#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2202226.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202226_Fobs loop_ _publ_author_name 'Wu, Jing' 'Guo, Rongwei' 'Zhou, Zhongyuan' 'Chen, Hua' 'Yeung, Chihung' _publ_section_title ; 3-Bromo-4-(dicyclohexylphosphinoyl)-2,6-dimethoxypyridine ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o493 _journal_page_last o494 _journal_volume 59 _journal_year 2003 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.009 _cell_angle_gamma 90.000 _cell_length_a 9.2025 _cell_length_b 18.7589 _cell_length_c 23.7611 _exptl_crystal_F_000 1792.00 _reflns_d_resolution_high 0.7686 _[local]_cod_data_source_file ww6064Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ABCWJ1 in P2(1)/n C19H29NO3PBr' _shelx_refln_list_code 4 _shelx_f_calc_maximum 453.23 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 5393.27 4882.92 141.53 o 4 0 0 15035.31 14131.93 324.31 o 6 0 0 6484.48 7585.08 309.98 o 8 0 0 7073.69 7169.67 361.55 o 10 0 0 6.52 1.52 114.45 o 2 1 0 513.99 648.01 49.00 o 3 1 0 12085.02 12601.80 189.80 o 4 1 0 335.63 408.73 62.38 o 5 1 0 4120.20 3705.28 147.86 o 6 1 0 2877.46 2418.17 139.35 o 7 1 0 2069.44 2053.22 149.70 o 8 1 0 606.30 678.97 119.22 o 9 1 0 78.51 65.63 85.52 o 10 1 0 497.42 688.96 123.65 o 11 1 0 206.39 177.98 93.73 o 0 2 0 1333.56 1408.29 36.59 o 1 2 0 25043.21 25999.09 448.74 o 2 2 0 19162.87 22440.48 195.77 o 3 2 0 2334.85 2346.71 61.33 o 4 2 0 1609.56 1510.04 75.85 o 5 2 0 1963.56 1974.24 83.51 o 6 2 0 3048.90 2549.90 116.62 o 7 2 0 648.30 644.36 73.27 o 8 2 0 49.60 -12.41 61.59 o 9 2 0 358.96 421.15 101.11 o 10 2 0 47.89 101.83 103.63 o 11 2 0 60.00 7.93 107.33 o 1 3 0 2730.70 2540.34 65.50 o 2 3 0 4856.36 5877.20 148.86 o 3 3 0 883.06 884.67 46.04 o 4 3 0 1976.40 2146.67 71.32 o 5 3 0 1454.79 1553.22 74.01 o 6 3 0 622.66 601.79 62.99 o 7 3 0 119.15 122.04 54.01 o 8 3 0 223.23 242.98 70.85 o 9 3 0 84.57 110.61 86.55 o 10 3 0 0.39 -14.10 91.08 o 11 3 0 35.70 -63.52 101.04 o 0 4 0 84550.66 91291.93 546.38 o 1 4 0 15287.73 15714.50 276.06 o 2 4 0 333.80 411.53 29.24 o 3 4 0 89.67 149.88 29.13 o 4 4 0 5702.29 5517.95 270.55 o 5 4 0 80.85 128.07 42.66 o 6 4 0 1803.98 1724.25 84.68 o 7 4 0 479.66 470.06 68.88 o 8 4 0 13.65 -24.15 69.00 o 9 4 0 131.75 146.54 97.88 o 10 4 0 8.94 105.96 131.24 o 11 4 0 167.56 88.91 144.25 o 1 5 0 24384.55 21653.94 161.35 o 2 5 0 14545.17 14656.48 327.58 o 3 5 0 