#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2202206.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202206_Fobs loop_ _publ_author_name 'Kruger, Gert J.' 'Rademeyer, Melanie' 'Billing, David G.' _publ_section_title ; n-Undecylammonium bromide monohydrate ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o480 _journal_page_last o482 _journal_volume 59 _journal_year 2003 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 105.650 _cell_angle_gamma 90.000 _cell_length_a 4.8094 _cell_length_b 40.3526 _cell_length_c 7.8823 _exptl_crystal_F_000 576.00 _reflns_d_resolution_high 0.7494 _[local]_cod_data_source_file wn6139Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' C11Br.H2O in P 21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 158.60 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 109.88 180.29 22.14 o 2 0 0 17835.29 17238.62 163.21 o 3 0 0 1629.05 1496.70 60.10 o 4 0 0 23.53 36.72 18.88 o 5 0 0 427.87 417.51 61.36 o 1 1 0 1848.59 2135.04 28.59 o 2 1 0 4649.78 4436.94 53.90 o 3 1 0 2585.20 2319.49 43.26 o 4 1 0 1107.48 1136.43 28.10 o 5 1 0 139.26 176.74 28.00 o 0 2 0 6052.88 0.00 2.24 o 1 2 0 19.95 48.38 7.91 o 2 2 0 3053.40 2907.12 56.30 o 3 2 0 1359.86 1290.73 36.62 o 4 2 0 431.15 448.89 29.28 o 5 2 0 441.67 492.21 38.24 o 1 3 0 4449.14 4802.39 110.24 o 2 3 0 2071.30 2029.37 32.21 o 3 3 0 1672.03 1623.17 36.93 o 4 3 0 967.43 952.01 28.26 o 5 3 0 27.96 58.04 24.34 o 0 4 0 7895.17 7375.85 110.70 o 1 4 0 40.60 72.87 8.53 o 2 4 0 3644.89 3501.44 77.10 o 3 4 0 808.40 796.30 25.53 o 4 4 0 339.81 364.23 25.75 o 5 4 0 243.49 303.88 34.95 o 6 4 0 0.85 0.00 69.58 o 1 5 0 7309.96 7707.63 94.02 o 2 5 0 779.34 796.63 37.38 o 3 5 0 738.13 721.75 34.05 o 4 5 0 531.52 548.74 27.13 o 5 5 0 4.69 21.96 24.57 o 6 5 0 66.51 20.24 63.89 o 0 6 0 4302.85 4475.76 40.48 o 1 6 0 238.56 272.84 9.92 o 2 6 0 2525.06 2461.79 36.23 o 3 6 0 375.03 395.01 27.20 o 4 6 0 218.71 246.91 22.34 o 5 6 0 112.81 127.08 30.75 o 6 6 0 0.69 0.00 58.20 o 1 7 0 5247.79 5228.17 78.49 o 2 7 0 151.80 166.06 12.14 o 3 7 0 124.92 137.35 15.52 o 4 7 0 227.52 283.72 22.54 o 5 7 0 4.81 16.49 32.94 o 6 7 0 20.58 47.44 67.69 o 0 8 0 27.46 59.41 33.84 o 1 8 0 561.19 635.12 13.92 o 2 8 0 719.65 673.49 16.75 o 3 8 0 70.89 82.74 14.94 o 4 8 0 100.79 126.30 25.42 o 5 8 0 15.04 41.86 