#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/21/2202132.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202132_Fobs loop_ _publ_author_name 'Scholz, Stefan' 'Lerner, Hans-Wolfram' 'Bolte, Michael' _publ_section_title ; Tribromo(tetrahydrofuran)aluminium(III) ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m289 _journal_page_last m290 _journal_volume 59 _journal_year 2003 _space_group_IT_number 11 _symmetry_space_group_name_Hall '-P 2yb' _symmetry_space_group_name_H-M 'P 1 21/m 1' _cell_angle_alpha 90.000 _cell_angle_beta 106.971 _cell_angle_gamma 90.000 _cell_length_a 6.3475 _cell_length_b 10.7790 _cell_length_c 7.4326 _exptl_crystal_F_000 316.00 _reflns_d_resolution_high 0.8387 _[local]_cod_data_source_file ob6237Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' wa95 in P2(1)/m' _shelx_refln_list_code 4 _shelx_f_calc_maximum 193.67 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' '-x, -y, -z' 'x, -y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 3658.33 3445.36 149.93 o 2 0 0 2775.15 2877.26 187.83 o 3 0 0 2947.30 3108.13 264.24 o 4 0 0 838.23 946.64 61.35 o 5 0 0 1628.28 1550.93 70.60 o 6 0 0 613.82 635.25 40.39 o 7 0 0 312.18 333.03 39.56 o 1 1 0 219.73 163.23 65.75 o 2 1 0 2573.28 2641.02 65.07 o 3 1 0 6036.16 5681.95 210.24 o 4 1 0 50.43 45.69 37.92 o 5 1 0 1949.20 1926.47 48.17 o 6 1 0 92.36 102.90 32.86 o 7 1 0 173.70 172.87 30.89 o 0 2 0 1589.34 1326.55 153.96 o 1 2 0 2277.56 2164.89 71.71 o 2 2 0 1824.42 1707.17 59.24 o 3 2 0 1652.64 1663.26 55.60 o 4 2 0 4936.55 4761.32 64.65 o 5 2 0 16.62 55.94 35.51 o 6 2 0 944.48 1020.68 28.46 o 7 2 0 97.92 85.49 28.71 o 1 3 0 13151.55 12806.77 209.64 o 2 3 0 4578.32 4798.11 103.35 o 3 3 0 0.90 -15.90 40.12 o 4 3 0 555.42 541.06 44.64 o 5 3 0 311.65 334.41 38.11 o 6 3 0 845.64 902.22 29.86 o 7 3 0 579.97 535.66 31.21 o 0 4 0 561.07 430.92 76.06 o 1 4 0 71.52 18.05 45.82 o 2 4 0 688.16 857.41 42.81 o 3 4 0 655.15 667.78 35.45 o 4 4 0 1834.74 1969.94 52.06 o 5 4 0 264.24 254.37 27.89 o 6 4 0 1278.55 1247.15 78.11 o 1 5 0 189.90 167.82 40.82 o 2 5 0 4256.34 4332.99 119.95 o 3 5 0 3632.89 3612.51 94.90 o 4 5 0 224.89 263.80 31.47 o 5 5 0 662.65 743.53 48.27 o 6 5 0 410.33 388.55 35.87 o 0 6 0 9912.74 10593.18 225.64 o 1 6 0 3089.79 2985.94 123.29 o 2 6 0 1092.29 1159.66 35.56 o 3 6 0 943.36 937.91 35.79 o 4 6 0 382.71 394.61 36.67 o 5 6 0 523.98 617.62 33.40 o 6 6 0 103.24 170.90 26.08 o 1 7 0 12.62 58.66 32.02 o 2 7 0 151.97 192.04 35.24 o 3 7 0 266.97 376.72 37.89 o 4 7 0 9.36 55.83 28.94 o 5 7 0 251.24 253.27 26.58 o 6 7 0 0.02 48.81 25.91 o 0 8 0 18.80 81.86 46.94 o 1 8 0 239.82 313.77 33.78 o 2 8 0 264.91 269.81 32.01 o 3 8 0 656.66 664.58 31.08 o 4 8 0 738.81 719.45 29.80 o 5 8 0 84.95 82.31 27.12 o 1 9 0 379.90 410.78 30.73 o 2 9 0 546.46 508.58 37.39 o 3 9 0 25.53 68.51 31.60 o 4 9 0 208.52 201.22 28.79 o 5 9 0 161.48 150.10 25.59 o 0 10 0 354.33 379.66 45.54 o 1 10 0 56.21 85.26 29.02 o 2 10 0 1.45 32.93 25.41 o 3 10 0 79.44 97.04 26.16 o 4 10 0 0.17 -6.51 28.03 o 1 11 0 156.18 264.62 27.13 o 2 11 0 313.84 325.89 25.29 o 3 11 0 348.20 326.63 37.94 o 0 12 0 364.92 224.75 36.06 o 1 12 0 102.17 88.73 26.10 o 2 12 0 12.51 2.02 30.54 o -7 0 1 2.62 -13.80 43.50 o -6 0 1 16.78 15.91 47.50 o -5 0 1 1030.48 1116.16 47.65 o -4 0 1 1956.78 1988.68 97.85 o -3 0 1 3145.45 3216.44 176.26 o -2 0 1 37508.87 36899.91 289.83 o -1 0 1 722.49 769.29 126.78 