#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/22/2202233.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202233_Fobs loop_ _publ_author_name 'Chen, Yun' 'Liu, Ping' 'Wang, Jian' 'Cheng, Wen-Dan' _publ_section_title ; Polymeric aqua(\m~4~-maleato-\k^4^O)pyridylnickel(II) ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m393 _journal_page_last m395 _journal_volume 59 _journal_year 2003 _space_group_IT_number 62 _symmetry_space_group_name_Hall '-P 2ac 2n' _symmetry_space_group_name_H-M 'P n m a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 17.9522 _cell_length_b 7.5712 _cell_length_c 7.4092 _exptl_crystal_F_000 552.00 _reflns_d_resolution_high 0.8399 _[local]_cod_data_source_file ww6072Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' C in Pnma' _shelx_refln_list_code 4 _shelx_f_calc_maximum 155.20 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z' 'x+1/2, -y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z' '-x-1/2, y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 21042.91 22129.66 559.35 o 4 0 0 1467.63 1544.08 49.80 o 6 0 0 77.08 113.83 16.40 o 8 0 0 136.94 176.56 19.52 o 10 0 0 671.20 679.34 41.56 o 12 0 0 1301.27 1358.85 66.89 o 14 0 0 1804.46 1799.77 88.58 o 16 0 0 219.68 241.63 55.44 o 18 0 0 1821.56 2030.38 110.27 o 20 0 0 3.22 -45.12 45.12 o 2 1 0 5045.59 5122.27 291.69 o 4 1 0 1239.89 1221.07 42.34 o 6 1 0 2473.29 2453.85 54.87 o 8 1 0 1519.27 1544.13 41.95 o 10 1 0 1533.09 1347.00 42.65 o 12 1 0 3487.43 3570.97 141.03 o 14 1 0 142.15 133.15 56.65 o 16 1 0 581.60 630.29 45.85 o 18 1 0 1099.34 948.21 84.07 o 20 1 0 824.76 1164.85 106.63 o 0 2 0 24086.45 21285.84 384.53 o 2 2 0 673.69 707.90 20.88 o 4 2 0 1809.79 1610.10 70.41 o 6 2 0 761.84 713.26 19.53 o 8 2 0 157.09 135.67 22.90 o 10 2 0 9134.50 9239.46 184.12 o 12 2 0 10936.81 11532.32 230.45 o 14 2 0 5557.65 5070.04 178.73 o 16 2 0 169.56 341.75 64.38 o 18 2 0 576.38 555.10 83.72 o 20 2 0 0.66 188.44 74.61 o 2 3 0 3858.43 3711.96 108.99 o 4 3 0 713.12 549.79 25.18 o 6 3 0 4873.55 5059.10 135.26 o 8 3 0 8207.03 8350.87 135.36 o 10 3 0 3538.23 3355.30 126.32 o 12 3 0 1260.15 1049.46 71.06 o 14 3 0 206.27 182.81 53.79 o 16 3 0 63.48 228.35 67.07 o 18 3 0 22.47 85.63 72.27 o 20 3 0 