#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/22/2202205.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202205_Fobs loop_ _publ_author_name 'Ravishankar, T.' 'Chinnakali, K.' 'Rajakumar, P.' 'Murali, V.' 'Usman, Anwar' 'Fun, Hoong-Kun' _publ_section_title ; 7,16-Dioxatetracyclo[16.2^4,5^.2^21,22^.2^23,24^.0^9,14^]tetracosa-1,3,5,9,11,13,17,19,21,23-decaene ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o293 _journal_page_last o295 _journal_volume 59 _journal_year 2003 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.463 _cell_angle_gamma 90.000 _cell_length_a 13.3086 _cell_length_b 5.8168 _cell_length_c 20.8145 _exptl_crystal_F_000 664.00 _reflns_d_resolution_high 0.7965 _[local]_cod_data_source_file wn6138Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title 'wn6138 in P2(1)/c (-90 degrees Celcius)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 140.73 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 23.59 25.66 9.25 o 4 0 0 19806.07 19112.13 1451.51 o 5 0 0 133.28 105.41 16.21 o 6 0 0 508.26 460.47 45.05 o 7 0 0 7.16 0.04 9.80 o 8 0 0 2944.98 2847.95 237.79 o 9 0 0 44.85 35.92 14.79 o 10 0 0 1226.09 1257.45 82.67 o 11 0 0 1.89 3.03 21.84 o 12 0 0 296.77 314.59 53.58 o 13 0 0 0.68 21.28 28.87 o 14 0 0 906.53 866.06 101.54 o 15 0 0 0.47 17.95 29.51 o 16 0 0 73.79 50.09 32.27 o 2 1 0 0.41 5.97 5.92 o 3 1 0 12425.99 13978.27 756.96 o 4 1 0 684.79 764.59 375.76 o 5 1 0 208.61 203.45 14.89 o 6 1 0 0.01 5.19 6.54 o 7 1 0 594.11 489.98 28.61 o 8 1 0 218.53 224.05 18.31 o 9 1 0 71.88 62.40 15.92 o 10 1 0 11.08 26.65 15.42 o 11 1 0 246.80 239.45 28.54 o 12 1 0 7.82 6.82 15.95 o 13 1 0 428.59 379.11 32.04 o 14 1 0 0.18 -0.11 13.36 o 15 1 0 12.48 24.50 20.82 o 16 1 0 2.02 9.00 21.02 o 0 2 0 6214.29 6357.89 329.81 o 1 2 0 230.75 161.39 26.88 o 2 2 0 602.24 511.34 27.26 o 3 2 0 402.69 376.80 35.00 o 4 2 0 1141.55 1129.61 72.16 o 5 2 0 258.46 249.53 31.59 o 6 2 0 942.48 975.88 65.73 o 7 2 0 402.17 439.32 51.22 o 8 2 0 400.31 435.61 39.69 o 9 2 0 9.43 -2.81 12.88 o 10 2 0 321.44 359.04 83.45 o 11 2 0 28.86 37.66 25.93 o 12 2 0 104.97 93.64 26.64 o 13 2 0 0.05 14.84 21.40 o 14 2 0 23.27 3.97 21.71 o 1 3 0 1349.19 1386.37 88.54 o 2 3 0 197.99 218.17 21.93 o 3 3 0 2253.21 2224.36 111.17 o 4 3 0 3.24 10.73 7.61 o 5 3 0 128.93 184.98 