o 0 0 1 3675.36 3252.38 113.77 o 1 0 1 4756.13 4813.73 102.55 o 2 0 1 4961.60 4544.71 151.21 o 3 0 1 8639.69 8344.87 114.91 o 4 0 1 720.72 671.91 53.53 o 5 0 1 2666.05 2522.58 182.00 o 6 0 1 3542.06 3294.23 155.56 o -7 1 1 562.68 477.28 32.21 o -6 1 1 27.20 75.88 31.42 o -5 1 1 1233.53 1248.77 35.86 o -4 1 1 29.77 69.41 40.17 o -3 1 1 271.73 289.87 45.74 o -2 1 1 259.21 285.14 58.91 o -1 1 1 877.94 851.95 106.18 o 0 1 1 2995.97 2600.88 122.94 o 1 1 1 11396.76 10972.65 172.55 o 2 1 1 240.27 169.93 47.04 o 3 1 1 6201.62 6024.33 104.86 o 4 1 1 695.26 693.19 45.60 o 5 1 1 14.33 32.26 31.41 o 6 1 1 101.20 113.23 27.18 o -7 2 1 187.52 249.18 32.17 o -6 2 1 2548.91 2505.21 64.41 o -5 2 1 558.95 657.46 35.62 o -4 2 1 794.64 725.98 39.28 o -3 2 1 168.19 145.30 54.72 o -2 2 1 117.53 112.08 59.13 o -1 2 1 7904.32 7724.75 174.52 o 0 2 1 4741.17 4300.41 281.76 o 1 2 1 2044.58 2005.80 76.89 o 2 2 1 8380.07 7962.17 202.93 o 3 2 1 22.35 61.88 37.30 o 4 2 1 894.84 963.38 36.06 o 5 2 1 8.56 25.25 32.97 o 6 2 1 7.20 36.80 29.89 o -7 3 1 53.50 69.08 29.91 o -6 3 1 425.17 448.84 30.53 o -5 3 1 11.42 14.27 44.31 o -4 3 1 4004.96 4205.34 52.30 o -3 3 1 10424.80 10849.51 160.90 o -2 3 1 350.37 346.86 49.61 o -1 3 1 6882.45 6829.60 181.63 o 0 3 1 4973.09 4953.81 144.70 o 1 3 1 1195.72 1074.07 46.68 o 2 3 1 217.88 203.28 43.25 o 3 3 1 218.99 266.47 36.49 o 4 3 1 2519.50 2456.52 86.62 o 5 3 1 1502.97 1423.15 31.60 o 6 3 1 285.50 267.04 29.67 o -7 4 1 2.32 72.50 30.95 o -6 4 1 1108.28 963.46 42.75 o -5 4 1 378.24 376.75 34.01 o -4 4 1 36.60 77.36 36.24 o -3 4 1 646.49 556.12 40.50 o -2 4 1 171.38 146.39 46.78 o -1 4 1 1602.58 1477.32 47.78 o 0 4 1 4851.79 4457.47 134.95 o 1 4 1 178.51 209.66 44.60 o 2 4 1 2641.72 2846.58 75.82 o 3 4 1 445.69 468.28 38.62 o 4 4 1 1142.82 1095.51 33.33 o 5 4 1 12.01 102.32 27.52 o 6 4 1 51.98 60.94 29.52 o -6 5 1 121.70 202.10 32.26 o -5 5 1 1149.33 1224.80 33.60 o -4 5 1 638.66 696.79 34.79 o -3 5 1 51.50 96.47 36.33 o -2 5 1 130.10 83.91 38.29 o -1 5 1 524.53 443.58 44.68 o 0 5 1 6461.13 6678.42 122.56 o 1 5 1 3202.77 3119.40 49.94 o 2 5 1 31.18 50.90 36.56 o 3 5 1 2824.13 3043.53 132.07 o 4 5 1 1460.47 1409.87 46.64 o 5 5 1 106.02 111.17 27.55 o 6 5 1 116.54 143.25 25.61 o -6 6 1 2.40 17.37 36.62 o -5 6 1 450.51 381.19 30.56 o -4 6 1 822.63 798.30 33.09 o -3 6 1 1400.12 1424.22 75.84 o -2 6 1 5408.92 5685.77 259.83 o -1 6 1 1431.37 1396.36 64.69 o 0 6 1 1366.09 1505.35 42.48 o 1 6 1 1046.63 1101.21 35.42 o 2 6 1 1753.79 1804.25 42.06 o 3 6 1 2343.11 2576.64 72.87 o 4 6 1 178.19 212.45 34.21 o 5 6 1 1239.79 1186.33 35.10 o 6 6 1 891.33 782.34 27.11 o -6 7 1 39.16 80.75 31.53 o -5 7 1 1.10 3.15 30.59 o -4 7 1 81.93 30.16 30.77 o -3 7 1 7.30 36.42 35.34 o -2 7 1 59.77 102.18 36.17 o -1 7 1 51.83 119.06 34.19 o 0 7 1 301.26 414.86 36.99 o 1 7 1 442.54 492.92 31.80 o 2 7 1 9.02 85.45 32.40 o 3 7 1 860.04 861.09 32.17 o 4 7 1 59.70 15.71 27.65 o 5 7 1 52.74 93.24 24.19 o -5 8 1 366.15 323.71 27.21 o -4 8 1 111.98 119.24 30.06 o -3 8 1 211.68 283.75 31.96 o -2 8 1 149.86 212.45 30.83 o -1 8 1 997.99 991.24 37.96 o 0 8 1 659.43 724.58 34.97 o 1 8 1 741.08 796.36 43.76 o 2 8 1 696.70 720.41 31.54 o 3 8 1 71.00 118.58 31.64 o 4 8 1 70.11 49.93 26.05 o 5 8 1 20.28 49.93 31.62 o -5 9 1 12.25 -4.32 28.32 o -4 9 1 723.90 529.19 29.56 o -3 9 1 895.28 834.61 40.67 o -2 9 1 287.65 334.24 28.18 o -1 9 1 75.60 88.75 31.87 o 0 9 1 