#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2202239.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202239_Fobs loop_ _publ_author_name 'Shao, Ting' 'Zhang, Hong-Tao' _publ_section_title ; Diaquatris(4-pyridylcarboxylato)neodymium(III) ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m353 _journal_page_last m355 _journal_volume 59 _journal_year 2003 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.190 _cell_angle_gamma 90.000 _cell_length_a 9.5260 _cell_length_b 19.0530 _cell_length_c 10.7870 _exptl_crystal_F_000 1076.00 _reflns_d_resolution_high 0.8419 _[local]_cod_data_source_file ww6080Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ZH4 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 321.51 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 521.23 871.20 26.10 o 2 0 0 103366.74 116148.00 649.83 o 3 0 0 51.14 160.98 27.05 o 4 0 0 15270.85 16129.52 357.02 o 5 0 0 2072.11 2416.43 93.73 o 6 0 0 31471.43 34035.93 654.78 o 7 0 0 959.86 978.84 79.82 o 8 0 0 23382.51 23835.84 665.07 o 9 0 0 431.73 559.72 72.58 o 10 0 0 7676.63 7120.88 259.47 o 11 0 0 21.79 25.15 109.35 o 1 1 0 496.82 662.97 21.34 o 2 1 0 1294.89 1453.59 43.82 o 3 1 0 3359.28 3597.02 101.16 o 4 1 0 1.64 56.20 26.10 o 5 1 0 2117.96 2704.29 98.87 o 6 1 0 647.36 810.81 61.53 o 7 1 0 0.47 97.92 69.92 o 8 1 0 154.72 0.00 90.49 o 9 1 0 254.00 306.91 58.68 o 10 1 0 94.41 147.45 63.44 o 11 1 0 413.70 505.04 94.49 o 0 2 0 74098.97 55099.47 1180.02 o 1 2 0 3493.44 3677.03 89.16 o 2 2 0 18102.52 21292.53 267.67 o 3 2 0 6295.89 7137.07 193.75 o 4 2 0 8291.83 9010.17 256.05 o 5 2 0 1856.00 2147.24 84.21 o 6 2 0 25348.55 26428.87 575.72 o 7 2 0 3.06 77.54 44.39 o 8 2 0 16789.86 16417.38 395.88 o 9 2 0 13.15 113.54 80.40 o 10 2 0 7857.44 7328.92 254.14 o 11 2 0 204.97 308.82 79.63 o 1 3 0 60.40 148.60 16.76 o 2 3 0 9595.22 10614.07 199.08 o 3 3 0 6451.71 7279.57 198.70 o 4 3 0 248.62 215.47 30.29 o 5 3 0 340.77 452.84 47.82 o 6 3 0 136.97 204.42 44.96 o 7 3 0 858.09 1009.89 75.25 o 8 3 0 521.41 369.78 70.49 o 9 3 0 157.44 155.27 64.96 o 10 3 0 124.88 -53.34 102.11 o 11 3 0 249.17 322.91 87.25 o 0 4 0 27132.73 26727.40 278.33 o 1 4 0 7.50 82.87 16.57 o 2 4 0 33304.47 34872.08 381.59 o 3 4 0 97.63 32.20 41.72 o 4 4 0 32503.08 36186.41 511.14 o 5 4 0 122.48 141.93 30.29 o 6 4 0 20871.04 22415.97 510.19 o 7 4 0 17.06 -69.54 80.40 o 8 4 0 7163.84 7064.30 211.28 o 9 4 0 255.04 352.25 