30.85 o 6 8 0 1.91 76.54 74.65 o 1 9 0 1075.96 1105.63 16.62 o 2 9 0 1.72 3.30 7.03 o 3 9 0 14.69 15.73 11.28 o 4 9 0 24.54 37.18 27.77 o 5 9 0 0.37 0.00 32.42 o 6 9 0 0.04 0.00 60.73 o 0 10 0 3394.57 3411.58 43.81 o 1 10 0 303.90 295.54 12.27 o 2 10 0 6.90 0.00 7.57 o 3 10 0 4.94 0.00 11.09 o 4 10 0 4.60 0.00 20.11 o 5 10 0 3.36 0.00 32.57 o 6 10 0 0.13 0.00 57.57 o 1 11 0 111.34 125.53 8.84 o 2 11 0 222.24 235.85 14.36 o 3 11 0 183.14 217.95 14.72 o 4 11 0 19.20 13.65 18.70 o 5 11 0 0.01 26.16 37.05 o 6 11 0 11.71 18.98 61.36 o 0 12 0 7595.32 7228.73 159.73 o 1 12 0 74.46 124.31 9.13 o 2 12 0 845.73 837.71 34.06 o 3 12 0 328.77 299.59 17.52 o 4 12 0 29.31 24.16 21.59 o 5 12 0 54.52 0.00 37.68 o 6 12 0 0.21 25.30 72.75 o 1 13 0 1234.00 1367.22 20.19 o 2 13 0 1054.87 1021.56 19.48 o 3 13 0 197.79 211.40 18.74 o 4 13 0 311.74 318.25 28.51 o 5 13 0 0.80 0.00 33.59 o 0 14 0 7372.31 6963.04 207.49 o 1 14 0 1803.15 2129.53 29.80 o 2 14 0 2197.25 2167.66 26.12 o 3 14 0 1733.74 1556.21 42.26 o 4 14 0 115.17 102.60 24.14 o 5 14 0 304.05 281.84 43.32 o 1 15 0 2769.14 2856.28 52.55 o 2 15 0 1918.10 1954.98 30.83 o 3 15 0 676.69 665.69 25.86 o 4 15 0 929.58 938.65 41.28 o 5 15 0 22.78 50.90 34.41 o 0 16 0 6041.08 6163.98 68.66 o 1 16 0 4232.86 5152.58 106.14 o 2 16 0 3694.92 3559.39 46.39 o 3 16 0 520.26 506.01 24.51 o 4 16 0 301.99 301.07 28.29 o 5 16 0 15.31 8.13 33.09 o 1 17 0 5867.62 5715.02 47.97 o 2 17 0 2606.95 2500.93 71.58 o 3 17 0 728.78 753.96 28.08 o 4 17 0 1401.55 1299.54 46.03 o 5 17 0 25.31 45.80 37.37 o 0 18 0 5657.75 5178.01 65.08 o 1 18 0 2086.64 2211.27 31.59 o 2 18 0 3677.23 3493.85 75.54 o 3 18 0 1799.00 1660.97 45.03 o 4 18 0 288.63 352.63 30.89 o 5 18 0 364.53 366.97 51.35 o 1 19 0 5749.56 5478.30 98.98 o 2 19 0 874.20 885.38 21.62 o 3 19 0 496.59 533.66 32.34 o 4 19 0 803.61 717.35 48.98 o 5 19 0 14.17 0.00 40.43 o 0 20 0 5647.48 5679.77 73.13 o 1 20 0 1165.23 1220.32 32.80 o 2 20 0 3409.73 3278.20 35.37 o 3 20 0 1043.54 972.49 38.75 o 4 20 0 289.18 312.86 42.78 o 5 20 0 225.26 308.81 50.97 o 1 21 0 4727.35 4517.74 46.69 o 2 21 0 236.13 246.89 15.19 o 3 21 0 656.51 678.26 34.54 o 4 21 0 406.40 479.23 63.26 o 5 21 0 31.78 58.56 58.83 o 0 22 0 4450.79 4516.06 69.90 o 1 22 0 436.19 459.59 24.01 o 2 22 0 2276.19 2188.45 43.64 o 3 22 0 575.39 561.91 