#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2202157.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202157_Fobs loop_ _publ_author_name 'Holmes, Brian T.' 'Padgett, Clifford W.' 'Pennington, William T.' _publ_section_title ; 2-Amino-6-bromopyridinium bromide ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o862 _journal_page_last o864 _journal_volume 59 _journal_year 2003 _space_group_IT_number 64 _symmetry_space_group_name_Hall '-C 2ac 2' _symmetry_space_group_name_H-M 'C m c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 6.9230 _cell_length_b 11.6160 _cell_length_c 19.4130 _exptl_crystal_F_000 960.00 _reflns_d_resolution_high 0.8404 _[local]_cod_data_source_file om61411sup2.hkl _[local]_cod_data_source_block 1 #BEGIN Tags that were not found in dictionaries: _shelx_title ' BD1167 in Cmca' _shelx_refln_list_code 6 _shelx_f_calc_maximum 675.78 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y+1/2, z+1/2' '-x, y+1/2, -z+1/2' 'x, -y, -z' 'x+1/2, y+1/2, z' '-x+1/2, -y+1, z+1/2' '-x+1/2, y+1, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x, y-1/2, -z-1/2' 'x, -y-1/2, z-1/2' '-x, y, z' '-x+1/2, -y+1/2, -z' 'x+1/2, y, -z-1/2' 'x+1/2, -y, z-1/2' '-x+1/2, y+1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_sigma _refln_F_calc _refln_phase_calc 2 0 0 421417.94 1947.46 674.92 0.0 4 0 0 71005.98 451.52 313.12 0.0 6 0 0 11205.36 190.18 119.77 0.0 8 0 0 1265.68 49.31 37.58 0.0 0 2 0 4669.34 90.65 65.37 180.0 2 2 0 2752.92 72.34 50.72 180.0 4 2 0 1048.20 33.55 34.53 180.0 6 2 0 503.88 34.53 22.87 180.0 8 2 0 0.00 137.05 11.52 180.0 0 4 0 69574.17 531.01 253.87 0.0 2 4 0 44006.70 393.41 204.91 0.0 4 4 0 12888.56 222.27 113.79 0.0 6 4 0 2279.31 72.63 45.07 0.0 0 6 0 37377.58 402.75 175.31 0.0 2 6 0 21789.66 317.68 141.67 0.0 4 6 0 6145.03 198.92 78.18 0.0 6 6 0 944.28 54.24 30.95 0.0 0 8 0 2925.48 94.29 49.33 0.0 2 8 0 1774.59 57.14 38.37 0.0 4 8 0 331.27 53.74 17.59 0.0 6 8 0 0.00 175.00 4.07 0.0 0 10 0 29860.33 438.29 163.85 0.0 2 10 0 20376.09 380.61 135.65 0.0 4 10 0 6608.25 199.58 77.71 0.0 0 12 0 0.00 175.63 16.58 0.0 2 12 0 189.51 61.14 11.76 0.0 4 12 0 75.20 197.69 3.38 0.0 1 1 1 8447.12 79.07 99.92 0.0 3 1 1 2977.98 74.58 62.22 0.0 5 1 1 648.62 27.63 26.36 0.0 7 1 1 0.00 100.50 7.24 0.0 0 2 1 3805.26 67.84 57.60 0.0 2 2 1 2592.48 65.75 53.65 0.0 4 2 1 1251.64 38.68 38.54 0.0 6 2 1 355.53 34.55 19.38 0.0 8 2 1 56.79 91.39 6.96 0.0 1 3 1 52389.79 362.77 221.87 0.0 3 3 1 16726.42 198.41 137.52 0.0 5 3 1 3377.24 88.94 61.99 0.0 7 3 1 435.28 44.36 20.76 0.0 0 4 1 47023.00 397.87 210.47 180.0 2 4 1 26539.14 268.42 164.44 180.0 4 4 1 7795.63 165.15 89.59 180.0 6 4 1 1546.25 51.41 38.48 180.0 1 5 1 6798.94 156.88 78.55 0.0 3 5 1 1820.47 53.24 42.90 0.0 5 5 1 228.92 36.40 13.77 0.0 7 5 1 0.00 132.71 2.01 0.0 0 6 1 35407.02 388.70 176.50 0.0 2 6 1 23334.70 311.70 145.60 0.0 4 6 1 7672.32 202.42 86.41 0.0 6 6 1 1591.57 56.13 39.19 0.0 1 7 1 21764.52 319.74 141.59 0.0 3 7 1 9717.15 232.47 96.02 0.0 5 7 1 2257.24 75.18 45.75 0.0 7 7 1 423.09 59.51 15.67 0.0 0 8 1 6052.64 197.59 71.28 180.0 2 8 1 4118.15 