#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2202122.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202122_Fobs loop_ _publ_author_name 'Zhou, Jian-Liang' 'Li, Yi-Zhi' 'Zheng, He-Gen' 'Xin, Xin-Quan' 'Xu, Lin-Lin' _publ_section_title ; Di-\m~3~-bromo-dibromotetrakis[\m-diphenyl(2-pyridyl)phosphine)]tetracopper(I) dichloromethane hexasolvate ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m176 _journal_page_last m178 _journal_volume 59 _journal_year 2003 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 104.850 _cell_angle_gamma 90.000 _cell_length_a 13.8180 _cell_length_b 17.7930 _cell_length_c 19.2920 _exptl_crystal_F_000 2120.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file ob6225Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' OB1113 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 424.06 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 33205.09 31735.88 56.74 o 3 0 0 427.30 402.36 4.36 o 4 0 0 53988.90 51661.20 94.87 o 5 0 0 20781.74 21429.24 78.00 o 6 0 0 50820.57 48206.46 54.97 o 7 0 0 40759.93 39461.25 49.45 o 8 0 0 2810.05 2741.95 10.09 o 9 0 0 4275.15 4060.40 18.98 o 10 0 0 6269.40 6055.77 26.66 o 11 0 0 11518.27 11289.63 29.04 o 12 0 0 701.99 763.58 25.50 o 13 0 0 453.27 475.41 30.63 o 14 0 0 0.28 1.26 31.89 o 15 0 0 34.17 38.18 33.99 o 1 1 0 1598.58 1696.44 9.65 o 2 1 0 266.25 395.51 5.68 o 3 1 0 60116.14 57509.88 53.50 o 4 1 0 48.34 79.83 4.82 o 5 1 0 3731.70 3657.98 9.22 o 6 1 0 9265.46 9194.25 15.21 o 7 1 0 12405.38 11911.41 14.49 o 8 1 0 12174.04 11686.07 11.96 o 9 1 0 117.26 218.10 11.06 o 10 1 0 1006.38 944.63 10.56 o 11 1 0 1.08 6.95 11.74 o 12 1 0 34.53 35.13 14.55 o 13 1 0 2.98 2.49 16.02 o 14 1 0 338.09 306.88 17.97 o 15 1 0 74.23 85.63 24.74 o 0 2 0 1647.76 1916.73 13.85 o 1 2 0 2126.22 2348.82 80.98 o 2 2 0 3953.48 3724.60 5.94 o 3 2 0 6650.32 6232.07 26.96 o 4 2 0 5158.36 5263.10 23.62 o 5 2 0 16364.88 16180.89 32.22 o 6 2 0 45263.70 42942.02 25.74 o 7 2 0 10459.57 10361.25 21.78 o 8 2 0 6026.96 5993.87 17.73 o 9 2 0 178.78 192.89 10.09 o 10 2 0 428.58 415.60 10.18 o 11 2 0 412.05 433.06 12.53 o 12 2 0 2350.90 2281.32 17.86 o 13 2 0 1191.71 1162.43 18.33 o 14 2 0 6.17 17.08 17.79 o 15 2 0 1.55 0.00 18.72 o 1 3 0 325.30 389.86 14.92 o 2 3 0 341.78 353.86 5.48 o 3 3 0 679.40 641.77 4.17 o 4 3 0 121.31 165.16 6.81 o 5 3 0 9776.28 8824.37 5.80 o 6 3 0 1024.28 972.28 5.47 o 7 3 0 90.58 94.91 7.26 o 8 