#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:00:44 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180941 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/21/2202190.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202190_Fobs loop_ _publ_author_name 'Kalaitzis, John A.' 'de Almeida Leone, Priscila' 'Quinn, Ronald J.' 'Healy, Peter C.' _publ_section_title ; Zwitterionic 2-(methylamino)ethanesulfonic acid ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o726 _journal_page_last o727 _journal_volume 59 _journal_year 2003 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.0610 _cell_length_b 11.9306 _cell_length_c 5.4924 _exptl_crystal_F_000 296.00 _reflns_d_resolution_high 0.7698 _cod_data_source_file tk6103Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 563rq34 (rpt rpt 392rq28) methyltaurine' _shelx_refln_list_code 6 _shelx_f_calc_maximum 117.04 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_sigma _refln_F_calc _refln_phase_calc 2 0 0 9012.16 87.69 97.23 0.0 4 0 0 414.68 27.32 21.02 0.0 6 0 0 230.03 3.76 15.66 180.0 8 0 0 45.20 1.49 6.75 180.0 10 0 0 231.66 3.76 15.33 180.0 1 1 0 1052.84 7.90 34.05 90.0 2 1 0 1468.89 11.43 38.92 0.0 3 1 0 1018.34 96.07 32.30 90.0 4 1 0 890.70 57.29 31.30 0.0 5 1 0 951.27 69.09 32.32 90.0 6 1 0 143.04 2.17 11.69 0.0 7 1 0 139.38 2.32 11.39 90.0 8 1 0 171.02 2.77 13.72 180.0 9 1 0 0.94 0.40 0.83 270.0 10 1 0 98.56 2.47 10.13 180.0 11 1 0 95.88 2.55 9.56 270.0 0 2 0 349.49 3.62 17.93 180.0 1 2 0 1291.60 9.95 35.24 270.0 2 2 0 42.43 2.53 7.16 180.0 3 2 0 735.81 54.52 27.34 270.0 4 2 0 269.29 16.87 15.76 180.0 5 2 0 395.07 37.76 21.42 90.0 6 2 0 354.55 4.92 19.26 0.0 7 2 0 2125.32 21.07 46.54 90.0 8 2 0 115.63 2.30 10.99 0.0 9 2 0 428.30 6.72 20.42 90.0 10 2 0 16.72 1.23 3.84 0.0 11 2 0 24.34 1.55 4.92 90.0 1 3 0 2501.09 72.28 52.64 270.0 2 3 0 507.47 51.56 23.12 0.0 3 3 0 890.24 29.76 30.69 270.0 4 3 0 943.08 71.43 31.11 0.0 5 3 0 378.44 35.81 20.71 270.0 6 3 0 374.26 5.15 19.57 0.0 7 3 0 159.69 2.56 12.64 90.0 8 3 0 22.36 1.21 5.22 0.0 9 3 0 100.14 2.32 10.04 90.0 10 3 0 3.56 0.49 2.02 0.0 11 3 0 217.95 3.96 15.00 90.0 0 4 0 2639.06 19.71 52.62 180.0 1 4 0 2854.93 166.70 54.60 90.0 2 4 0 122.92 12.48 12.86 180.0 3 4 0 230.41 20.57 15.38 270.0 4 4 0 64.65 3.55 8.29 0.0 5 4 0 398.89 5.09 19.64 270.0 6 4 0 150.27 2.37 12.58 0.0 7 4 0 192.99 2.90 14.40 270.0 8 4 0 60.03 1.71 7.14 0.0 9 4 0 30.88 1.50 5.71 270.0 10 4 0 21.98 1.43 4.91 0.0 11 4 0 49.85 2.05 7.06 270.0 1 5 0 41.65 3.32 6.57 90.0 2 5 0 837.34 75.55 29.86 180.0 3 5 0 53.69 5.27 7.20 270.0 4 5 0 1228.24 66.64 36.94 180.0 5 5 0 54.32 1.40 7.35 90.0 6 5 0 596.46 9.47 24.51 180.0 7 5 0 51.98 1.61 6.87 270.0 8 5 0 30.41 1.38 5.80 0.0 9 5 0 6.27 0.55 2.38 270.0 10 5 0 158.43 3.19 12.53 0.0 11 5 0 2.38 0.53 1.24 90.0 0 6 0 1345.86 13.01 34.84 0.0 1 6 0 362.01 15.56 18.03 270.0 2 6 0 282.87 26.23 17.54 0.0 3 6 0 346.87 35.16 17.90 270.0 4 6 0 88.69 1.70 9.29 0.0 5 6 0 467.20 6.01 21.46 270.0 6 6 0 727.51 10.95 27.63 180.0 7 6 0 298.68 3.88 17.71 270.0 8 6 0 280.06 3.96 17.15 