130.84 62.34 180.0 4 8 1 1961.33 64.32 41.53 180.0 6 8 1 485.16 60.27 21.01 180.0 1 9 1 1598.09 55.56 37.43 0.0 3 9 1 591.02 52.99 23.22 0.0 5 9 1 0.00 115.72 8.71 0.0 0 10 1 2810.14 93.10 49.52 0.0 2 10 1 1879.26 63.74 41.41 0.0 4 10 1 165.85 187.83 24.80 0.0 1 11 1 2305.03 77.81 45.69 0.0 3 11 1 1018.41 66.98 31.09 0.0 0 12 1 142.42 162.63 6.19 0.0 2 12 1 102.55 172.34 5.19 0.0 4 12 1 0.00 200.63 3.02 0.0 1 13 1 1944.50 76.73 44.73 0.0 0 0 2 12654.97 78.76 110.14 180.0 2 0 2 6130.30 76.25 93.26 180.0 4 0 2 2467.95 79.52 56.70 180.0 6 0 2 654.63 32.38 26.09 180.0 8 0 2 0.00 123.76 9.36 180.0 1 1 2 424.55 19.69 19.97 180.0 3 1 2 1023.55 31.97 37.35 180.0 5 1 2 707.57 28.12 28.15 180.0 7 1 2 178.87 36.88 11.71 180.0 0 2 2 4427.46 66.30 60.74 0.0 2 2 2 2805.56 67.27 56.65 0.0 4 2 2 1354.98 45.83 40.27 0.0 6 2 2 456.83 34.50 20.45 0.0 8 2 2 28.29 131.93 7.71 0.0 1 3 2 22778.28 198.90 143.15 0.0 3 3 2 7060.29 127.09 89.74 0.0 5 3 2 1623.24 52.80 43.06 0.0 7 3 2 100.14 122.66 16.20 0.0 0 4 2 4840.50 110.38 67.42 180.0 2 4 2 2875.75 90.84 54.19 180.0 4 4 2 901.45 31.12 31.20 180.0 6 4 2 224.12 37.73 14.00 180.0 1 5 2 1139.21 37.98 34.33 180.0 3 5 2 611.11 29.36 24.18 180.0 5 5 2 207.35 35.49 14.09 180.0 7 5 2 86.82 45.95 6.72 180.0 0 6 2 1585.75 51.28 36.18 0.0 2 6 2 747.94 32.42 25.87 0.0 4 6 2 0.00 103.04 10.75 0.0 6 6 2 55.19 44.53 3.24 0.0 1 7 2 807.64 40.29 28.46 180.0 3 7 2 501.94 39.00 20.00 180.0 5 7 2 225.23 44.50 10.49 180.0 7 7 2 0.00 157.31 4.22 180.0 0 8 2 581.37 43.95 24.88 0.0 2 8 2 495.79 43.12 21.38 0.0 4 8 2 25.20 130.85 13.54 0.0 6 8 2 53.35 158.58 6.35 0.0 1 9 2 6668.92 220.54 76.98 0.0 3 9 2 3234.34 99.18 57.01 0.0 5 9 2 967.59 62.20 31.74 0.0 0 10 2 1477.96 59.43 36.07 180.0 2 10 2 1074.42 58.05 30.65 180.0 4 10 2 407.95 60.03 19.00 180.0 1 11 2 2810.60 89.77 52.05 180.0 3 11 2 1577.64 69.82 39.73 180.0 0 12 2 468.53 63.63 19.83 0.0 2 12 2 346.48 65.50 17.61 0.0 4 12 2 173.21 206.09 12.09 0.0 1 13 2 2254.95 79.95 46.77 0.0 1 1 3 4538.83 60.52 69.56 180.0 3 1 3 1295.08 41.77 41.88 180.0 5 1 3 206.32 25.14 15.68 180.0 7 1 3 75.25 99.71 2.70 180.0 0 2 3 83.52 9.71 8.04 0.0 2 2 3 26.32 36.30 4.70 0.0 4 2 3 0.00 62.68 0.41 0.0 6 2 3 5.02 93.51 0.50 180.0 8 2 3 38.11 56.03 0.18 180.0 1 3 3 93973.73 539.59 293.18 180.0 3 3 3 32051.13 279.86 189.38 180.0 5 3 3 7708.47 166.37 90.38 180.0 7 3 3 1091.74 47.28 32.78 180.0 0 4 3 291.45 19.61 17.29 0.0 2 4 3 162.01 19.70 13.83 0.0 4 4 3 26.17 72.39 7.14 0.0 6 4 3 45.09 102.49 2.35 0.0 1 5 3 37.73 62.84 10.60 0.0 3 5 3 401.72 27.51 19.43 0.0 5 5 3 432.40 35.98 19.35 0.0 7 5 3 111.90 47.23 11.44 0.0 0 6 3 376.29 30.86 11.98 0.0 2 6 3 42.81 81.56 8.56 0.0 4 6 3 0.00 94.44 3.48 0.0 6 6 3 0.00 120.64 0.85 0.0 1 7 3 43893.86 444.83 206.43 180.0 3 7 3 19318.20 293.83 141.31 180.0 5 7 3 5170.95 140.93 68.78 180.0 7 7 3 738.21 61.03 24.31 180.0 0 8 3 421.33 42.70 20.06 0.0 2 8 3 324.34 40.91 17.34 0.0 4 8 3 104.57 124.07 11.12 0.0 6 8 3 0.00 152.56 5.24 0.0 1 9 3 366.00 44.81 18.94 180.0 3 9 3 156.86 47.59 9.88 180.0 5 9 3 63.96 67.79 1.84 180.0 0 10 3 79.59 142.48 4.02 180.0 2 10 3 