3 0 1205.11 1245.65 11.23 o 9 3 0 213.87 222.95 9.57 o 10 3 0 47.39 57.34 9.99 o 11 3 0 5.05 10.26 11.52 o 12 3 0 7.95 1.02 15.07 o 13 3 0 225.99 246.46 16.57 o 14 3 0 41.54 38.06 17.69 o 15 3 0 20.31 14.61 19.55 o 0 4 0 74731.59 72460.64 60.42 o 1 4 0 7064.65 7312.12 59.20 o 2 4 0 4223.96 4073.76 26.64 o 3 4 0 4885.71 4297.53 5.46 o 4 4 0 16465.33 15575.46 25.26 o 5 4 0 1822.90 1712.09 5.72 o 6 4 0 64.63 277.55 11.51 o 7 4 0 2898.07 2742.15 29.29 o 8 4 0 5137.03 4644.69 19.94 o 9 4 0 365.19 338.90 9.54 o 10 4 0 66.52 71.08 10.17 o 11 4 0 30.10 33.93 11.44 o 12 4 0 5.95 7.75 14.90 o 13 4 0 440.86 440.23 17.02 o 14 4 0 71.44 79.76 18.54 o 15 4 0 135.58 127.57 24.47 o 1 5 0 1939.33 1838.00 4.98 o 2 5 0 2437.11 2189.70 5.80 o 3 5 0 8361.36 8075.25 17.32 o 4 5 0 499.43 483.96 8.48 o 5 5 0 3090.10 3087.01 6.06 o 6 5 0 166.03 184.38 6.90 o 7 5 0 269.12 310.19 8.24 o 8 5 0 1582.79 1482.73 11.22 o 9 5 0 7.99 35.81 9.65 o 10 5 0 1706.11 1644.77 8.98 o 11 5 0 0.56 18.37 11.52 o 12 5 0 11.48 17.01 15.71 o 13 5 0 1.59 13.27 24.47 o 14 5 0 66.44 55.73 24.60 o 15 5 0 77.97 73.43 26.96 o 0 6 0 13025.61 12082.37 6.38 o 1 6 0 16951.32 16010.31 28.47 o 2 6 0 8.78 0.32 6.02 o 3 6 0 6566.79 6457.57 53.71 o 4 6 0 1081.10 1153.71 10.72 o 5 6 0 7904.24 7571.72 22.95 o 6 6 0 2268.85 2250.22 23.14 o 7 6 0 3636.76 3521.39 25.86 o 8 6 0 7719.83 7521.47 10.26 o 9 6 0 778.25 645.20 9.19 o 10 6 0 25.43 63.79 11.42 o 11 6 0 14.24 31.50 15.22 o 12 6 0 1539.79 1546.76 21.79 o 13 6 0 148.17 131.69 22.99 o 14 6 0 599.14 563.15 27.74 o 15 6 0 5.02 0.00 25.66 o 1 7 0 101.95 374.05 21.42 o 2 7 0 5195.11 4837.84 23.37 o 3 7 0 14953.96 15100.79 128.51 o 4 7 0 9885.55 10464.38 87.93 o 5 7 0 13127.13 13037.96 34.52 o 6 7 0 893.38 1021.45 10.40 o 7 7 0 8211.19 7768.76 7.99 o 8 7 0 624.48 592.59 8.50 o 9 7 0 1715.72 1697.31 14.06 o 10 7 0 2124.07 2128.36 20.22 o 11 7 0 3455.29 3205.01 24.77 o 12 7 0 23.61 27.11 21.47 o 13 7 0 1.94 18.34 24.01 o 14 7 0 9.31 17.86 26.16 o 0 8 0 67831.29 67496.16 400.09 o 1 8 0 46780.19 46203.96 267.39 o 2 8 0 3980.69 4682.21 82.51 o 3 8 0 7872.72 7615.23 10.69 o 4 8 0 2028.00 1894.86 11.12 o 5 8 0 5244.11 4924.99 14.13 o 6 8 0 2949.42 2937.02 21.01 o 7 8 0 4991.46 4662.91 12.81 o 8 8 0 2906.76 2721.46 13.06 o 9 8 0 1356.93 1280.99 15.54 o 10 8 0 980.72 1010.37 17.00 o 11 8 0 2040.28 2006.77 24.62 o 12 8 0 789.11 755.03 24.33 o 13 8 0 5.07 4.08 25.95 o 14 8 0 33.44 46.55 25.51 o 