#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/21/2202180.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202180_Fobs loop_ _publ_author_name 'Duggan, Peter J.' 'Humphrey, David G.' 'Price, David J.' 'Tyndall, Edward M.' _publ_section_title ; 1,6-Dibenzoyloxy-2:4,3:5-O^2^:O^4^,O^3^:O^5^-bis(phenylboronoyloxy)-D-mannitol ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o372 _journal_page_last o373 _journal_volume 59 _journal_year 2003 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 5.9646 _cell_length_b 18.0749 _cell_length_c 25.8911 _exptl_crystal_F_000 1176.00 _reflns_d_resolution_high 0.7475 _[local]_cod_data_source_file tk6093Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' et0197b in P 21 21 21' _shelx_refln_list_code 4 _shelx_f_calc_maximum 211.23 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1705.87 1738.91 33.36 o 4 0 0 79.33 75.40 14.50 o 6 0 0 527.74 517.13 36.68 o 1 1 0 828.30 777.53 25.21 o 2 1 0 147.33 132.41 10.35 o 3 1 0 230.14 254.35 20.59 o 4 1 0 445.09 435.63 13.68 o 5 1 0 3.85 9.21 12.00 o 6 1 0 1.72 -20.33 20.33 o 7 1 0 38.96 236.29 165.20 o 1 2 0 43.34 49.53 10.55 o 2 2 0 3313.92 3210.68 42.78 o 3 2 0 781.35 795.93 17.72 o 4 2 0 302.84 317.95 14.31 o 5 2 0 40.78 55.99 9.38 o 6 2 0 14.60 14.67 54.50 o 7 2 0 95.04 99.30 99.98 o 1 3 0 10510.15 9974.28 141.27 o 2 3 0 476.28 460.31 16.94 o 3 3 0 1267.87 1291.25 37.53 o 4 3 0 3.20 20.36 20.51 o 5 3 0 39.36 50.47 23.24 o 6 3 0 0.28 -23.48 28.37 o 7 3 0 243.85 485.41 225.35 o 0 4 0 44617.91 40534.66 906.50 o 1 4 0 11606.08 11014.12 145.52 o 2 4 0 343.43 387.24 17.25 o 3 4 0 123.40 168.89 15.50 o 4 4 0 81.82 73.25 16.14 o 5 4 0 174.60 256.78 154.37 o 6 4 0 35.85 -15.00 31.46 o 7 4 0 0.91 258.21 207.77 o 1 5 0 5172.02 4821.60 74.53 o 2 5 0 26.82 33.32 6.22 o 3 5 0 350.52 321.93 21.51 o 4 5 0 14.10 17.60 19.93 o 5 5 0 130.62 83.59 49.07 o 6 5 0 101.26 113.37 39.43 o 7 5 0 0.99 -59.85 80.80 o 0 6 0 3891.96 3850.40 79.54 o 1 6 0 4170.46 4104.86 60.36 o 2 6 0 449.79 418.72 13.64 o 3 6 0 44.00 67.87 21.99 o 4 6 0 84.94 100.89 25.33 o 5 6 0 121.57 151.13 42.74 o 6 6 0 13.61 5.05 49.69 o 7 6 0 3.77 20.01 121.70 o 1 7 0 940.11 939.12 21.97 o 2 7 0 0.18 -0.02 7.35 o 3 7 0 932.75 885.93 33.15 o 4 7 0 299.19 319.64 38.82 o 5 7 0 225.74 299.95 38.34 o 6 7 0 415.74 394.24 85.30 o 7 7 0 0.54 96.14 95.32 o 0 8 0 503.32 453.43 37.54 o 1 8 0 1366.04 1405.20 34.59 o 2 8 0 1135.33 1109.49 24.31 o 3 8 0 8.27 23.39 8.20 o 4 8 0 972.05 962.21 40.07 o 5 8 0 286.51 374.18 53.02 o 6 8 0 110.41 66.18 50.55 o 7 8 0 10.58 -65.42 84.90 o 1 9 0 30.60 32.25 11.96 o 2 9 0 571.76 623.94 18.37 o 3 9 0 7.05 16.52 11.21 o 4 9 0 134.72 153.70 29.80 o 5 9 0 110.82 134.33 49.05 o 6 9 0 138.40 147.69 97.84 o 7 9 0 138.88 101.27 83.31 o 0 10 0 6130.12 5973.78 123.64 o 1 10 0 72.89 53.79 14.65 o 2 10 0 500.63 564.28 19.76 o 3 10 