75.44 o 10 4 0 3989.88 3926.22 185.94 o 11 4 0 622.56 594.39 100.21 o 1 5 0 3199.39 3495.86 84.59 o 2 5 0 887.72 842.63 39.82 o 3 5 0 5630.42 6011.16 135.64 o 4 5 0 183.33 215.66 37.53 o 5 5 0 318.75 341.97 42.29 o 6 5 0 0.42 75.06 46.87 o 7 5 0 274.69 249.00 50.10 o 8 5 0 90.37 168.22 52.20 o 9 5 0 293.66 269.57 66.49 o 10 5 0 337.84 361.59 67.44 o 11 5 0 1189.33 1072.19 118.12 o 0 6 0 789.80 983.22 40.20 o 1 6 0 2452.34 2572.65 80.78 o 2 6 0 26787.99 27132.23 386.54 o 3 6 0 1815.60 1824.13 65.92 o 4 6 0 31296.49 35026.58 534.95 o 5 6 0 7.60 45.72 49.15 o 6 6 0 15499.69 16648.28 449.41 o 7 6 0 120.33 90.68 78.87 o 8 6 0 6300.37 6448.57 197.56 o 9 6 0 371.96 213.94 138.31 o 10 6 0 3956.82 3698.18 178.32 o 1 7 0 109.25 69.54 41.72 o 2 7 0 1302.60 1325.38 55.44 o 3 7 0 8533.03 8623.43 254.33 o 4 7 0 1.29 32.58 51.44 o 5 7 0 4271.17 4316.96 127.45 o 6 7 0 150.93 101.35 64.58 o 7 7 0 988.03 1003.23 84.21 o 8 7 0 331.94 359.49 64.96 o 9 7 0 1324.67 1273.94 109.73 o 10 7 0 16.81 -131.45 131.45 o 0 8 0 6976.70 6440.95 143.07 o 1 8 0 253.56 280.81 27.62 o 2 8 0 25350.61 25675.02 425.22 o 3 8 0 2263.42 2225.92 81.92 o 4 8 0 19292.21 20450.48 442.36 o 5 8 0 448.41 474.18 48.96 o 6 8 0 5456.72 5552.60 159.08 o 7 8 0 72.86 113.16 44.58 o 8 8 0 9356.26 9331.37 294.91 o 9 8 0 585.61 542.57 76.78 o 10 8 0 4302.56 4325.72 190.32 o 1 9 0 20597.50 20447.62 390.93 o 2 9 0 9.27 59.25 41.91 o 3 9 0 9662.57 10617.12 309.96 o 4 9 0 55.90 130.50 36.39 o 5 9 0 8039.76 8472.55 227.28 o 6 9 0 1279.08 1373.39 81.16 o 7 9 0 3638.94 3890.78 151.84 o 8 9 0 1003.87 977.32 96.02 o 9 9 0 2407.20 2389.38 134.50 o 10 9 0 17.95 112.21 65.73 o 0 10 0 14169.50 12805.89 329.96 o 1 10 0 396.52 382.73 43.44 o 2 10 0 15070.54 14974.08 363.11 o 3 10 0 161.66 164.41 38.86 o 4 10 0 10165.58 9990.53 241.00 o 5 10 0 56.97 45.15 65.92 o 6 10 0 6444.99 6420.57 183.84 o 7 10 0 1217.93 1167.44 95.25 o 8 10 0 6454.25 6644.41 210.13 o 9 10 0 1004.53 875.20 95.45 o 10 10 0 3656.44 3469.76 181.75 o 1 11 0 13277.36 13128.99 357.21 o 2 11 0 105.62 111.07 33.91 o 3 11 0 7977.77 7808.05 211.85 o 4 11 0 276.26 232.80 48.58 o 5 11 0 7017.88 7106.97 225.56 o 6 11 0 8.07 80.97 57.34 o 7 11 0 4507.63 4669.02 171.46 o 8 11 0 285.80 264.05 71.25 o 9 11 0 3642.43 3669.60 171.46 o 0 12 0 4923.17 4614.72 157.93 o 1 12 0 92.94 97.35 26.86 o 2 12 0 9300.00 9296.12 227.47 o 3 12 0 3.34 21.15 47.25 o 4 12 0 6392.40 6071.93 205.94 o 5 