1 9 0 1897.15 1987.88 12.75 o 2 9 0 2699.11 3317.90 59.90 o 3 9 0 30114.65 29460.21 126.07 o 4 9 0 8661.04 8477.99 39.86 o 5 9 0 5832.24 5489.55 8.60 o 6 9 0 66.69 221.21 15.87 o 7 9 0 7599.94 7792.98 22.99 o 8 9 0 4709.70 4776.50 22.66 o 9 9 0 2346.57 2298.62 20.51 o 10 9 0 3012.71 2832.98 18.85 o 11 9 0 318.27 332.82 21.79 o 12 9 0 264.93 264.06 23.18 o 13 9 0 42.65 41.58 26.39 o 14 9 0 153.42 165.53 29.37 o 0 10 0 32624.68 31635.51 30.92 o 1 10 0 3031.27 3236.96 19.23 o 2 10 0 241.64 311.60 11.24 o 3 10 0 6416.45 5928.37 10.57 o 4 10 0 7087.80 6818.81 10.79 o 5 10 0 3406.49 3374.29 11.54 o 6 10 0 794.24 828.02 11.21 o 7 10 0 0.69 5.55 12.39 o 8 10 0 2126.24 1979.32 14.76 o 9 10 0 902.70 954.00 19.73 o 10 10 0 2586.03 2622.53 18.91 o 11 10 0 829.72 826.00 22.75 o 12 10 0 225.23 251.14 23.44 o 13 10 0 363.29 366.96 24.77 o 1 11 0 4158.65 3961.95 11.26 o 2 11 0 4815.60 4819.95 17.57 o 3 11 0 8834.50 8446.21 26.98 o 4 11 0 5743.90 5480.56 15.49 o 5 11 0 3.80 7.01 10.52 o 6 11 0 2963.68 2930.91 14.36 o 7 11 0 8063.70 7896.35 16.78 o 8 11 0 1658.97 1618.09 13.36 o 9 11 0 150.59 136.61 16.10 o 10 11 0 114.45 115.04 17.99 o 11 11 0 0.07 0.00 22.97 o 12 11 0 44.41 49.41 25.20 o 13 11 0 1.08 9.99 27.05 o 0 12 0 3222.09 3039.16 28.11 o 1 12 0 2448.49 2274.54 16.90 o 2 12 0 467.58 459.20 10.82 o 3 12 0 2.25 23.93 11.70 o 4 12 0 32.14 37.07 11.72 o 5 12 0 128.27 170.19 13.54 o 6 12 0 1161.44 1250.47 14.67 o 7 12 0 26.12 96.57 14.30 o 8 12 0 829.24 782.22 16.84 o 9 12 0 4431.11 4213.78 15.02 o 10 12 0 138.22 170.64 15.56 o 11 12 0 770.14 709.17 17.31 o 12 12 0 18.39 8.23 24.18 o 13 12 0 131.03 119.61 27.90 o 1 13 0 277.61 250.84 17.04 o 2 13 0 2371.83 2222.74 20.91 o 3 13 0 4483.01 4431.75 18.38 o 4 13 0 2667.55 2661.83 18.67 o 5 13 0 260.22 253.98 14.64 o 6 13 0 108.83 102.76 12.44 o 7 13 0 953.90 788.88 13.15 o 8 13 0 117.73 177.94 13.75 o 9 13 0 1195.31 1226.30 16.50 o 10 13 0 379.12 444.19 20.35 o 11 13 0 107.68 129.35 20.06 o 12 13 0 18.25 17.09 20.21 o 0 14 0 538.00 613.87 31.47 o 1 14 0 3826.62 3691.28 20.47 o 2 14 0 624.96 671.78 19.47 o 3 14 0 228.12 201.97 16.90 o 4 14 0 18.13 28.02 17.20 o 5 14 0 148.16 137.98 14.51 o 6 14 0 1650.94 1788.35 14.39 o 7 14 0 85.69 134.86 14.90 o 8 14 0 9.02 61.16 15.23 o 9 14 0 56.42 98.12 14.25 o 10 14 0 35.87 45.13 18.10 o 11 14 0 27.09 29.38 18.23 o 1 15 0 452.52 463.66 22.10 o 2 15 0 4120.93 4024.07 22.66 o 3 15 0 1554.19 1565.40 