180.0 9 6 0 90.54 2.36 9.42 270.0 10 6 0 20.25 1.38 4.53 180.0 1 7 0 623.13 41.11 25.54 90.0 2 7 0 960.85 11.32 29.77 0.0 3 7 0 1531.49 15.78 38.21 90.0 4 7 0 270.83 4.36 15.59 0.0 5 7 0 906.75 12.28 30.20 90.0 6 7 0 39.34 1.38 6.68 0.0 7 7 0 76.07 2.00 8.90 90.0 8 7 0 4.75 0.48 2.34 0.0 9 7 0 3.05 0.48 1.57 270.0 10 7 0 14.63 1.29 3.94 0.0 0 8 0 86.48 1.66 9.79 0.0 1 8 0 1489.53 15.58 38.34 270.0 2 8 0 383.87 5.22 20.49 0.0 3 8 0 21.20 1.04 4.54 270.0 4 8 0 96.06 1.96 9.94 0.0 5 8 0 85.33 1.98 8.91 90.0 6 8 0 39.74 1.51 6.56 0.0 7 8 0 162.14 2.95 12.33 90.0 8 8 0 40.67 1.66 6.01 180.0 9 8 0 69.34 2.25 8.19 90.0 10 8 0 0.00 1.01 1.27 180.0 1 9 0 79.34 1.73 8.33 270.0 2 9 0 296.57 3.57 16.79 0.0 3 9 0 115.22 2.19 10.49 270.0 4 9 0 568.81 7.29 23.22 0.0 5 9 0 648.00 8.19 25.29 270.0 6 9 0 193.86 3.20 14.21 0.0 7 9 0 11.40 1.11 2.94 270.0 8 9 0 24.40 1.42 4.75 0.0 9 9 0 19.70 1.42 4.47 90.0 0 10 0 529.55 6.85 22.81 180.0 1 10 0 32.89 1.29 6.21 270.0 2 10 0 271.20 3.55 16.44 180.0 3 10 0 22.42 1.17 4.62 270.0 4 10 0 6.15 0.53 2.82 180.0 5 10 0 0.00 0.82 0.31 90.0 6 10 0 168.62 3.11 13.83 0.0 7 10 0 0.55 0.76 0.27 270.0 8 10 0 117.94 2.83 10.85 0.0 1 11 0 14.48 1.05 3.95 90.0 2 11 0 344.91 4.28 18.32 180.0 3 11 0 67.76 1.88 8.33 270.0 4 11 0 93.20 2.23 9.77 180.0 5 11 0 66.00 2.03 8.49 270.0 6 11 0 0.55 0.44 0.50 180.0 7 11 0 39.43 1.72 6.13 270.0 8 11 0 11.34 0.95 3.52 0.0 0 12 0 6.68 0.65 2.47 0.0 1 12 0 195.29 3.21 14.57 90.0 2 12 0 63.46 1.93 8.73 180.0 3 12 0 19.77 1.30 4.82 90.0 4 12 0 30.31 1.45 5.72 180.0 5 12 0 19.16 1.37 4.24 270.0 6 12 0 81.86 2.37 9.05 180.0 7 12 0 66.63 2.28 7.87 270.0 1 13 0 7.22 0.61 2.75 90.0 2 13 0 24.43 1.42 5.22 180.0 3 13 0 80.51 2.21 8.70 90.0 4 13 0 0.00 0.91 0.87 180.0 5 13 0 68.80 2.20 8.71 90.0 6 13 0 12.12 0.87 3.24 0.0 0 14 0 23.47 1.41 4.33 0.0 1 14 0 160.76 3.25 12.38 270.0 2 14 0 70.63 2.17 8.39 0.0 3 14 0 46.02 1.90 6.64 270.0 4 14 0 5.20 0.54 2.22 180.0 5 14 0 0.00 0.95 0.09 90.0 1 15 0 30.62 1.70 5.77 270.0 2 15 0 41.05 1.82 6.06 0.0 1 0 1 901.50 7.57 26.35 90.0 2 0 1 1462.06 52.38 38.41 90.0 3 0 1 2468.04 55.73 49.83 90.0 4 0 1 1787.77 30.31 41.98 90.0 5 0 1 36.86 1.29 5.59 90.0 6 0 1 197.30 2.63 13.46 90.0 7 0 1 1096.90 13.69 33.29 270.0 8 0 1 3.20 0.39 1.65 270.0 9 0 1 393.70 6.43 20.19 270.0 10 0 1 50.61 1.84 7.34 270.0 11 0 1 83.32 2.42 8.86 270.0 0 1 1 1409.00 10.62 34.58 270.0 1 1 1 1382.92 10.79 36.51 39.3 2 1 1 892.11 22.01 30.46 220.1 3 1 1 766.86 11.72 28.13 340.6 4 1 1 1011.63 7.41 32.62 141.6 5 1 1 86.28 1.05 9.88 90.9 6 1 1 495.79 8.02 21.61 138.5 7 1 1 123.62 2.19 10.67 196.9 8 1 1 145.65 2.59 11.58 97.3 9 1 1 31.29 1.42 5.77 205.7 10 1 1 18.33 1.31 4.35 106.0 11 1 1 125.83 2.96 11.25 278.9 0 2 1 13714.15 347.71 117.04 0.0 1 2 1 538.85 19.95 24.22 312.5 2 2 1 1286.27 56.20 37.44 345.6 3 2 1 1709.95 44.63 41.79 17.8 4 2 1 370.76 9.17 19.75 329.9 5 2 1 281.95 2.83 17.42 15.9 6 2 1 7.61 0.51 2.79 244.1 7 2 1 39.15 1.35 6.05 22.3 8 2 1 5.80 0.60 2.32 133.4 9 2 1 34.72 1.51 5.98 155.4 10 2 1 150.42 3.04 12.08 159.4 11 2 1 76.23 2.38 8.94 139.7 