0 215.53 198.80 13.50 o 4 10 0 1211.15 1306.51 56.97 o 5 10 0 48.84 -8.26 35.26 o 6 10 0 339.06 356.37 77.60 o 7 10 0 231.72 216.36 85.03 o 1 11 0 101.89 120.95 16.76 o 2 11 0 1361.09 1354.67 30.44 o 3 11 0 335.60 370.85 19.32 o 4 11 0 362.61 354.54 37.89 o 5 11 0 8.46 75.60 46.16 o 6 11 0 249.11 159.55 87.78 o 7 11 0 57.54 -25.32 89.74 o 0 12 0 1295.02 1282.14 53.04 o 1 12 0 125.23 131.99 17.93 o 2 12 0 6.54 7.81 17.73 o 3 12 0 1450.82 1494.53 63.53 o 4 12 0 49.25 -11.61 45.25 o 5 12 0 20.19 136.25 64.20 o 6 12 0 288.54 339.97 94.05 o 1 13 0 0.16 -13.14 20.35 o 2 13 0 170.64 151.95 22.48 o 3 13 0 1150.89 1144.29 35.37 o 4 13 0 248.96 296.09 89.53 o 5 13 0 62.65 5.98 50.73 o 6 13 0 1.06 44.44 79.51 o 0 14 0 311.97 272.09 44.42 o 1 14 0 333.72 308.27 25.27 o 2 14 0 154.87 212.16 24.23 o 3 14 0 1046.37 980.35 33.51 o 4 14 0 194.81 104.59 28.72 o 5 14 0 69.60 107.05 91.66 o 6 14 0 80.65 187.10 91.69 o 1 15 0 242.31 245.70 34.49 o 2 15 0 74.21 81.81 28.47 o 3 15 0 209.26 213.46 31.26 o 4 15 0 6.08 18.78 57.04 o 5 15 0 66.87 -57.80 58.58 o 6 15 0 94.15 118.68 66.15 o 0 16 0 135.11 253.27 58.68 o 1 16 0 193.82 198.19 34.10 o 2 16 0 21.99 38.38 26.45 o 3 16 0 2.66 52.47 30.79 o 4 16 0 196.02 110.00 82.63 o 5 16 0 96.27 207.32 83.24 o 1 17 0 396.30 413.56 39.13 o 2 17 0 114.96 88.31 30.17 o 3 17 0 80.65 93.33 37.53 o 4 17 0 6.50 36.94 73.13 o 5 17 0 0.04 -79.66 87.57 o 0 18 0 0.00 -27.35 44.47 o 1 18 0 2.82 -42.67 45.17 o 2 18 0 245.51 153.66 48.04 o 3 18 0 261.14 264.47 61.51 o 4 18 0 0.25 153.29 86.20 o 5 18 0 3.05 -51.10 51.10 o 1 19 0 9.18 8.12 48.48 o 2 19 0 0.67 26.53 49.11 o 3 19 0 225.56 108.78 76.68 o 4 19 0 229.19 47.69 97.28 o 0 20 0 448.83 427.74 99.37 o 1 20 0 3.50 47.04 44.45 o 2 20 0 22.68 31.70 49.80 o 3 20 0 2.05 46.74 177.00 o 4 20 0 85.57 123.05 209.45 o 1 21 0 0.65 54.31 67.14 o 2 21 0 29.88 17.42 72.53 o 3 21 0 59.77 243.26 112.91 o 0 22 0 0.41 -101.98 110.01 o 1 22 0 64.80 132.31 68.05 o 2 22 0 203.62 504.26 221.71 o 3 22 0 18.54 -138.42 138.42 o 1 23 0 0.01 88.36 82.29 o 2 23 0 5.49 -40.95 90.68 o 0 24 0 118.68 15.50 106.70 o 1 0 1 305.78 281.07 7.70 o 2 0 1 1920.53 1912.97 25.90 o 3 0 1 8296.75 8617.54 111.53 o 4 0 1 50.65 32.71 9.03 o 5 0 1 125.45 134.27 13.59 o 6 0 1 24.27 20.16 19.82 o 7 0 1 6.34 203.96 365.33 o 1 1 1 426.99 346.20 8.67 o 2 1 1 1460.42 1510.61 15.35 o 3 1 1 2942.77 3052.09 30.90 o 4 1 1 492.21 506.02 13.29 o 5 1 1 58.13 75.77 9.13 o 6 1 1 27.99 22.63 27.43 o 7 1 1 2.73 -46.47 79.07 o 0 2 1 1.62 2.13 4.29 o 1 2 1 2843.50 2726.91 28.00 o 2 2 1 2104.17 2020.41 21.21 o 3 2 1 2272.68 2412.60 24.81 o 4 2 1 795.91 840.39 13.26 o 5 2 1 259.00 292.68 18.49 o 6 2 1 215.50 215.63 54.68 o 7 2 1 152.68 188.73 81.62 o 0 3 1 3694.92 3647.21 83.74 o 1 3 1 6841.61 6577.73 67.23 o 2 3 1 2263.97 2209.08 34.21 o 3 3 1 718.63 744.40 16.79 o 4 3 1 807.73 773.61 22.86 o 