3383.00 3402.85 73.73 o 4 5 0 715.29 730.90 59.66 o 5 5 0 232.49 354.23 57.62 o 6 5 0 239.11 214.34 63.65 o 7 5 0 2905.98 2614.10 124.79 o 8 5 0 8.14 2.93 99.87 o 9 5 0 641.17 520.10 134.85 o 10 5 0 259.57 208.14 142.61 o 11 5 0 66.38 111.73 224.61 o 0 6 0 1998.49 2440.10 190.52 o 1 6 0 5426.44 5379.49 99.88 o 2 6 0 1373.41 1234.80 52.61 o 3 6 0 6649.34 6067.11 163.59 o 4 6 0 1138.41 1064.79 59.22 o 5 6 0 7080.32 6910.07 167.18 o 6 6 0 681.97 684.43 80.16 o 7 6 0 513.52 564.44 82.39 o 8 6 0 37.06 5.97 101.45 o 9 6 0 908.98 1226.61 164.07 o 10 6 0 92.62 78.90 133.39 o 11 6 0 37.94 71.05 202.26 o 1 7 0 1545.06 1260.41 55.38 o 2 7 0 13278.76 12664.78 194.26 o 3 7 0 11774.66 12333.16 366.78 o 4 7 0 1852.74 1937.13 73.54 o 5 7 0 2202.98 2209.61 102.40 o 6 7 0 1488.48 1509.73 103.38 o 7 7 0 366.38 391.07 79.42 o 8 7 0 470.43 569.04 128.70 o 9 7 0 200.83 259.46 133.13 o 10 7 0 355.39 472.81 156.14 o 11 7 0 240.25 428.01 273.31 o 0 8 0 48391.16 53403.75 462.39 o 1 8 0 6197.85 6729.53 111.44 o 2 8 0 1431.18 1718.85 60.45 o 3 8 0 405.91 369.36 43.26 o 4 8 0 6697.71 6334.67 144.84 o 5 8 0 680.96 800.33 78.90 o 6 8 0 1989.14 1909.31 110.70 o 7 8 0 2.51 31.80 89.54 o 8 8 0 1856.01 2362.44 192.61 o 9 8 0 305.02 327.86 138.11 o 10 8 0 52.44 -20.05 190.80 o 11 8 0 31.79 21.25 173.47 o 1 9 0 318.04 338.80 43.14 o 2 9 0 4138.49 3881.27 93.94 o 3 9 0 1332.59 1318.47 63.14 o 4 9 0 82.75 105.61 43.05 o 5 9 0 875.21 980.75 69.85 o 6 9 0 1130.75 1468.38 105.00 o 7 9 0 859.28 763.54 131.14 o 8 9 0 252.62 304.88 121.96 o 9 9 0 80.88 111.98 131.39 o 10 9 0 421.47 591.55 204.82 o 11 9 0 7.80 -80.70 188.60 o 0 10 0 2.74 70.21 55.91 o 1 10 0 4.88 11.66 38.00 o 2 10 0 937.56 1103.92 64.71 o 3 10 0 135.79 93.45 36.88 o 4 10 0 332.62 313.13 50.97 o 5 10 0 56.90 82.65 54.31 o 6 10 0 333.50 297.91 83.59 o 7 10 0 38.60 -10.10 91.61 o 8 10 0 86.04 -1.58 107.24 o 9 10 0 3.51 108.31 108.77 o 10 10 0 35.81 5.12 164.77 o 1 11 0 486.80 577.56 58.69 o 2 11 0 1429.10 1322.69 72.43 o 3 11 0 200.09 227.37 49.44 o 4 11 0 46.30 52.32 54.74 o 5 11 0 8.53 41.78 56.59 o 6 11 0 439.35 540.21 79.65 o 7 11 0 473.46 523.16 108.69 o 8 11 0 98.86 132.30 105.29 o 9 11 0 26.63 -16.22 144.81 o 10 11 0 46.57 43.62 174.47 o 0 12 0 6500.47 6828.50 200.98 o 1 12 0 390.68 425.12 59.21 o 2 12 0 385.71 436.85 57.39 o 3 12 0 1027.38 1028.49 71.46 o 4 12 0 4605.19 4335.15 160.02 o 5 12 0 3016.24 2705.52 121.40 o 6 12 0 927.78 