536.29 691.35 39.11 o 1 9 1 116.96 195.70 32.90 o 2 9 1 0.59 7.98 26.52 o 3 9 1 10.70 36.81 29.88 o 4 9 1 210.91 223.25 25.84 o -4 10 1 99.78 196.94 28.22 o -3 10 1 178.18 226.07 27.89 o -2 10 1 171.05 178.60 27.81 o -1 10 1 137.14 118.91 29.07 o 0 10 1 392.15 376.99 29.45 o 1 10 1 3.26 21.86 29.05 o 2 10 1 16.07 58.88 25.20 o 3 10 1 86.09 104.96 24.38 o 4 10 1 122.66 60.76 28.29 o -3 11 1 20.32 -4.26 26.44 o -2 11 1 47.80 109.36 25.89 o -1 11 1 265.18 412.73 28.10 o 0 11 1 380.75 371.96 27.91 o 1 11 1 216.16 170.55 27.58 o 2 11 1 2.08 35.54 24.04 o 3 11 1 172.65 123.23 25.19 o -2 12 1 177.78 99.25 25.67 o -1 12 1 44.20 48.84 26.37 o 0 12 1 17.65 38.81 26.24 o 1 12 1 96.87 91.77 24.40 o 2 12 1 86.02 139.78 24.98 o -7 0 2 622.17 634.98 47.75 o -6 0 2 1424.01 1450.67 53.14 o -5 0 2 606.33 667.21 56.25 o -4 0 2 6446.54 7194.73 127.40 o -3 0 2 63.65 172.57 67.68 o -2 0 2 1612.89 1514.35 103.06 o -1 0 2 43.74 31.79 122.73 o 0 0 2 4852.43 4665.52 100.76 o 1 0 2 14481.42 15023.03 223.12 o 2 0 2 138.32 139.63 70.00 o 3 0 2 7448.86 7296.23 393.24 o 4 0 2 8670.40 8390.64 104.67 o 5 0 2 141.97 153.31 38.91 o 6 0 2 151.29 157.86 56.56 o -7 1 2 131.91 121.23 32.47 o -6 1 2 206.92 252.87 36.33 o -5 1 2 141.74 136.35 37.99 o -4 1 2 1067.68 1104.49 43.66 o -3 1 2 164.27 129.80 48.59 o -2 1 2 1023.70 1057.47 73.35 o -1 1 2 6678.45 6484.43 167.28 o 0 1 2 1842.34 1751.41 65.19 o 1 1 2 6204.29 6074.00 66.94 o 2 1 2 505.04 528.41 45.50 o 3 1 2 46.89 35.26 40.71 o 4 1 2 253.55 247.52 36.55 o 5 1 2 34.19 71.68 33.32 o 6 1 2 1126.64 1024.96 26.34 o -7 2 2 1.25 62.68 32.04 o -6 2 2 641.57 648.85 33.11 o -5 2 2 23.26 60.43 38.70 o -4 2 2 45.86 92.16 42.76 o -3 2 2 5769.75 6001.26 74.57 o -2 2 2 3266.22 3457.91 73.12 o -1 2 2 5672.94 5444.50 77.15 o 0 2 2 11280.88 10388.53 297.51 o 1 2 2 22.19 11.87 44.54 o 2 2 2 70.97 97.65 42.30 o 3 2 2 145.68 163.89 37.07 o 4 2 2 26.02 53.11 35.41 o 5 2 2 1184.27 1074.36 51.84 o 6 2 2 81.09 86.25 26.46 o -7 3 2 5.44 34.10 34.72 o -6 3 2 1589.06 1694.37 53.00 o -5 3 2 3373.31 3626.74 81.21 o -4 3 2 9.75 63.73 45.27 o -3 3 2 3211.50 3380.59 116.31 o -2 3 2 3644.95 3809.80 170.24 o -1 3 2 3479.04 3307.00 115.62 o 0 3 2 3597.29 3481.48 55.31 o 1 3 2 360.83 428.16 43.82 o 2 3 2 6435.29 6405.17 155.68 o 3 3 2 5447.45 5535.45 143.94 o 4 3 2 95.10 86.95 35.61 o 5 3 2 1660.20 1543.63 57.50 o 6 3 2 81.95 55.82 33.87 o -7 4 2 0.52 48.81 28.29 o -6 4 2 89.54 141.93 47.28 o -5 4 2 365.13 479.48 35.06 o -4 4 2 11.45 36.29 39.70 o -3 4 2 3003.81 2958.69 49.56 o -2 4 2 4426.76 4274.21 115.71 o -1 4 2 389.99 556.69 47.85 o 0 4 2 3832.47 4138.73 160.60 o 1 4 2 7.90 15.84 42.01 o 2 4 2 21.89 31.28 35.03 o 3 4 2 779.83 842.15 50.88 o 4 4 2 14.24 25.71 30.83 o 5 4 2 234.41 301.72 27.79 o 6 4 2 2.14 13.83 24.11 o -6 5 2 23.37 50.57 30.18 o -5 5 2 18.02 9.22 32.10 o -4 5 2 12.47 70.10 41.32 o -3 5 2 19.70 19.65 40.25 o -2 5 2 3314.82 3172.73 125.19 o -1 5 2 987.77 985.65 51.33 o 0 5 2 727.55 630.15 41.49 o 1 5 2 4146.41 4024.92 139.52 o 2 5 2 1451.98 1537.65 46.90 o 3 5 2 59.67 87.66 33.55 o 4 5 2 31.57 58.05 28.08 o 5 5 2 23.48 31.15 25.29 o -6 6 2 726.15 708.38 48.10 o -5 6 2 146.74 170.32 31.99 o -4 6 2 1284.90 1281.37 51.42 o -3 6 2 296.02 318.75 38.64 o -2 6 2 176.28 252.17 37.61 o -1 6 2 52.65 64.09 35.93 o 0 6 2 1130.72 1184.46 38.20 o 1 6 2 3159.93 3428.27 120.08 o 2 6 2 77.50 61.26 32.64 o 3 6 2 2948.67 3090.30 106.85 o 4 6 2 