5 3 1 106.49 133.18 17.96 o 6 3 1 423.28 364.36 36.16 o 7 3 1 64.51 177.50 104.84 o 0 4 1 9368.75 8812.71 131.78 o 1 4 1 474.41 491.54 9.02 o 2 4 1 255.79 251.90 6.41 o 3 4 1 2588.26 2786.78 37.60 o 4 4 1 567.54 588.91 20.34 o 5 4 1 91.87 172.46 109.53 o 6 4 1 208.88 212.02 38.60 o 7 4 1 139.73 279.25 121.20 o 0 5 1 970.34 1056.84 21.01 o 1 5 1 5498.69 5277.41 55.04 o 2 5 1 141.35 123.70 4.19 o 3 5 1 2241.53 2271.06 34.44 o 4 5 1 160.28 175.92 15.76 o 5 5 1 61.20 61.69 21.08 o 6 5 1 469.25 551.18 41.89 o 7 5 1 107.20 42.48 73.31 o 0 6 1 1247.56 1212.48 26.73 o 1 6 1 1869.36 1915.85 23.02 o 2 6 1 729.19 738.86 12.69 o 3 6 1 578.12 630.26 23.72 o 4 6 1 41.44 62.03 17.42 o 5 6 1 232.75 256.17 24.29 o 6 6 1 82.70 90.81 33.84 o 7 6 1 140.97 234.31 131.18 o 0 7 1 4102.73 4023.74 57.99 o 1 7 1 2702.47 2646.45 32.45 o 2 7 1 12.59 17.58 5.20 o 3 7 1 166.20 186.27 16.50 o 4 7 1 331.27 332.51 31.67 o 5 7 1 183.42 213.93 26.53 o 6 7 1 176.34 209.35 48.28 o 7 7 1 112.49 122.38 105.20 o 0 8 1 3.61 -9.71 9.71 o 1 8 1 1042.71 946.99 17.05 o 2 8 1 391.72 407.73 10.38 o 3 8 1 581.98 598.88 15.21 o 4 8 1 67.97 67.55 18.59 o 5 8 1 378.84 313.99 33.00 o 6 8 1 180.60 129.52 37.37 o 7 8 1 104.42 13.62 56.45 o 0 9 1 1.28 -3.58 8.85 o 1 9 1 1401.28 1402.16 25.60 o 2 9 1 129.81 110.73 8.45 o 3 9 1 533.80 590.28 11.79 o 4 9 1 1740.07 1718.80 40.16 o 5 9 1 652.56 661.54 43.51 o 6 9 1 20.37 44.44 48.03 o 7 9 1 234.83 159.07 46.95 o 0 10 1 1277.88 1276.37 30.23 o 1 10 1 337.14 326.33 13.26 o 2 10 1 1474.64 1506.21 21.89 o 3 10 1 1160.46 1122.87 17.36 o 4 10 1 1316.56 1339.91 43.92 o 5 10 1 136.39 230.40 43.83 o 6 10 1 110.11 105.81 49.25 o 7 10 1 239.65 130.02 55.91 o 0 11 1 14.45 25.41 17.39 o 1 11 1 612.44 615.32 16.49 o 2 11 1 212.95 210.82 12.17 o 3 11 1 837.24 846.77 22.48 o 4 11 1 370.19 323.29 32.16 o 5 11 1 37.58 33.23 36.86 o 6 11 1 417.05 430.15 61.72 o 7 11 1 17.94 69.85 87.78 o 0 12 1 458.31 435.85 25.70 o 1 12 1 1033.51 1116.10 24.60 o 2 12 1 72.34 74.96 12.63 o 3 12 1 1110.18 1169.47 26.77 o 4 12 1 57.65 64.04 26.26 o 5 12 1 85.15 95.24 39.15 o 6 12 1 387.99 439.64 56.44 o 0 13 1 1967.64 1980.23 45.45 o 1 13 1 535.24 536.32 20.42 o 2 13 1 578.96 620.83 21.97 o 3 13 1 1694.85 1677.06 29.47 o 4 13 1 214.44 271.93 35.14 o 5 13 1 120.46 189.62 42.56 o 6 13 1 69.94 217.81 59.93 o 0 14 1 8.96 -25.47 25.47 o 1 14 1 299.59 317.06 20.22 o 2 14 1 650.33 693.26 22.67 o 3 14 1 6.61 -11.25 13.11 o 4 14 1 300.26 245.27 34.91 o 5 14 1 13.49 51.06 48.34 o 6 14 1 19.32 42.97 51.89 o 0 15 1 1653.59 1656.78 44.38 o 1 15 1 339.63 357.91 23.71 o 2 15 1 944.46 973.38 28.02 o 3 15 1 373.48 363.83 25.37 o 4 15 1 166.76 154.71 35.62 o 5 15 1 114.95 92.12 46.59 o 6 15 1 52.07 29.84 53.63 o 0 16 1 7.92 4.69 29.89 o 1 16 1 107.54 98.18 21.11 o 2 16 1 499.85 541.55 24.52 o 3 16 1 181.87 171.72 20.88 o 4 16 1 116.08 125.15 52.66 