213.02 222.54 85.63 o 0 4 0 22015.21 22013.92 407.85 o 2 4 0 3477.99 3414.66 65.53 o 4 4 0 2992.07 2704.64 70.23 o 6 4 0 2.88 7.71 18.57 o 8 4 0 394.27 374.27 33.37 o 10 4 0 1414.10 1135.35 75.05 o 12 4 0 1970.19 1646.98 96.04 o 14 4 0 2492.70 2456.72 126.32 o 16 4 0 175.31 218.55 68.54 o 18 4 0 282.91 165.80 72.71 o 2 5 0 3771.02 3725.40 74.50 o 4 5 0 318.97 267.76 28.59 o 6 5 0 70.27 98.65 26.94 o 8 5 0 1090.76 961.81 50.67 o 10 5 0 1552.68 1505.33 62.54 o 12 5 0 628.83 651.05 73.75 o 14 5 0 282.36 205.45 65.59 o 16 5 0 273.43 323.18 89.36 o 0 6 0 9891.16 10043.61 303.14 o 2 6 0 2587.80 2554.58 80.76 o 4 6 0 1254.64 1181.12 84.45 o 6 6 0 7.29 66.89 38.83 o 8 6 0 116.69 44.92 123.16 o 10 6 0 106.66 30.70 33.56 o 12 6 0 568.05 448.38 72.71 o 14 6 0 1838.36 1827.18 123.98 o 2 7 0 1419.41 1162.61 120.60 o 4 7 0 641.57 686.94 50.23 o 6 7 0 759.26 755.43 46.12 o 8 7 0 1445.19 1378.12 70.72 o 10 7 0 838.78 798.61 95.70 o 12 7 0 135.12 160.05 71.23 o 0 8 0 603.24 673.18 70.54 o 2 8 0 76.64 33.17 41.21 o 4 8 0 309.92 355.19 47.34 o 6 8 0 82.95 115.05 50.27 o 8 8 0 84.55 83.15 46.91 o 1 0 1 59.15 45.72 6.00 o 2 0 1 1271.70 1463.30 33.19 o 3 0 1 7871.24 8485.64 391.46 o 4 0 1 8102.23 8435.79 159.78 o 5 0 1 357.83 351.61 17.05 o 6 0 1 5669.86 6008.19 163.41 o 7 0 1 127.35 118.17 14.21 o 8 0 1 707.73 631.04 38.17 o 9 0 1 1184.12 1300.55 41.60 o 10 0 1 1512.11 1526.29 86.50 o 11 0 1 13.19 5.41 15.45 o 12 0 1 888.36 940.15 40.57 o 13 0 1 601.64 698.39 37.41 o 14 0 1 21.68 -7.75 92.70 o 15 0 1 2955.64 3088.70 87.70 o 16 0 1 413.54 390.57 39.52 o 17 0 1 406.14 423.59 88.15 o 18 0 1 2337.25 2419.61 95.05 o 19 0 1 39.38 69.80 36.99 o 20 0 1 1516.73 1775.04 122.59 o 0 1 1 16531.76 16916.67 249.87 o 1 1 1 1794.81 1795.08 61.09 o 2 1 1 15226.08 15503.95 178.00 o 3 1 1 2240.61 2350.70 60.15 o 4 1 1 2180.43 2209.05 30.99 o 5 1 1 14.42 -12.27 12.27 o 6 1 1 480.12 421.07 16.37 o 7 1 1 3068.20 3512.27 61.35 o 8 1 1 461.96 505.77 18.47 o 9 1 1 476.97 489.61 17.70 o 10 1 1 1389.62 1401.54 57.32 o 11 1 1 17.49 32.10 24.72 o 12 1 1 4335.86 4660.74 81.17 o 13 1 1 33.03 62.74 16.78 o 14 1 1 1520.15 1505.72 45.96 o 15 1 1 787.10 938.57 32.13 o 16 1 1 1856.36 1957.12 52.26 o 17 1 1 30.18 64.38 27.90 o 18 1 1 667.11 