12 0 86.57 89.35 89.35 o 6 12 0 5912.30 5736.83 184.60 o 7 12 0 116.19 111.26 79.44 o 8 12 0 2215.85 2078.65 132.98 o 9 12 0 53.33 20.19 131.83 o 1 13 0 8293.66 7759.66 214.13 o 2 13 0 259.31 250.71 42.48 o 3 13 0 10912.43 11218.56 271.48 o 4 13 0 211.19 98.87 76.39 o 5 13 0 9457.25 9303.74 273.38 o 6 13 0 190.13 149.74 108.02 o 7 13 0 3298.19 3063.02 150.12 o 8 13 0 323.61 390.35 75.06 o 9 13 0 3127.83 2875.18 167.27 o 0 14 0 7386.44 7109.64 215.66 o 1 14 0 106.67 33.72 49.15 o 2 14 0 5832.02 5888.85 165.93 o 3 14 0 477.65 378.16 65.34 o 4 14 0 6354.88 6253.30 185.56 o 5 14 0 370.23 216.42 67.06 o 6 14 0 3437.53 3065.30 144.98 o 7 14 0 80.49 139.64 98.87 o 8 14 0 1463.79 1298.13 128.98 o 1 15 0 6430.55 6735.48 221.18 o 2 15 0 0.83 -12.57 67.44 o 3 15 0 10715.83 10633.50 287.29 o 4 15 0 28.97 42.67 95.25 o 5 15 0 8520.33 8252.32 222.33 o 6 15 0 1.60 -33.15 77.54 o 7 15 0 3327.70 3554.72 162.70 o 8 15 0 0.46 121.35 99.07 o 0 16 0 4747.25 4437.36 154.12 o 1 16 0 25.18 -114.69 114.69 o 2 16 0 2556.46 2738.58 126.31 o 3 16 0 220.83 180.79 55.06 o 4 16 0 1996.88 1911.77 116.21 o 5 16 0 38.69 -32.39 85.54 o 6 16 0 1272.12 1332.05 109.73 o 7 16 0 3.23 0.00 80.78 o 1 17 0 4901.94 4854.95 163.84 o 2 17 0 9.80 44.01 67.25 o 3 17 0 4817.42 4904.87 177.56 o 4 17 0 99.00 129.74 100.02 o 5 17 0 3379.94 3531.67 166.70 o 6 17 0 30.43 -73.92 94.11 o 7 17 0 2540.06 2699.72 154.12 o 0 18 0 2864.07 2991.77 141.17 o 1 18 0 28.72 -76.39 130.50 o 2 18 0 597.21 664.50 76.58 o 3 18 0 0.28 -81.35 98.87 o 4 18 0 1046.86 974.84 98.11 o 5 18 0 94.28 30.67 58.11 o 6 18 0 415.61 401.98 84.21 o 1 19 0 8036.18 7788.81 234.52 o 2 19 0 24.93 101.92 83.25 o 3 19 0 5531.45 5577.18 204.80 o 4 19 0 224.18 73.92 70.49 o 5 19 0 2592.42 2823.74 155.08 o 6 19 0 22.60 -103.07 114.69 o 0 20 0 157.00 124.40 62.49 o 1 20 0 490.55 268.05 114.31 o 2 20 0 1222.49 1116.77 104.78 o 3 20 0 0.39 131.45 94.11 o 4 20 0 650.70 582.96 90.49 o 5 20 0 14.21 -98.11 98.11 o 1 21 0 5807.98 6144.14 221.37 o 2 21 0 2.20 38.86 120.02 o 3 21 0 2625.84 2870.79 158.50 o 4 21 0 67.88 125.55 88.78 o 0 22 0 150.65 142.69 113.54 o 1 22 0 3.40 -177.36 177.36 o 2 22 0 31.09 -112.02 112.02 o -11 1 1 346.55 351.87 91.64 o -10 1 1 3650.45 3234.86 174.51 o -9 1 1 944.37 1000.18 101.35 o -8 1 1 12272.06 12642.62 342.92 o -7 1 1 4837.12 4965.45 163.46 o -6 1 1 20477.30 20862.74 517.42 o -5 1 1 192.29 183.84 34.48 o -4 1 1 18152.70 18520.99 