954.09 118.98 o 7 12 0 6.68 -46.37 89.35 o 8 12 0 60.51 136.69 109.00 o 9 12 0 141.44 201.27 182.19 o 10 12 0 165.63 187.41 198.62 o 1 13 0 4407.04 3956.00 117.66 o 2 13 0 215.06 178.80 54.86 o 3 13 0 1177.86 1354.73 108.43 o 4 13 0 523.36 615.53 97.73 o 5 13 0 15.39 31.44 79.30 o 6 13 0 220.28 320.02 101.43 o 7 13 0 1145.32 1131.63 158.01 o 8 13 0 7.34 -9.50 110.71 o 9 13 0 164.69 186.12 186.10 o 10 13 0 10.22 110.78 194.04 o 0 14 0 250.07 264.02 84.49 o 1 14 0 1403.88 1492.39 87.84 o 2 14 0 114.72 19.09 64.73 o 3 14 0 920.67 1069.86 105.49 o 4 14 0 1571.09 1702.10 129.11 o 5 14 0 1791.41 1744.28 140.46 o 6 14 0 105.29 71.71 91.68 o 7 14 0 311.08 325.54 119.22 o 8 14 0 22.54 70.32 158.68 o 9 14 0 336.21 356.75 198.47 o 1 15 0 21.81 9.96 51.84 o 2 15 0 1888.59 1917.70 124.52 o 3 15 0 367.59 508.51 95.82 o 4 15 0 637.94 773.03 109.92 o 5 15 0 18.37 6.02 87.65 o 6 15 0 429.93 551.99 118.36 o 7 15 0 136.76 72.00 111.47 o 8 15 0 1.01 -64.03 168.54 o 9 15 0 16.94 111.93 184.72 o 0 16 0 1167.71 896.60 127.67 o 1 16 0 863.49 1042.85 105.89 o 2 16 0 105.25 145.76 80.43 o 3 16 0 82.91 134.10 78.39 o 4 16 0 735.00 733.96 112.40 o 5 16 0 2.13 -10.94 96.68 o 6 16 0 78.07 72.40 103.31 o 7 16 0 59.74 237.95 163.30 o 8 16 0 102.87 238.78 180.29 o 9 16 0 30.98 73.05 204.35 o 1 17 0 235.33 186.28 87.09 o 2 17 0 79.48 50.30 79.95 o 3 17 0 253.33 277.99 96.46 o 4 17 0 11.47 62.12 88.17 o 5 17 0 43.89 57.85 95.99 o 6 17 0 68.32 70.75 105.28 o 7 17 0 74.24 -5.45 158.88 o 8 17 0 8.37 -5.15 170.61 o 0 18 0 610.23 697.89 179.92 o 1 18 0 197.61 200.16 90.07 o 2 18 0 73.67 58.41 83.31 o 3 18 0 186.28 215.31 100.10 o 4 18 0 138.11 175.70 101.29 o 5 18 0 36.97 60.26 103.36 o 6 18 0 18.03 41.64 146.12 o 7 18 0 3.59 23.42 159.88 o 8 18 0 145.21 285.21 209.64 o 1 19 0 33.56 52.41 102.79 o 2 19 0 286.96 293.36 96.74 o 3 19 0 70.33 243.83 103.13 o 4 19 0 2.12 -53.36 92.93 o 5 19 0 157.16 108.12 110.97 o 6 19 0 238.30 455.68 183.91 o 7 19 0 82.78 56.93 181.27 o 0 20 0 5.19 54.43 167.88 o 1 20 0 4.61 -71.21 98.74 o 2 20 0 217.76 262.72 131.93 o 3 20 0 152.85 62.01 84.21 o 4 20 0 219.88 195.24 109.28 o 5 20 0 286.48 369.40 161.21 o 6 20 0 73.40 267.60 171.54 o 1 21 0 134.07 92.86 129.34 o 2 21 0 3.83 -28.55 124.79 o 3 21 0 48.81 43.28 84.76 o 4 21 0 1.50 -58.08 103.67 o 5 21 0 37.28 101.83 150.15 o 6 21 0 4.49 44.42 165.05 o 0 22 0 2.56 70.48 177.05 o 1 22 0 151.68 254.51 139.08 o 2 22 0 5.97 49.00 