2059.87 2072.95 57.38 o 5 6 2 124.69 94.54 33.35 o -6 7 2 196.57 253.39 28.58 o -5 7 2 0.00 32.78 30.66 o -4 7 2 496.04 555.18 34.32 o -3 7 2 766.08 829.59 36.97 o -2 7 2 5.60 3.97 36.69 o -1 7 2 200.11 149.63 35.05 o 0 7 2 7.32 -12.71 37.95 o 1 7 2 557.79 598.75 32.28 o 2 7 2 0.77 42.33 34.66 o 3 7 2 26.96 28.52 34.02 o 4 7 2 0.80 14.69 27.36 o 5 7 2 2.49 30.11 25.29 o -5 8 2 251.08 340.26 29.16 o -4 8 2 330.76 327.74 34.85 o -3 8 2 1263.04 1191.24 50.40 o -2 8 2 265.01 261.83 32.12 o -1 8 2 1445.12 1484.26 67.27 o 0 8 2 1452.29 1563.58 39.52 o 1 8 2 270.88 331.55 30.96 o 2 8 2 1.68 41.72 27.25 o 3 8 2 1.31 25.39 32.79 o 4 8 2 82.91 111.96 25.23 o -5 9 2 479.99 365.89 29.19 o -4 9 2 153.98 207.56 31.43 o -3 9 2 70.33 52.66 34.23 o -2 9 2 768.81 661.21 36.61 o -1 9 2 799.23 832.02 35.28 o 0 9 2 301.33 306.17 31.13 o 1 9 2 24.93 43.85 30.87 o 2 9 2 660.30 707.14 34.65 o 3 9 2 349.63 347.14 35.95 o 4 9 2 0.97 33.46 30.15 o -4 10 2 50.69 66.32 31.15 o -3 10 2 357.57 341.80 30.39 o -2 10 2 616.36 615.48 28.60 o -1 10 2 24.07 135.95 30.17 o 0 10 2 2.23 6.90 27.94 o 1 10 2 10.53 12.18 29.10 o 2 10 2 29.18 60.90 25.57 o 3 10 2 121.40 60.42 24.39 o -3 11 2 87.59 134.34 28.26 o -2 11 2 183.09 108.75 26.68 o -1 11 2 51.47 43.26 25.92 o 0 11 2 51.01 57.89 25.70 o 1 11 2 322.84 273.12 25.66 o 2 11 2 228.83 292.82 26.72 o -2 12 2 8.06 59.10 25.13 o -1 12 2 4.11 14.92 23.97 o 0 12 2 26.81 48.69 25.81 o 1 12 2 98.14 68.08 24.08 o -7 0 3 233.94 183.47 52.05 o -6 0 3 1326.53 1412.94 63.03 o -5 0 3 0.85 84.86 99.03 o -4 0 3 5.60 30.00 67.52 o -3 0 3 1603.00 1533.16 75.82 o -2 0 3 1443.69 1761.43 99.72 o -1 0 3 10769.23 10005.07 170.19 o 0 0 3 521.87 432.95 77.80 o 1 0 3 6435.80 6562.37 245.74 o 2 0 3 7553.70 7833.46 77.42 o 3 0 3 60.48 148.37 51.68 o 4 0 3 163.76 51.66 57.61 o 5 0 3 169.70 174.68 42.29 o 6 0 3 979.95 874.02 37.48 o -7 1 3 1.01 9.08 35.65 o -6 1 3 1168.19 1169.56 37.59 o -5 1 3 400.40 515.82 43.84 o -4 1 3 696.55 686.51 56.32 o -3 1 3 2097.03 2241.72 55.51 o -2 1 3 368.52 357.70 66.28 o -1 1 3 934.17 932.00 55.89 o 0 1 3 92.52 51.71 52.20 o 1 1 3 228.24 267.26 47.03 o 2 1 3 1283.98 1292.92 40.18 o 3 1 3 193.06 144.52 40.90 o 4 1 3 1947.89 1957.37 45.96 o 5 1 3 557.08 555.49 32.02 o 6 1 3 447.73 381.06 34.53 o -7 2 3 40.92 55.44 34.07 o -6 2 3 0.97 -14.95 46.52 o -5 2 3 1650.81 1737.53 44.41 o -4 2 3 297.16 375.07 47.92 o -3 2 3 5915.74 5795.63 78.58 o -2 2 3 5286.47 5406.17 158.01 o -1 2 3 16.24 52.30 56.33 o 0 2 3 33.70 95.87 44.26 o 1 2 3 137.34 170.51 43.38 o 2 2 3 1294.31 1281.33 41.73 o 3 2 3 4324.33 4328.72 168.97 o 4 2 3 232.31 272.36 30.91 o 5 2 3 648.54 628.20 28.42 o -7 3 3 359.81 246.33 35.12 o -6 3 3 144.57 183.78 37.51 o -5 3 3 986.77 1051.77 42.97 o -4 3 3 458.37 472.14 49.93 o -3 3 3 1290.88 1442.77 69.96 o -2 3 3 2391.59 2435.43 64.91 o -1 3 3 554.36 613.72 47.30 o 0 3 3 10374.18 10364.85 105.47 o 1 3 3 9830.83 9801.31 143.07 o 2 3 3 4.79 6.15 33.97 o 3 3 3 1911.49 1955.57 39.34 o 4 3 3 467.45 418.28 29.31 o 5 3 3 340.51 329.35 23.76 o -7 4 3 280.85 380.52 36.76 o -6 4 3 54.40 65.10 34.05 o -5 4 3 978.45 1013.14 47.86 o -4 4 3 821.22 948.54 42.92 o -3 4 3 718.29 768.53 47.50 o -2 4 3 1932.50 1880.66 120.55 o -1 4 3 0.90 8.29 42.72 o 0 4 3 158.25 103.18 38.89 o 1 4 3 1639.35 1571.77 39.85 o 2 4 3 341.46 404.91 32.63 o 3 4 3 2077.98 2123.32 48.80 o 4 4 3 151.66 204.83 29.07 o 5 4 3 128.90 119.17 24.84 o -6 5 3 209.97 