0 3 1 509.88 37.78 22.71 270.0 1 3 1 1192.91 28.98 36.07 167.0 2 3 1 45.69 0.62 5.79 212.4 3 3 1 842.52 16.04 29.56 108.3 4 3 1 74.37 1.00 9.07 77.3 5 3 1 572.59 8.33 23.24 51.9 6 3 1 107.89 1.96 10.55 15.8 7 3 1 438.72 6.08 20.39 51.3 8 3 1 57.96 1.69 7.76 160.4 9 3 1 53.44 1.74 7.55 28.7 10 3 1 101.23 2.54 9.98 151.5 11 3 1 11.94 0.96 3.70 241.9 0 4 1 8.58 0.70 2.44 0.0 1 4 1 755.37 5.67 26.97 107.2 2 4 1 97.65 3.14 10.28 275.1 3 4 1 960.86 40.17 31.40 147.4 4 4 1 638.36 19.31 26.00 220.4 5 4 1 521.23 8.14 21.66 114.0 6 4 1 244.41 3.12 15.60 334.4 7 4 1 587.23 7.39 24.18 90.2 8 4 1 133.66 2.58 11.65 17.9 9 4 1 133.82 2.78 12.01 62.9 10 4 1 88.72 2.39 9.27 50.3 11 4 1 14.55 1.01 3.81 36.9 0 5 1 332.71 16.34 18.83 90.0 1 5 1 434.37 5.28 21.34 286.7 2 5 1 246.71 6.18 16.49 84.5 3 5 1 308.53 5.15 18.79 244.1 4 5 1 193.43 2.51 13.15 323.8 5 5 1 360.35 5.10 19.13 246.5 6 5 1 256.43 3.32 15.34 286.0 7 5 1 5.17 0.46 1.82 285.8 8 5 1 201.20 3.25 14.33 265.3 9 5 1 1.01 0.40 0.82 187.3 10 5 1 29.81 1.53 5.26 235.4 11 5 1 65.54 2.32 8.07 93.2 0 6 1 9.35 0.56 3.17 180.0 1 6 1 357.57 4.15 19.56 108.3 2 6 1 348.87 12.59 19.36 104.3 3 6 1 99.07 1.69 9.43 213.1 4 6 1 421.18 5.44 19.69 78.8 5 6 1 19.30 1.03 3.94 239.1 6 6 1 55.26 1.60 6.90 57.9 7 6 1 37.94 1.40 6.03 273.0 8 6 1 34.42 1.48 6.01 349.4 9 6 1 28.10 1.51 5.53 286.2 10 6 1 36.70 1.81 6.20 274.2 0 7 1 184.82 2.40 13.42 270.0 1 7 1 617.99 8.65 24.70 3.8 2 7 1 549.89 8.20 22.53 222.8 3 7 1 93.11 1.79 8.96 328.2 4 7 1 751.01 10.65 27.02 182.8 5 7 1 368.73 5.51 18.93 108.9 6 7 1 498.74 6.85 21.60 170.5 7 7 1 83.50 2.10 9.64 143.5 8 7 1 28.02 1.44 5.62 145.4 9 7 1 50.65 1.94 7.03 153.1 10 7 1 37.65 1.81 6.22 339.3 0 8 1 205.74 2.70 14.17 0.0 1 8 1 113.96 1.97 11.52 66.4 2 8 1 103.24 1.94 10.17 342.9 3 8 1 330.61 5.03 17.63 357.9 4 8 1 103.53 2.09 10.35 12.7 5 8 1 326.37 4.02 16.79 315.8 6 8 1 154.86 2.77 12.40 152.6 7 8 1 68.68 1.96 8.34 291.3 8 8 1 73.76 2.13 8.71 175.8 9 8 1 84.64 2.45 9.20 234.5 0 9 1 111.83 2.07 10.36 270.0 1 9 1 179.92 2.66 12.93 144.1 2 9 1 296.26 3.60 16.27 327.4 3 9 1 505.80 6.68 21.12 91.4 4 9 1 34.49 1.35 5.50 334.0 5 9 1 375.73 4.53 18.76 68.5 6 9 1 52.65 1.76 7.47 59.7 7 9 1 100.80 2.43 9.71 54.3 8 9 1 74.99 2.28 8.64 64.5 9 9 1 31.52 1.66 5.58 326.6 0 10 1 276.35 3.57 17.06 0.0 1 10 1 333.74 5.31 18.04 274.8 2 10 1 763.37 11.63 26.76 334.4 3 10 1 38.60 1.41 6.25 253.2 4 10 1 142.98 2.65 12.65 307.1 5 10 1 5.60 0.56 2.27 49.3 6 10 1 32.45 1.51 5.77 323.9 7 10 1 42.51 1.74 6.50 70.8 8 10 1 23.68 1.50 4.55 180.7 0 11 1 97.05 2.19 9.49 90.0 1 11 1 36.54 1.46 5.77 182.0 2 11 1 195.16 3.13 14.87 33.9 3 11 1 6.36 0.66 2.44 187.7 4 11 1 97.26 2.35 10.30 350.7 5 11 1 101.83 2.45 10.49 266.3 6 11 1 26.11 1.54 5.13 281.6 7 11 1 4.68 0.53 2.10 349.1 8 11 1 20.42 1.58 4.61 286.0 0 12 1 110.03 2.41 10.88 180.0 1 12 1 4.31 0.42 2.30 241.8 2 12 1 116.93 2.54 11.49 165.2 3 12 1 23.56 1.30 5.02 169.0 4 12 1 13.85 1.19 3.59 55.6 5 12 1 73.51 2.20 8.33 156.8 6 12 1 70.01 2.27 8.34 355.1 7 12 1 6.73 0.67 2.36 156.6 0 13 1 0.58 0.81 0.50 270.0 1 13 