25.69 o 4 15 0 1798.07 1769.97 23.12 o 5 15 0 1481.68 1638.33 21.07 o 6 15 0 1616.13 1477.56 19.73 o 7 15 0 179.64 277.95 15.31 o 8 15 0 359.07 454.35 15.85 o 9 15 0 498.17 431.89 16.14 o 10 15 0 11.70 34.40 19.03 o 11 15 0 4.32 0.00 19.60 o 0 16 0 1.64 14.69 28.95 o 1 16 0 105.64 98.78 17.48 o 2 16 0 332.29 353.89 19.34 o 3 16 0 870.89 869.37 21.20 o 4 16 0 233.27 192.72 17.95 o 5 16 0 1010.41 1076.22 20.32 o 6 16 0 69.63 28.74 20.47 o 7 16 0 922.38 791.25 19.53 o 8 16 0 1095.03 1169.70 20.27 o 9 16 0 30.49 38.92 20.13 o 10 16 0 57.91 44.64 19.78 o 1 17 0 2152.70 2125.00 22.53 o 2 17 0 100.33 124.67 23.42 o 3 17 0 1922.86 1857.73 22.96 o 4 17 0 41.66 45.76 22.40 o 5 17 0 127.62 170.84 20.01 o 6 17 0 22.53 21.65 21.50 o 7 17 0 207.28 173.16 19.35 o 8 17 0 291.65 259.02 21.65 o 9 17 0 43.48 62.28 20.55 o 0 18 0 3257.09 3199.03 36.92 o 1 18 0 662.22 713.87 26.82 o 2 18 0 1134.12 1162.30 23.65 o 3 18 0 16.72 29.20 23.14 o 4 18 0 146.56 164.20 23.98 o 5 18 0 743.27 688.69 24.58 o 6 18 0 120.92 115.24 23.39 o 7 18 0 138.63 135.26 21.47 o 8 18 0 613.12 665.11 22.07 o 1 19 0 940.69 956.71 25.79 o 2 19 0 769.45 736.98 26.88 o 3 19 0 1603.56 1525.16 29.37 o 4 19 0 853.12 858.18 28.19 o 5 19 0 239.64 233.69 25.93 o 6 19 0 36.45 47.08 26.28 o 0 20 0 3648.76 3556.95 43.64 o 1 20 0 670.26 702.96 29.39 o 2 20 0 270.37 302.23 27.00 o 3 20 0 20.62 30.61 25.51 o 4 20 0 123.51 134.10 24.55 o 5 20 0 34.60 56.63 26.54 o 1 21 0 38.88 42.87 27.41 o -16 1 1 44.08 43.46 23.43 o -15 1 1 193.92 190.75 22.54 o -14 1 1 1746.61 1760.00 19.22 o -13 1 1 1205.54 1196.73 18.87 o -12 1 1 403.46 432.69 18.17 o -11 1 1 1406.30 1393.50 13.15 o -10 1 1 322.86 336.65 8.95 o -9 1 1 3052.17 2930.22 8.50 o -8 1 1 17693.43 17248.85 19.65 o -7 1 1 19690.18 19315.90 30.09 o -6 1 1 462.01 867.81 11.99 o -5 1 1 1264.90 1171.02 5.16 o -4 1 1 681.99 1054.29 9.62 o -3 1 1 147772.69 143931.42 135.49 o -2 1 1 9985.54 10566.19 49.88 o -1 1 1 55314.46 55474.97 133.85 o 1 1 1 11942.32 11675.22 23.50 o 2 1 1 1375.90 1254.18 1.86 o 3 1 1 16698.74 16528.99 60.30 o 4 1 1 22048.38 21741.71 17.80 o 5 1 1 17411.31 16849.29 17.14 o 6 1 1 926.07 1338.77 14.54 o 7 1 1 11429.97 11074.31 13.89 o 8 1 1 886.45 886.47 7.36 o 9 1 1 337.84 390.10 11.84 o 10 1 1 2264.44 2189.51 13.16 o 11 1 1 2567.00 2513.48 15.03 o 12 1 1 890.97 906.60 18.17 o 13 1 1 153.42 165.69 16.75 o 14 1 1 666.98 656.68 21.31 o 15 1 1 23.69 28.44 24.88 o -15 2 1 10.31 