136.34 35.45 o -5 5 3 13.16 38.09 34.53 o -4 5 3 1612.04 1611.53 86.62 o -3 5 3 590.35 642.21 48.70 o -2 5 3 388.34 453.92 44.93 o -1 5 3 1532.34 1472.86 46.17 o 0 5 3 317.55 317.66 39.00 o 1 5 3 3.32 39.75 32.93 o 2 5 3 11.33 61.88 35.68 o 3 5 3 143.98 184.98 31.29 o 4 5 3 2079.97 2163.60 45.74 o 5 5 3 340.14 344.31 25.09 o -6 6 3 365.43 289.11 31.72 o -5 6 3 114.90 46.85 34.27 o -4 6 3 144.06 113.93 40.66 o -3 6 3 343.97 399.02 48.15 o -2 6 3 225.37 171.27 40.42 o -1 6 3 3433.97 3284.79 166.66 o 0 6 3 318.16 300.11 43.16 o 1 6 3 1908.81 2146.70 80.34 o 2 6 3 1513.48 1601.17 52.21 o 3 6 3 71.56 80.36 37.15 o 4 6 3 30.03 18.51 26.03 o 5 6 3 161.87 117.12 25.41 o -6 7 3 549.48 619.72 32.21 o -5 7 3 680.10 826.14 64.03 o -4 7 3 2.33 24.42 23.72 o -3 7 3 220.23 243.28 39.76 o -2 7 3 291.83 326.45 39.51 o -1 7 3 49.42 40.98 34.51 o 0 7 3 478.68 540.65 36.07 o 1 7 3 10.42 48.84 39.30 o 2 7 3 118.62 111.36 27.53 o 3 7 3 31.30 36.47 26.79 o 4 7 3 226.02 257.60 26.72 o -5 8 3 449.25 315.02 34.08 o -4 8 3 0.42 55.25 34.86 o -3 8 3 1781.19 1828.53 56.49 o -2 8 3 1629.07 1460.66 66.79 o -1 8 3 205.94 188.79 34.97 o 0 8 3 1.61 2.77 33.33 o 1 8 3 140.32 201.05 35.33 o 2 8 3 578.57 615.58 27.54 o 3 8 3 788.16 818.27 35.76 o 4 8 3 62.17 67.54 26.54 o -5 9 3 20.91 7.28 33.13 o -4 9 3 307.90 181.41 34.35 o -3 9 3 523.36 360.31 34.30 o -2 9 3 292.43 216.07 29.08 o -1 9 3 1.07 1.79 30.88 o 0 9 3 1436.18 1356.51 58.21 o 1 9 3 1024.52 1020.49 51.22 o 2 9 3 82.36 103.07 29.06 o 3 9 3 82.94 66.16 24.15 o -4 10 3 201.01 289.11 32.68 o -3 10 3 8.75 125.23 28.46 o -2 10 3 4.69 53.97 27.62 o -1 10 3 36.20 97.21 30.33 o 0 10 3 250.12 400.12 52.72 o 1 10 3 191.29 217.02 26.12 o 2 10 3 0.28 45.20 32.60 o 3 10 3 113.19 41.01 27.46 o -3 11 3 105.68 45.51 26.79 o -2 11 3 2.78 32.42 28.62 o -1 11 3 149.12 175.03 28.63 o 0 11 3 100.13 114.67 26.06 o 1 11 3 4.79 100.35 24.94 o 2 11 3 15.33 73.20 28.96 o -1 12 3 162.53 91.87 30.31 o 0 12 3 31.85 59.46 37.34 o -7 0 4 49.85 98.08 55.29 o -6 0 4 44.05 76.36 57.29 o -5 0 4 1250.54 1351.17 115.20 o -4 0 4 735.62 876.78 73.86 o -3 0 4 6976.95 7093.41 106.39 o -2 0 4 1110.06 1151.40 82.31 o -1 0 4 2840.64 2629.64 175.14 o 0 0 4 2322.85 2340.10 62.96 o 1 0 4 159.10 234.42 50.87 o 2 0 4 38.40 35.36 51.51 o 3 0 4 26.91 33.41 44.27 o 4 0 4 1798.75 1866.46 193.75 o 5 0 4 1302.79 1165.70 53.37 o -7 1 4 16.89 26.98 37.68 o -6 1 4 734.14 727.29 50.80 o -5 1 4 722.00 720.12 45.21 o -4 1 4 49.75 63.24 52.59 o -3 1 4 8.39 74.19 56.61 o -2 1 4 652.52 545.73 49.33 o -1 1 4 95.93 55.41 45.00 o 0 1 4 3986.83 3830.69 90.25 o 1 1 4 5.47 31.67 38.50 o 2 1 4 1424.52 1463.31 37.67 o 3 1 4 391.17 413.09 32.98 o 4 1 4 739.98 740.34 50.66 o 5 1 4 176.72 223.34 32.75 o -7 2 4 405.33 357.75 37.17 o -6 2 4 3.42 38.03 40.03 o -5 2 4 2030.68 2153.80 70.61 o -4 2 4 596.64 656.08 54.45 o -3 2 4 444.89 412.55 49.71 o -2 2 4 116.41 114.12 50.70 o -1 2 4 45.56 41.46 45.02 o 0 2 4 3000.81 3104.39 46.78 o 1 2 4 4673.20 4792.93 131.86 o 2 2 4 20.62 47.60 40.72 o 3 2 4 2035.49 2063.87 47.74 o 4 2 4 699.02 699.71 30.93 o 5 2 4 31.73 46.10 28.07 o -7 3 4 36.85 46.56 48.95 o -6 3 4 88.60 130.99 39.34 o -5 3 4 96.19 106.51 49.13 o -4 3 4 912.76 889.61 67.31 o -3 3 4 212.36 216.26 50.83 o -2 3 4 6108.06 6422.94 302.91 o -1 3 4 4138.05 3975.89 111.02 o 0 3 4 156.44 138.53 43.82 o 1 3 4 1975.60 2072.60 86.58 o 2 3 4 1069.72 1131.95 36.90 o 3 3 4 1656.04 