384.26 o -3 1 1 587.79 628.87 38.67 o -2 1 1 17094.48 18913.25 272.43 o -1 1 1 1964.17 2105.52 52.20 o 0 1 1 66139.10 50907.07 1693.73 o 1 1 1 497.83 594.01 24.39 o 2 1 1 25088.03 27626.42 307.29 o 3 1 1 2631.37 2897.85 86.30 o 4 1 1 8873.50 9506.06 267.67 o 5 1 1 856.12 955.60 61.34 o 6 1 1 18480.22 19375.24 495.90 o 7 1 1 1681.09 1691.73 102.88 o 8 1 1 16122.93 15885.86 397.21 o 9 1 1 2.25 -61.53 102.11 o 10 1 1 9587.26 8954.16 286.15 o 11 1 1 12.30 -101.16 123.07 o -11 2 1 23.38 58.30 73.92 o -10 2 1 207.10 283.86 70.30 o -9 2 1 756.80 593.63 85.73 o -8 2 1 56.69 16.19 99.07 o -7 2 1 1239.93 1419.11 92.59 o -6 2 1 82.17 57.72 73.73 o -5 2 1 245.85 290.15 44.77 o -4 2 1 950.96 1035.61 57.72 o -3 2 1 87.22 117.74 24.19 o -2 2 1 14723.89 16700.67 256.62 o 0 2 1 112.74 121.64 28.58 o 1 2 1 2187.19 2453.58 57.72 o 2 2 1 3007.35 3245.15 78.11 o 3 2 1 1164.14 1319.66 48.77 o 4 2 1 162.99 377.02 33.72 o 5 2 1 94.79 78.11 49.91 o 6 2 1 1292.13 1733.64 84.59 o 7 2 1 176.50 286.34 50.49 o 8 2 1 24.61 97.73 97.73 o 9 2 1 1310.23 1085.91 108.78 o 10 2 1 422.89 369.02 90.87 o 11 2 1 432.15 430.93 96.02 o -11 3 1 1389.72 1241.93 136.21 o -10 3 1 4672.00 4266.66 197.75 o -9 3 1 747.30 722.79 95.06 o -8 3 1 7728.26 7866.16 221.18 o -7 3 1 1906.75 1974.25 107.45 o -6 3 1 18179.10 19643.29 496.85 o -5 3 1 4168.88 4653.78 156.03 o -4 3 1 35523.43 39202.75 554.00 o -3 3 1 7555.24 8379.58 220.42 o -2 3 1 38583.56 41297.60 412.07 o -1 3 1 4339.48 4310.86 114.88 o 0 3 1 38706.77 38319.84 222.39 o 1 3 1 10857.17 11487.56 185.56 o 2 3 1 46479.36 50428.55 445.22 o 3 3 1 899.61 976.74 43.63 o 4 3 1 18355.58 19504.60 366.16 o 5 3 1 714.44 759.18 49.34 o 6 3 1 18206.39 20750.53 494.18 o 7 3 1 1315.20 1480.26 92.40 o 8 3 1 9796.97 9682.48 295.67 o 9 3 1 510.20 659.74 78.11 o 10 3 1 6962.33 6667.85 243.09 o 11 3 1 37.36 -86.87 86.87 o -11 4 1 258.01 24.77 183.27 o -10 4 1 3.55 -108.02 108.02 o -9 4 1 1269.72 1132.20 109.92 o -8 4 1 6.56 15.81 96.59 o -7 4 1 667.05 746.99 71.82 o -6 4 1 1768.36 1987.78 93.73 o -5 4 1 539.97 565.81 51.25 o -4 4 1 3772.21 4156.35 132.98 o -3 4 1 9572.12 10892.21 257.19 o -2 4 1 865.34 930.45 41.53 o -1 4 1 62984.75 65013.42 479.70 o 0 4 1 4770.52 4812.90 89.99 o 1 4 1 6083.21 6553.35 154.69 o 2 4 1 153.97 169.74 22.67 o 3 4 1 7390.65 8170.21 214.51 o 4 4 1 374.06 355.30 37.53 o 5 4 1 4064.86 4738.36 148.60 o 6 4 1 762.26 792.90 66.68 o 7 4 1 1155.33 1276.80 86.49 