33.56 o 4 22 0 180.45 227.92 40.25 o 5 22 0 153.36 166.83 44.30 o 1 23 0 2489.73 2382.60 54.05 o 2 23 0 122.42 128.48 15.71 o 3 23 0 618.53 630.79 52.95 o 4 23 0 229.24 271.98 44.28 o 5 23 0 36.69 25.48 38.19 o 0 24 0 2141.54 2110.13 65.16 o 1 24 0 123.67 174.93 17.73 o 2 24 0 964.95 932.54 27.84 o 3 24 0 307.91 368.63 30.06 o 4 24 0 77.16 81.91 35.33 o 5 24 0 91.86 23.79 38.67 o 1 25 0 685.30 659.96 25.94 o 2 25 0 79.03 67.99 19.76 o 3 25 0 407.36 418.73 32.00 o 4 25 0 70.54 100.70 37.25 o 5 25 0 27.76 0.00 38.88 o 0 26 0 699.22 792.96 40.02 o 1 26 0 16.72 18.59 14.41 o 2 26 0 186.99 256.63 24.90 o 3 26 0 104.92 139.83 29.68 o 4 26 0 21.04 28.80 34.36 o 5 26 0 34.61 56.72 42.58 o 1 27 0 62.98 43.72 16.07 o 2 27 0 39.70 24.49 27.06 o 3 27 0 155.30 161.20 37.57 o 4 27 0 5.57 0.00 32.89 o 5 27 0 22.03 0.00 42.50 o 0 28 0 254.40 294.36 59.46 o 1 28 0 6.63 0.00 15.23 o 2 28 0 1.96 0.00 28.34 o 3 28 0 4.82 0.00 38.59 o 4 28 0 0.25 0.00 33.43 o 5 28 0 4.68 0.00 45.52 o 1 29 0 0.47 0.00 14.99 o 2 29 0 0.22 0.00 32.89 o 3 29 0 20.65 27.12 31.25 o 4 29 0 30.06 32.63 36.77 o 5 29 0 4.60 11.94 47.86 o 0 30 0 310.19 404.58 35.30 o 1 30 0 44.66 46.71 17.24 o 2 30 0 0.66 29.15 43.02 o 3 30 0 21.75 56.53 32.21 o 4 30 0 7.42 0.00 36.48 o 5 30 0 3.35 0.00 72.75 o 1 31 0 108.22 116.37 19.96 o 2 31 0 209.31 217.84 37.99 o 3 31 0 13.12 29.97 35.70 o 4 31 0 112.79 110.90 44.40 o 5 31 0 1.88 0.00 45.62 o 0 32 0 7698.25 7976.69 111.90 o 1 32 0 75.08 46.56 18.07 o 2 32 0 1434.65 1045.12 54.55 o 3 32 0 94.22 83.88 55.04 o 4 32 0 23.37 57.16 43.77 o 1 33 0 62.39 103.75 20.33 o 2 33 0 180.15 199.98 35.99 o 3 33 0 105.99 81.29 40.70 o 4 33 0 126.10 90.89 46.55 o 0 34 0 569.07 606.86 44.73 o 1 34 0 49.06 50.17 23.65 o 2 34 0 286.92 256.75 38.34 o 3 34 0 164.73 124.96 39.99 o 4 34 0 23.48 15.68 40.58 o 1 35 0 555.03 592.72 29.66 o 2 35 0 203.69 195.56 37.57 o 3 35 0 187.33 191.81 41.76 o 4 35 0 157.07 100.84 43.28 o 0 36 0 980.40 947.10 72.75 o 1 36 0 30.91 59.91 20.76 o 2 36 0 408.89 443.31 65.79 o 3 36 0 172.76 137.18 38.91 o 4 36 0 33.97 0.00 40.28 o 1 37 0 1035.42 898.23 52.33 o 2 37 0 217.06 209.10 62.31 o 3 37 0 229.73 243.84 43.01 o 4 37 0 129.94 76.86 43.15 o 0 38 0 1058.72 1250.32 73.38 o 1 38 0 17.05 0.00 27.06 o 2 38 0 430.61 411.19 44.72 o 3 38 0 131.48 123.30 42.02 o 4 38 