142.35 o 3 22 0 1.75 -73.57 133.23 o 4 22 0 9.68 -70.80 129.78 o 5 22 0 1.67 -87.60 145.64 o 1 23 0 2.26 158.89 149.99 o 2 23 0 2.10 101.33 148.82 o 3 23 0 9.26 -79.54 132.44 o 4 23 0 4.07 -52.71 241.80 o 0 24 0 4.89 50.42 185.64 o 1 24 0 24.69 -80.46 144.97 o 2 24 0 34.85 -93.72 145.24 o -11 0 1 336.23 333.93 145.57 o -9 0 1 388.15 118.61 161.01 o -7 0 1 2460.19 2362.39 212.57 o -5 0 1 19277.27 21380.10 444.63 o -3 0 1 4887.36 5585.96 176.48 o -1 0 1 30762.72 30121.45 320.29 o 3 0 1 2306.56 2843.12 139.81 o 5 0 1 9.36 -48.70 74.49 o 7 0 1 3420.49 3228.73 249.82 o 9 0 1 0.10 97.41 143.24 o 11 0 1 0.35 -88.36 124.91 o -11 1 1 31.51 25.19 80.16 o -10 1 1 42.00 3.99 93.75 o -9 1 1 1317.80 1584.15 115.62 o -8 1 1 1153.03 1303.05 140.02 o -7 1 1 870.46 793.72 108.16 o -6 1 1 835.79 861.99 96.98 o -5 1 1 6082.01 6187.01 174.20 o -4 1 1 2241.75 2341.06 103.72 o -3 1 1 4671.18 5748.06 136.37 o -2 1 1 2214.13 2732.27 80.22 o -1 1 1 35492.62 39260.27 297.56 o 1 1 1 12017.61 12108.17 80.16 o 2 1 1 42525.40 45378.83 274.53 o 3 1 1 4329.94 3725.22 113.64 o 4 1 1 4040.22 4795.11 176.76 o 5 1 1 7846.56 8396.94 206.21 o 6 1 1 42.31 -28.64 64.23 o 7 1 1 1006.93 1029.24 119.04 o 8 1 1 862.87 702.35 103.73 o 9 1 1 40.19 54.02 87.79 o 10 1 1 141.61 130.21 99.27 o 11 1 1 74.10 139.57 97.02 o -11 2 1 10.10 4.52 101.74 o -10 2 1 58.38 34.28 95.17 o -9 2 1 106.33 100.50 84.21 o -8 2 1 121.92 107.64 67.14 o -7 2 1 1795.96 1765.21 98.47 o -6 2 1 4207.08 4417.62 175.19 o -5 2 1 3131.91 2755.77 129.68 o -4 2 1 1935.32 1673.09 92.97 o -3 2 1 12496.09 13593.59 272.59 o -2 2 1 56.55 52.27 18.14 o -1 2 1 8553.10 10257.32 176.86 o 0 2 1 15243.32 18054.24 131.53 o 1 2 1 9808.17 9477.85 126.12 o 2 2 1 76.92 49.92 16.78 o 3 2 1 1294.02 1184.98 49.93 o 4 2 1 26.74 86.74 42.37 o 5 2 1 19680.39 20256.33 261.49 o 6 2 1 476.16 499.96 75.86 o 7 2 1 92.85 66.69 65.43 o 8 2 1 712.67 958.57 113.03 o 9 2 1 528.28 574.80 110.52 o 10 2 1 0.53 -88.87 88.87 o 11 2 1 287.62 261.63 116.89 o -11 3 1 156.78 139.52 111.84 o -10 3 1 115.17 180.17 97.73 o -9 3 1 9.54 -32.20 80.81 o -8 3 1 1217.05 1548.51 103.94 o -7 3 1 571.37 521.10 69.60 o -6 3 1 2064.13 2154.49 90.59 o -5 3 1 3140.87 3029.30 90.94 o -4 3 1 1028.41 995.06 55.47 o -3 3 1 42.56 58.78 25.16 o -2 3 1 24547.56 23943.04 353.16 o 0 3 1 19777.31 20935.59 609.87 o 1 3 1 142.19 170.52 18.03 o 2 3 1 32956.23 37749.59 837.44 o 3 3 1 7936.02 7518.66 136.56 o 4 