o 8 4 1 1.58 75.44 62.11 o 9 4 1 781.97 782.04 91.06 o 10 4 1 16.07 -114.88 114.88 o 11 4 1 868.63 1025.32 110.50 o -11 5 1 1444.53 1259.65 130.31 o -10 5 1 4768.84 4197.12 206.51 o -9 5 1 1365.50 1371.67 119.45 o -8 5 1 5912.26 5880.85 192.42 o -7 5 1 2478.74 2619.70 120.59 o -6 5 1 20132.47 21286.24 524.28 o -5 5 1 7642.66 8379.39 211.85 o -4 5 1 24422.83 26522.98 462.37 o -3 5 1 13205.55 14541.81 307.10 o -2 5 1 14917.11 14597.63 274.14 o -1 5 1 3408.95 3287.82 84.59 o 0 5 1 26403.15 24586.53 220.18 o 1 5 1 8170.26 8431.21 189.75 o 2 5 1 50830.31 53006.91 515.33 o 3 5 1 402.77 460.46 36.77 o 4 5 1 35964.40 38897.75 546.00 o 5 5 1 416.12 469.80 47.82 o 6 5 1 17901.88 18872.29 472.27 o 7 5 1 351.70 458.94 61.73 o 8 5 1 7191.76 7176.51 248.04 o 9 5 1 368.25 250.90 71.82 o 10 5 1 3800.69 3747.71 182.89 o -10 6 1 129.06 0.00 111.64 o -9 6 1 2523.85 2304.60 132.98 o -8 6 1 49.48 94.68 77.35 o -7 6 1 331.38 317.77 53.53 o -6 6 1 1941.12 2302.50 102.49 o -5 6 1 56.71 142.50 29.53 o -4 6 1 5077.13 5596.23 155.84 o -3 6 1 12864.21 13528.87 308.44 o -2 6 1 843.40 669.26 39.63 o -1 6 1 14972.24 14701.84 269.38 o 0 6 1 4043.38 4118.94 70.91 o 1 6 1 1062.01 1309.18 48.20 o 2 6 1 26.50 16.38 36.96 o 3 6 1 3409.55 3786.19 113.54 o 4 6 1 41.44 69.35 48.20 o 5 6 1 7939.47 8368.91 203.08 o 6 6 1 409.58 428.84 57.72 o 7 6 1 1065.61 1088.00 85.54 o 8 6 1 627.92 655.93 75.06 o 9 6 1 267.73 336.25 57.92 o 10 6 1 105.79 182.13 116.21 o -10 7 1 4093.63 3986.61 193.37 o -9 7 1 2092.45 1821.08 136.41 o -8 7 1 8512.53 8126.20 220.61 o -7 7 1 55.14 95.25 89.16 o -6 7 1 14410.84 14182.70 306.72 o -5 7 1 846.59 796.33 67.63 o -4 7 1 21095.08 21461.71 441.60 o -3 7 1 262.77 168.03 29.53 o -2 7 1 23065.89 23472.54 389.02 o -1 7 1 162.85 141.55 25.34 o 0 7 1 32237.68 30338.24 640.11 o 1 7 1 6457.60 6492.96 194.32 o 2 7 1 35823.68 35805.20 479.70 o 3 7 1 1136.02 1089.91 57.72 o 4 7 1 24605.29 24759.05 474.37 o 5 7 1 5.11 38.48 60.77 o 6 7 1 8565.81 8330.05 236.61 o 7 7 1 39.07 -89.92 89.92 o 8 7 1 10736.76 10426.42 313.39 o 9 7 1 267.57 292.24 73.54 o 10 7 1 6387.13 6385.89 230.90 o -10 8 1 651.20 843.96 94.87 o -9 8 1 1694.72 1798.41 133.36 o -8 8 1 292.44 80.40 135.64 o -7 8 1 373.21 427.31 61.73 o -6 8 1 664.07 664.69 65.54 o -5 8 1 2940.13 3062.83 111.64 o -4 8 1 304.47 279.10 44.58 o -3 8 1 10807.03 11468.89 315.87 o -2 8 1 3441.94 3303.06 92.40 o -1 8 1 12407.16 12562.22 288.05 o 0 8 1 