746.06 55.76 o 19 1 1 163.20 188.72 60.56 o 20 1 1 1.18 121.60 94.53 o 21 1 1 72.29 112.71 46.82 o 1 2 1 7583.14 7808.28 139.07 o 2 2 1 11.60 2.23 10.14 o 3 2 1 4277.26 4250.35 53.75 o 4 2 1 2567.55 2561.35 47.47 o 5 2 1 4405.18 4532.82 79.86 o 6 2 1 8531.71 8369.32 102.35 o 7 2 1 43.96 48.26 9.80 o 8 2 1 6350.81 6340.11 128.85 o 9 2 1 2.36 7.64 14.10 o 10 2 1 4162.11 4195.52 92.63 o 11 2 1 47.31 94.87 24.93 o 12 2 1 604.19 639.28 31.52 o 13 2 1 192.72 210.28 22.45 o 14 2 1 8.39 -8.58 41.30 o 15 2 1 6.39 50.09 25.79 o 16 2 1 70.32 138.69 34.10 o 17 2 1 201.31 182.05 53.66 o 18 2 1 581.32 572.78 55.23 o 19 2 1 12.35 37.54 152.14 o 20 2 1 500.36 627.44 61.14 o 0 3 1 999.40 892.23 22.52 o 1 3 1 373.27 340.14 12.08 o 2 3 1 3987.87 4114.96 46.54 o 3 3 1 3125.77 3178.49 37.22 o 4 3 1 2516.39 2501.34 32.93 o 5 3 1 2182.77 2304.01 38.70 o 6 3 1 446.87 423.35 18.11 o 7 3 1 0.52 -32.86 32.86 o 8 3 1 990.95 1018.27 39.41 o 9 3 1 178.31 239.63 34.63 o 10 3 1 3147.38 2998.74 142.11 o 11 3 1 1.15 6.45 32.01 o 12 3 1 5255.43 4889.93 121.49 o 13 3 1 659.45 673.43 46.52 o 14 3 1 1515.01 1423.68 142.59 o 15 3 1 106.27 163.07 35.40 o 16 3 1 1100.48 1060.21 63.65 o 17 3 1 207.65 173.19 44.47 o 18 3 1 304.37 376.95 70.54 o 19 3 1 0.35 -37.74 190.87 o 20 3 1 9.67 -45.27 45.27 o 1 4 1 1677.67 1655.99 29.87 o 2 4 1 775.55 732.02 15.19 o 3 4 1 65.62 70.74 13.12 o 4 4 1 1988.96 1954.34 38.16 o 5 4 1 3.96 -16.57 20.03 o 6 4 1 2965.04 2930.71 55.34 o 7 4 1 23.74 62.67 21.24 o 8 4 1 2465.20 2439.81 51.93 o 9 4 1 635.60 669.86 39.62 o 10 4 1 1899.25 1825.60 51.71 o 11 4 1 64.11 47.53 44.25 o 12 4 1 237.28 237.03 107.67 o 13 4 1 130.57 94.27 33.69 o 14 4 1 13.59 -30.32 63.03 o 15 4 1 335.90 320.51 63.90 o 16 4 1 73.79 123.67 43.16 o 17 4 1 4.68 50.48 77.00 o 18 4 1 756.56 614.31 61.92 o 19 4 1 79.06 109.59 85.72 o 0 5 1 5787.16 5883.95 89.85 o 1 5 1 355.28 360.21 15.27 o 2 5 1 5976.42 6195.07 122.07 o 3 5 1 451.72 382.35 17.84 o 4 5 1 1619.00 1640.57 50.12 o 5 5 1 397.53 405.31 33.71 o 6 5 1 33.44 33.09 17.86 o 7 5 1 125.62 167.04 21.25 o 8 5 1 205.92 211.10 25.34 o 9 5 1 93.97 76.55 20.86 o 10 5 1 161.05 159.44 25.72 o 11 5 1 194.16 162.19 53.30 o 12 5 1 974.32 947.03 56.58 o 13 5 1 11.57 19.21 33.88 o 14 5 1 