20.10 o 6 3 0 47.66 37.85 16.16 o 7 3 0 103.28 183.12 28.06 o 8 3 0 92.72 73.48 22.52 o 9 3 0 1218.41 891.42 98.94 o 10 3 0 460.51 454.92 89.31 o 11 3 0 208.26 178.76 31.85 o 12 3 0 88.21 65.40 27.58 o 13 3 0 483.44 487.18 56.81 o 14 3 0 21.31 30.80 29.61 o 15 3 0 48.88 62.72 46.56 o 0 4 0 551.49 691.71 93.42 o 1 4 0 15.78 18.19 7.58 o 2 4 0 356.90 289.66 26.99 o 3 4 0 114.33 238.50 19.80 o 4 4 0 7.07 11.63 11.59 o 5 4 0 156.38 146.54 20.15 o 6 4 0 7.59 5.40 14.24 o 7 4 0 7.12 62.09 17.87 o 8 4 0 129.43 109.25 21.81 o 9 4 0 229.51 221.26 29.76 o 10 4 0 739.70 747.65 54.91 o 11 4 0 84.02 54.29 23.27 o 12 4 0 43.80 57.24 30.97 o 13 4 0 0.13 12.13 28.21 o 1 5 0 0.22 10.08 12.87 o 2 5 0 7.93 6.67 11.61 o 3 5 0 0.27 -1.95 10.32 o 4 5 0 13.22 25.73 13.95 o 5 5 0 37.78 65.06 19.33 o 6 5 0 9.13 6.57 17.00 o 7 5 0 211.76 223.01 29.83 o 8 5 0 35.28 47.03 22.59 o 9 5 0 8.97 20.39 24.83 o 10 5 0 28.27 31.24 30.41 o 11 5 0 74.22 54.93 33.66 o 12 5 0 2.69 -28.91 33.96 o 0 6 0 65.20 70.87 37.36 o 1 6 0 8.99 26.87 24.30 o 2 6 0 63.76 79.84 23.09 o 3 6 0 0.01 10.73 23.53 o 4 6 0 91.18 74.31 23.75 o 5 6 0 73.95 74.17 32.26 o 6 6 0 9.68 7.37 37.55 o 7 6 0 1.17 -3.48 34.07 o 8 6 0 140.70 120.49 36.11 o 9 6 0 51.33 87.23 37.63 o 1 7 0 16.67 10.78 27.83 o 2 7 0 81.73 84.21 48.75 o 3 7 0 82.98 112.59 46.84 o -16 1 1 51.89 53.71 25.87 o -15 1 1 65.54 40.14 23.48 o -14 1 1 25.02 9.40 15.15 o -13 1 1 34.54 56.79 21.44 o -12 1 1 30.15 23.55 16.52 o -11 1 1 17.52 23.08 16.65 o -10 1 1 652.54 537.01 44.96 o -9 1 1 3.67 2.68 11.37 o -8 1 1 376.80 352.47 33.30 o -7 1 1 522.23 498.90 62.17 o -6 1 1 157.99 159.69 15.99 o -5 1 1 876.94 700.90 39.03 o -4 1 1 4301.48 4684.67 183.00 o -3 1 1 2604.00 2878.21 399.90 o -2 1 1 151.93 126.61 10.66 o -1 1 1 699.21 575.60 39.69 o 0 1 1 894.30 478.82 143.20 o 1 1 1 13.87 14.59 5.37 o 2 1 1 2911.91 3102.51 173.42 o 3 1 1 454.01 389.92 34.98 o 4 1 1 5441.20 4952.81 274.88 o 5 1 1 6.64 5.02 5.47 o 6 1 1 1757.96 1405.22 68.39 o 7 1 1 546.58 835.50 76.05 o 8 1 1 66.62 57.06 13.97 o 9 1 1 26.10 28.52 15.24 o 10 1 1 48.79 44.28 16.96 o 11 1 1 2.17 3.38 19.95 o 12 1 1 329.55 265.02 32.41 o 13 1 1 30.83 43.11 19.12 o 14 1 1 99.32 92.15 24.35 o 15 1 1 6.80 8.18 18.58 o 16 1 1 72.65 65.04 30.21 o -16 2 1 9.46 -5.42 32.17 o -15 2 1 178.98 142.39 37.42 o -14 2 1 29.88 