1 46.16 1.70 6.96 42.0 2 13 1 49.27 1.79 6.98 189.0 3 13 1 27.03 1.45 5.26 273.5 4 13 1 30.69 1.60 5.20 166.8 5 13 1 35.37 1.73 6.05 224.7 6 13 1 4.35 0.54 2.06 251.9 0 14 1 15.65 1.28 3.99 0.0 1 14 1 97.28 2.53 9.72 77.3 2 14 1 21.93 1.36 4.41 89.1 3 14 1 31.52 1.66 5.61 20.0 4 14 1 14.56 1.31 3.58 83.0 0 15 1 37.63 1.83 5.69 270.0 1 15 1 6.34 0.58 2.51 95.6 2 15 1 51.62 2.06 7.19 214.0 0 0 2 10312.96 305.75 97.79 180.0 1 0 2 8.70 0.33 3.12 180.0 2 0 2 1371.64 29.05 36.84 180.0 3 0 2 804.71 8.76 28.32 180.0 4 0 2 486.78 10.91 21.83 180.0 5 0 2 422.40 5.32 20.83 180.0 6 0 2 16.55 0.92 3.35 180.0 7 0 2 435.35 6.18 20.29 180.0 8 0 2 10.96 0.99 3.40 180.0 9 0 2 0.00 0.83 0.09 0.0 10 0 2 79.30 2.29 9.01 0.0 11 0 2 65.53 2.27 8.28 0.0 0 1 2 788.17 38.48 28.10 90.0 1 1 2 145.67 1.56 13.45 327.8 2 1 2 160.05 1.74 12.98 82.8 3 1 2 463.99 11.16 21.81 346.5 4 1 2 137.10 1.39 11.69 273.9 5 1 2 161.56 2.28 12.40 287.4 6 1 2 19.78 0.99 4.39 257.9 7 1 2 126.06 2.32 11.08 222.2 8 1 2 98.26 2.17 9.78 302.8 9 1 2 77.62 2.08 9.23 195.6 10 1 2 80.01 2.29 8.97 282.2 11 1 2 14.34 1.40 3.82 77.3 0 2 2 2.13 0.15 1.25 180.0 1 2 2 35.64 0.98 5.49 153.7 2 2 2 77.78 0.92 9.14 97.7 3 2 2 134.13 1.30 11.85 63.3 4 2 2 742.07 7.02 27.90 64.7 5 2 2 6.69 0.71 2.68 256.9 6 2 2 301.12 4.72 16.80 110.0 7 2 2 275.83 3.60 17.07 274.9 8 2 2 20.82 1.28 4.90 141.5 9 2 2 72.77 2.04 8.84 260.4 10 2 2 52.23 1.94 7.66 248.8 11 2 2 17.68 1.46 4.07 252.4 0 3 2 230.16 13.32 14.18 90.0 1 3 2 466.03 16.37 21.71 26.2 2 3 2 166.89 1.88 12.87 187.1 3 3 2 698.17 14.48 26.29 346.3 4 3 2 443.02 7.14 20.31 153.0 5 3 2 48.38 1.31 6.65 359.8 6 3 2 216.76 2.95 14.40 143.7 7 3 2 151.28 2.60 12.02 221.6 8 3 2 277.37 3.88 17.00 104.9 9 3 2 19.15 1.25 4.26 198.8 10 3 2 76.68 2.24 8.74 109.7 11 3 2 41.62 1.91 6.34 285.5 0 4 2 2.60 0.18 0.83 0.0 1 4 2 113.87 2.12 10.97 313.8 2 4 2 21.57 0.91 4.15 155.5 3 4 2 346.67 3.19 18.86 30.6 4 4 2 35.21 1.11 6.09 234.2 5 4 2 56.61 1.46 7.51 31.0 6 4 2 43.36 1.40 6.63 252.8 7 4 2 15.97 1.08 3.97 31.3 8 4 2 17.26 1.17 4.10 272.2 9 4 2 15.87 1.18 4.26 158.1 10 4 2 35.98 1.72 5.84 101.0 0 5 2 245.61 12.53 15.16 270.0 1 5 2 410.08 13.25 20.86 179.7 2 5 2 26.90 0.64 5.48 47.8 3 5 2 214.58 3.62 14.40 128.9 4 5 2 170.57 2.43 13.47 50.7 5 5 2 33.87 1.24 5.52 341.4 6 5 2 149.52 2.56 12.64 33.0 7 5 2 80.13 1.99 8.85 23.9 8 5 2 2.36 0.43 1.49 94.8 9 5 2 91.26 2.41 9.77 356.2 10 5 2 40.14 1.77 5.92 125.5 0 6 2 2.09 0.28 2.03 180.0 1 6 2 221.85 3.62 13.30 77.2 2 6 2 14.42 0.83 4.00 260.2 3 6 2 377.72 5.21 18.59 131.8 4 6 2 211.56 2.92 14.19 232.8 5 6 2 282.51 3.59 16.71 127.1 6 6 2 122.64 2.36 11.12 314.8 7 6 2 104.65 2.30 10.95 134.0 8 6 2 38.96 1.58 6.60 45.0 9 6 2 23.86 1.48 4.91 48.9 10 6 2 74.06 2.37 8.28 75.6 0 7 2 285.50 4.33 16.71 90.0 1 7 2 90.69 1.76 8.83 264.3 2 7 2 368.82 5.12 18.72 115.7 3 7 2 222.68 2.97 14.96 268.4 4 7 2 13.24 0.94 3.70 130.9 5 7 2 163.35 2.73 13.25 272.9 6 7 2 168.55 2.89 12.70 251.9 7 7 2 35.01 1.49 6.06 294.4 8 7 2 304.50 4.42 17.84 254.7 9 7 2 29.69 1.64 5.36 199.7 0 8 2 75.41 1.70 8.38 180.0 1 8 2 