947.47 923.10 63.10 o 15 5 1 242.28 301.35 52.44 o 16 5 1 1145.03 1144.83 99.30 o 17 5 1 49.45 78.91 45.96 o 1 6 1 345.05 312.72 37.83 o 2 6 1 716.47 643.39 22.69 o 3 6 1 0.70 21.02 24.08 o 4 6 1 1371.33 1304.37 33.50 o 5 6 1 37.86 33.07 16.35 o 6 6 1 1121.06 1133.69 51.11 o 7 6 1 2.78 -5.85 27.05 o 8 6 1 963.46 999.46 39.02 o 9 6 1 512.70 489.54 33.22 o 10 6 1 918.36 933.61 45.70 o 11 6 1 1.30 -25.45 25.45 o 12 6 1 136.79 228.38 36.88 o 13 6 1 465.45 380.36 52.77 o 14 6 1 0.19 -52.94 110.92 o 15 6 1 246.45 257.21 59.30 o 0 7 1 697.87 724.31 46.93 o 1 7 1 155.92 119.12 21.03 o 2 7 1 1071.86 1115.02 39.36 o 3 7 1 135.75 88.47 36.28 o 4 7 1 554.55 672.38 40.40 o 5 7 1 14.45 57.43 50.88 o 6 7 1 35.29 39.35 38.22 o 7 7 1 5.89 19.13 27.78 o 8 7 1 223.85 199.50 28.29 o 9 7 1 42.48 86.89 39.60 o 10 7 1 546.53 539.88 33.69 o 11 7 1 0.70 -33.86 33.86 o 12 7 1 1142.89 1070.17 59.30 o 13 7 1 263.75 330.16 58.05 o 1 8 1 340.52 296.96 57.36 o 2 8 1 52.16 121.86 27.48 o 3 8 1 432.56 442.92 34.46 o 4 8 1 376.29 427.11 34.92 o 5 8 1 91.57 165.74 31.07 o 6 8 1 855.68 894.57 57.84 o 7 8 1 7.43 207.26 76.15 o 8 8 1 1023.41 970.89 69.10 o 9 8 1 6.00 -31.98 31.98 o 0 0 2 576.31 676.13 35.75 o 1 0 2 292.52 290.95 26.51 o 2 0 2 239.65 296.06 17.91 o 3 0 2 99.25 174.83 25.20 o 4 0 2 3843.10 3823.78 82.42 o 5 0 2 7556.39 7646.11 151.50 o 6 0 2 1244.24 1126.65 36.27 o 7 0 2 4398.15 5320.86 555.18 o 8 0 2 1874.17 2193.83 59.23 o 9 0 2 110.68 108.32 19.02 o 10 0 2 1025.47 977.92 62.64 o 11 0 2 241.20 221.64 25.05 o 12 0 2 3094.40 3252.91 84.23 o 13 0 2 0.45 -18.70 23.82 o 14 0 2 5254.99 5371.42 128.95 o 15 0 2 726.97 675.54 87.85 o 16 0 2 2226.78 2261.24 153.74 o 17 0 2 1.41 22.69 34.40 o 18 0 2 227.93 382.11 44.02 o 19 0 2 118.18 100.01 139.55 o 1 1 2 277.23 264.03 11.68 o 2 1 2 5760.39 5644.83 70.51 o 3 1 2 110.62 113.63 8.44 o 4 1 2 4659.39 4398.63 51.41 o 5 1 2 597.04 530.39 15.69 o 6 1 2 12112.35 11651.55 179.77 o 7 1 2 2104.04 2116.05 38.88 o 8 1 2 7130.05 6567.22 116.04 o 9 1 2 17.24 50.23 25.69 o 10 1 2 1963.67 2078.54 76.23 o 11 1 2 42.17 36.88 24.85 o 12 1 2 183.01 279.76 36.72 o 13 1 2 241.27 225.57 19.05 o 14 1 2 0.03 115.60 30.92 o 15 1 2 161.72 149.82 32.41 o 16 1 2 371.44 465.65 30.93 o 17 1 2 149.47 