0.00 148.99 3.27 180.0 4 10 3 0.00 160.36 1.97 180.0 1 11 3 2562.00 87.90 47.67 180.0 3 11 3 1071.90 65.23 32.70 180.0 0 12 3 8.54 169.26 0.40 0.0 2 12 3 0.00 179.36 0.08 0.0 1 13 3 2277.98 79.92 47.47 180.0 0 0 4 126597.65 616.76 366.10 180.0 2 0 4 69732.27 396.86 280.72 180.0 4 0 4 18274.76 195.75 148.07 180.0 6 0 4 3186.38 90.32 60.20 180.0 8 0 4 499.01 45.48 19.20 180.0 1 1 4 50910.13 297.81 214.80 0.0 3 1 4 14854.72 158.10 136.18 0.0 5 1 4 3530.40 116.66 67.59 0.0 7 1 4 689.88 39.55 26.16 0.0 0 2 4 20888.71 162.79 135.96 180.0 2 2 4 8951.48 115.45 99.83 180.0 4 2 4 1656.88 46.81 44.35 180.0 6 2 4 54.80 96.96 11.29 180.0 8 2 4 0.00 73.90 0.31 180.0 1 3 4 17433.23 167.35 126.34 180.0 3 3 4 6108.61 119.73 82.35 180.0 5 3 4 1575.01 51.24 40.62 180.0 7 3 4 75.90 123.08 15.52 180.0 0 4 4 50973.57 368.45 218.80 180.0 2 4 4 29880.71 267.99 172.70 180.0 4 4 4 7268.79 155.76 90.52 180.0 6 4 4 1255.21 43.29 33.18 180.0 1 5 4 4.13 60.17 3.98 180.0 3 5 4 9.72 71.60 1.74 0.0 5 5 4 20.21 97.74 3.12 0.0 7 5 4 77.72 125.84 1.66 0.0 0 6 4 25342.36 292.15 155.30 180.0 2 6 4 15989.43 230.36 125.09 180.0 4 6 4 4547.43 112.31 67.86 180.0 6 6 4 771.49 47.97 26.03 180.0 1 7 4 4444.03 146.61 63.15 0.0 3 7 4 1833.05 56.58 43.26 0.0 5 7 4 535.53 45.78 21.90 0.0 0 8 4 14145.62 269.74 115.22 180.0 2 8 4 8386.27 213.93 92.71 180.0 4 8 4 2258.35 71.37 49.37 180.0 6 8 4 360.40 54.98 17.93 180.0 1 9 4 4455.77 139.86 66.03 180.0 3 9 4 2497.09 76.77 49.66 180.0 5 9 4 840.88 57.59 28.14 180.0 0 10 4 7104.49 241.21 87.20 180.0 2 10 4 4733.69 129.78 71.67 180.0 4 10 4 1608.49 67.40 39.77 180.0 1 11 4 5106.84 164.65 74.33 0.0 3 11 4 2547.90 80.99 53.97 0.0 0 12 4 1664.19 70.97 41.95 180.0 2 12 4 1142.35 68.14 34.28 180.0 1 13 4 994.98 73.37 33.11 180.0 1 1 5 51906.91 310.43 215.71 180.0 3 1 5 13601.72 153.70 128.49 180.0 5 1 5 2500.11 70.88 54.96 180.0 7 1 5 455.06 38.73 17.74 180.0 0 2 5 9747.30 108.47 93.86 180.0 2 2 5 5208.26 90.97 73.94 180.0 4 2 5 1380.53 46.59 40.73 180.0 6 2 5 202.32 33.80 17.04 180.0 1 3 5 478.64 16.38 22.12 180.0 3 3 5 27.10 59.02 8.78 180.0 5 3 5 0.00 84.16 2.26 0.0 7 3 5 54.09 115.23 4.51 0.0 0 4 5 11204.49 148.72 103.63 0.0 2 4 5 7663.35 134.04 87.25 0.0 4 4 5 3018.77 82.34 53.88 0.0 6 4 5 732.72 41.22 24.97 0.0 1 5 5 43422.95 357.24 203.82 180.0 3 5 5 19053.04 242.65 138.75 180.0 5 5 5 4414.87 111.49 68.20 180.0 7 5 5 707.20 50.02 24.83 180.0 0 6 5 15762.77 225.02 121.47 180.0 2 6 5 11119.81 193.20 102.46 180.0 4 6 5 4087.94 107.13 63.32 180.0 6 6 5 989.79 49.88 29.78 180.0 1 7 5 0.00 87.01 7.51 180.0 3 7 5 32.26 93.84 2.14 180.0 5 7 5 0.00 120.46 2.23 0.0 0 8 5 6779.58 196.54 83.73 0.0 2 8 5 5275.07 177.97 71.31 0.0 4 8 5 2067.83 69.81 45.14 0.0 6 8 5 413.69 57.34 22.01 0.0 1 9 5 6083.13 149.13 77.81 180.0 3 9 5 2947.97 100.49 53.50 180.0 5 9 5 644.65 56.98 25.51 180.0 0 10 5 1744.37 60.32 41.79 180.0 2 10 5 1206.77 58.09 35.64 180.0 4 10 5 481.43 57.07 22.42 180.0 1 11 5 1949.13 67.36 46.61 180.0 3 11 5 984.04 64.41 30.79 180.0 0 12 5 26.58 174.07 8.65 180.0 2 12 5 81.36 104.25 7.18 180.0 1 13 5 716.30 70.42 27.75 180.0 0 0 6 