60.82 29.01 o -13 2 1 25.13 41.44 34.57 o -12 2 1 231.84 205.61 31.30 o -11 2 1 2.08 -10.14 28.72 o -10 2 1 1.58 12.78 16.44 o -9 2 1 105.99 135.58 24.41 o -8 2 1 394.03 333.34 32.78 o -7 2 1 2129.52 2054.41 160.33 o -6 2 1 1311.28 1326.40 65.55 o -5 2 1 2230.83 1970.90 139.45 o -4 2 1 97.97 154.45 37.24 o -3 2 1 197.78 228.18 14.12 o -2 2 1 1805.02 1623.09 60.05 o -1 2 1 339.88 271.16 12.84 o 0 2 1 4.03 1.43 3.76 o 1 2 1 3227.72 2998.39 97.66 o 2 2 1 1627.95 1557.86 127.61 o 3 2 1 891.41 728.10 49.89 o 4 2 1 0.08 195.59 29.62 o 5 2 1 703.46 573.54 43.57 o 6 2 1 70.36 102.16 18.39 o 7 2 1 8.52 8.81 17.86 o 8 2 1 11.11 21.83 16.16 o 9 2 1 470.88 393.83 39.68 o 10 2 1 264.35 197.33 26.82 o 11 2 1 15.23 8.51 18.74 o 12 2 1 48.38 37.81 22.24 o 13 2 1 264.18 255.48 37.17 o 14 2 1 7.06 -1.31 20.20 o 15 2 1 14.14 22.86 37.18 o -15 3 1 3.63 51.01 53.89 o -14 3 1 145.42 158.94 55.24 o -13 3 1 69.98 88.47 30.30 o -12 3 1 2.26 23.31 24.70 o -11 3 1 212.29 237.47 38.55 o -10 3 1 317.04 281.14 36.41 o -9 3 1 709.82 682.19 57.12 o -8 3 1 943.39 863.39 89.26 o -7 3 1 64.85 42.89 14.62 o -6 3 1 460.49 495.33 34.45 o -5 3 1 321.19 332.24 28.99 o -4 3 1 351.63 378.40 20.25 o -3 3 1 535.21 807.68 48.93 o -2 3 1 962.70 890.61 47.80 o -1 3 1 315.29 255.94 24.53 o 0 3 1 788.47 862.76 69.41 o 1 3 1 1.74 10.14 6.10 o 2 3 1 93.95 105.34 10.84 o 3 3 1 1135.50 1096.23 44.29 o 4 3 1 740.08 671.82 55.65 o 5 3 1 630.94 626.18 98.82 o 6 3 1 25.90 34.40 16.57 o 7 3 1 58.80 58.18 19.46 o 8 3 1 1497.05 1486.31 124.62 o 9 3 1 196.31 195.87 31.95 o 10 3 1 23.47 65.71 25.91 o 11 3 1 39.96 25.17 29.60 o 12 3 1 33.42 57.34 26.75 o 13 3 1 212.31 195.41 38.21 o 14 3 1 6.67 15.24 25.43 o 15 3 1 13.67 4.13 27.79 o -13 4 1 46.34 28.03 31.72 o -12 4 1 12.91 30.30 40.10 o -11 4 1 16.66 6.81 24.32 o -10 4 1 124.60 123.28 24.81 o -9 4 1 456.14 386.55 36.73 o -8 4 1 297.79 302.86 30.88 o -7 4 1 178.32 165.21 22.42 o -6 4 1 215.81 212.65 24.29 o -5 4 1 215.46 219.26 24.34 o -4 4 1 80.93 70.47 13.60 o -3 4 1 878.02 820.37 42.33 o -2 4 1 0.14 -0.75 7.05 o -1 4 1 36.29 35.26 8.50 o 0 4 1 536.13 666.00 43.66 o 1 4 1 3.04 2.19 7.46 o 2 4 1 13.16 15.28 7.35 o 3 4 1 17.05 29.24 13.38 o 4 4 1 55.78 49.79 12.97 o 5 4 1 126.82 125.62 19.52 o 6 4 1 651.36 634.94 44.22 o 7 4 1 278.45 309.19 30.23 o 8 4 1 289.23 294.19 