154.28 76.32 o 18 1 2 537.51 545.61 77.52 o 19 1 2 35.80 40.90 167.49 o 20 1 2 1385.06 1304.42 70.36 o 0 2 2 10805.47 11098.10 298.73 o 1 2 2 2.25 0.14 6.22 o 2 2 2 8180.60 7954.90 118.96 o 3 2 2 2142.16 2245.74 30.66 o 4 2 2 4046.57 4217.13 51.29 o 5 2 2 1075.39 1148.32 26.99 o 6 2 2 432.45 440.97 14.45 o 7 2 2 368.34 368.00 33.14 o 8 2 2 1328.72 1492.33 32.63 o 9 2 2 1.05 22.35 16.83 o 10 2 2 158.39 173.34 34.59 o 11 2 2 0.91 -18.97 18.97 o 12 2 2 426.22 385.59 20.38 o 13 2 2 78.75 53.45 15.88 o 14 2 2 1417.47 1394.98 111.79 o 15 2 2 77.92 51.79 29.15 o 16 2 2 1095.62 1170.19 141.07 o 17 2 2 574.71 454.00 53.18 o 18 2 2 482.95 611.46 133.35 o 19 2 2 85.99 162.19 41.17 o 20 2 2 125.00 421.79 55.16 o 1 3 2 1078.92 1097.82 20.93 o 2 3 2 708.32 649.79 14.64 o 3 3 2 2621.57 2665.01 34.61 o 4 3 2 1563.09 1594.42 23.86 o 5 3 2 623.75 620.34 19.74 o 6 3 2 6472.82 6649.77 111.12 o 7 3 2 370.89 421.17 20.97 o 8 3 2 3582.80 3492.04 52.61 o 9 3 2 41.35 29.93 17.48 o 10 3 2 1277.47 1111.23 79.95 o 11 3 2 403.83 442.08 35.04 o 12 3 2 347.17 233.42 29.89 o 13 3 2 131.47 33.83 23.71 o 14 3 2 36.53 71.53 30.29 o 15 3 2 140.77 145.57 35.16 o 16 3 2 1471.38 1413.36 81.60 o 17 3 2 0.08 -33.10 33.10 o 18 3 2 1370.64 1250.53 157.69 o 19 3 2 82.96 96.27 47.48 o 0 4 2 3173.95 3163.63 62.25 o 1 4 2 0.29 -12.69 12.69 o 2 4 2 1798.32 1774.95 33.24 o 3 4 2 65.92 114.16 19.07 o 4 4 2 1160.09 1102.60 20.78 o 5 4 2 253.00 214.79 12.30 o 6 4 2 755.33 705.45 29.02 o 7 4 2 1.03 -38.14 38.14 o 8 4 2 201.30 231.50 41.95 o 9 4 2 31.89 18.56 18.16 o 10 4 2 576.59 503.29 51.41 o 11 4 2 40.40 40.73 27.50 o 12 4 2 1347.70 1347.50 101.81 o 13 4 2 11.91 70.44 29.88 o 14 4 2 1677.18 1882.21 90.27 o 15 4 2 6.29 34.53 30.44 o 16 4 2 1078.04 879.34 73.79 o 17 4 2 57.12 93.58 40.64 o 18 4 2 454.48 253.21 229.18 o 1 5 2 0.51 -14.26 31.56 o 2 5 2 863.28 867.40 44.57 o 3 5 2 54.53 28.25 35.45 o 4 5 2 3157.43 3207.24 65.44 o 5 5 2 77.76 122.36 23.72 o 6 5 2 6087.25 6566.81 94.58 o 7 5 2 472.63 438.38 22.95 o 8 5 2 1752.72 1642.98 40.88 o 9 5 2 227.85 260.40 66.88 o 10 5 2 245.50 168.30 27.76 o 11 5 2 2.16 3.97 47.98 o 12 5 2 274.35 284.98 30.82 o 13 5 2 905.00 864.79 52.57 o 14 5 2 69.23 71.42 105.93 o 15 5 2 205.83 187.33 42.14 