o 5 16 1 44.89 62.04 47.94 o 0 17 1 456.25 419.80 39.42 o 1 17 1 684.31 645.63 32.49 o 2 17 1 242.95 223.71 22.95 o 3 17 1 138.04 121.37 28.01 o 4 17 1 65.06 141.86 56.90 o 5 17 1 206.53 97.44 48.57 o 0 18 1 5.97 -32.67 44.92 o 1 18 1 426.37 394.77 30.25 o 2 18 1 93.16 75.96 32.43 o 3 18 1 28.52 30.29 34.21 o 4 18 1 118.91 196.86 66.41 o 5 18 1 102.63 67.49 42.91 o 0 19 1 460.77 437.96 59.90 o 1 19 1 61.23 42.73 33.27 o 2 19 1 375.95 414.12 61.43 o 3 19 1 65.36 38.60 45.27 o 4 19 1 433.05 623.17 75.05 o 0 20 1 16.08 15.31 44.56 o 1 20 1 41.51 97.41 50.33 o 2 20 1 498.26 504.11 41.47 o 3 20 1 23.09 -64.08 72.90 o 4 20 1 76.18 344.09 151.58 o 0 21 1 448.43 549.08 65.14 o 1 21 1 54.55 39.16 43.47 o 2 21 1 17.69 -2.57 41.96 o 3 21 1 317.78 302.69 113.30 o 0 22 1 12.95 195.53 82.86 o 1 22 1 36.80 67.42 43.06 o 2 22 1 8.79 -4.10 74.22 o 3 22 1 268.01 209.52 95.58 o 0 23 1 2.24 39.23 53.50 o 1 23 1 20.67 63.06 66.30 o 2 23 1 156.19 74.59 84.69 o 0 24 1 15.51 84.06 88.10 o 1 0 2 4267.24 3826.73 56.48 o 2 0 2 954.33 996.78 16.32 o 3 0 2 83.79 95.58 7.95 o 4 0 2 1298.20 1353.70 26.57 o 5 0 2 11.71 3.23 12.25 o 6 0 2 15.06 9.12 20.02 o 7 0 2 70.35 198.05 125.87 o 1 1 2 8184.79 7446.69 79.02 o 2 1 2 691.43 663.07 9.74 o 3 1 2 255.62 261.12 6.99 o 4 1 2 31.46 47.87 6.69 o 5 1 2 130.47 143.10 9.86 o 6 1 2 488.03 470.61 19.53 o 7 1 2 11.82 -66.73 93.37 o 1 2 2 26504.55 24424.13 235.20 o 2 2 2 3754.42 3719.14 36.41 o 3 2 2 629.80 633.89 11.59 o 4 2 2 342.86 328.06 8.46 o 5 2 2 6.55 25.68 13.43 o 6 2 2 42.47 21.72 23.87 o 7 2 2 442.18 240.15 81.66 o 0 3 2 1968.60 1705.12 53.98 o 1 3 2 11902.02 11383.24 109.96 o 2 3 2 1690.22 1729.68 20.78 o 3 3 2 814.02 851.05 14.28 o 4 3 2 195.60 196.32 12.30 o 5 3 2 18.07 41.38 16.85 o 6 3 2 316.64 274.53 28.78 o 7 3 2 22.13 64.45 96.14 o 0 4 2 12431.22 11779.17 174.24 o 1 4 2 9061.31 8709.01 78.88 o 2 4 2 548.46 562.05 8.88 o 3 4 2 257.69 312.59 13.45 o 4 4 2 523.32 557.75 20.26 o 5 4 2 128.97 200.46 102.27 o 6 4 2 9.86 -22.77 23.66 o 7 4 2 15.00 153.24 117.81 o 0 5 2 5525.40 5326.25 91.44 o 1 5 2 1704.30 1675.44 20.16 o 2 5 2 46.21 47.11 6.52 o 3 5 2 402.54 399.49 15.91 o 4 5 2 142.43 118.06 16.93 o 5 5 2 47.04 57.27 24.25 o 6 5 2 32.06 81.40 28.16 o 7 5 2 84.63 -1.89 95.84 o 0 6 2 4575.88 4490.17 67.19 o 1 6 2 323.74 322.44 8.33 o 2 6 2 366.48 376.92 8.07 o 3 6 2 468.12 486.66 20.98 o 4 6 2 485.29 477.10 21.45 o 5 6 2 628.62 655.43 31.81 o 6 6 2 50.94 55.72 37.77 o 7 6 2 0.75 23.46 58.65 o 0 7 2 499.16 508.22 15.51 o 1 7 2 582.57 606.95 11.88 o 2 7 2 66.05 73.43 5.85 o 3 7 2 360.87 331.34 18.20 o 4 7 2 80.23 78.10 17.00 o 5 7 2 527.78 542.56 28.83 o 6 7 2 128.01 140.32 34.69 o 7 7 2 3.76 64.28 92.71 o 0 8 2 6011.28 6001.00 85.99 o 1 8 2 945.48 1003.73 16.18 o 2 8 2 125.90 140.59 8.90 o 3 8 2 94.37 107.98 8.80 o 4 8 2 1253.79 1339.27 33.41 o 5 8 2 584.33 649.85 