72370.73 397.34 265.88 0.0 2 0 6 42273.29 283.89 210.71 0.0 4 0 6 11345.29 161.60 118.58 0.0 6 0 6 2757.15 87.24 52.53 0.0 1 1 6 413.21 14.35 19.49 180.0 3 1 6 418.24 18.43 20.74 180.0 5 1 6 194.60 27.08 14.87 180.0 7 1 6 128.28 38.30 7.61 180.0 0 2 6 53761.39 336.42 217.39 180.0 2 2 6 30510.18 243.39 172.72 180.0 4 2 6 8123.74 145.49 97.63 180.0 6 2 6 1617.37 53.36 43.56 180.0 1 3 6 1247.12 41.63 34.76 0.0 3 3 6 387.30 22.36 20.75 0.0 5 3 6 87.04 30.59 9.00 0.0 7 3 6 41.50 66.67 3.23 0.0 0 4 6 16724.17 185.90 125.62 0.0 2 4 6 10469.82 155.64 101.33 0.0 4 4 6 3248.19 84.33 57.93 0.0 6 4 6 632.48 41.94 25.59 0.0 1 5 6 0.00 60.11 1.16 0.0 3 5 6 0.00 32.70 0.02 180.0 5 5 6 13.87 98.10 0.25 0.0 7 5 6 0.00 131.14 0.71 0.0 0 6 6 63.91 73.55 10.12 0.0 2 6 6 25.66 78.23 8.07 0.0 4 6 6 7.91 92.96 4.20 0.0 6 6 6 64.10 120.46 1.32 0.0 1 7 6 416.02 33.47 18.54 180.0 3 7 6 159.65 34.52 12.79 180.0 5 7 6 80.96 113.50 6.38 180.0 0 8 6 3166.86 105.69 56.20 180.0 2 8 6 2407.40 80.77 47.43 180.0 4 8 6 861.29 47.34 28.98 180.0 6 8 6 164.74 54.94 13.01 180.0 1 9 6 704.46 46.27 25.78 180.0 3 9 6 244.32 45.32 16.34 180.0 5 9 6 0.00 147.93 7.12 180.0 0 10 6 3653.36 118.92 62.53 0.0 2 10 6 2764.12 92.36 53.44 0.0 4 10 6 1205.43 60.93 33.48 0.0 1 11 6 87.88 112.15 10.77 180.0 3 11 6 0.00 172.65 6.88 180.0 0 12 6 1741.07 74.00 42.23 180.0 2 12 6 1439.64 70.50 36.60 180.0 1 13 6 0.00 195.15 1.06 0.0 1 1 7 24976.46 196.72 152.92 0.0 3 1 7 6962.79 115.44 89.65 0.0 5 1 7 1044.94 34.51 35.04 0.0 7 1 7 0.30 112.84 9.13 0.0 0 2 7 4679.83 84.96 67.40 0.0 2 2 7 3410.17 85.82 57.58 0.0 4 2 7 1202.44 37.34 36.30 0.0 6 2 7 313.42 34.70 16.80 0.0 1 3 7 35324.82 276.10 178.10 0.0 3 3 7 12338.28 171.89 114.87 0.0 5 3 7 2657.14 87.25 52.88 0.0 7 3 7 361.96 43.12 18.24 0.0 0 4 7 25278.34 238.98 151.80 180.0 2 4 7 17047.03 201.32 125.51 180.0 4 4 7 5299.91 141.79 74.30 180.0 6 4 7 1058.12 44.77 33.01 180.0 1 5 7 1262.18 40.83 36.43 0.0 3 5 7 617.53 30.08 24.21 0.0 5 5 7 71.13 35.61 9.59 0.0 7 5 7 118.59 128.72 1.87 0.0 0 6 7 16659.74 228.19 127.63 0.0 2 6 7 12476.12 202.12 108.24 0.0 4 6 7 4783.62 160.89 67.77 0.0 6 6 7 1198.93 51.42 32.28 0.0 1 7 7 7804.88 178.82 87.80 0.0 3 7 7 3523.44 106.52 59.72 0.0 5 7 7 905.47 47.79 27.51 0.0 0 8 7 11625.52 235.11 110.73 180.0 2 8 7 8293.00 211.85 94.18 180.0 4 8 7 3200.53 98.39 58.90 180.0 6 8 7 743.81 58.19 27.79 180.0 1 9 7 4202.72 125.83 69.21 0.0 3 9 7 2055.95 65.15 46.54 0.0 5 9 7 438.81 55.04 21.74 0.0 0 10 7 847.80 54.06 30.96 0.0 2 10 7 746.53 52.48 26.64 0.0 4 10 7 361.14 55.37 17.26 0.0 1 11 7 2307.51 74.54 48.73 0.0 3 11 7 915.41 64.20 32.56 0.0 0 12 7 0.00 177.66 0.74 0.0 2 12 7 48.29 175.73 0.97 0.0 1 13 7 855.61 72.70 32.52 0.0 0 0 8 757.69 25.86 27.88 0.0 2 0 8 404.54 17.52 19.71 0.0 4 0 8 25.30 23.11 4.95 0.0 6 0 8 0.00 94.41 2.82 180.0 1 1 8 5757.52 93.34 77.24 180.0 3 1 8 3020.55 86.59 57.29 180.0 5 1 8 954.22 33.57 31.12 180.0 7 1 8 118.02 41.63 12.23 180.0 0 2 8 74867.15 457.36 265.18 0.0 2 2 8 49190.61 352.88 215.40 0.0 4 2 8 13007.41 189.73 121.24 0.0 6 2 8 2365.31 74.67 49.38 0.0 1 3 8 42.00 18.46 8.91 0.0 