.70 1396.34 597.43 o 1 19 0 1132.30 1892.90 163.00 o 2 19 0 1436.45 1768.71 162.72 o 3 19 0 193.04 608.00 393.08 o 4 19 0 16.60 681.88 510.60 o 5 19 0 235.74 866.17 426.39 o 6 19 0 418.51 1302.39 178.32 o 7 19 0 350.45 1341.67 461.52 o 8 19 0 481.77 1151.88 184.57 o 0 20 0 3342.94 3410.92 298.32 o 1 20 0 184.91 752.01 559.59 o 2 20 0 6.76 553.27 552.45 o 3 20 0 126.59 1175.91 523.68 o 4 20 0 55.59 683.46 333.37 o 5 20 0 760.07 1889.67 219.64 o 6 20 0 136.00 1229.28 217.15 o 1 21 0 3.96 1307.28 350.11 o 2 21 0 451.18 1650.37 436.06 o 3 21 0 528.29 1625.55 214.34 o -19 0 1 1052.27 425.25 199.64 o -17 0 1 656.90 1127.73 208.53 o -15 0 1 12486.45 11848.52 436.94 o -13 0 1 15079.90 13188.44 438.50 o -11 0 1 454.19 237.65 107.75 o -9 0 1 60785.18 55010.09 1440.35 o -7 0 1 67.15 252.29 77.94 o -5 0 1 102298.49 99541.93 2523.62 o -3 0 1 15669.19 12983.22 348.19 o -1 0 1 54789.05 2909.47 81.77 o 1 0 1 257.66 90.32 12.20 o 3 0 1 88215.86 84160.45 2126.62 o 5 0 1 341.01 209.58 42.19 o 7 0 1 48355.60 48336.63 1257.98 o 9 0 1 146045.72 154634.67 3934.51 o 11 0 1 9412.76 8835.82 312.79 o 13 0 1 9197.50 10331.62 374.34 o 15 0 1 633.96 -117.52 127.98 o 17 0 1 3539.57 3637.23 270.77 o -19 1 1 279.62 135.47 128.11 o -18 1 1 476.07 326.92 225.70 o -17 1 1 3390.27 2786.27 244.80 o -16 1 1 725.42 617.67 162.15 o -15 1 1 1283.19 1564.73 143.44 o -14 1 1 2083.20 1966.56 180.46 o -13 1 1 330.97 227.47 153.52 o -12 1 1 149.32 262.75 95.70 o -11 1 1 3895.59 3883.09 147.36 o -10 1 1 4134.10 3251.45 204.78 o -9 1 1 13271.39 12801.19 279.26 o -8 1 1 31010.70 28229.26 431.30 o -7 1 1 7671.85 6689.90 159.11 o -6 1 1 1.37 23.71 36.25 o -5 1 1 6747.42 7534.09 163.11 o -4 1 1 27506.48 25267.04 702.48 o -3 1 1 7064.97 9291.95 180.90 o -2 1 1 4.05 1034.59 172.44 o -1 1 1 117505.14 69190.80 8692.63 o 0 1 1 13319.30 3781.54 1480.01 o 1 1 1 213281.66 196810.42 2845.23 o 2 1 1 14865.90 14616.08 597.53 o 3 1 1 12417.27 14966.46 668.23 o 4 1 1 29376.12 22070.46 2734.04 o 5 1 1 2554.96 1759.17 256.25 o 6 1 1 1002.60 1389.94 169.21 o 7 1 1 5108.72 4935.29 146.98 o 8 1 1 3.95 90.74 299.98 o 9 1 1 88429.84 83249.76 1516.93 o 10 1 1 1690.37 1629.60 94.82 o 11 1 1 20187.07 19599.66 409.59 o 12 1 1 943.22 808.27 98.59 o 13 1 1 2188.57 1707.07 125.26 o 14 1 1 29.61 -41.48 119.08 o 15 1 1 3197.74 2924.25 166.25 o 16 1 1 183.98 314.02 211.32 o 17 1 1 1271.81 1376.07 300.85 o 18 1 1 227.90 670.28 190.66 o -18 2 1 101.60 -168.78 168.78 o -17 2 1 35.01 87.43 377.04 o -16 2 1 3410.03 3829.19 269.12 o -15 2 1 7869.77 7650.58 247.90 o -14 2 1 121.02 271.69 114.41 o -13 2 1 4651.35 4922.89 219.95 o -12 2 1 594.61 631.33 149.25 o -11 2 1 5559.44 5490.63 166.94 o -10 2 1 24130.23 22796.81 619.05 o -9 2 1 12026.32 8592.64 1345.47 o -8 2 1 6851.10 7689.53 325.42 o -7 2 1 9353.20 8478.49 590.44 o -6 2 1 39473.15 37954.31 1761.69 o -5 2 1 29460.37 29033.74 539.55 o -4 2 1 104.06 318.42 41.95 o -3 2 1 87.74 108.61 18.54 o -2 2 1 20905.76 25870.25 412.72 o -1 2 1 10958.35 12820.17 611.38 o 0 2 1 200185.69 196438.83 2840.60 o 1 2 1 34234.78 33783.79 494.57 o 2 2 1 851.41 533.22 32.14 o 3 2 1 104139.57 114015.95 1434.17 o 4 2 1 10158.46 12965.98 350.89 o 5 2 1 2112.55 3715.99 130.84 o 6 2 1 1526.83 1667.35 71.87 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