50.77 o 6 8 2 6.06 45.10 32.04 o 7 8 2 154.41 67.11 65.15 o 0 9 2 3208.25 3163.42 50.06 o 1 9 2 4720.52 4773.46 52.92 o 2 9 2 1492.25 1501.24 21.08 o 3 9 2 310.07 335.15 10.76 o 4 9 2 184.47 152.42 19.33 o 5 9 2 188.33 150.96 35.89 o 6 9 2 3.60 -45.26 45.26 o 7 9 2 27.43 -28.84 50.59 o 0 10 2 603.64 642.16 23.43 o 1 10 2 1402.20 1431.76 23.03 o 2 10 2 104.29 143.31 12.70 o 3 10 2 133.38 139.01 11.63 o 4 10 2 1129.77 1111.95 37.87 o 5 10 2 370.83 401.50 37.83 o 6 10 2 160.98 270.25 54.50 o 7 10 2 250.45 257.22 62.32 o 0 11 2 1136.44 1164.28 34.03 o 1 11 2 773.38 804.40 18.41 o 2 11 2 267.17 261.53 12.82 o 3 11 2 212.26 210.25 14.87 o 4 11 2 1304.10 1242.48 65.93 o 5 11 2 304.23 228.04 65.69 o 6 11 2 338.14 510.52 99.09 o 7 11 2 93.56 51.26 45.32 o 0 12 2 709.94 729.76 32.42 o 1 12 2 12.28 15.43 13.40 o 2 12 2 283.82 290.06 21.48 o 3 12 2 2451.57 2513.65 38.08 o 4 12 2 310.60 270.50 44.17 o 5 12 2 81.85 100.13 34.16 o 6 12 2 559.85 572.91 54.97 o 0 13 2 2741.29 2874.69 56.84 o 1 13 2 1740.28 1822.59 31.50 o 2 13 2 317.83 326.29 16.78 o 3 13 2 140.36 164.33 18.78 o 4 13 2 263.44 226.71 22.63 o 5 13 2 155.79 154.32 50.12 o 6 13 2 41.29 30.99 60.67 o 0 14 2 78.06 98.92 20.62 o 1 14 2 7.36 -0.70 14.95 o 2 14 2 385.11 405.45 27.64 o 3 14 2 754.43 768.60 22.24 o 4 14 2 15.11 -4.77 18.90 o 5 14 2 25.94 16.24 51.81 o 6 14 2 45.94 62.44 48.84 o 0 15 2 2.38 3.10 23.62 o 1 15 2 767.46 757.13 27.53 o 2 15 2 277.52 302.44 21.21 o 3 15 2 999.99 1011.76 25.07 o 4 15 2 140.97 222.33 50.32 o 5 15 2 28.92 32.56 42.90 o 6 15 2 150.41 124.31 78.37 o 0 16 2 753.53 715.96 61.71 o 1 16 2 415.40 467.91 22.99 o 2 16 2 320.84 328.60 25.39 o 3 16 2 264.09 273.53 25.47 o 4 16 2 100.35 16.44 47.73 o 5 16 2 27.00 54.28 54.23 o 0 17 2 1227.80 1220.74 60.33 o 1 17 2 36.79 53.71 24.97 o 2 17 2 680.89 615.47 27.29 o 3 17 2 40.57 47.09 24.24 o 4 17 2 34.70 59.25 47.84 o 5 17 2 49.34 37.71 35.21 o 0 18 2 661.97 589.55 55.44 o 1 18 2 120.03 109.08 30.13 o 2 18 2 221.87 208.76 36.41 o 3 18 2 68.08 13.84 27.49 o 4 18 2 27.50 85.51 69.46 o 5 18 2 66.21 -17.77 38.91 o 0 19 2 296.83 376.78 51.18 o 1 19 2 195.01 215.97 53.59 o 2 19 2 866.20 897.79 50.24 o 3 19 2 57.13 -9.28 39.83 o 4 19 2 20.01 150.97 58.76 o 0 20 2 0.57 12.60 56.61 o 1 20 2 0.06 45.05 40.68 o 2 20 2 203.62 190.17 38.02 o 3 20 2 48.44 -66.04 99.85 o 4 20 2 55.41 138.90 96.97 o 0 21 2 139.84 145.21 55.14 o 1 21 2 1.01 65.42 41.84 o 2 21 2 19.17 0.94 43.52 o 3 21 2 211.30 365.35 111.28 o 0 22 2 189.00 222.05 81.20 o 1 22 2 490.19 478.09 59.84 o 2 22 2 42.63 -32.36 60.82 o 3 22 2 94.84 -38.85 88.78 o 0 23 2 0.58 82.12 83.55 o 1 23 2 20.39 66.36 49.95 o 2 23 2 14.31 129.97 94.98 o 0 24 2 0.21 32.21 70.23 o 1 0 3 1062.61 981.56 22.05 o 2 0 3 2700.22 2637.85 38.11 o 3 0 3 3537.32 3652.68 47.94 o 4 0 3 82.26 84.80 10.11 o 5 0 3 0.34 19.75 13.60 o 6 0 3 195.93 237.83 33.94 