3 1 25066.84 23878.41 206.13 o 5 3 1 695.10 917.68 61.44 o 6 3 1 309.13 124.99 49.42 o 7 3 1 703.76 930.01 79.97 o 8 3 1 3376.23 3383.23 157.66 o 9 3 1 494.63 552.10 107.06 o 10 3 1 210.61 166.47 97.12 o 11 3 1 197.83 109.11 114.28 o -11 4 1 39.52 -75.63 207.99 o -10 4 1 22.94 -5.36 120.12 o -9 4 1 133.00 171.31 93.30 o -8 4 1 2344.70 2377.79 114.31 o -7 4 1 66.78 82.69 55.45 o -6 4 1 692.41 870.10 70.14 o -5 4 1 4973.58 5449.21 115.78 o -4 4 1 1196.37 1430.76 75.00 o -3 4 1 1792.57 1888.17 70.17 o -2 4 1 8032.94 7229.28 163.83 o -1 4 1 122.71 101.46 17.77 o 0 4 1 7240.16 6682.49 78.62 o 1 4 1 8338.17 9262.43 112.24 o 2 4 1 18221.32 20791.25 464.62 o 3 4 1 1724.87 1666.72 63.93 o 4 4 1 4417.28 4750.83 112.76 o 5 4 1 867.88 1062.10 68.20 o 6 4 1 14128.71 13170.26 188.97 o 7 4 1 285.21 347.84 67.24 o 8 4 1 284.89 267.27 83.49 o 9 4 1 17.91 15.68 85.98 o 10 4 1 306.15 271.74 140.83 o 11 4 1 6.84 -78.18 124.28 o -11 5 1 163.93 169.60 235.49 o -10 5 1 30.78 28.00 126.75 o -9 5 1 0.12 27.01 112.04 o -8 5 1 1226.42 1519.82 117.64 o -7 5 1 261.21 210.07 71.53 o -6 5 1 1558.05 1849.75 103.90 o -5 5 1 42.85 62.42 49.37 o -4 5 1 4536.29 4263.28 166.87 o -3 5 1 11830.50 11807.61 260.75 o -2 5 1 2100.66 1915.99 57.05 o -1 5 1 88.66 90.87 20.17 o 0 5 1 1656.51 1833.99 51.75 o 1 5 1 743.68 867.61 48.99 o 2 5 1 967.29 1201.42 47.39 o 3 5 1 21205.90 22537.54 322.37 o 4 5 1 5221.65 4771.97 98.95 o 5 5 1 4573.44 4544.06 125.48 o 6 5 1 275.04 204.27 62.14 o 7 5 1 629.19 746.87 84.17 o 8 5 1 1743.12 1948.05 171.56 o 9 5 1 302.54 315.33 132.42 o 10 5 1 43.73 143.85 131.43 o 11 5 1 311.13 309.62 159.39 o -11 6 1 7.49 -73.34 223.46 o -10 6 1 1009.99 1235.15 185.38 o -9 6 1 11.38 33.90 112.34 o -8 6 1 236.42 178.09 108.19 o -7 6 1 183.57 205.55 71.16 o -6 6 1 5438.85 5452.67 240.71 o -5 6 1 451.68 471.14 64.12 o -4 6 1 3897.38 4002.52 112.14 o -3 6 1 361.31 441.17 38.60 o -2 6 1 6579.22 6065.09 210.73 o -1 6 1 15872.60 16773.08 252.08 o 0 6 1 4742.64 5467.05 87.56 o 1 6 1 16.53 54.50 29.50 o 2 6 1 1103.00 1134.48 49.47 o 3 6 1 1434.78 1788.06 63.95 o 4 6 1 3054.27 2735.49 84.60 o 5 6 1 1706.26 1769.83 93.72 o 6 6 1 451.61 555.57 132.17 o 7 6 1 246.16 244.24 71.89 o 8 6 1 1.57 5.64 92.98 o 9 6 1 3.10 -15.17 116.46 o 10 6 1 0.38 21.02 125.62 o 11 6 1 0.39 -78.88 139.12 o -11 7 1 10.62 -8.56 176.63 o -10 7 1 23.64 139.23 220.60 o -9 7 1 138.87 95.71 118.14 o -8 7 1 266.46 271.26 114.24 o -7 7 1 921.61 972.36 99.49 o -6 7 1 162.54 85.21 60.26 o -5 7 1 1907.93 1771.49 96.18 o -4 7 1 1182.83 1017.88 72.32 o -3 7 1 3344.17 3369.33 118.56 o -2 7 1 1852.20 1901.59 55.47 o -1 7 1 4822.03 5148.30 182.52 o 0 7 1 92.91 101.32 28.99 o 1 7 1 2652.45 2538.61 68.76 o 2 7 1 2112.97 2194.70 78.14 o 3 7 1 102.39 108.48 35.74 o 4 7 1 3602.16 3401.67 91.38 o 5 7 1 530.31 739.56 62.13 o 6 7 1 450.61 412.62 71.59 o 7 7 1 152.12 110.39 96.81 o 8 7 1 61.11 47.65 103.90 o 9 7 1 90.87 33.50 119.76 o 10 7 1 12.20 65.50 130.59 o 11 7 1 0.01 -84.23 218.88 o -11 8 1 233.59 154.12 281.05 o -10 8 1 56.29 64.29 157.75 o -9 8 1 479.81 618.76 143.86 o -8 8 1 274.88 327.61 117.54 o -7 8 1 1150.34 1106.57 102.69 o -6 8 1 131.77 231.20 66.63 o -5 8 1 1639.12 1731.88 99.64 o -4 8 1 1280.91 1474.31 65.51 o -3 8 1 1294.43 1405.62 56.92 o -2 8 1 3937.84 4353.11 84.93 o -1 8 1 6385.83 5948.90 103.66 o 0 8 1 11323.53 11823.40 145.00 o 1 8 1 9902.95 9231.58 131.02 o 2 8 1 3148.34 3129.72 191.26 o 3 8 1 3022.18 3174.69 115.12 o 4 8 1 474.87 539.57 53.92 o 5 8 1 379.88 392.04 53.57 o 6 8 1 29.17 76.81 62.83 o 7 8 1 615.98 728.88 124.50 o 8 8 1 3.40 -51.57 103.23 o 9 8 1 139.12 87.21 124.59 o 10 8 1 257.86 332.61 153.74 o 11 8 1 7.98 -177.05 202.26 o -11 9 1 11.79 -155.54 184.79 o -10 9 1 0.34 93.66 162.34 o -9 9 1 580.16 596.00 129.47 o -8 9 1 364.63 375.04 106.96 o -7 9 1 153.80 257.99 78.15 o -6 9 1 2741.48 2435.48 120.54 o -5 9 1 916.68 846.48 75.60 o -4 9 1 371.88 366.58 49.58 o -3 9 1 500.96 422.74 41.91 o -2 9 1 936.47 1011.24 52.81 o -1 9 1 2076.29 1993.87 73.43 o 0 9 1 746.10 959.79 60.88 o 1 9 1 751.77 896.82 57.21 o 2 9 1 2405.82 2339.90 79.51 o 3 9 1 7235.01 6654.94 122.27 o 4 9 1 753.37 814.12 62.59 o 5 9 1 532.44 670.75 63.30 o 6 9 1 442.75 558.19 81.66 o 7 9 1 3426.05 3668.68 205.65 o 8 9 1 200.30 137.69 112.78 o 9 9 1 273.93 312.98 144.95 o 10 9 1 58.62 88.04 155.97 o 11 9 1 8.70 37.82 262.42 o -10 10 1 85.05 97.17 176.92 o -9 10 1 3.40 -86.39 135.07 o -8 10 1 82.14 80.38 95.36 o -7 10 1 159.42 243.83 100.15 o -6 10 1 60.93 79.76 61.75 o -5 10 1 5.69 25.10 51.83 o -4 10 1 3652.42 3988.12 121.27 o -3 10 1 4888.76 4892.72 99.39 o -2 10 1 117.59 129.28 40.15 o -1 10 1 829.99 1024.71 63.21 o 0 10 1 735.35 664.59 56.63 o 1 10 1 15574.08 14853.66 183.31 o 2 10 1 2853.70 2789.98 90.81 o 3 10 1 218.26 182.27 46.92 o 4 10 1 862.40 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