239.72 3.11 14.93 140.5 2 8 2 378.84 5.44 18.85 140.4 3 8 2 183.77 2.79 13.44 177.0 4 8 2 197.01 2.97 13.94 109.2 5 8 2 60.34 1.77 7.57 182.0 6 8 2 50.60 1.70 7.72 112.0 7 8 2 1.18 0.88 1.39 279.6 8 8 2 33.65 1.60 5.61 44.0 9 8 2 6.23 0.63 2.22 273.5 0 9 2 12.92 0.95 3.28 270.0 1 9 2 731.63 11.08 26.45 2.0 2 9 2 185.84 2.87 13.76 230.9 3 9 2 94.82 2.13 9.35 351.0 4 9 2 130.48 2.51 11.73 198.4 5 9 2 131.43 2.63 12.39 107.5 6 9 2 34.82 1.54 6.22 192.8 7 9 2 75.67 2.21 8.70 159.8 8 9 2 19.95 1.42 4.39 136.4 0 10 2 57.07 1.68 8.07 0.0 1 10 2 100.94 2.17 10.21 83.6 2 10 2 95.00 2.12 9.90 43.5 3 10 2 123.71 2.47 11.65 17.4 4 10 2 76.55 2.03 9.15 73.9 5 10 2 190.86 3.32 14.50 347.4 6 10 2 62.15 2.03 8.19 118.3 7 10 2 36.18 1.71 5.38 340.6 8 10 2 9.41 0.85 2.88 185.1 0 11 2 165.60 2.92 13.72 270.0 1 11 2 16.67 1.16 4.12 227.5 2 11 2 74.72 2.04 9.01 306.7 3 11 2 27.15 1.37 5.55 88.1 4 11 2 0.00 0.89 0.37 336.7 5 11 2 34.34 1.55 5.68 40.4 6 11 2 139.12 2.95 10.95 100.3 7 11 2 49.79 1.93 6.48 22.1 0 12 2 10.78 0.77 3.68 0.0 1 12 2 43.37 1.66 6.87 297.9 2 12 2 262.31 3.95 16.40 302.1 3 12 2 5.04 0.49 2.44 304.8 4 12 2 121.64 2.75 10.96 282.4 5 12 2 21.89 1.36 4.44 26.9 6 12 2 20.86 1.57 4.87 308.8 0 13 2 80.83 2.25 8.77 90.0 1 13 2 58.51 2.00 8.23 178.0 2 13 2 71.19 2.22 8.71 54.5 3 13 2 3.17 0.49 1.99 249.0 4 13 2 1.21 0.99 1.25 4.1 5 13 2 9.15 0.84 2.84 322.8 0 14 2 3.46 0.52 1.75 180.0 1 14 2 47.99 1.93 6.72 127.2 2 14 2 23.31 1.49 4.84 182.6 3 14 2 89.24 2.54 9.16 151.7 1 0 3 313.86 6.97 16.51 270.0 2 0 3 936.61 18.41 30.51 270.0 3 0 3 192.88 2.51 13.79 270.0 4 0 3 1979.58 19.11 43.14 270.0 5 0 3 0.00 0.66 0.28 270.0 6 0 3 438.75 6.21 19.86 270.0 7 0 3 52.71 1.66 7.80 90.0 8 0 3 4.09 0.45 2.01 270.0 9 0 3 1.74 0.46 1.72 90.0 10 0 3 63.77 2.15 7.66 90.0 0 1 3 367.73 12.88 18.75 90.0 1 1 3 864.56 7.11 28.34 195.2 2 1 3 226.91 2.13 15.02 62.0 3 1 3 833.96 10.48 27.69 172.1 4 1 3 335.51 4.80 18.11 288.4 5 1 3 18.52 0.98 3.98 154.8 6 1 3 172.19 2.75 13.18 277.4 7 1 3 219.69 3.31 14.28 33.8 8 1 3 204.83 3.36 14.78 269.6 9 1 3 52.07 1.92 7.62 13.2 10 1 3 63.16 2.19 7.80 293.1 0 2 3 960.49 30.46 28.91 180.0 1 2 3 294.89 2.83 17.27 144.5 2 2 3 89.19 1.59 8.99 151.0 3 2 3 1379.91 14.61 35.78 185.7 4 2 3 44.78 1.30 6.59 117.4 5 2 3 441.71 5.93 20.17 191.6 6 2 3 8.50 0.65 2.95 99.8 7 2 3 161.47 2.82 11.98 186.8 8 2 3 26.41 1.38 5.60 182.1 9 2 3 20.91 1.28 4.55 0.8 10 2 3 32.07 1.60 5.54 273.5 0 3 3 767.19 51.34 27.22 90.0 1 3 3 671.18 8.97 25.21 1.2 2 3 3 78.52 1.56 8.53 96.5 3 3 3 92.14 1.76 9.43 322.7 4 3 3 71.47 1.64 7.77 287.6 5 3 3 172.06 2.66 13.07 199.6 6 3 3 41.57 1.45 5.89 304.9 7 3 3 180.51 3.04 14.35 209.0 8 3 3 48.35 1.74 7.48 326.4 9 3 3 79.07 2.28 9.19 200.0 10 3 3 78.28 2.42 8.40 279.0 0 4 3 58.04 1.37 7.16 0.0 1 4 3 284.17 4.22 15.76 279.7 2 4 3 94.08 1.77 9.03 82.9 3 4 3 593.18 9.08 24.16 331.0 4 4 3 345.26 5.18 18.30 79.1 5 4 3 113.19 2.21 10.81 318.7 6 4 3 148.74 2.61 11.92 131.8 7 4 3 12.15 1.09 4.03 299.0 8 4 3 30.18 1.56 5.46 251.1 9 4 3 35.55 1.68 5.97 168.5 10 4 3 115.45 2.86 10.39 269.0 0 5 3 