3768.30 3628.95 77.91 o 1 8 1 192.66 125.93 24.58 o 2 8 1 1350.88 1276.04 62.11 o 3 8 1 5291.16 5882.37 159.65 o 4 8 1 549.71 537.81 48.58 o 5 8 1 6906.41 6859.50 198.51 o 6 8 1 158.21 210.51 47.82 o 7 8 1 5147.72 5282.84 167.46 o 8 8 1 4.19 -30.48 88.78 o 9 8 1 1029.64 914.83 89.16 o 10 8 1 184.05 183.65 73.54 o -10 9 1 5263.90 4919.73 216.80 o -9 9 1 1704.21 1966.06 129.74 o -8 9 1 5779.89 5822.75 195.27 o -7 9 1 2310.97 2196.39 124.97 o -6 9 1 7394.39 7588.01 237.76 o -5 9 1 3074.82 3161.32 119.64 o -4 9 1 8933.16 8829.18 219.28 o -3 9 1 247.13 193.18 36.58 o -2 9 1 9395.24 9350.99 196.99 o -1 9 1 5733.18 5978.01 150.12 o 0 9 1 26642.68 24405.09 299.66 o 1 9 1 3700.09 3721.99 120.02 o 2 9 1 29841.45 29461.41 493.42 o 3 9 1 306.26 276.81 39.05 o 4 9 1 13781.79 13553.83 383.12 o 5 9 1 156.52 193.37 47.25 o 6 9 1 4673.63 5074.23 158.31 o 7 9 1 381.46 382.73 66.30 o 8 9 1 10912.45 11276.85 318.72 o 9 9 1 3.06 72.97 106.50 o 10 9 1 2734.90 2953.86 161.93 o -10 10 1 233.71 313.39 89.54 o -9 10 1 1874.61 1676.30 134.69 o -8 10 1 1698.53 1959.78 127.45 o -7 10 1 7339.52 7748.61 214.70 o -6 10 1 61.99 78.49 45.34 o -5 10 1 2229.68 2213.34 102.30 o -4 10 1 38.91 10.29 61.92 o -3 10 1 4600.95 4501.18 124.21 o -2 10 1 895.66 897.30 58.68 o -1 10 1 2892.91 2682.19 88.97 o 0 10 1 334.61 317.04 27.20 o 1 10 1 6209.84 6025.64 167.08 o 2 10 1 91.00 122.31 39.82 o 3 10 1 3780.14 3415.27 112.02 o 4 10 1 3640.44 4042.43 126.50 o 5 10 1 6789.43 6851.31 215.09 o 6 10 1 82.66 51.44 75.06 o 7 10 1 1703.47 1690.59 106.30 o 8 10 1 2.16 148.79 94.87 o 9 10 1 1847.40 1804.32 128.02 o 10 10 1 106.22 -157.36 157.36 o -9 11 1 1513.16 1437.97 119.07 o -8 11 1 4032.29 3946.98 175.08 o -7 11 1 841.11 944.74 95.06 o -6 11 1 4736.02 4841.05 160.41 o -5 11 1 166.90 73.16 99.07 o -4 11 1 6983.60 6686.14 211.66 o -3 11 1 1301.64 1392.25 75.06 o -2 11 1 24150.43 23248.69 490.75 o -1 11 1 2795.68 2612.27 95.45 o 0 11 1 13219.73 13516.42 256.89 o 1 11 1 363.43 293.00 48.01 o 2 11 1 8557.46 8530.08 207.85 o 3 11 1 1019.80 1077.91 70.68 o 4 11 1 10699.59 10765.33 258.14 o 5 11 1 374.67 387.31 56.77 o 6 11 1 7808.24 7855.49 249.00 o 7 11 1 113.47 45.72 94.87 o 8 11 1 3468.87 3704.47 164.98 o 9 11 1 401.27 135.26 126.69 o -9 12 1 2531.96 2551.12 155.84 o -8 12 1 302.61 387.50 64.20 o -7 12 1 4254.23 4180.36 170.89 o -6 12 1 205.37 158.69 98.87 o -5 12 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