3 3 8 195.64 23.96 14.76 0.0 5 3 8 156.43 31.83 12.13 0.0 7 3 8 7.15 60.11 5.80 0.0 0 4 8 10824.00 155.56 103.75 0.0 2 4 8 6619.24 133.09 80.58 0.0 4 4 8 1503.42 45.51 38.68 0.0 6 4 8 0.00 116.54 11.04 0.0 1 5 8 418.95 25.30 19.92 180.0 3 5 8 155.23 29.32 13.45 180.0 5 5 8 120.69 35.85 6.38 180.0 7 5 8 0.00 139.52 2.09 180.0 0 6 8 21391.51 261.51 140.44 0.0 2 6 8 13687.89 216.01 112.85 0.0 4 6 8 3834.47 105.51 60.41 0.0 6 6 8 583.11 48.63 22.53 0.0 1 7 8 175.08 32.59 14.42 180.0 3 7 8 24.80 106.95 12.34 180.0 5 7 8 119.33 123.79 8.07 180.0 0 8 8 18523.20 291.66 137.95 0.0 2 8 8 12670.65 253.59 114.02 0.0 4 8 8 4333.68 128.33 65.26 0.0 6 8 8 971.84 59.68 26.57 0.0 1 9 8 1542.33 51.15 40.48 0.0 3 9 8 872.52 50.88 29.98 0.0 5 9 8 0.00 166.86 16.89 0.0 0 10 8 64.49 141.83 10.99 0.0 2 10 8 14.05 96.44 7.02 0.0 4 10 8 0.08 146.45 0.09 0.0 1 11 8 1599.82 65.62 42.78 180.0 3 11 8 931.96 62.26 31.65 180.0 0 12 8 5490.07 187.07 81.19 0.0 2 12 8 4197.93 125.53 68.38 0.0 1 1 9 24615.70 211.29 153.49 0.0 3 1 9 9787.38 148.62 101.84 0.0 5 1 9 2235.77 65.86 48.30 0.0 7 1 9 339.03 42.84 17.00 0.0 0 2 9 166.65 17.79 13.53 180.0 2 2 9 201.63 19.76 14.19 180.0 4 2 9 137.51 26.14 12.43 180.0 6 2 9 39.52 103.89 7.72 180.0 1 3 9 405.49 20.64 19.62 180.0 3 3 9 412.33 25.69 20.01 180.0 5 3 9 286.10 33.07 16.74 180.0 7 3 9 14.66 126.82 9.97 180.0 0 4 9 7326.16 133.91 78.82 0.0 2 4 9 4558.77 116.64 63.34 0.0 4 4 9 1186.97 37.60 35.55 0.0 6 4 9 299.99 39.82 15.42 0.0 1 5 9 40135.51 353.77 194.05 0.0 3 5 9 19111.41 253.63 134.75 0.0 5 5 9 4472.86 119.23 67.34 0.0 0 6 9 791.82 33.00 29.76 180.0 2 6 9 619.46 32.75 25.03 180.0 4 6 9 252.18 37.18 15.08 180.0 6 6 9 59.96 130.75 6.51 180.0 1 7 9 0.00 92.36 1.84 0.0 3 7 9 31.84 36.21 3.78 180.0 5 7 9 0.00 124.37 6.15 180.0 0 8 9 0.00 107.52 9.41 180.0 2 8 9 33.16 111.99 7.26 180.0 4 8 9 36.29 72.57 3.86 180.0 1 9 9 6336.99 206.67 80.55 0.0 3 9 9 2944.18 101.46 55.92 0.0 5 9 9 755.09 58.80 27.09 0.0 0 10 9 59.23 77.44 4.37 0.0 2 10 9 0.00 134.04 4.02 0.0 4 10 9 44.90 159.30 3.03 0.0 1 11 9 583.01 57.74 24.11 0.0 3 11 9 300.04 58.03 16.17 0.0 0 12 9 77.14 101.74 3.91 0.0 2 12 9 0.00 177.97 3.25 0.0 0 0 10 2056.08 68.47 44.47 180.0 2 0 10 1421.76 41.32 38.57 180.0 4 0 10 597.07 28.99 25.33 180.0 6 0 10 179.11 36.76 12.71 180.0 1 1 10 28223.32 239.94 163.66 0.0 3 1 10 12860.14 176.20 113.99 0.0 5 1 10 3180.13 93.34 59.20 0.0 7 1 10 582.28 46.33 23.43 0.0 0 2 10 3817.74 92.29 54.74 0.0 2 2 10 2252.04 59.90 43.41 0.0 4 2 10 527.93 29.29 24.08 0.0 6 2 10 108.97 37.06 10.77 0.0 1 3 10 11907.84 163.00 103.20 180.0 3 3 10 5524.47 131.56 72.33 180.0 5 3 10 1467.00 49.41 37.70 180.0 7 3 10 271.27 44.63 14.85 180.0 0 4 10 2862.18 70.12 50.36 180.0 2 4 10 1913.96 54.16 40.44 180.0 4 4 10 496.50 33.71 22.32 180.0 6 4 10 58.85 82.74 9.34 180.0 1 5 10 524.51 28.96 22.41 0.0 3 5 10 219.27 32.25 16.00 0.0 5 5 10 58.05 110.03 8.08 0.0 0 6 10 325.41 30.59 14.20 180.0 2 6 10 67.71 84.80 10.41 180.0 4 6 10 0.00 109.81 4.03 180.0 6 6 10 55.39 138.73 0.47 180.0 1 7 10 4359.81 105.76 62.67 0.0 3 7 10 1931.80 59.82 44.25 0.0 5 7 10 