o 16 5 2 155.63 149.98 65.68 o 17 5 2 10.78 10.70 117.34 o 0 6 2 1347.94 1371.02 61.64 o 1 6 2 34.41 21.57 26.52 o 2 6 2 699.55 671.04 34.55 o 3 6 2 139.43 132.81 38.53 o 4 6 2 412.40 314.28 32.91 o 5 6 2 546.33 508.73 37.31 o 6 6 2 255.58 246.98 27.93 o 7 6 2 21.04 10.54 25.71 o 8 6 2 187.65 138.80 30.46 o 9 6 2 0.19 -15.90 55.71 o 10 6 2 744.36 685.80 38.22 o 11 6 2 2.93 65.93 52.31 o 12 6 2 972.50 894.36 46.07 o 13 6 2 15.11 -33.21 177.25 o 14 6 2 761.43 877.80 85.50 o 15 6 2 0.92 -29.41 134.31 o 1 7 2 99.67 141.58 33.29 o 2 7 2 25.98 -3.93 43.17 o 3 7 2 265.71 210.27 47.08 o 4 7 2 356.06 354.49 71.86 o 5 7 2 38.82 -19.81 45.02 o 6 7 2 1700.41 1751.90 71.82 o 7 7 2 90.13 136.00 54.72 o 8 7 2 1083.06 1114.44 39.56 o 9 7 2 42.80 93.55 30.01 o 10 7 2 465.48 462.37 35.53 o 11 7 2 43.59 61.39 39.60 o 12 7 2 259.48 234.04 78.02 o 0 8 2 1568.22 1648.03 77.50 o 1 8 2 0.72 0.53 62.25 o 2 8 2 971.35 970.38 44.28 o 3 8 2 58.12 5.11 68.79 o 4 8 2 398.55 456.25 58.56 o 5 8 2 111.69 195.79 68.73 o 6 8 2 57.21 148.04 71.03 o 7 8 2 101.91 105.22 72.49 o 8 8 2 78.09 66.75 81.97 o 1 0 3 423.28 429.12 25.85 o 2 0 3 1317.46 1231.61 61.36 o 3 0 3 85.35 88.74 15.81 o 4 0 3 5329.19 5282.96 114.12 o 5 0 3 181.73 201.17 20.06 o 6 0 3 8020.81 7796.43 159.13 o 7 0 3 501.38 464.09 60.52 o 8 0 3 12428.41 12101.24 338.45 o 9 0 3 53.66 29.02 71.14 o 10 0 3 6055.22 6277.19 139.07 o 11 0 3 3.34 -32.39 37.35 o 12 0 3 22.92 -1.31 75.87 o 13 0 3 74.41 118.39 26.99 o 14 0 3 54.46 128.95 83.77 o 15 0 3 0.05 -29.28 29.28 o 16 0 3 72.55 -19.95 47.94 o 17 0 3 202.99 228.74 81.82 o 18 0 3 149.65 134.21 95.52 o 19 0 3 2.01 199.01 85.68 o 0 1 3 336.56 445.43 25.74 o 1 1 3 212.96 193.33 22.77 o 2 1 3 3710.30 3737.75 59.80 o 3 1 3 80.51 123.89 26.12 o 4 1 3 3077.91 3321.36 48.75 o 5 1 3 772.21 761.08 25.94 o 6 1 3 3.39 147.81 54.84 o 7 1 3 78.26 102.38 36.59 o 8 1 3 255.99 272.87 38.19 o 9 1 3 67.35 59.60 25.47 o 10 1 3 1064.22 1054.06 46.30 o 11 1 3 203.96 286.19 23.08 o 12 1 3 1616.11 1512.59 40.50 o 13 1 3 443.65 486.54 27.73 o 14 1 3 2421.81 2522.85 57.72 o 15 1 3 132.74 60.19 38.33 o 16 1 3 1762.35 1817.12 106.86 o 17 1 3 1.96 -19.76 32.24 o 18 1 3 100.29 81.10 98.00 o 19 1 3 3.31 -15.96 38.35 o 1 2 3 248.49 256.22 25.48 