167.39 2.40 13.44 270.0 1 5 3 48.02 1.33 6.18 80.7 2 5 3 235.39 2.97 14.94 289.4 3 5 3 100.63 1.94 9.21 21.6 4 5 3 46.72 1.43 6.64 80.8 5 5 3 33.36 1.26 5.72 12.3 6 5 3 308.66 4.01 17.06 93.5 7 5 3 26.84 1.41 5.41 217.8 8 5 3 441.07 7.27 20.85 95.5 9 5 3 3.60 0.51 2.06 53.1 0 6 3 168.33 2.49 13.28 180.0 1 6 3 122.81 2.16 10.43 332.9 2 6 3 367.45 5.31 18.56 250.3 3 6 3 175.46 2.66 12.83 26.1 4 6 3 369.28 5.66 18.91 264.0 5 6 3 30.89 1.31 5.53 47.7 6 6 3 69.06 1.92 8.61 294.8 7 6 3 2.51 0.46 1.77 163.7 8 6 3 9.77 0.80 3.20 318.0 9 6 3 11.82 0.88 3.35 214.7 0 7 3 84.28 1.88 9.67 90.0 1 7 3 1200.88 14.55 34.16 189.2 2 7 3 292.67 3.65 16.23 85.3 3 7 3 165.41 2.70 12.49 201.2 4 7 3 31.07 1.31 5.55 50.4 5 7 3 126.97 2.52 11.76 303.1 6 7 3 10.35 0.79 3.71 10.8 7 7 3 88.78 2.33 9.60 354.9 8 7 3 13.47 1.29 3.38 313.5 9 7 3 86.62 2.57 9.14 351.5 0 8 3 2.31 0.39 1.78 180.0 1 8 3 27.93 1.27 4.84 127.6 2 8 3 4.92 0.49 1.96 273.1 3 8 3 385.97 6.02 19.11 175.3 4 8 3 58.81 1.79 7.91 254.7 5 8 3 246.95 3.70 16.32 179.8 6 8 3 86.70 2.31 9.69 279.4 7 8 3 42.76 1.77 6.44 202.7 8 8 3 6.24 0.54 2.20 158.3 0 9 3 335.28 4.19 18.37 90.0 1 9 3 78.29 1.95 8.88 13.6 2 9 3 263.13 3.63 15.68 119.5 3 9 3 0.70 0.79 1.26 20.2 4 9 3 21.34 1.30 5.09 132.3 5 9 3 37.46 1.53 5.79 171.2 6 9 3 135.92 2.93 11.69 266.8 7 9 3 32.13 1.67 5.60 198.0 8 9 3 177.46 3.60 13.02 267.3 0 10 3 0.00 0.78 0.05 180.0 1 10 3 30.03 1.41 5.62 177.9 2 10 3 310.69 4.21 18.72 114.2 3 10 3 9.68 0.72 3.10 173.8 4 10 3 195.22 3.36 14.50 112.5 5 10 3 47.46 1.87 7.06 164.2 6 10 3 61.09 2.01 7.76 145.3 7 10 3 13.98 1.28 3.90 136.0 0 11 3 94.70 2.32 10.27 270.0 1 11 3 168.28 3.11 13.36 358.0 2 11 3 103.85 2.50 10.50 284.5 3 11 3 22.50 1.34 4.70 336.5 4 11 3 21.05 1.38 4.55 22.9 5 11 3 0.87 0.68 1.00 100.8 6 11 3 41.50 1.88 6.26 57.0 0 12 3 13.07 1.24 3.70 180.0 1 12 3 6.98 0.62 2.63 325.5 2 12 3 0.83 0.78 0.37 57.2 3 12 3 62.95 2.09 7.68 357.2 4 12 3 1.11 0.48 1.03 243.8 5 12 3 188.22 3.69 13.03 2.0 0 13 3 5.95 0.50 2.38 270.0 1 13 3 68.04 2.18 8.25 220.9 2 13 3 4.19 0.55 1.81 143.7 3 13 3 11.58 0.93 3.57 277.7 4 13 3 10.91 0.90 3.10 188.8 0 14 3 2.84 0.54 1.68 180.0 1 14 3 20.64 1.50 4.61 127.8 0 0 4 33.65 1.19 7.07 180.0 1 0 4 104.06 1.93 9.71 0.0 2 0 4 79.31 1.73 9.05 180.0 3 0 4 1087.53 13.63 31.83 0.0 4 0 4 110.86 2.20 10.58 0.0 5 0 4 350.01 5.66 18.51 0.0 6 0 4 188.40 3.10 14.56 0.0 7 0 4 224.29 3.59 15.30 0.0 8 0 4 157.02 3.15 12.85 0.0 9 0 4 2.85 0.49 1.52 180.0 0 1 4 593.44 9.11 24.01 270.0 1 1 4 347.52 5.01 17.69 197.8 2 1 4 423.83 5.76 20.80 215.4 3 1 4 364.70 5.39 18.68 223.9 4 1 4 498.59 6.72 22.17 152.2 5 1 4 50.91 1.57 6.87 298.1 6 1 4 91.05 2.24 10.20 152.2 7 1 4 69.55 2.04 8.72 356.8 8 1 4 41.48 1.71 6.29 85.4 9 1 4 48.45 1.90 6.65 34.0 0 2 4 31.19 1.16 5.86 0.0 1 2 4 440.60 5.81 20.51 91.0 2 2 4 245.21 3.17 14.93 286.6 3 2 4 119.57 2.22 10.85 161.4 4 2 4 647.46 7.89 24.98 257.4 5 2 4 95.03 2.10 9.30 262.6 6 2 4 125.29 2.55 11.70 255.9 7 2 4 99.95 2.36 10.05 272.3 8 2 4 8.32 0.64 2.78 176.8 9 2 4 49.83 2.06 6.95 297.8 0 3 4 7.61 0.55 1.85 90.0 1 3 4 