0 46.94 95.70 45.29 o 1 39 0 936.87 843.56 51.88 o 2 39 0 187.26 200.73 37.12 o 3 39 0 187.91 99.70 43.33 o 4 39 0 95.52 94.77 49.75 o 0 40 0 683.78 728.74 50.77 o 1 40 0 19.84 15.23 28.85 o 2 40 0 304.59 236.01 44.28 o 3 40 0 96.99 71.97 43.81 o 4 40 0 47.23 47.35 54.72 o 1 41 0 533.07 581.62 49.55 o 2 41 0 114.46 124.03 37.00 o 3 41 0 106.64 102.49 42.95 o 0 42 0 230.34 249.36 57.57 o 1 42 0 13.27 38.32 34.56 o 2 42 0 139.18 157.08 41.48 o 3 42 0 57.32 40.68 51.24 o 1 43 0 209.01 230.56 42.51 o 2 43 0 40.07 0.00 45.86 o 3 43 0 51.69 83.44 41.42 o 0 44 0 73.11 30.01 33.32 o 1 44 0 0.84 0.50 37.64 o 2 44 0 59.70 70.68 41.42 o 3 44 0 11.97 33.35 39.24 o 1 45 0 91.52 39.26 35.96 o 2 45 0 0.13 0.00 39.04 o 3 45 0 46.80 46.94 42.49 o 0 46 0 5.21 0.00 55.67 o 1 46 0 12.46 2.90 33.92 o 2 46 0 10.49 0.00 39.95 o 3 46 0 21.40 0.00 44.47 o 1 47 0 44.64 87.71 38.20 o 2 47 0 7.92 0.00 39.04 o 3 47 0 2.61 0.00 43.38 o 1 48 0 130.47 161.32 44.94 o 2 48 0 1.66 0.00 51.56 o 1 49 0 4.67 43.68 56.93 o 2 49 0 111.43 80.10 42.99 o 1 50 0 3.95 0.00 41.68 o 2 50 0 10.96 0.00 42.56 o 1 51 0 29.82 0.00 40.97 o 1 52 0 7.92 17.47 41.87 o 1 53 0 54.16 1.27 57.57 o -5 1 1 334.62 329.97 26.72 o -4 1 1 15.77 9.52 20.73 o -3 1 1 88.54 15.97 18.56 o -2 1 1 454.57 444.97 25.30 o -1 1 1 20001.42 17742.16 149.92 o 0 1 1 23.16 56.87 3.65 o 1 1 1 22582.81 20352.47 141.48 o 2 1 1 3.69 0.57 7.25 o 3 1 1 589.79 628.30 19.90 o 4 1 1 19.51 22.87 17.51 o 5 1 1 55.46 55.48 33.75 o -5 2 1 0.24 0.00 19.37 o -4 2 1 47.80 55.87 18.68 o -3 2 1 246.83 289.04 25.93 o -2 2 1 228.94 259.72 55.98 o -1 2 1 5680.45 6017.35 53.38 o 0 2 1 337.96 314.53 6.33 o 1 2 1 5188.72 5239.67 31.20 o 2 2 1 9.98 7.99 7.63 o 3 2 1 52.30 66.34 12.12 o 4 2 1 187.61 201.59 22.42 o 5 2 1 4.71 18.57 36.10 o -5 3 1 137.75 162.92 26.30 o -4 3 1 185.70 193.24 22.71 o -3 3 1 228.99 243.29 18.78 o -2 3 1 2842.97 2755.63 46.17 o -1 3 1 212.20 235.02 11.06 o 0 3 1 311.19 371.16 12.94 o 1 3 1 746.99 826.22 36.00 o 2 3 1 171.85 176.96 10.97 o 3 3 1 653.93 695.03 21.81 o 4 3 1 98.12 95.30 18.36 o 5 3 1 76.08 74.91 35.39 o -5 4 1 95.13 144.17 23.47 o -4 4 1 321.29 365.47 34.55 o -3 4 1 951.22 924.52 28.64 o -2 4 1 601.09 641.34 20.64 o -1 4 1 4970.16 5013.47 74.69 o 0 4 1 75.24 69.01 5.55 o 1 4 1 10089.87 9768.77 47.35 o 2 4 1 148.22 139.13 