o 7 0 3 177.67 -204.53 212.86 o 0 1 3 656.49 610.44 19.46 o 1 1 3 2265.20 2086.62 22.58 o 2 1 3 2147.12 2047.17 20.49 o 3 1 3 770.61 774.80 11.51 o 4 1 3 89.45 90.44 7.47 o 5 1 3 38.68 53.90 9.01 o 6 1 3 204.33 205.30 18.84 o 7 1 3 419.20 472.27 107.10 o 0 2 3 540.12 444.30 17.70 o 1 2 3 9313.70 8824.54 85.81 o 2 2 3 5193.25 5193.09 54.36 o 3 2 3 6012.64 6093.07 57.44 o 4 2 3 101.21 124.95 7.29 o 5 2 3 127.77 125.83 9.47 o 6 2 3 200.60 125.45 32.16 o 7 2 3 12.56 55.45 100.32 o 0 3 3 288.88 268.07 9.02 o 1 3 3 18485.76 17650.76 160.65 o 2 3 3 1798.41 1820.88 21.31 o 3 3 3 1013.76 1030.41 13.30 o 4 3 3 1386.97 1387.99 23.99 o 5 3 3 184.77 187.12 22.29 o 6 3 3 91.05 86.08 28.90 o 7 3 3 70.98 399.54 115.51 o 0 4 3 29231.01 28175.91 416.53 o 1 4 3 869.49 843.44 11.50 o 2 4 3 1274.55 1249.87 15.42 o 3 4 3 1952.60 1970.86 27.13 o 4 4 3 43.59 49.88 14.77 o 5 4 3 206.92 218.01 84.05 o 6 4 3 41.43 34.23 27.28 o 7 4 3 15.23 84.12 102.84 o 0 5 3 1366.93 1340.43 24.69 o 1 5 3 2553.63 2538.84 26.73 o 2 5 3 93.83 81.22 5.10 o 3 5 3 445.64 432.83 10.20 o 4 5 3 249.43 266.42 17.84 o 5 5 3 4.27 25.57 20.67 o 6 5 3 112.85 74.68 25.88 o 7 5 3 197.36 89.71 101.72 o 0 6 3 4440.66 4389.32 65.81 o 1 6 3 219.06 230.90 8.39 o 2 6 3 570.81 638.71 10.63 o 3 6 3 604.77 571.70 14.55 o 4 6 3 219.52 241.49 20.82 o 5 6 3 863.52 924.40 33.81 o 6 6 3 91.25 89.62 37.74 o 7 6 3 14.58 -27.01 60.87 o 0 7 3 883.83 885.75 21.45 o 1 7 3 1224.54 1208.10 18.69 o 2 7 3 1075.16 1049.90 15.26 o 3 7 3 384.85 386.07 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o 1 14 27 313.63 281.26 68.11 o 0 15 27 16.36 244.19 118.18 o 0 0 28 383.97 461.55 96.66 o 1 0 28 383.14 410.61 82.49 o 2 0 28 32.08 184.87 78.51 o 3 0 28 117.46 236.16 74.17 o 4 0 28 244.63 137.39 70.97 o 0 1 28 38.03 85.10 49.97 o 1 1 28 49.46 131.05 47.87 o 2 1 28 210.23 239.96 50.88 o 3 1 28 191.55 141.59 63.79 o 4 1 28 92.28 118.76 47.77 o 0 2 28 26.91 28.73 47.17 o 1 2 28 266.25 257.36 46.10 o 2 2 28 47.48 131.02 51.75 o 3 2 28 2.96 100.46 57.73 o 4 2 28 50.92 66.10 42.41 o 0 3 28 855.51 982.35 79.87 o 1 3 28 279.13 286.39 46.25 o 2 3 28 3.15 67.14 39.79 o 3 3 28 133.37 205.21 68.63 o 4 3 28 16.48 42.11 52.09 o 0 4 28 16.40 -31.31 55.98 o 1 4 28 135.25 56.22 50.97 o 2 4 28 20.92 8.69 45.71 o 3 4 28 243.59 154.39 55.62 o 4 4 28 72.04 54.77 32.91 o 0 5 28 6.38 18.95 60.02 o 1 5 28 37.85 -3.55 45.25 o 2 5 28 27.75 14.63 46.50 o 3 5 28 122.25 118.85 48.34 o 4 5 28 120.66 77.82 69.62 o 0 6 28 124.12 101.08 93.53 o 1 6 28 6.38 8.61 43.21 o 2 6 28 28.11 1.96 53.29 o 3 6 28 10.10 -28.38 40.94 o 4 6 28 32.27 58.75 37.67 o 0 7 28 36.56 98.48 57.98 o 1 7 28 186.11 179.55 54.81 o 2 7 28 40.54 152.38 46.80 o 3 7 28 25.06 -40.10 40.10 o 4 7 28 197.70 59.55 37.73 o 0 8 28 1.79 -0.34 58.74 o 1 8 28 82.37 165.28 60.70 o 2 8 28 9.83 5.35 56.78 o 3 8 28 60.09 118.33 72.71 o 0 9 