211.91 2.92 14.10 146.2 2 3 4 35.87 1.30 5.65 89.6 3 3 4 937.57 12.72 29.97 128.1 4 3 4 172.62 2.82 12.97 266.4 5 3 4 262.53 3.61 15.98 117.0 6 3 4 118.73 2.48 11.53 271.2 7 3 4 61.11 1.93 8.13 38.7 8 3 4 219.52 3.77 14.86 281.6 9 3 4 32.21 1.71 5.70 293.6 0 4 4 401.86 5.69 20.99 0.0 1 4 4 181.04 2.74 13.61 238.9 2 4 4 307.48 3.74 16.97 29.2 3 4 4 215.97 3.11 14.24 199.0 4 4 4 105.41 2.21 10.32 86.8 5 4 4 40.65 1.55 6.66 117.9 6 4 4 72.25 2.02 9.15 153.0 7 4 4 46.88 1.77 6.96 97.2 8 4 4 86.37 2.41 8.85 173.2 9 4 4 24.38 1.59 4.76 40.2 0 5 4 12.24 0.93 3.41 90.0 1 5 4 471.37 6.43 21.07 0.7 2 5 4 276.29 3.63 16.25 332.0 3 5 4 53.69 1.65 7.55 320.5 4 5 4 269.55 3.73 15.69 340.4 5 5 4 56.35 1.76 7.81 183.1 6 5 4 26.33 1.39 5.15 338.0 7 5 4 39.63 1.67 6.43 185.7 8 5 4 9.52 0.83 2.90 166.8 0 6 4 310.34 3.90 17.85 180.0 1 6 4 181.20 2.89 13.50 275.5 2 6 4 179.33 2.87 12.55 185.9 3 6 4 375.55 4.49 18.86 335.6 4 6 4 30.41 1.35 5.86 49.7 5 6 4 82.81 2.15 9.61 359.7 6 6 4 77.61 2.17 8.55 34.1 7 6 4 49.38 1.91 6.79 51.2 8 6 4 83.25 2.53 8.83 329.5 0 7 4 142.77 2.63 12.35 270.0 1 7 4 79.99 1.99 9.04 208.7 2 7 4 175.78 2.98 13.13 251.8 3 7 4 95.86 2.23 10.37 268.7 4 7 4 16.58 1.10 4.17 207.1 5 7 4 79.86 2.19 9.09 296.7 6 7 4 99.06 2.51 9.93 81.8 7 7 4 0.17 0.98 0.68 296.2 8 7 4 218.18 4.03 14.30 75.9 0 8 4 5.64 0.52 2.15 180.0 1 8 4 211.41 3.35 15.15 63.8 2 8 4 164.35 2.95 13.38 276.2 3 8 4 29.76 1.45 5.70 46.5 4 8 4 128.84 2.74 11.76 269.8 5 8 4 51.86 1.84 7.18 298.4 6 8 4 23.49 1.47 4.83 302.9 7 8 4 82.79 2.51 8.97 271.4 0 9 4 65.52 1.96 8.59 90.0 1 9 4 323.93 4.39 18.96 171.7 2 9 4 181.17 3.25 14.29 116.9 3 9 4 107.41 2.52 10.62 132.9 4 9 4 53.96 1.87 7.20 174.9 5 9 4 3.16 0.50 1.72 99.4 6 9 4 25.40 1.51 4.54 191.5 0 10 4 90.06 2.36 9.88 0.0 1 10 4 21.17 1.33 4.75 274.8 2 10 4 27.71 1.51 5.70 352.2 3 10 4 45.47 1.76 6.93 187.8 4 10 4 14.86 1.30 3.48 243.9 5 10 4 126.19 2.99 10.78 171.8 6 10 4 108.81 2.81 9.94 223.4 0 11 4 21.74 1.36 4.79 90.0 1 11 4 16.58 1.25 4.16 49.6 2 11 4 46.96 1.86 6.39 12.5 3 11 4 14.70 1.29 3.72 111.1 4 11 4 71.29 2.36 8.14 15.9 5 11 4 70.83 2.36 7.82 132.3 0 12 4 14.94 1.39 4.14 180.0 1 12 4 46.15 1.91 6.49 259.2 2 12 4 104.94 2.77 9.96 113.6 3 12 4 10.34 0.91 2.98 327.6 1 0 5 164.55 2.76 12.56 270.0 2 0 5 0.00 0.76 0.06 90.0 3 0 5 22.61 1.19 4.62 270.0 4 0 5 64.02 1.91 8.65 90.0 5 0 5 47.10 1.67 6.92 90.0 6 0 5 42.83 1.71 6.46 90.0 7 0 5 208.56 3.69 13.58 90.0 8 0 5 37.43 1.75 5.85 90.0 0 1 5 59.90 1.70 8.26 90.0 1 1 5 58.70 1.68 7.50 302.3 2 1 5 45.27 1.56 7.02 18.6 3 1 5 396.70 6.27 21.42 312.0 4 1 5 160.75 2.90 13.37 37.8 5 1 5 188.22 3.24 14.17 303.0 6 1 5 50.87 1.85 7.28 337.0 7 1 5 38.07 1.70 5.99 261.4 8 1 5 9.85 0.83 2.81 112.5 0 2 5 341.50 4.19 18.40 180.0 1 2 5 8.77 0.70 3.24 122.1 2 2 5 171.35 2.92 13.10 162.7 3 2 5 22.15 1.30 4.92 0.9 4 2 5 6.21 0.56 2.67 53.6 5 2 5 5.87 0.55 2.47 270.9 6 2 5 64.27 2.07 8.26 359.8 7 2 5 71.19 2.23 8.33 340.5 8 2 5 94.52 2.67 9.71 349.1 0 3 5 160.62 2.77 12.53 270.0 1 3 5 23.85 1.22 5.21 318.1 2 3 5 122.50 2.46 11.48 189.4 3 3 5 15.46 1.16 