1669.14 40.36 o 4 3 4 1270.79 1258.77 29.92 o 5 3 4 238.18 236.64 23.58 o -7 4 4 214.12 209.20 33.05 o -6 4 4 75.00 156.14 35.19 o -5 4 4 234.86 159.72 42.60 o -4 4 4 87.09 76.66 46.82 o -3 4 4 337.12 441.02 63.81 o -2 4 4 97.91 109.03 50.92 o -1 4 4 1376.16 1335.21 44.19 o 0 4 4 866.30 955.95 38.29 o 1 4 4 2892.22 2963.67 94.73 o 2 4 4 123.40 100.14 33.13 o 3 4 4 235.41 260.32 29.59 o 4 4 4 233.64 230.62 27.53 o 5 4 4 1.75 6.44 23.63 o -6 5 4 926.03 1038.19 121.75 o -5 5 4 435.22 350.80 38.03 o -4 5 4 99.50 176.02 43.70 o -3 5 4 283.64 390.40 44.30 o -2 5 4 89.32 123.38 49.95 o -1 5 4 189.75 217.92 38.73 o 0 5 4 295.09 351.87 38.35 o 1 5 4 48.30 42.84 32.91 o 2 5 4 2132.81 2224.15 34.78 o 3 5 4 162.10 208.60 27.71 o 4 5 4 434.51 447.89 26.94 o -6 6 4 156.70 144.14 37.39 o -5 6 4 313.40 417.56 40.45 o -4 6 4 206.06 169.86 41.79 o -3 6 4 3165.34 2881.74 110.92 o -2 6 4 795.39 792.59 65.98 o -1 6 4 442.20 464.89 39.39 o 0 6 4 558.48 565.77 36.82 o 1 6 4 146.86 101.40 35.03 o 2 6 4 187.30 204.48 26.92 o 3 6 4 15.90 21.88 26.80 o 4 6 4 382.94 421.90 26.27 o -6 7 4 20.29 -35.84 35.84 o -5 7 4 193.71 241.52 34.95 o -4 7 4 309.94 367.55 46.42 o -3 7 4 378.12 525.13 40.60 o -2 7 4 544.61 595.87 33.80 o -1 7 4 76.75 131.18 34.97 o 0 7 4 1170.03 1338.85 39.65 o 1 7 4 561.61 559.49 30.62 o 2 7 4 57.48 83.19 25.79 o 3 7 4 4.49 -27.09 28.42 o 4 7 4 35.20 34.22 26.01 o -5 8 4 680.15 717.08 74.61 o -4 8 4 453.42 339.47 41.05 o -3 8 4 2.51 33.65 40.85 o -2 8 4 22.22 88.47 31.73 o -1 8 4 492.35 546.57 32.76 o 0 8 4 1047.98 1064.69 33.24 o 1 8 4 1047.14 1112.97 30.61 o 2 8 4 0.91 47.50 26.23 o 3 8 4 491.39 431.60 24.12 o -5 9 4 99.58 128.21 58.56 o -4 9 4 151.18 137.90 35.06 o -3 9 4 2.33 3.34 32.88 o -2 9 4 868.16 509.57 30.32 o -1 9 4 754.42 599.54 32.00 o 0 9 4 37.83 73.46 29.87 o 1 9 4 111.76 100.81 27.83 o 2 9 4 285.15 282.20 26.90 o 3 9 4 336.00 267.52 53.57 o -4 10 4 48.56 33.53 47.51 o -3 10 4 8.24 -6.30 47.15 o -2 10 4 190.51 254.39 31.61 o -1 10 4 164.42 205.36 31.31 o 0 10 4 0.54 18.59 28.84 o 1 10 4 225.32 217.30 28.14 o 2 10 4 79.14 96.83 26.29 o -2 11 4 146.32 154.68 30.18 o -1 11 4 69.68 74.33 29.80 o 0 11 4 8.41 21.56 27.78 o -7 0 5 314.07 245.36 60.00 o -6 0 5 442.93 312.00 98.62 o -5 0 5 2644.84 2514.33 121.32 o -4 0 5 107.93 182.40 65.02 o -3 0 5 1324.88 1284.54 77.03 o -2 0 5 577.15 616.63 61.38 o -1 0 5 367.07 513.26 63.66 o 0 0 5 1036.99 1114.13 57.74 o 1 0 5 800.47 820.94 49.94 o 2 0 5 2609.16 2664.38 53.63 o 3 0 5 2047.62 2103.36 75.70 o 4 0 5 1.92 74.46 83.10 o -7 1 5 40.20 30.30 40.63 o -6 1 5 181.82 164.81 41.99 o -5 1 5 4.45 57.23 49.30 o -4 1 5 259.33 298.60 50.85 o -3 1 5 668.81 696.37 55.50 o -2 1 5 3396.12 3391.61 139.69 o -1 1 5 2.28 28.54 43.35 o 0 1 5 1722.06 1763.16 70.22 o 1 1 5 369.75 417.29 36.22 o 2 1 5 163.24 122.21 35.08 o 3 1 5 27.87 108.37 29.83 o 4 1 5 141.96 112.01 33.61 o -7 2 5 339.42 337.42 50.54 o -6 2 5 5.27 53.11 42.75 o -5 2 5 611.98 615.46 44.80 o -4 2 5 5.24 40.94 48.27 o -3 2 5 256.69 244.73 48.11 o -2 2 5 1102.88 1237.06 66.21 o -1 2 5 1642.06 1712.89 80.59 o 0 2 5 227.77 192.53 37.11 o 1 2 5 3099.75 3202.20 43.36 o 2 2 5 439.68 446.62 33.11 o 3 2 5 57.51 97.29 35.23 o 4 2 5 47.43 110.31 25.60 o -6 3 5 571.43 519.35 54.29 o -5 3 5 4.89 18.57 40.98 o -4 3 5 1174.42 1247.80 145.21 o -3 3 5 319.90 321.88 51.38 o -2 3 5 308.58 322.87 46.91 o -1 3 5 486.24 498.94 47.30 o 0 3 5 163.57 156.66 