28 12.87 -47.59 94.93 o 1 9 28 211.76 138.21 56.23 o 2 9 28 65.60 98.55 50.89 o 3 9 28 195.76 64.56 38.60 o 0 10 28 276.79 270.34 90.70 o 1 10 28 74.19 106.26 55.01 o 2 10 28 53.51 296.35 155.22 o 3 10 28 273.97 234.04 74.64 o 0 11 28 5.06 5.36 93.72 o 1 11 28 76.73 144.72 50.88 o 2 11 28 43.91 -17.53 48.48 o 0 12 28 56.44 49.24 71.73 o 1 12 28 116.29 27.28 64.20 o 2 12 28 6.61 -25.70 52.44 o 0 13 28 249.66 258.24 76.49 o 1 13 28 336.49 471.25 88.72 o 0 14 28 2.58 39.05 68.45 o 1 0 29 207.30 243.28 62.29 o 2 0 29 11.94 8.53 57.52 o 3 0 29 26.41 60.45 88.25 o 4 0 29 139.78 92.21 69.54 o 0 1 29 259.70 248.92 53.20 o 1 1 29 148.97 139.55 51.27 o 2 1 29 92.79 -8.07 57.28 o 3 1 29 10.55 -7.24 54.86 o 4 1 29 40.69 -31.11 45.50 o 0 2 29 43.62 -15.87 85.83 o 1 2 29 315.25 326.31 60.00 o 2 2 29 240.98 232.95 56.19 o 3 2 29 9.13 63.26 56.19 o 4 2 29 9.97 6.91 52.33 o 0 3 29 13.18 14.11 71.98 o 1 3 29 88.94 73.07 48.16 o 2 3 29 22.92 95.60 59.44 o 3 3 29 60.74 53.21 47.99 o 4 3 29 167.39 160.81 56.10 o 0 4 29 106.19 116.83 65.66 o 1 4 29 98.08 63.12 54.46 o 2 4 29 105.09 73.53 79.91 o 3 4 29 121.92 90.22 69.38 o 4 4 29 3.66 58.04 42.83 o 0 5 29 7.70 -11.27 55.23 o 1 5 29 1.83 55.99 48.27 o 2 5 29 2.13 129.16 53.76 o 3 5 29 176.71 13.95 47.83 o 0 6 29 834.14 910.96 84.22 o 1 6 29 252.08 270.13 61.37 o 2 6 29 468.30 440.49 63.98 o 3 6 29 281.08 199.82 91.89 o 0 7 29 19.99 -11.24 65.99 o 1 7 29 39.52 113.38 53.41 o 2 7 29 11.65 15.42 54.95 o 3 7 29 177.31 59.68 28.05 o 0 8 29 614.21 787.73 97.92 o 1 8 29 124.23 103.94 51.18 o 2 8 29 176.22 290.04 72.31 o 3 8 29 115.88 16.21 38.08 o 0 9 29 76.12 -74.41 74.41 o 1 9 29 111.87 101.20 59.41 o 2 9 29 51.38 105.74 45.50 o 3 9 29 50.17 69.13 60.25 o 0 10 29 27.28 -60.37 60.37 o 1 10 29 396.87 513.35 70.53 o 2 10 29 26.12 49.94 58.46 o 0 11 29 0.02 129.87 98.14 o 1 11 29 46.86 28.58 62.12 o 2 11 29 8.87 -53.16 53.16 o 0 12 29 4.35 12.99 88.90 o 1 12 29 80.15 192.83 75.06 o 0 13 29 22.08 135.11 120.09 o 0 0 30 65.21 69.70 111.20 o 1 0 30 83.38 59.61 75.11 o 2 0 30 116.15 123.49 80.12 o 3 0 30 232.21 176.73 143.13 o 0 1 30 199.09 155.38 66.09 o 1 1 30 98.38 101.48 48.72 o 2 1 30 154.68 113.41 55.91 o 3 1 30 78.35 71.13 63.69 o 0 2 30 120.50 224.63 88.44 o 1 2 30 14.45 3.73 46.97 o 2 2 30 126.46 241.84 59.62 o 3 2 30 31.86 -16.44 93.81 o 0 3 30 295.59 449.80 77.78 o 1 3 30 75.62 86.84 44.25 o 2 3 30 73.38 95.99 49.73 o 3 3 30 68.73 -7.18 48.14 o 0 4 30 92.71 149.54 90.69 o 1 4 30 126.29 168.25 54.58 o 2 4 30 183.42 225.70 51.40 o 3 4 30 11.18 -16.97 45.61 o 0 5 30 103.88 286.16 89.58 o 1 5 30 264.65 272.92 58.57 o 2 5 30 16.60 57.93 50.55 o 3 5 30 26.39 18.35 41.09 o 0 6 30 217.98 241.23 81.79 o 1 6 30 26.69 16.74 56.50 o 2 6 30 65.90 97.87 64.96 o 3 6 30 17.55 -32.42 32.42 o 0 7 30 78.45 68.99 93.61 o 1 7 30 54.84 27.39 49.43 o 2 7 30 11.42 78.85 47.13 o 3 7 