4.11 248.0 4 3 5 247.07 3.75 16.39 161.3 5 3 5 6.18 0.60 2.42 236.3 6 3 5 93.83 2.45 9.95 175.6 7 3 5 13.52 1.24 3.27 178.5 8 3 5 0.06 1.06 0.26 53.0 0 4 5 42.59 1.61 7.21 0.0 1 4 5 223.56 3.41 15.69 69.8 2 4 5 60.54 1.77 8.07 36.7 3 4 5 56.23 1.77 7.78 102.1 4 4 5 0.00 0.86 0.16 212.1 5 4 5 26.24 1.40 4.70 309.9 6 4 5 20.47 1.41 4.35 186.0 7 4 5 122.12 2.92 10.45 257.2 0 5 5 99.34 2.27 10.41 270.0 1 5 5 40.58 1.55 6.93 121.6 2 5 5 1.02 0.89 1.70 322.7 3 5 5 193.25 3.27 14.68 114.4 4 5 5 4.74 0.49 2.12 251.2 5 5 5 119.04 2.75 11.06 99.4 6 5 5 1.44 0.46 1.14 223.1 7 5 5 33.40 1.67 5.56 32.5 0 6 5 176.72 3.12 14.04 0.0 1 6 5 171.80 3.09 13.85 253.7 2 6 5 66.42 1.99 8.48 351.9 3 6 5 25.91 1.40 5.07 251.9 4 6 5 1.41 0.45 1.42 356.1 5 6 5 18.96 1.34 4.48 47.7 6 6 5 22.03 1.42 4.43 171.0 7 6 5 59.04 2.23 7.50 63.6 0 7 5 9.36 0.78 3.17 90.0 1 7 5 110.52 2.54 10.40 4.9 2 7 5 149.07 3.01 11.96 320.8 3 7 5 19.36 1.33 4.44 342.5 4 7 5 142.86 3.08 12.24 333.5 5 7 5 4.32 0.53 2.03 307.9 6 7 5 92.74 2.63 9.05 316.1 0 8 5 146.48 3.01 12.15 180.0 1 8 5 31.95 1.57 5.78 217.8 2 8 5 83.01 2.26 9.10 172.6 3 8 5 1.00 0.98 1.59 304.5 4 8 5 19.68 1.39 4.06 104.4 5 8 5 14.91 1.30 3.38 47.6 0 9 5 18.33 1.37 4.74 270.0 1 9 5 27.89 1.51 4.98 300.6 2 9 5 35.94 1.64 5.67 221.8 3 9 5 91.89 2.49 8.85 273.5 4 9 5 23.54 1.60 4.46 221.1 0 10 5 2.86 0.52 1.52 180.0 1 10 5 148.57 3.26 11.51 56.2 2 10 5 18.04 1.43 4.38 270.6 3 10 5 26.55 1.71 5.23 24.8 0 11 5 5.46 0.55 1.93 270.0 0 0 6 267.51 4.00 16.22 0.0 1 0 6 2.88 0.44 1.71 0.0 2 0 6 70.85 2.09 8.47 0.0 3 0 6 20.35 1.41 4.55 180.0 4 0 6 0.27 0.88 0.26 180.0 5 0 6 1.00 0.49 1.27 0.0 6 0 6 14.22 1.38 3.59 180.0 0 1 6 5.66 0.50 2.42 90.0 1 1 6 23.37 1.34 4.62 114.9 2 1 6 27.01 1.39 5.13 4.4 3 1 6 54.26 1.89 7.14 68.2 4 1 6 100.84 2.62 10.34 329.8 5 1 6 32.12 1.64 5.67 74.8 6 1 6 65.75 2.26 8.07 16.3 0 2 6 2.00 0.44 1.59 0.0 1 2 6 49.66 1.79 6.76 256.9 2 2 6 1.79 0.45 1.43 283.5 3 2 6 26.48 1.54 5.51 292.9 4 2 6 0.11 0.93 1.08 123.4 5 2 6 15.67 1.33 3.77 133.6 6 2 6 4.59 0.55 1.78 317.5 0 3 6 128.49 2.77 11.18 90.0 1 3 6 24.96 1.39 5.18 293.3 2 3 6 23.74 1.38 4.80 66.6 3 3 6 115.78 2.67 11.14 313.7 4 3 6 73.78 2.24 8.78 55.5 5 3 6 84.05 2.47 8.91 304.8 0 4 6 232.47 3.83 15.36 180.0 1 4 6 23.91 1.51 4.72 101.3 2 4 6 73.45 2.19 8.63 174.8 3 4 6 4.41 0.51 2.02 178.1 4 4 6 1.16 0.49 1.27 156.8 5 4 6 41.13 1.87 6.34 189.9 0 5 6 1.78 0.49 1.71 270.0 1 5 6 7.52 0.77 2.78 271.1 2 5 6 55.04 1.96 7.29 139.2 3 5 6 12.60 0.85 3.33 290.0 4 5 6 66.40 2.24 8.16 164.5 5 5 6 0.29 0.98 0.40 53.1 0 6 6 41.78 1.86 6.13 0.0 1 6 6 50.61 1.93 7.04 64.7 2 6 6 60.97 2.13 7.54 43.8 3 6 6 9.75 0.86 3.33 127.2 4 6 6 31.09 1.75 5.48 49.3 0 7 6 13.99 1.39 3.81 270.0 1 7 6 22.84 1.56 4.95 66.4 2 7 6 2.53 0.51 1.44 347.7 3 7 6 75.83 2.42 8.52 93.3 0 8 6 56.07 2.07 7.60 0.0 1 8 6 96.76 2.70 9.75 256.0 1 0 7 33.57 1.79 5.85 90.0 2 0 7 16.80 1.45 4.21 90.0 0 1 7 83.54 2.56 9.39 270.0 1 1 7 38.90 1.84 5.98 64.1 2 1 7 37.38 1.84 5.98 229.9 0 2 7 259.59 4.41 16.00 0.0 1 2 7 24.68 1.52 4.66 328.6 0 3 7 0.00 1.10 0.44 90.0