5.46 19.50 o -14 2 1 72.67 75.16 18.21 o -13 2 1 280.13 270.10 15.54 o -12 2 1 14.74 12.04 13.96 o -11 2 1 2790.92 2649.94 17.75 o -10 2 1 3816.05 3665.85 13.14 o -9 2 1 1260.53 1268.77 10.59 o -8 2 1 1036.81 952.47 7.86 o -7 2 1 2554.10 2370.03 9.23 o -6 2 1 1053.17 1113.76 7.25 o -5 2 1 3559.49 3278.63 5.41 o -4 2 1 16372.70 15566.77 39.35 o -3 2 1 3866.02 3749.83 12.09 o -2 2 1 460.12 519.79 4.74 o -1 2 1 546.42 680.24 8.89 o 0 2 1 29200.84 29190.70 39.02 o 1 2 1 41703.00 41770.53 150.01 o 2 2 1 8574.10 8403.22 16.44 o 3 2 1 1661.03 1628.72 12.40 o 4 2 1 17.99 188.61 9.87 o 5 2 1 14015.31 12856.64 7.39 o 6 2 1 683.52 809.76 9.50 o 7 2 1 39.65 43.45 7.57 o 8 2 1 1297.37 1261.92 8.99 o 9 2 1 15.28 9.56 9.28 o 10 2 1 2975.27 2834.24 12.46 o 11 2 1 330.70 355.02 13.36 o 12 2 1 290.38 271.56 12.71 o 13 2 1 406.44 402.70 16.48 o 14 2 1 20.84 28.22 18.40 o 15 2 1 40.77 37.55 23.88 o -15 3 1 18.42 34.22 19.75 o -14 3 1 21.61 22.53 18.05 o -13 3 1 314.05 327.60 16.23 o -12 3 1 38.79 49.82 15.28 o -11 3 1 52.93 64.14 12.99 o -10 3 1 1.91 0.00 9.55 o -9 3 1 288.78 299.09 9.07 o -8 3 1 3144.27 3061.19 9.40 o -7 3 1 1364.10 1526.58 12.24 o -6 3 1 1395.25 2306.41 43.05 o -5 3 1 59453.51 56229.97 83.21 o -4 3 1 4007.47 4841.60 55.96 o -3 3 1 26141.50 24648.91 20.24 o -2 3 1 2033.35 1888.56 6.24 o -1 3 1 788.78 779.48 4.73 o 0 3 1 4357.03 4003.43 2.46 o 1 3 1 15159.27 14784.91 38.81 o 2 3 1 12.77 457.79 22.65 o 3 3 1 29872.05 28559.60 47.30 o 4 3 1 2184.06 2836.46 36.64 o 5 3 1 28082.29 27007.59 24.99 o 6 3 1 1788.83 1746.45 20.99 o 7 3 1 572.27 586.75 7.80 o 8 3 1 6462.16 6217.42 8.90 o 9 3 1 4580.61 4392.36 10.62 o 10 3 1 184.98 185.22 10.89 o 11 3 1 1366.10 1370.79 13.00 o 12 3 1 376.83 389.05 14.97 o 13 3 1 123.83 127.89 17.29 o 14 3 1 122.90 135.95 18.63 o 15 3 1 84.47 76.99 21.10 o -15 4 1 2.30 0.00 26.09 o -14 4 1 15.26 18.27 18.58 o -13 4 1 640.44 592.26 17.27 o -12 4 1 340.64 317.44 15.74 o -11 4 1 2609.42 2529.72 16.40 o -10 4 1 928.15 908.00 11.42 o -9 4 1 12.42 29.63 9.00 o -8 4 1 637.94 589.30 6.20 o -7 4 1 135.45 193.68 16.10 o -6 4 1 16888.14 16023.51 23.74 o -5 4 1 3026.89 2918.88 9.51 o -4 4 1 149.44 188.96 5.53 o -3 4 1 2796.40 3082.34 38.70 o -2 4 1 15609.10 14908.80 37.09 o -1 4 1 58598.06 56195.63 84.38 o 0 4 1 324.90 586.28 10.56 o 1 4 1 8066.47 7457.99 7.86 o 2 4 1 45165.98 43025.05 216.93 o 3 4 1 20960.01 20810.87 130.33 o 4 4 1 18161.92 18107.27 100.17 