44.77 o 1 3 5 1643.63 1772.74 44.27 o 2 3 5 1299.83 1346.16 32.66 o 3 3 5 892.93 956.95 29.45 o 4 3 5 2464.73 2306.35 64.87 o -6 4 5 61.37 164.73 66.45 o -5 4 5 445.53 547.15 41.18 o -4 4 5 154.84 258.17 47.17 o -3 4 5 1329.26 1577.62 83.97 o -2 4 5 145.01 117.05 45.46 o -1 4 5 1061.44 1065.58 57.67 o 0 4 5 6.60 29.24 38.61 o 1 4 5 224.30 295.20 34.87 o 2 4 5 97.46 112.10 28.35 o 3 4 5 14.49 -6.08 27.27 o 4 4 5 137.15 142.92 24.76 o -6 5 5 135.80 271.83 46.15 o -5 5 5 97.81 233.83 52.33 o -4 5 5 97.14 158.64 40.68 o -3 5 5 581.08 561.90 72.30 o -2 5 5 527.61 484.35 50.12 o -1 5 5 87.13 156.92 39.35 o 0 5 5 2459.72 2623.07 59.72 o 1 5 5 270.20 219.80 32.12 o 2 5 5 264.39 278.05 30.59 o 3 5 5 25.20 63.59 26.98 o 4 5 5 3.60 21.16 29.23 o -6 6 5 176.33 77.99 37.37 o -5 6 5 1298.05 1050.16 107.29 o -4 6 5 245.68 283.65 36.56 o -3 6 5 212.36 181.04 40.85 o -2 6 5 285.56 149.53 41.51 o -1 6 5 425.81 343.03 37.90 o 0 6 5 1241.19 1250.47 33.46 o 1 6 5 64.90 84.59 31.20 o 2 6 5 430.07 416.97 31.12 o 3 6 5 899.89 847.89 46.25 o -5 7 5 103.30 225.78 35.67 o -4 7 5 151.08 315.45 40.97 o -3 7 5 221.55 220.42 41.70 o -2 7 5 1517.26 1511.83 58.21 o -1 7 5 589.85 704.95 35.40 o 0 7 5 33.88 46.13 32.32 o 1 7 5 83.08 78.42 30.06 o 2 7 5 69.60 50.50 27.07 o 3 7 5 147.16 130.06 24.51 o -5 8 5 5.80 24.41 34.64 o -4 8 5 0.88 53.69 36.78 o -3 8 5 138.54 164.63 34.31 o -2 8 5 520.43 453.91 30.70 o -1 8 5 463.86 350.76 31.94 o 0 8 5 144.26 252.13 31.42 o 1 8 5 858.80 943.06 36.13 o 2 8 5 441.33 403.65 28.05 o -4 9 5 142.96 71.37 34.97 o -3 9 5 211.93 124.78 34.71 o -2 9 5 10.99 40.52 32.30 o -1 9 5 2.72 23.69 28.80 o 0 9 5 158.56 111.91 28.24 o 1 9 5 352.40 302.48 28.59 o -3 10 5 263.12 322.97 54.47 o -2 10 5 63.55 141.53 30.31 o -1 10 5 47.95 35.58 28.65 o 0 10 5 42.20 90.19 27.91 o -6 0 6 115.85 199.07 58.98 o -5 0 6 633.07 570.08 60.15 o -4 0 6 46.78 102.22 66.69 o -3 0 6 49.47 100.65 52.91 o -2 0 6 1003.09 984.34 89.15 o -1 0 6 391.99 446.65 55.79 o 0 0 6 3054.38 3060.59 221.64 o 1 0 6 2464.00 2650.14 135.51 o 2 0 6 84.85 116.26 45.80 o 3 0 6 298.09 325.22 36.75 o -6 1 6 144.78 149.34 42.21 o -5 1 6 268.57 217.56 46.92 o -4 1 6 897.80 904.71 41.48 o -3 1 6 244.04 221.97 43.67 o -2 1 6 1656.31 1615.45 102.48 o -1 1 6 86.87 126.79 40.49 o 0 1 6 3.32 13.76 34.82 o 1 1 6 144.92 131.10 41.09 o 2 1 6 122.00 117.98 30.79 o 3 1 6 670.31 637.32 27.32 o -6 2 6 208.93 120.56 46.73 o -5 2 6 407.00 343.72 45.45 o -4 2 6 276.47 329.71 42.17 o -3 2 6 535.84 502.79 43.31 o -2 2 6 299.82 322.09 41.29 o -1 2 6 1067.21 1066.84 62.23 o 0 2 6 6.69 46.20 37.34 o 1 2 6 5.57 18.80 31.72 o 2 2 6 12.86 43.58 28.53 o 3 2 6 22.50 -11.35 30.49 o -6 3 6 216.37 143.90 54.05 o -5 3 6 4.02 -29.16 41.59 o -4 3 6 47.06 37.88 44.47 o -3 3 6 66.60 81.84 46.18 o -2 3 6 133.24 159.03 42.50 o -1 3 6 887.26 864.35 51.26 o 0 3 6 837.51 862.51 41.47 o 1 3 6 675.79 709.38 39.00 o 2 3 6 1815.60 1957.28 50.86 o 3 3 6 153.88 181.92 27.64 o -6 4 6 242.78 343.38 58.57 o -5 4 6 866.51 1114.63 146.23 o -4 4 6 16.76 100.71 42.28 o -3 4 6 319.93 315.62 47.68 o -2 4 6 29.86 74.85 37.15 o -1 4 6 1.42 19.37 38.97 o 0 4 6 123.81 146.51 31.35 o 1 4 6 15.59 42.94 29.83 o 2 4 6 159.58 139.83 28.67 o 3 4 6 75.03 101.60 25.81 o -6 5 6 6.02 24.16 52.31 o -5 5 6 220.48 105.64 38.84 o -4 5 6 129.10 -20.71 41.41 o -3 5 6 340.57 502.04 44.79 o -2 5 6 2045.41 1863.72 107.78 o -1 5 6 246.02 214.18 40.75 o 0 5 6 