464.18 47.69 22.82 0.0 0 8 10 97.31 38.84 8.92 180.0 2 8 10 58.81 107.94 7.23 180.0 4 8 10 13.85 125.36 4.09 180.0 1 9 10 2847.03 84.43 54.59 180.0 3 9 10 1667.46 56.32 40.16 180.0 5 9 10 547.97 59.22 22.02 180.0 0 10 10 83.13 48.28 6.05 180.0 2 10 10 0.00 145.63 5.20 180.0 4 10 10 54.22 155.16 3.17 180.0 1 11 10 2611.11 82.68 54.27 0.0 3 11 10 1498.58 67.30 39.71 0.0 0 12 10 0.00 185.81 10.32 0.0 2 12 10 0.00 186.72 8.64 0.0 1 1 11 18993.01 198.24 136.24 180.0 3 1 11 7858.78 147.17 89.64 180.0 5 1 11 1771.41 56.93 40.64 180.0 7 1 11 238.96 45.50 12.91 180.0 0 2 11 973.98 31.25 32.82 180.0 2 2 11 734.69 25.09 26.92 180.0 4 2 11 285.83 29.53 15.23 180.0 6 2 11 0.00 113.66 6.07 180.0 1 3 11 814.10 26.12 26.96 180.0 3 3 11 199.60 26.81 13.67 180.0 5 3 11 0.00 93.17 2.42 180.0 7 3 11 0.00 134.86 1.06 0.0 0 4 11 4760.16 123.04 65.77 0.0 2 4 11 3269.53 82.11 56.41 0.0 4 4 11 1301.86 41.11 35.50 0.0 6 4 11 328.04 41.75 16.35 0.0 1 5 11 29279.70 306.61 165.65 180.0 3 5 11 14170.73 227.94 115.53 180.0 5 5 11 3649.72 116.07 57.66 180.0 0 6 11 5831.76 152.81 74.37 180.0 2 6 11 4357.22 144.01 63.51 180.0 4 6 11 1830.94 61.68 40.37 180.0 6 6 11 515.03 50.41 19.64 180.0 1 7 11 438.31 37.16 19.53 0.0 3 7 11 235.55 40.18 18.22 0.0 5 7 11 130.03 47.83 14.02 0.0 0 8 11 5358.88 178.89 75.34 0.0 2 8 11 4086.08 121.26 63.77 0.0 4 8 11 1592.34 54.86 39.47 0.0 1 9 11 8082.14 238.12 96.53 180.0 3 9 11 4348.86 141.68 68.15 180.0 0 10 11 0.00 147.84 2.59 180.0 2 10 11 0.00 142.97 3.40 180.0 4 10 11 0.00 163.15 4.21 180.0 1 11 11 1057.84 63.23 35.44 180.0 3 11 11 492.53 63.73 23.80 180.0 0 12 11 76.43 180.42 8.38 0.0 0 0 12 56.40 19.94 7.43 180.0 2 0 12 9.82 62.68 0.30 0.0 4 0 12 181.84 29.22 10.80 0.0 6 0 12 136.65 40.18 11.67 0.0 1 1 12 2401.71 62.13 47.13 180.0 3 1 12 1363.71 45.30 35.64 180.0 5 1 12 404.76 36.04 20.45 180.0 7 1 12 0.00 135.77 9.08 180.0 0 2 12 55161.49 404.59 235.13 180.0 2 2 12 38760.09 331.79 194.32 180.0 4 2 12 12605.41 209.91 112.48 180.0 6 2 12 2433.63 76.29 47.45 180.0 1 3 12 1992.70 64.59 44.10 0.0 3 3 12 967.06 31.91 31.12 0.0 5 3 12 285.41 35.97 16.30 0.0 0 4 12 3411.34 114.06 57.58 180.0 2 4 12 2055.65 61.80 44.92 180.0 4 4 12 400.49 35.92 20.97 180.0 6 4 12 79.75 42.32 4.99 180.0 1 5 12 39.74 28.89 6.54 180.0 3 5 12 51.10 91.87 5.32 180.0 5 5 12 0.00 115.26 3.44 180.0 0 6 12 9332.55 191.86 95.42 180.0 2 6 12 6552.24 175.20 78.38 180.0 4 6 12 1993.98 64.59 43.83 180.0 6 6 12 288.93 51.04 16.96 180.0 1 7 12 0.00 102.07 6.93 0.0 3 7 12 0.00 118.59 4.46 0.0 5 7 12 73.31 132.77 1.99 0.0 0 8 12 7765.30 214.24 91.11 180.0 2 8 12 5492.18 138.62 76.05 180.0 4 8 12 2067.48 69.86 44.40 180.0 1 9 12 107.68 46.68 12.20 0.0 3 9 12 0.00 141.98 9.22 0.0 0 10 12 206.06 51.16 14.99 180.0 2 10 12 0.00 148.93 10.65 180.0 1 11 12 208.00 57.09 12.96 180.0 1 1 13 6728.08 133.73 81.50 180.0 3 1 13 3103.85 83.27 55.34 180.0 5 1 13 730.77 39.49 26.36 180.0 0 2 13 6835.02 134.19 80.06 0.0 2 2 13 4506.05 125.34 67.46 0.0 4 2 13 1856.49 58.11 41.68 0.0 6 2 13 460.61 44.45 19.79 0.0 1 3 13 1876.85 55.07 42.60 180.0 3 3 13 728.14 32.63 27.17 180.0 5 3 13 