o 2 2 3 2508.71 2510.87 65.28 o 3 2 3 0.50 13.67 12.99 o 4 2 3 7124.28 7403.73 151.63 o 5 2 3 5.38 21.57 10.41 o 6 2 3 2926.96 2725.72 43.40 o 7 2 3 53.84 35.49 18.90 o 8 2 3 1845.64 1856.21 45.19 o 9 2 3 69.14 42.46 38.07 o 10 2 3 1272.34 1334.18 37.30 o 11 2 3 373.00 504.81 62.45 o 12 2 3 14.23 103.87 51.84 o 13 2 3 110.92 12.29 42.26 o 14 2 3 38.58 -8.71 53.88 o 15 2 3 31.61 -28.01 28.01 o 16 2 3 940.29 748.63 52.44 o 17 2 3 55.02 -34.66 34.66 o 18 2 3 1827.59 1655.63 76.13 o 19 2 3 251.19 363.68 138.86 o 0 3 3 7081.86 7911.96 132.56 o 1 3 3 2478.19 2595.84 38.88 o 2 3 3 8630.87 8991.72 104.13 o 3 3 3 82.10 81.48 11.59 o 4 3 3 1687.53 1639.82 31.71 o 5 3 3 30.62 26.18 20.54 o 6 3 3 88.86 116.64 17.68 o 7 3 3 505.36 588.08 38.83 o 8 3 3 159.88 179.16 30.15 o 9 3 3 9.11 -17.53 17.53 o 10 3 3 5.31 57.91 28.11 o 11 3 3 13.54 -7.71 81.73 o 12 3 3 242.99 199.67 79.00 o 13 3 3 1.45 -24.03 24.03 o 14 3 3 1002.28 1005.40 161.81 o 15 3 3 24.85 69.97 34.28 o 16 3 3 1481.14 1434.61 68.78 o 17 3 3 48.41 284.91 189.05 o 18 3 3 280.68 346.02 49.82 o 1 4 3 98.75 77.86 12.97 o 2 4 3 253.98 237.38 20.87 o 3 4 3 31.47 3.46 25.11 o 4 4 3 4550.31 4708.58 57.43 o 5 4 3 189.55 204.47 20.47 o 6 4 3 4363.50 4335.55 90.49 o 7 4 3 168.69 184.57 21.95 o 8 4 3 2119.82 1810.70 173.47 o 9 4 3 1.24 40.89 20.54 o 10 4 3 1089.95 1089.17 60.38 o 11 4 3 11.34 207.48 93.35 o 12 4 3 215.32 149.52 33.93 o 13 4 3 5.19 116.66 48.15 o 14 4 3 8.54 -21.79 30.97 o 15 4 3 20.14 -25.79 56.09 o 16 4 3 569.84 521.38 70.32 o 17 4 3 2.20 13.12 40.20 o 0 5 3 45.02 68.39 26.80 o 1 5 3 15.22 15.80 15.41 o 2 5 3 374.41 443.54 22.84 o 3 5 3 0.32 37.93 22.30 o 4 5 3 135.46 113.67 28.46 o 5 5 3 524.28 447.79 21.47 o 6 5 3 73.35 36.14 15.60 o 7 5 3 163.52 135.93 44.21 o 8 5 3 26.20 7.99 25.62 o 9 5 3 13.97 4.71 40.29 o 10 5 3 1838.06 2011.47 87.49 o 11 5 3 401.91 248.28 47.15 o 12 5 3 2041.07 1921.67 76.88 o 13 5 3 387.35 425.37 101.68 o 14 5 3 744.37 714.84 53.66 o 15 5 3 49.50 22.48 159.55 o 16 5 3 609.01 664.96 94.48 o 1 6 3 6.88 -14.14 43.54 o 2 6 3 1.77 3.20 52.91 o 3 6 3 0.39 24.64 26.97 o 4 6 3 1648.04 1649.57 61.76 o 5 6 3 95.03 32.93 37.65 o 6 6 3 2930.40 2979.20 56.65 o 7 6 3 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