14.92 o 3 4 1 292.13 319.22 17.51 o 4 4 1 447.01 426.94 26.92 o 5 4 1 13.66 2.10 33.85 o -5 5 1 325.99 366.54 43.67 o -4 5 1 293.95 385.78 45.30 o -3 5 1 434.98 450.71 25.47 o -2 5 1 4815.19 4519.25 105.33 o -1 5 1 895.75 940.76 14.81 o 0 5 1 2285.09 2564.37 39.84 o 1 5 1 596.16 715.89 66.56 o 2 5 1 879.88 898.87 26.38 o 3 5 1 1553.57 1528.24 27.42 o 4 5 1 190.22 239.01 26.11 o 5 5 1 210.36 222.49 99.32 o -5 6 1 119.87 149.56 38.44 o -4 6 1 673.84 641.53 32.18 o -3 6 1 1715.53 1578.93 41.60 o -2 6 1 677.85 669.37 19.45 o -1 6 1 7380.77 7353.52 119.33 o 0 6 1 418.76 485.88 12.15 o 1 6 1 13720.15 13812.92 102.10 o 2 6 1 751.57 752.88 17.55 o 3 6 1 645.95 680.62 27.77 o 4 6 1 658.37 607.95 29.35 o 5 6 1 2.42 11.02 33.29 o -6 7 1 1.69 14.55 62.63 o -5 7 1 465.54 465.16 46.38 o -4 7 1 432.37 508.63 27.46 o -3 7 1 751.83 724.79 24.39 o -2 7 1 5476.58 5479.17 62.28 o -1 7 1 204.94 240.35 11.78 o 0 7 1 6832.62 7572.86 49.67 o 1 7 1 2148.07 2428.68 116.94 o 2 7 1 2155.37 2151.20 45.71 o 3 7 1 2325.81 2203.73 31.51 o 4 7 1 199.22 183.29 25.86 o 5 7 1 323.05 342.37 47.13 o -6 8 1 119.71 116.40 65.79 o -5 8 1 146.45 157.30 38.67 o -4 8 1 798.36 743.67 33.13 o -3 8 1 2564.26 2265.21 43.55 o -2 8 1 645.99 687.53 18.40 o -1 8 1 11717.06 11712.94 90.31 o 0 8 1 1250.54 1246.44 48.85 o 1 8 1 12743.34 12359.59 121.79 o 2 8 1 1519.55 1456.39 45.40 o 3 8 1 875.41 940.62 28.85 o 4 8 1 807.83 764.29 38.28 o 5 8 1 0.10 31.08 28.60 o -6 9 1 4.71 0.00 55.04 o -5 9 1 434.20 495.91 46.91 o -4 9 1 488.20 496.55 28.17 o -3 9 1 1078.97 964.57 26.46 o -2 9 1 5104.41 5054.98 42.63 o -1 9 1 0.77 2.96 9.48 o 0 9 1 10761.44 10397.16 164.32 o 1 9 1 3799.65 4135.89 46.16 o 2 9 1 3161.43 3133.16 68.28 o 3 9 1 2438.90 2356.13 37.76 o 4 9 1 186.39 181.71 27.92 o 5 9 1 437.49 458.44 41.20 o -6 10 1 151.56 158.80 47.19 o -5 10 1 117.67 122.72 33.27 o -4 10 1 768.50 728.53 29.46 o -3 10 1 3088.57 2797.43 46.47 o -2 10 1 644.12 705.78 19.61 o -1 10 1 15949.06 15927.88 230.66 o 0 10 1 448.42 434.44 15.24 o 1 10 1 7775.56 7611.17 118.56 o 2 10 1 1775.71 1655.43 21.57 o 3 10 1 851.25 866.67 34.00 o 4 10 1 739.68 757.77 37.83 o 5 10 1 7.03 3.23 29.10 o -6 11 1 7.74 0.00 70.85 o -5 11 1 396.61 441.11 44.67 o -4 11 1 567.34 577.33 25.56 o -3 11 1 1341.08 1259.52 28.76 o -2 11 1 4157.41 3929.00 40.54 o -1 11 1 