31.97 o 9 4 1 0.00 4.82 18.95 o 10 4 1 814.72 833.77 59.18 o 11 4 1 116.68 133.19 27.30 o 12 4 1 21.31 57.33 29.59 o 13 4 1 4.25 31.56 28.21 o -12 5 1 8.25 -13.35 27.47 o -11 5 1 140.96 127.76 38.53 o -10 5 1 42.42 75.19 32.69 o -9 5 1 50.22 67.53 32.44 o -8 5 1 0.12 -4.32 18.88 o -7 5 1 31.49 17.21 19.27 o -6 5 1 59.42 63.69 21.97 o -5 5 1 89.88 56.44 15.13 o -4 5 1 240.27 200.37 22.07 o -3 5 1 0.11 0.50 10.39 o -2 5 1 20.63 17.81 12.28 o -1 5 1 10.53 13.32 11.75 o 0 5 1 322.83 373.85 24.48 o 1 5 1 22.31 13.50 12.95 o 2 5 1 109.27 85.38 15.66 o 3 5 1 0.00 -1.52 14.27 o 4 5 1 20.40 15.84 13.33 o 5 5 1 22.47 12.58 15.79 o 6 5 1 163.42 152.66 24.62 o 7 5 1 76.21 68.88 21.06 o 8 5 1 12.29 33.03 20.63 o 9 5 1 90.82 81.61 25.74 o 10 5 1 5.00 17.38 21.85 o 11 5 1 28.88 -9.20 23.78 o 12 5 1 3.04 -25.17 34.86 o -9 6 1 13.05 3.64 27.55 o -8 6 1 26.49 42.98 36.16 o -7 6 1 0.11 16.29 26.38 o -6 6 1 1.81 16.19 28.65 o -5 6 1 251.22 243.86 46.36 o -4 6 1 7.17 5.38 17.35 o -3 6 1 3.97 37.01 21.01 o -2 6 1 2.91 -16.19 16.35 o -1 6 1 444.34 441.15 49.41 o 0 6 1 9.82 -2.44 19.56 o 1 6 1 576.25 519.81 52.90 o 2 6 1 2.44 11.46 17.93 o 3 6 1 65.41 71.28 21.73 o 4 6 1 70.81 77.50 27.10 o 5 6 1 289.39 255.15 43.47 o 6 6 1 4.73 15.97 25.53 o 7 6 1 10.83 14.25 40.06 o 8 6 1 63.59 79.18 40.88 o 9 6 1 46.55 67.28 35.37 o -4 7 1 17.01 23.83 36.66 o -3 7 1 6.16 13.54 44.88 o -2 7 1 9.47 68.67 50.38 o -1 7 1 4.29 18.40 41.25 o 0 7 1 17.99 21.65 27.57 o 1 7 1 0.27 -11.28 24.47 o 2 7 1 76.52 50.27 33.24 o 3 7 1 17.72 21.74 29.49 o -16 0 2 190.76 153.45 49.01 o -15 0 2 2.61 -15.00 23.67 o -14 0 2 20.17 12.64 33.78 o -13 0 2 385.82 439.58 65.69 o -12 0 2 766.19 683.54 82.96 o -11 0 2 649.66 636.32 165.65 o -10 0 2 0.49 -4.68 8.93 o -9 0 2 3.23 2.28 11.93 o -8 0 2 7.26 9.61 15.30 o -7 0 2 192.16 200.40 28.59 o -6 0 2 21.60 23.05 12.31 o -5 0 2 2230.41 1411.05 117.62 o -4 0 2 18.43 -0.52 4.87 o -2 0 2 114.95 74.78 10.28 o 2 0 2 629.42 676.45 66.00 o 4 0 2 1015.71 1082.40 65.53 o 5 0 2 2627.94 2442.33 194.10 o 6 0 2 243.37 274.06 42.06 o 7 0 2 140.99 155.31 20.52 o 8 0 2 17.53 20.11 12.40 o 9 0 2 783.88 775.89 82.59 o 10 0 2 18.81 24.83 15.24 o 11 0 2 671.21 769.88 89.70 o 12 0 2 793.05 701.25 79.91 o 13 0 2 172.49 226.01 50.90 o 14 0 2 19.62 2.43 24.99 o 15 0 2 119.28 87.26 33.19 o 16 0 2 253.79 