139.45 211.35 31.83 o 1 5 6 1.52 30.12 29.38 o 2 5 6 85.62 65.78 27.90 o 3 5 6 378.28 392.58 41.63 o -5 6 6 163.26 81.11 40.57 o -4 6 6 55.61 53.96 37.61 o -3 6 6 193.12 111.88 42.04 o -2 6 6 963.72 808.23 39.03 o -1 6 6 25.65 51.52 33.79 o 0 6 6 709.31 598.37 31.86 o 1 6 6 1419.13 1319.02 39.87 o 2 6 6 120.31 117.51 28.89 o -5 7 6 53.13 77.79 38.14 o -4 7 6 433.14 531.97 35.11 o -3 7 6 67.51 210.05 33.26 o -2 7 6 67.66 81.07 42.73 o -1 7 6 109.49 91.19 31.71 o 0 7 6 168.47 213.65 33.92 o 1 7 6 449.91 514.11 31.38 o 2 7 6 109.55 99.94 28.37 o -4 8 6 169.00 183.00 34.99 o -3 8 6 193.79 98.64 31.72 o -2 8 6 56.75 161.75 37.31 o -1 8 6 393.41 458.88 30.28 o 0 8 6 163.07 147.62 30.67 o 1 8 6 9.81 15.94 27.42 o -3 9 6 99.26 87.75 46.58 o -2 9 6 4.81 21.11 35.99 o -1 9 6 198.41 107.76 30.47 o 0 9 6 188.62 146.98 28.04 o -6 0 7 81.96 180.10 59.58 o -5 0 7 42.62 115.80 57.96 o -4 0 7 274.00 230.29 51.22 o -3 0 7 39.85 34.52 53.39 o -2 0 7 1682.08 1557.16 295.41 o -1 0 7 1153.30 1207.42 123.52 o 0 0 7 15.86 21.55 47.20 o 1 0 7 191.84 205.00 47.55 o 2 0 7 98.84 98.46 44.54 o -6 1 7 121.01 63.93 45.03 o -5 1 7 342.14 284.04 38.59 o -4 1 7 406.63 379.53 40.61 o -3 1 7 90.13 113.76 37.17 o -2 1 7 64.86 94.67 39.16 o -1 1 7 66.82 158.67 35.73 o 0 1 7 24.06 52.90 34.68 o 1 1 7 1285.24 1257.28 34.31 o 2 1 7 410.71 432.60 25.68 o -6 2 7 249.08 213.50 56.10 o -5 2 7 286.41 234.96 45.15 o -4 2 7 94.30 149.61 41.35 o -3 2 7 82.29 119.43 39.07 o -2 2 7 190.35 185.11 41.21 o -1 2 7 16.37 50.35 34.66 o 0 2 7 203.14 224.85 35.05 o 1 2 7 1.35 36.31 29.33 o 2 2 7 443.38 385.69 40.06 o -5 3 7 215.83 293.61 41.20 o -4 3 7 107.80 180.44 41.16 o -3 3 7 646.44 475.78 43.76 o -2 3 7 735.62 652.68 76.29 o -1 3 7 145.93 160.08 37.34 o 0 3 7 493.58 443.82 39.65 o 1 3 7 3.72 54.10 34.14 o 2 3 7 1.11 -24.23 27.36 o -5 4 7 169.38 151.16 41.52 o -4 4 7 9.82 24.10 40.10 o -3 4 7 96.73 157.23 43.68 o -2 4 7 367.29 576.54 52.85 o -1 4 7 15.43 -0.69 36.51 o 0 4 7 383.24 408.07 31.97 o 1 4 7 287.84 344.57 28.06 o 2 4 7 52.54 40.67 27.38 o -5 5 7 219.46 292.05 39.68 o -4 5 7 577.95 547.46 52.95 o -3 5 7 2.09 16.40 44.95 o -2 5 7 206.03 254.12 39.75 o -1 5 7 4.08 26.02 33.19 o 0 5 7 246.32 263.04 30.52 o 1 5 7 678.48 663.23 31.01 o -4 6 7 235.72 159.36 39.87 o -3 6 7 1.51 22.08 35.02 o -2 6 7 494.99 359.64 37.50 o -1 6 7 703.51 533.27 41.33 o 0 6 7 52.07 33.67 31.16 o 1 6 7 25.21 78.33 28.12 o -3 7 7 1.28 49.48 32.22 o -2 7 7 15.97 29.50 36.51 o -1 7 7 279.25 452.17 41.21 o 0 7 7 25.12 79.46 31.39 o -5 0 8 23.85 48.21 46.73 o -4 0 8 400.89 270.30 51.06 o -3 0 8 82.75 57.07 52.53 o -2 0 8 316.91 353.66 91.67 o -1 0 8 42.49 71.28 47.33 o 0 0 8 20.82 71.54 42.77 o 1 0 8 189.39 192.80 36.15 o -5 1 8 274.79 340.39 37.70 o -4 1 8 62.80 102.48 36.15 o -3 1 8 132.01 159.87 40.35 o -2 1 8 16.72 75.64 36.71 o -1 1 8 556.26 550.99 37.41 o 0 1 8 35.22 51.17 30.87 o 1 1 8 299.93 281.65 29.51 o -4 2 8 92.37 128.39 37.72 o -3 2 8 20.06 6.96 41.06 o -2 2 8 492.50 385.81 40.89 o -1 2 8 7.32 59.65 34.11 o 0 2 8 213.88 261.50 31.06 o -4 3 8 295.42 181.84 40.73 o -3 3 8 114.96 79.65 41.99 o -2 3 8 107.85 40.85 38.69 o -1 3 8 11.33 25.51 42.30 o 0 3 8 85.88 93.98 39.02 o -4 4 8 131.32 242.37 81.34 o -3 4 8 16.63 11.40 35.65 o -2 4 8 468.15 531.52 52.45 o -1 4 8 252.70 349.35 37.22 o 0 4 8 17.47 43.22 30.88 o -3 5 8 12.69 -30.45 38.96 o -2 5 8 83.82 93.90 40.05 o -1 5 8 329.73 277.00 36.54 o