1.05 0.00 9.85 o 0 11 1 10752.46 10940.35 179.49 o 1 11 1 3524.06 3814.28 98.36 o 2 11 1 3036.06 2937.60 34.30 o 3 11 1 1955.02 1940.90 62.06 o 4 11 1 82.69 71.45 23.35 o 5 11 1 399.81 428.78 42.22 o -6 12 1 128.21 163.21 73.38 o -5 12 1 109.56 152.03 36.44 o -4 12 1 589.60 571.29 24.72 o -3 12 1 3218.50 3166.10 76.34 o -2 12 1 524.97 536.03 19.02 o -1 12 1 15557.64 15246.36 294.98 o 0 12 1 68.13 78.96 10.33 o 1 12 1 3042.59 3235.66 31.51 o 2 12 1 1185.63 1168.90 33.51 o 3 12 1 454.71 464.21 30.52 o 4 12 1 500.41 565.61 38.93 o 5 12 1 4.38 0.00 31.42 o -6 13 1 19.84 37.32 62.63 o -5 13 1 290.69 342.49 44.49 o -4 13 1 606.70 626.92 36.78 o -3 13 1 1209.86 1223.97 37.74 o -2 13 1 2093.84 2216.42 39.03 o -1 13 1 5.04 0.00 11.01 o 0 13 1 7417.33 7326.11 54.11 o 1 13 1 2020.07 2022.04 49.57 o 2 13 1 2932.08 2643.83 33.10 o 3 13 1 1181.82 1148.96 40.48 o 4 13 1 35.35 19.97 23.51 o 5 13 1 275.47 221.42 43.95 o -6 14 1 65.02 0.00 57.57 o -5 14 1 81.60 107.72 39.58 o -4 14 1 60.91 40.81 22.26 o -3 14 1 2211.27 2138.32 62.50 o -2 14 1 16.51 15.75 9.30 o -1 14 1 9357.89 9695.93 61.28 o 0 14 1 398.90 429.89 25.02 o 1 14 1 1007.50 1026.78 16.78 o 2 14 1 639.67 638.91 30.41 o 3 14 1 237.72 270.81 27.52 o 4 14 1 387.18 460.61 35.02 o 5 14 1 2.55 29.10 55.04 o -6 15 1 4.73 56.93 67.69 o -5 15 1 118.59 87.17 39.85 o -4 15 1 45.29 40.09 28.46 o -3 15 1 470.98 470.16 24.43 o -2 15 1 1730.76 1955.58 26.86 o -1 15 1 23.81 18.19 10.23 o 0 15 1 2347.47 2375.96 89.66 o 1 15 1 706.77 681.51 14.93 o 2 15 1 7396.94 6937.36 86.92 o 3 15 1 507.26 540.74 34.09 o 4 15 1 847.81 840.21 39.49 o 5 15 1 143.95 138.38 42.69 o -6 16 1 33.37 53.77 71.48 o -5 16 1 27.33 10.62 37.17 o -4 16 1 105.87 154.04 31.53 o -3 16 1 756.19 754.24 27.71 o -2 16 1 69.25 75.51 10.80 o -1 16 1 3454.18 3339.48 75.24 o 0 16 1 14.57 13.04 10.19 o 1 16 1 319.77 308.71 13.78 o 2 16 1 662.15 688.54 26.02 o 3 16 1 164.14 202.91 26.88 o 4 16 1 144.68 169.54 25.83 o 5 16 1 6.56 49.60 38.59 o -5 17 1 21.83 27.05 38.03 o -4 17 1 938.05 907.01 48.98 o -3 17 1 82.72 88.82 16.27 o -2 17 1 6074.99 6028.23 64.94 o -1 17 1 93.34 100.86 12.70 o 0 17 1 2169.06 2357.61 32.66 o 1 17 1 42.22 26.15 8.62 o 2 17 1 339.41 355.26 21.62 o 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66.42 o -4 11 9 34.39 0.00 38.34 o -3 11 9 206.71 