236.90 54.65 o -16 1 2 18.95 16.32 22.05 o -15 1 2 151.07 129.94 27.64 o -14 1 2 73.03 77.95 30.59 o -13 1 2 81.25 81.78 21.13 o -12 1 2 5.08 -5.22 12.91 o -11 1 2 27.76 9.24 16.11 o -10 1 2 194.86 256.60 28.63 o -9 1 2 2.38 2.77 8.61 o -8 1 2 1534.20 1517.60 267.00 o -7 1 2 274.69 318.89 19.82 o -6 1 2 1324.30 1272.10 63.00 o -5 1 2 543.35 438.80 32.04 o -4 1 2 65.37 197.53 161.85 o -3 1 2 124.32 153.50 19.41 o -2 1 2 2988.20 2681.48 95.03 o -1 1 2 43.44 36.87 4.97 o 0 1 2 8046.45 10672.49 366.50 o 1 1 2 1.14 4.64 9.61 o 2 1 2 4937.86 5284.27 291.07 o 3 1 2 427.46 435.09 118.24 o 4 1 2 619.96 619.85 143.85 o 5 1 2 174.90 175.38 14.57 o 6 1 2 1475.62 1480.33 115.23 o 7 1 2 425.05 395.97 39.48 o 8 1 2 155.49 130.92 18.95 o 9 1 2 30.54 16.03 12.32 o 10 1 2 123.41 187.24 24.65 o 11 1 2 141.69 135.08 22.93 o 12 1 2 4.53 5.40 12.30 o 13 1 2 102.15 86.49 23.53 o 14 1 2 0.41 6.06 16.31 o 15 1 2 53.99 33.59 23.35 o 16 1 2 18.40 21.58 31.50 o -15 2 2 23.06 35.35 43.70 o -14 2 2 3.79 -0.53 21.88 o -13 2 2 41.86 50.92 26.10 o -12 2 2 0.99 -12.85 17.03 o -11 2 2 93.15 144.73 30.85 o -10 2 2 12.67 29.85 18.05 o -9 2 2 960.23 814.76 69.36 o -8 2 2 1067.25 932.44 116.75 o -7 2 2 175.35 223.61 25.21 o -6 2 2 132.42 142.79 31.93 o -5 2 2 1689.99 1568.78 101.47 o -4 2 2 1267.36 1140.06 44.73 o -3 2 2 424.66 374.97 34.43 o -2 2 2 93.83 81.06 7.60 o -1 2 2 23.04 19.40 4.09 o 0 2 2 442.38 464.93 23.06 o 1 2 2 55.46 48.35 5.44 o 2 2 2 155.74 146.97 10.95 o 3 2 2 171.94 154.93 18.49 o 4 2 2 157.60 127.03 18.52 o 5 2 2 426.41 382.66 45.64 o 6 2 2 37.90 71.33 46.37 o 7 2 2 8.95 14.25 13.93 o 8 2 2 622.22 631.43 51.65 o 9 2 2 931.24 959.87 71.03 o 10 2 2 110.91 195.25 30.61 o 11 2 2 77.51 70.67 21.78 o 12 2 2 16.34 25.92 19.74 o 13 2 2 90.03 102.69 27.82 o 14 2 2 1.18 -3.18 20.14 o 15 2 2 38.93 26.08 21.62 o -15 3 2 0.72 14.47 42.52 o -14 3 2 27.97 12.95 36.70 o -13 3 2 15.83 17.17 36.21 o -12 3 2 430.73 397.62 46.04 o -11 3 2 187.94 233.47 36.62 o -10 3 2 149.45 212.97 33.97 o -9 3 2 804.91 782.72 52.03 o -8 3 2 5.05 8.11 12.79 o -7 3 2 723.03 769.25 48.85 o -6 3 2 0.00 3.60 9.60 o -5 3 2 19.39 19.39 10.65 o -4 3 2 12.71 32.47 13.98 o -3 3 2 923.46 978.49 53.73 o -2 3 2 74.28 71.91 7.80 o -1 3 2 652.34 619.49 67.96 o 0 3 2 523.06 398.83 92.61 o 1 3 2 2004.02 1920.79 115.99 o 2 3 2 