167.70 37.00 10.56 180.0 0 4 13 9718.28 173.93 95.95 180.0 2 4 13 7158.98 161.49 82.87 180.0 4 4 13 2937.27 97.51 53.63 180.0 6 4 13 660.75 47.09 26.23 180.0 1 5 13 4132.79 135.15 62.63 180.0 3 5 13 1751.79 55.48 41.50 180.0 5 5 13 362.37 44.17 18.55 180.0 0 6 13 6990.23 174.43 82.12 0.0 2 6 13 5467.26 168.47 70.50 0.0 4 6 13 2301.87 74.50 44.78 0.0 1 7 13 3172.69 105.75 56.72 180.0 3 7 13 1513.05 49.44 38.72 180.0 5 7 13 304.01 51.28 18.72 180.0 0 8 13 2804.93 92.42 53.48 180.0 2 8 13 2148.57 68.60 45.34 180.0 4 8 13 818.91 52.99 27.82 180.0 1 9 13 1134.15 53.79 36.20 180.0 3 9 13 612.33 52.71 23.73 180.0 0 10 13 96.18 110.13 16.93 0.0 2 10 13 213.10 53.94 14.70 0.0 1 11 13 418.49 60.61 22.25 180.0 0 0 14 7789.98 145.03 87.83 180.0 2 0 14 5953.23 136.70 75.31 180.0 4 0 14 2212.10 72.22 47.85 180.0 6 0 14 607.57 45.63 22.62 180.0 1 1 14 1308.17 44.42 36.84 180.0 3 1 14 736.53 33.29 26.63 180.0 5 1 14 108.05 114.21 13.78 180.0 0 2 14 11079.22 173.95 104.77 0.0 2 2 14 8294.42 160.47 87.93 0.0 4 2 14 2884.51 96.42 53.07 0.0 6 2 14 588.13 47.90 23.67 0.0 1 3 14 330.02 28.02 17.36 0.0 3 3 14 253.51 31.44 14.51 0.0 5 3 14 0.00 109.88 8.98 0.0 0 4 14 1362.32 45.99 35.66 180.0 2 4 14 955.18 35.02 30.32 180.0 4 4 14 385.22 37.37 18.99 180.0 6 4 14 72.01 126.64 8.95 180.0 1 5 14 422.21 35.16 21.99 180.0 3 5 14 184.31 36.70 15.16 180.0 5 5 14 62.49 88.24 7.44 180.0 0 6 14 349.97 37.79 16.66 180.0 2 6 14 217.56 38.67 13.86 180.0 4 6 14 25.71 120.46 8.29 180.0 1 7 14 250.90 41.18 18.55 180.0 3 7 14 134.19 42.69 13.58 180.0 5 7 14 58.38 146.45 7.34 180.0 0 8 14 2784.37 82.61 55.82 0.0 2 8 14 2143.45 71.45 47.47 0.0 4 8 14 911.16 55.38 29.46 0.0 1 9 14 344.69 50.23 20.75 0.0 3 9 14 239.50 52.92 15.55 0.0 0 10 14 1208.90 59.84 33.67 180.0 2 10 14 732.26 60.38 29.34 180.0 1 1 15 5492.11 136.63 75.32 0.0 3 1 15 2990.99 90.21 52.06 0.0 5 1 15 673.29 44.03 24.82 0.0 0 2 15 3278.11 81.95 57.64 180.0 2 2 15 2343.30 66.86 48.43 180.0 4 2 15 850.16 40.13 29.55 180.0 6 2 15 70.55 133.12 13.65 180.0 1 3 15 360.97 30.47 20.04 0.0 3 3 15 147.84 33.19 10.84 0.0 5 3 15 0.00 111.11 2.49 0.0 0 4 15 1907.97 56.97 41.78 0.0 2 4 15 1421.64 45.17 36.03 0.0 4 4 15 547.96 40.09 23.29 0.0 1 5 15 17345.42 260.93 130.42 0.0 3 5 15 8439.96 204.33 91.01 0.0 5 5 15 2313.00 79.01 45.22 0.0 0 6 15 1556.41 52.23 37.52 180.0 2 6 15 1035.96 44.10 31.71 180.0 4 6 15 364.07 46.20 19.16 180.0 1 7 15 0.00 118.04 3.63 180.0 3 7 15 58.32 89.12 6.71 180.0 0 8 15 47.30 92.12 8.17 0.0 2 8 15 0.00 132.14 6.88 0.0 4 8 15 8.95 148.44 4.03 0.0 1 9 15 3809.06 114.07 63.43 0.0 3 9 15 2031.29 66.13 45.06 0.0 0 10 15 148.76 160.94 10.12 180.0 0 0 16 2569.76 81.65 52.02 0.0 2 0 16 1681.72 55.69 41.56 0.0 4 0 16 504.26 39.03 20.61 0.0 1 1 16 9649.52 183.29 99.17 0.0 3 1 16 5405.25 158.09 71.81 0.0 5 1 16 1528.31 50.59 38.54 0.0 0 2 16 12004.12 198.22 108.92 0.0 2 2 16 8490.42 177.47 89.51 0.0 4 2 16 2753.16 86.24 50.56 0.0 1 3 16 2045.76 68.22 47.36 180.0 3 3 16 1422.00 48.77 36.17 180.0 5 3 16 433.64 46.29 20.71 180.0 0 4 16 4828.13 151.97 71.04 0.0 2 4 16 3243.63 97.03 58.12 0.0 4 4 16 