207.95 39.84 o -2 11 9 0.87 39.37 42.77 o -1 11 9 284.10 283.34 50.04 o 0 11 9 28.74 33.77 48.08 o 1 11 9 91.31 80.34 61.99 o -4 12 9 3.16 0.00 37.46 o -3 12 9 60.74 53.34 42.74 o -2 12 9 16.28 44.45 41.29 o -1 12 9 4.77 24.58 40.17 o 0 12 9 106.29 116.73 34.68 o 1 12 9 5.21 5.69 60.10 o -4 13 9 82.14 73.35 40.96 o -3 13 9 129.85 150.68 42.69 o -2 13 9 177.01 234.55 46.81 o -1 13 9 147.85 197.52 45.57 o 0 13 9 6.55 17.34 31.99 o 1 13 9 54.72 46.18 59.46 o -4 14 9 25.40 16.61 39.85 o -3 14 9 21.93 3.44 37.70 o -2 14 9 215.38 210.06 53.45 o -1 14 9 0.15 0.00 40.25 o 0 14 9 235.70 219.47 37.42 o 1 14 9 1.91 0.00 58.20 o -4 15 9 8.09 0.00 37.44 o -3 15 9 60.32 10.44 85.36 o -2 15 9 1.86 50.67 62.94 o -1 15 9 58.46 16.92 54.40 o 0 15 9 10.04 20.99 33.45 o 1 15 9 30.71 0.00 57.57 o -4 16 9 3.89 0.00 39.96 o -3 16 9 14.62 53.88 37.59 o -2 16 9 36.15 57.13 44.95 o -1 16 9 1.90 15.54 48.08 o 0 16 9 60.16 24.57 85.40 o 1 16 9 0.06 0.00 63.26 o -4 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o -1 26 9 0.84 5.88 55.72 o -2 27 9 17.92 55.41 52.32 o -1 27 9 101.93 49.62 57.37 o -3 0 10 95.31 124.62 77.18 o -2 0 10 9.44 18.84 44.02 o -3 1 10 29.10 21.36 51.43 o -2 1 10 83.09 93.04 35.80 o -1 1 10 2.63 0.00 56.93 o -3 2 10 94.30 43.27 59.15 o -2 2 10 3.69 19.54 50.11 o -1 2 10 131.30 31.63 61.99 o -3 3 10 12.92 9.70 41.14 o -2 3 10 110.87 15.01 49.24 o -1 3 10 0.92 60.10 72.75 o -3 4 10 47.28 51.09 41.98 o -2 4 10 19.30 23.02 44.28 o -1 4 10 75.02 142.96 63.26 o -3 5 10 1.12 27.21 40.43 o -2 5 10 60.84 80.49 44.97 o -1 5 10 0.19 0.00 57.57 o -3 6 10 23.59 0.00 40.48 o -2 6 10 5.29 47.17 46.20 o -1 6 10 15.48 6.96 61.99 o -3 7 10 1.93 0.00 55.53 o -2 7 10 57.97 55.01 47.11 o -1 7 10 0.01 0.63 61.99 o -3 8 10 0.45 1.06 40.52 o -2 8 10 0.04 21.73 51.07 o -1 8 10 0.25 0.00 62.63 o -3 9 10 2.31 0.00 42.13 o -2 9 10 10.57 5.98 47.19 o -1 9 10 2.17 0.00 63.89 o -3 10 10 11.18 12.57 48.79 o -2 10 10 2.29 0.00 83.50 o -1 10 10 5.56 5.99 43.81 o -3 11 10 6.90 16.70 46.51 o -2 11 10 10.70 0.00 46.87 o -1 11 10 24.96 0.00 50.61 o -2 12 10 0.26 0.00 44.47 o -1 12 10 3.35 29.83 48.21 o -2 13 10 48.40 44.16 50.33 o -1 13 10 9.70 52.09 55.67 o -2 14 10 1.20 0.00 46.91 o -1 14 10 73.46 77.27 82.55 o -2 15 10 65.35 130.79 55.42 o -1 15 10 9.21 0.00 62.63 o -2 16 10 2.18 0.00 73.70 o