30 109.28 44.19 34.03 o 0 8 30 13.16 60.48 103.06 o 1 8 30 108.93 223.70 81.42 o 2 8 30 180.58 88.24 61.61 o 0 9 30 656.83 1104.47 208.99 o 1 9 30 274.35 253.46 69.29 o 2 9 30 68.63 86.10 60.51 o 0 10 30 103.25 157.07 80.28 o 1 10 30 11.47 136.17 66.42 o 2 10 30 22.43 21.34 57.95 o 0 11 30 888.94 730.32 124.93 o 1 11 30 61.49 19.38 55.19 o 1 0 31 49.35 -28.28 91.76 o 2 0 31 67.05 -52.26 73.07 o 3 0 31 125.30 213.03 71.95 o 0 1 31 97.78 132.64 78.74 o 1 1 31 11.21 32.00 58.52 o 2 1 31 13.76 13.63 55.30 o 3 1 31 257.13 206.78 51.73 o 0 2 31 330.60 530.34 151.48 o 1 2 31 143.41 153.97 57.98 o 2 2 31 180.82 254.06 69.13 o 3 2 31 112.36 139.62 60.05 o 0 3 31 4.70 27.37 92.23 o 1 3 31 260.59 362.88 69.56 o 2 3 31 232.71 243.27 45.51 o 3 3 31 21.15 28.21 44.19 o 0 4 31 68.94 -4.39 99.27 o 1 4 31 97.79 58.27 59.30 o 2 4 31 122.54 133.55 100.75 o 3 4 31 461.68 127.74 96.94 o 0 5 31 0.34 19.07 98.84 o 1 5 31 15.77 -58.97 62.19 o 2 5 31 32.31 1.61 59.55 o 3 5 31 46.27 55.49 38.40 o 0 6 31 4.23 -20.67 92.26 o 1 6 31 26.19 28.77 52.81 o 2 6 31 46.94 -22.78 54.64 o 0 7 31 73.72 362.44 163.30 o 1 7 31 27.36 64.90 61.89 o 2 7 31 212.98 394.96 107.19 o 0 8 31 75.63 306.92 94.41 o 1 8 31 103.70 124.40 61.10 o 2 8 31 36.91 39.28 48.50 o 0 9 31 79.18 -116.48 116.48 o 1 9 31 131.23 186.65 90.10 o 0 10 31 70.26 140.99 112.15 o 1 10 31 164.21 91.94 67.27 o 0 0 32 22.35 -54.12 109.00 o 1 0 32 6.72 -39.29 61.14 o 2 0 32 118.82 236.29 91.35 o 0 1 32 11.00 -44.90 75.69 o 1 1 32 537.54 740.05 95.68 o 2 1 32 8.02 192.16 65.73 o 0 2 32 38.87 84.54 86.16 o 1 2 32 52.07 243.93 111.80 o 2 2 32 41.55 179.69 82.27 o 0 3 32 372.69 436.04 106.76 o 1 3 32 219.66 282.21 69.33 o 2 3 32 20.31 93.59 64.56 o 0 4 32 30.92 153.15 127.50 o 1 4 32 186.99 568.80 93.74 o 2 4 32 104.68 106.77 57.21 o 0 5 32 133.30 174.32 107.85 o 1 5 32 258.01 522.97 89.34 o 2 5 32 181.85 355.36 81.13 o 0 6 32 98.18 193.74 98.67 o 1 6 32 254.50 262.27 63.94 o 2 6 32 5.88 -20.29 44.22 o 0 7 32 323.47 245.10 105.17 o 1 7 32 54.51 127.59 62.00 o 0 8 32 174.15 307.48 88.11 o 1 8 32 63.46 -53.29 53.29 o 0 9 32 28.43 -168.90 168.90 o 1 0 33 0.05 29.99 93.09 o 2 0 33 51.25 106.98 107.47 o 0 1 33 8.66 114.06 95.57 o 1 1 33 61.97 234.02 94.76 o 2 1 33 135.91 58.15 64.02 o 0 2 33 29.03 76.13 113.35 o 1 2 33 2.22 21.96 81.75 o 2 2 33 12.17 134.64 60.45 o 0 3 33 2.22 -14.85 92.59 o 1 3 33 34.31 10.98 82.31 o 2 3 33 78.32 -44.02 52.07 o 0 4 33 1.81 39.59 140.69 o 1 4 33 85.58 86.15 75.73 o 0 5 33 165.52 355.84 155.75 o 1 5 33 275.69 321.55 74.79 o 0 6 33 158.74 343.59 99.06 o 1 6 33 1.58 117.25 75.95 o 0 7 33 0.44 -109.94 109.94 o 0 0 34 154.70 83.71 106.99 o 1 0 34 2.38 -122.76 122.76 o 0 1 34 1488.96 1850.81 138.65 o 1 1 34 99.46 -72.33 72.33 o 0 2 34 485.52 271.96 121.52 o 1 2 34 36.23 -65.90 65.90 o 0 3 34 297.60 137.95 110.35 o 0 4 34 125.98 102.27 198.12 o