o 5 4 1 26039.21 24901.74 68.86 o 6 4 1 63.06 165.15 9.41 o 7 4 1 8179.54 7753.12 13.03 o 8 4 1 691.36 695.32 11.74 o 9 4 1 1814.86 1724.19 9.24 o 10 4 1 2.12 5.43 10.49 o 11 4 1 520.52 506.23 11.78 o 12 4 1 221.11 199.00 15.67 o 13 4 1 430.21 393.70 16.48 o 14 4 1 4.52 4.29 24.28 o 15 4 1 156.47 161.63 24.74 o -15 5 1 1.06 0.00 26.55 o -14 5 1 528.99 594.72 24.67 o -13 5 1 79.26 89.02 23.88 o -12 5 1 509.26 521.27 14.68 o -11 5 1 5.52 36.28 13.68 o -10 5 1 3878.34 3675.33 19.12 o -9 5 1 300.21 313.83 8.57 o -8 5 1 1138.37 1065.33 10.40 o -7 5 1 2262.39 2625.90 28.71 o -6 5 1 63415.93 60622.77 105.50 o -5 5 1 54646.48 53273.14 149.11 o -4 5 1 26576.79 26992.51 144.48 o -3 5 1 58762.99 57280.04 213.12 o -2 5 1 50.51 259.87 13.62 o -1 5 1 44127.24 43392.22 75.02 o 0 5 1 5807.06 6285.41 45.84 o 1 5 1 24112.44 23352.27 63.92 o 2 5 1 7216.12 6624.81 8.96 o 3 5 1 7342.09 6999.43 28.66 o 4 5 1 4958.40 4980.14 49.84 o 5 5 1 29334.22 27997.93 73.16 o 6 5 1 21335.95 21525.60 86.49 o 7 5 1 6542.32 6773.45 36.10 o 8 5 1 193.78 188.09 9.63 o 9 5 1 1435.81 1412.90 10.83 o 10 5 1 3531.11 3333.18 20.20 o 11 5 1 126.66 147.18 12.19 o 12 5 1 746.27 748.33 16.74 o 13 5 1 110.90 131.67 24.15 o 14 5 1 113.09 112.81 24.60 o 15 5 1 33.90 37.04 26.75 o -15 6 1 10.42 3.47 26.92 o -14 6 1 320.06 332.20 25.81 o 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443.88 11.90 o 2 9 13 239.73 260.17 15.29 o 3 9 13 59.52 67.54 15.55 o 4 9 13 549.96 523.16 20.31 o 5 9 13 12.02 24.04 23.05 o 6 9 13 87.77 63.82 22.84 o 7 9 13 144.86 160.68 27.25 o 8 9 13 2.75 12.35 28.90 o -13 10 13 67.59 54.39 29.93 o -12 10 13 113.12 90.03 27.15 o -11 10 13 1272.26 1239.66 28.32 o -10 10 13 142.23 174.80 29.13 o -9 10 13 857.74 880.84 25.09 o -8 10 13 476.19 474.54 23.05 o -7 10 13 780.05 786.31 19.60 o -6 10 13 446.70 431.29 8.42 o -5 10 13 733.96 720.30 12.97 o -4 10 13 19.24 74.63 14.14 o -3 10 13 41.03 69.51 13.49 o -2 10 13 15.61 21.02 13.88 o -1 10 13 2047.90 1912.45 15.71 o 0 10 13 262.46 221.08 14.11 o 1 10 13 1.67 45.14 16.26 o 2 10 13 372.86 389.01 14.66 o 3 10 13 60.49 58.70 15.26 o 4 10 13 75.61 80.80 19.86 o 5 10 13 42.12 52.06 20.07 o 6 10 13 0.70 1.98 25.77 o 7 10 13 13.18 13.00 26.25 o 8 10 13 49.93 70.22 28.76 o -12 11 13 1.02 7.84 28.84 o -11 11 13 229.91 250.92 27.02 o -10 11 13 122.91 165.17 30.04 o -9 11 13 1190.89 1197.44 26.11 o -8 11 13 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