601.00 532.00 26.18 o 3 3 2 232.13 251.53 25.74 o 4 3 2 7.42 51.71 74.44 o 5 3 2 10.54 12.49 12.66 o 6 3 2 22.07 26.46 15.89 o 7 3 2 63.00 80.15 21.97 o 8 3 2 0.16 3.50 17.27 o 9 3 2 661.57 596.57 53.42 o 10 3 2 333.80 309.52 39.23 o 11 3 2 0.28 23.33 23.62 o 12 3 2 238.43 247.79 38.84 o 13 3 2 55.93 68.54 29.96 o 14 3 2 1.33 4.95 26.20 o -13 4 2 121.74 116.32 37.11 o -12 4 2 47.83 35.17 29.32 o -11 4 2 1.63 -4.37 20.10 o -10 4 2 64.56 106.73 30.38 o -9 4 2 0.45 26.73 17.85 o -8 4 2 0.45 9.24 13.60 o -7 4 2 439.35 430.85 35.16 o -6 4 2 130.26 117.92 19.60 o -5 4 2 1078.64 1038.54 52.81 o -4 4 2 1.07 -1.52 9.11 o -3 4 2 2.61 1.54 8.87 o -2 4 2 139.76 126.39 13.31 o -1 4 2 98.15 104.40 16.28 o 0 4 2 117.49 131.83 15.21 o 1 4 2 70.24 58.13 9.53 o 2 4 2 586.12 568.80 31.04 o 3 4 2 118.52 251.17 20.47 o 4 4 2 42.43 41.54 14.96 o 5 4 2 401.16 407.62 32.80 o 6 4 2 87.88 99.40 18.85 o 7 4 2 67.13 58.02 17.74 o 8 4 2 7.59 27.05 16.17 o 9 4 2 0.42 -0.72 20.32 o 10 4 2 94.17 99.84 38.17 o 11 4 2 0.08 -4.45 22.32 o 12 4 2 2.39 -16.29 23.55 o 13 4 2 1.01 6.36 41.33 o -12 5 2 0.05 -8.14 28.22 o -11 5 2 26.11 25.21 27.31 o -10 5 2 70.69 34.94 34.63 o -9 5 2 110.02 85.02 27.97 o -8 5 2 155.14 150.36 34.04 o -7 5 2 20.93 42.35 24.70 o -6 5 2 14.87 35.92 25.50 o -5 5 2 150.38 154.20 21.57 o -4 5 2 350.14 368.14 29.30 o -3 5 2 0.09 5.73 12.88 o -2 5 2 202.17 193.11 21.77 o -1 5 2 1.12 9.34 11.46 o 0 5 2 115.77 143.03 19.04 o 1 5 2 14.70 11.78 13.07 o 2 5 2 0.05 15.93 13.32 o 3 5 2 0.26 12.66 13.15 o 4 5 2 108.62 93.14 19.61 o 5 5 2 611.69 507.59 42.44 o 6 5 2 0.74 8.94 17.98 o 7 5 2 24.73 37.04 20.10 o 8 5 2 73.85 90.01 23.26 o 9 5 2 66.96 67.28 25.63 o 10 5 2 5.14 18.14 21.21 o 11 5 2 35.82 77.55 30.06 o -9 6 2 3.33 35.40 37.70 o -8 6 2 0.17 -6.21 27.33 o -7 6 2 0.47 14.23 28.08 o -6 6 2 1.79 -15.11 22.09 o -5 6 2 30.43 32.05 20.93 o -4 6 2 17.96 42.52 22.55 o -3 6 2 5.18 29.40 27.62 o -2 6 2 1.05 -1.49 20.08 o -1 6 2 38.47 41.96 25.35 o 0 6 2 29.82 17.24 23.20 o 1 6 2 74.65 54.31 25.76 o 2 6 2 49.16 40.39 21.87 o 3 6 2 139.13 150.27 29.58 o 4 6 2 182.58 159.25 36.04 o 5 6 2 13.12 2.35 21.85 o 6 6 2 19.03 22.37 28.32 o 7 6 2 13.86 15.01 28.04 o 8 6 2 141.20 186.24 43.76 o 9 6 2 31.00 36.79 34.75 o -4 7 2 124.16 118.05 54.51 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