1080.05 44.80 31.96 0.0 1 5 16 31.33 108.86 13.95 0.0 3 5 16 0.00 115.20 10.08 0.0 5 5 16 95.37 126.87 5.43 0.0 0 6 16 3749.74 116.56 60.26 0.0 2 6 16 2554.75 75.55 49.46 0.0 4 6 16 784.06 50.72 27.44 0.0 1 7 16 74.79 120.58 2.68 0.0 3 7 16 42.33 122.03 3.01 0.0 0 8 16 2133.72 68.27 49.29 0.0 2 8 16 1583.78 55.74 40.26 0.0 1 9 16 1920.09 63.71 45.00 180.0 1 1 17 1575.35 50.18 40.35 0.0 3 1 17 632.61 39.61 25.63 0.0 5 1 17 64.17 132.30 10.50 0.0 0 2 17 1899.28 57.48 42.50 180.0 2 2 17 1273.14 41.08 35.85 180.0 4 2 17 531.28 43.91 22.01 180.0 1 3 17 7097.96 172.18 85.46 0.0 3 3 17 3856.01 110.00 60.36 0.0 5 3 17 1154.77 52.06 30.44 0.0 0 4 17 1459.67 47.78 39.87 0.0 2 4 17 1027.38 40.78 34.43 0.0 4 4 17 503.30 44.63 22.30 0.0 1 5 17 1203.29 43.59 36.08 180.0 3 5 17 642.32 45.37 28.25 180.0 0 6 17 1079.99 46.40 31.77 180.0 2 6 17 799.02 45.85 27.23 180.0 4 6 17 333.40 48.71 17.26 180.0 1 7 17 6492.05 151.81 80.95 0.0 3 7 17 3567.71 108.82 58.91 0.0 0 8 17 435.19 52.53 23.81 0.0 2 8 17 339.12 52.80 20.23 0.0 1 9 17 49.33 57.11 4.99 180.0 0 0 18 1192.55 41.63 35.59 0.0 2 0 18 958.91 40.92 31.98 0.0 4 0 18 547.77 44.81 22.58 0.0 1 1 18 4558.69 152.17 67.49 180.0 3 1 18 2506.60 83.03 49.78 180.0 5 1 18 817.14 50.72 27.78 180.0 0 2 18 3823.96 101.57 62.10 180.0 2 2 18 2960.28 100.35 52.96 180.0 4 2 18 1321.29 49.55 33.14 180.0 1 3 18 1177.69 41.41 35.23 0.0 3 3 18 655.53 43.64 26.43 0.0 0 4 18 627.08 39.71 28.20 0.0 2 4 18 577.65 41.00 24.28 0.0 4 4 18 73.59 128.70 15.66 0.0 1 5 18 29.79 78.11 0.32 180.0 3 5 18 0.00 121.91 0.05 180.0 0 6 18 0.00 126.03 4.13 180.0 2 6 18 0.00 128.36 3.57 180.0 1 7 18 85.54 93.90 9.37 180.0 3 7 18 0.00 147.87 7.46 180.0 0 8 18 333.20 51.86 19.77 180.0 1 1 19 1161.79 42.96 35.25 180.0 3 1 19 580.99 43.76 23.01 180.0 0 2 19 1716.33 57.84 43.67 0.0 2 2 19 1298.85 46.08 37.17 0.0 4 2 19 590.27 48.14 23.21 0.0 1 3 19 4162.15 115.06 64.21 180.0 3 3 19 2012.28 68.26 44.52 180.0 0 4 19 1451.15 49.98 37.92 180.0 2 4 19 1218.08 47.76 33.40 180.0 4 4 19 629.75 50.96 22.63 180.0 1 5 19 620.40 43.09 23.58 180.0 3 5 19 294.41 46.62 15.27 180.0 0 6 19 2342.36 80.72 49.95 0.0 2 6 19 1832.34 63.37 42.75 0.0 1 7 19 1149.92 55.36 34.56 180.0 0 0 20 9470.63 216.12 100.63 180.0 2 0 20 7270.24 200.47 84.30 180.0 4 0 20 2795.32 87.65 49.61 180.0 1 1 20 423.16 41.58 22.50 180.0 3 1 20 252.01 44.32 16.34 180.0 0 2 20 20.52 113.81 4.07 180.0 2 2 20 47.81 84.67 2.10 180.0 1 3 20 95.23 119.81 14.79 0.0 3 3 20 0.00 134.56 10.48 0.0 0 4 20 4674.75 127.70 71.64 180.0 2 4 20 3754.32 122.44 59.85 180.0 1 5 20 29.62 43.62 3.53 0.0 0 6 20 1892.98 60.78 45.09 180.0 2 6 20 1250.72 55.49 36.78 180.0 1 1 21 19.72 87.67 12.27 180.0 3 1 21 0.00 132.81 7.65 180.0 0 2 21 437.82 43.12 19.78 180.0 2 2 21 254.02 45.17 16.71 180.0 1 3 21 3058.61 95.19 58.97 180.0 0 4 21 774.05 48.90 27.42 0.0 2 4 21 641.51 49.81 23.77 0.0 1 5 21 178.62 47.26 15.21 0.0 0 0 22 49.71 88.49 5.69 0.0 2 0 22 0.00 129.20 5.01 0.0 1 1 22 2194.15 70.75 47.50 0.0 0 2 22 6.76 124.45 1.00 0.0 2 2 22 24.51 127.99 0.82 0.0 1 3 22 926.65 51.97 32.64 180.0 0 4 22 0.00 140.04 7.51 0.0